SampleIdent,894F 3R1 52-58 GLYcrse,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,14-jan-1993 14:29,/ DataAngleRange, 2.0000, 23.9900,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 276, 272, 272, 279, 282, 279, 269, 222 259, 282, 243, 228, 259, 231, 246, 234 228, 210, 225, 213, 237, 210, 216, 207 222, 222, 202, 210, 180, 219, 199, 204 196, 240, 222, 219, 193, 193, 213, 213 213, 199, 196, 172, 202, 188, 225, 213 199, 196, 237, 210, 222, 234, 185, 219 210, 222, 225, 216, 204, 202, 207, 193 199, 204, 219, 213, 207, 225, 213, 188 210, 202, 182, 202, 210, 222, 207, 210 190, 185, 210, 204, 222, 199, 180, 202 188, 169, 174, 185, 161, 172, 182, 182 159, 151, 146, 169, 146, 144, 144, 144 128, 135, 132, 135, 137, 123, 132, 123 137, 135, 135, 123, 156, 112, 128, 132 104, 161, 130, 117, 142, 130, 125, 123 125, 123, 117, 96, 92, 114, 142, 121 128, 114, 125, 104, 121, 119, 119, 106 102, 108, 128, 100, 112, 108, 117, 137 112, 146, 112, 121, 96, 125, 123, 104 123, 132, 121, 112, 98, 119, 119, 108 102, 104, 104, 123, 108, 110, 119, 117 125, 117, 114, 121, 102, 114, 100, 128 117, 104, 106, 106, 110, 119, 96, 123 114, 108, 121, 114, 128, 117, 135, 104 108, 137, 117, 112, 121, 110, 121, 119 117, 102, 98, 128, 104, 117, 117, 112 117, 130, 100, 108, 106, 110, 114, 106 128, 121, 117, 121, 110, 135, 119, 130 130, 128, 121, 121, 104, 117, 123, 86 110, 110, 396, 110, 112, 130, 114, 144 106, 137, 125, 119, 121, 119, 121, 123 121, 123, 132, 121, 137, 121, 110, 139 196, 130, 123, 132, 121, 98, 139, 137 123, 104, 132, 142, 125, 119, 144, 130 144, 121, 123, 130, 139, 123, 125, 144 123, 142, 144, 149, 125, 151, 151, 137 144, 166, 137, 130, 142, 164, 146, 123 159, 149, 146, 128, 159, 144, 149, 144 154, 174, 174, 159, 164, 164, 164, 180 159, 166, 164, 164, 159, 159, 185, 190 174, 185, 190, 193, 188, 196, 190, 216 219, 210, 216, 222, 193, 222, 199, 225 237, 216, 219, 234, 213, 243, 240, 266 259, 259, 266, 253, 259, 259, 286, 276 276, 286, 269, 240, 250, 259, 279, 276 276, 250, 296, 276, 286, 306, 266, 289 259, 262, 262, 272, 243, 250, 266, 246 269, 266, 286, 246, 262, 246, 237, 253 222, 228, 237, 210, 219, 228, 199, 243 225, 216, 199, 228, 188, 207, 202, 202 222, 199, 182, 207, 216, 188, 199, 190 185, 177, 199, 169, 188, 188, 156, 169 169, 174, 125, 159, 144, 154, 142, 164 139, 132, 132, 161, 146, 132, 132, 151 137, 159, 449, 149, 154, 135, 130, 159 121, 142, 144, 135, 117, 121, 121, 123 123, 130, 144, 135, 106, 142, 119, 125 137, 142, 121, 132, 110, 125, 123, 128 130, 121, 104, 132, 121, 125, 137, 112 125, 137, 137, 123, 128, 139, 144, 112 137, 119, 121, 139, 121, 130, 121, 108 125, 123, 104, 121, 114, 110, 142, 137 110, 123, 110, 106, 137, 128, 137, 123 108, 132, 123, 149, 130, 121, 137, 102 108, 112, 130, 128, 123, 108, 123, 125 117, 137, 104, 110, 114, 102, 128, 130 106, 128, 112, 110, 119, 96, 121, 123 112, 117, 130, 114, 117, 119, 117, 128 117, 110, 102, 132, 104, 123, 110, 112 119, 108, 121, 123, 110, 114, 110, 125 114, 100, 112, 119, 102, 90, 117, 117 117, 108, 132, 117, 108, 96, 108, 125 104, 102, 104, 112, 110, 117, 119, 112 114, 110, 119, 119, 102, 114, 98, 121 108, 123, 98, 102, 123, 121, 85, 98 94, 106, 114, 102, 94, 125, 106, 121 149, 144, 110, 144, 117, 135, 110, 114 112, 94, 114, 100, 114, 104, 102, 130 112, 132, 119, 108, 130, 117, 408, 100 110, 104, 121, 96, 102, 121, 117, 117 108, 104, 128, 98, 102, 123, 104, 121 128, 112, 108, 123, 104, 114, 110, 108 110, 92, 106, 110, 102, 110, 98, 112 110, 104, 108, 114, 108, 110, 119, 112 102, 132, 123, 114, 104, 125, 135, 117 106, 125, 100, 106, 123, 121, 98, 112 100, 117, 121, 119, 119, 81, 128, 112 102, 117, 110, 108, 114, 121, 104, 102 102, 132, 117, 94, 104, 110, 96, 114 104, 110, 125, 123, 104, 114, 112, 104 117, 123, 142, 125, 121, 130, 102, 135 130, 112, 108, 130, 137, 132, 117, 121 114, 121, 149, 137, 123, 132, 130, 121 117, 132, 128, 132, 137, 130, 144, 142 149, 149, 139, 159, 196, 174, 180, 166 199, 172, 177, 177, 164, 193, 130, 154 146, 130, 139, 144, 128, 139, 119, 132 123, 128, 123, 125, 130, 130, 139, 135 123, 104, 137, 132, 100, 125, 121, 144 142, 125, 121, 121, 112, 144, 172, 135 123, 130, 137, 142, 130, 139, 139, 156 161, 177, 149, 180, 190, 188, 219, 219 216, 262, 266, 262, 253, 243, 250, 279 250, 289, 339, 365, 396, 441, 416, 458 502, 520, 520, 625, 605, 605, 630, 571 557, 467, 428, 369, 292, 266, 240, 219 207, 182, 196, 159, 149, 137, 146, 132 128, 121, 130, 125, 123, 119, 112, 114 130, 112, 123, 123, 114, 130, 132, 110 123, 135, 132, 123, 106, 128, 125, 123 121, 123, 123, 128, 139, 128, 132, 121 130, 132, 125, 104, 135, 139, 108, 121 121, 139, 110, 156, 130, 135, 144, 144 132, 139, 142, 135, 154, 159, 159, 169 142, 144, 144, 156, 146, 151, 159, 137 139, 174, 159, 146, 172, 172, 144, 154 177, 156, 190, 166, 154, 137, 182, 151 151, 146, 180, 154, 161, 169, 169, 174 161, 174, 190, 177, 159, 169, 156, 190 169, 144, 166, 164, 154, 142, 172, 154 144, 137, 161, 154, 146, 166, 154, 174 144, 154, 151, 154, 123, 139, 137, 130 144, 154, 161, 144, 149, 154, 151, 154 156, 164, 146, 137, 119, 154, 172, 180 182, 151, 169, 137, 154, 154, 149, 174 146, 144, 180, 159, 161, 180, 154, 151 169, 185, 149, 190, 188, 185, 182, 204 174, 185, 202, 172, 210, 228, 213, 237 234, 213, 234, 216, 253, 231, 253, 262 231, 259, 246, 262, 222, 231, 234, 210 202, 199, 193, 151, 144, 161, 169, 144 121, 121, 146, 130, 132, 121, 117, 135 132, 123, 104, 117, 119, 128, 117, 110 128, 108, 123, 121, 110, 96, 108, 125 130, 90, 108, 110, 114, 102, 117, 119 117, 121, 94, 104, 104, 112, 114, 100 108, 121, 112, 108, 112, 123, 90, 88 106, 106, 100, 96, 123, 104, 96, 119 114, 112, 98, 100, 88, 108, 98, 81 114, 106, 98, 98, 102, 102, 114, 100 88, 104, 98, 121, 100, 104, 94, 92 121, 104, 77, 110, 102, 100, 86, 110 106, 100, 104, 108, 102, 119, 104, 114 100, 125, 110, 114, 128, 151, 128, 121 149, 156, 149, 169, 164, 164, 137, 128 144, 161, 123, 154, 137, 149, 142, 159 137, 130, 164, 154, 123, 154, 123, 130 156, 132, 130, 149, 132, 146, 139, 142 144, 144, 137, 149, 119, 125, 100, 83 92, 85, 108, 92, 100, 92, 88, 94 81, 90, 86, 88, 94, 96, 98, 110 98, 96, 108, 114, 100, 86, 76, 90 100, 94, 117, 94, 94, 110, 90, 77 88, 83, 79, 92, 85, 90, 88, 106 85, 83, 92, 85, 94, 81, 94, 114 106, 79, 88, 92, 85, 85, 106, 92 88, 108, 98, 96, 85, 94, 88, 85 104, 72, 108, 79, 94, 98, 90, 92 81, 94, 79, 88, 100, 96, 108, 90 96, 94, 100, 90, 104, 98, 86, 96 96, 92, 92, 77, 98, 88, 412, 104 88, 98, 100, 110, 85, 117, 98, 98 96, 112, 92, 104, 79, 96, 110, 98 114, 94, 96, 108, 100, 77, 98, 98 114, 102, 83, 96, 98, 90, 94, 77 98, 102, 110, 98, 85, 98, 90, 102 102, 112, 100, 83, 108, 94, 72, 108 79, 102, 110, 74, 90, 90, 72, 86 86, 100, 98, 104, 100, 102, 90, 106 88, 130, 94, 121, 112, 112, 128, 130 100, 110, 121, 102, 123, 102, 125, 128 119, 132, 114, 139, 106, 114, 135, 96 114, 71, 106, 83, 100, 106, 88, 90 86, 100, 86, 83, 98, 81, 104, 76 85, 98, 106, 108, 102, 77, 92, 94 100, 81, 79, 112, 72, 104, 92, 90 100, 96, 86, 94, 98, 92, 102, 77 86, 85, 83, 79, 86, 92, 79, 83 94, 100, 88, 102, 92, 100, 90, 102 88, 106, 104, 104, 85, 102, 90, 102 88, 76, 104, 102, 110, 90, 96, 108 94, 96, 92, 106, 106, 90, 96, 123 396, 108, 102, 102, 123, 96, 94, 100 90, 112, 98, 86, 92, 110, 106, 119 108, 94, 86, 117, 117, 98, 100, 102 114, 90, 108, 119, 125, 98, 94, 102 125, 114, 130, 108, 102, 114, 112, 117 117, 130, 102, 112, 119, 110, 88, 125 114, 128, 121, 125, 119, 125, 130, 121 114, 104, 132, 130, 125, 144, 137, 135 135, 139, 144, 144, 144, 159, 137, 132 149, 139, 151, 142, 121, 135, 125, 104 121, 121, 102, 123, 117, 112, 128, 112 104, 117, 121, 130, 119, 102, 104, 106 121, 90, 112, 88, 117, 104, 108, 117 106, 117, 106, 114, 108, 98, 112, 112 119, 108, 94, 98, 104, 102, 104, 119 128, 96, 112, 119, 106, 88, 102, 376 117, 135, 98, 96, 108, 121, 106, 108 110, 119, 117, 132, 128, 112, 142, 123 123, 119, 100, 132, 151, 130, 130, 125 123, 130, 130, 128, 128, 125, 128, 117 125, 112, 130, 112, 112, 128, 108, 137 128, 130, 106, 110, 142, 108, 123, 121 130, 114, 128, 139, 135, 123, 137, 137 154, 130, 139, 151, 156, 159, 159, 154 177, 166, 151, 166, 169, 159, 185, 161 177, 193, 169, 182, 169, 182, 180, 199 182, 210, 177, 180, 177, 149, 156, 137 151, 154, 139, 149, 130, 149, 130, 123 119, 119, 149, 137, 151, 156, 156, 125 137, 142, 137, 142, 144, 146, 121, 128 123, 144, 139, 144, 137, 169, 156, 159 159, 151, 161, 177, 169, 182, 177, 185 207, 188, 174, 188, 196, 193, 166, 174 169, 174, 164, 169, 166, 146, 174, 174 182, 174, 159, 159, 174, 210, 204, 188 219, 222, 216, 216, 240, 262, 253, 243 243, 286, 246, 246, 219, 237, 243, 234 196, 202, 188, 222, 182, 144, 166, 149 146, 182, 180, 149, 174, 159, 156, 174 166, 154, 137, 142, 137, 154, 137, 149 146, 142, 151, 137, 151, 135, 149, 154 144, 144, 139, 159, 137, 130, 119, 119 137, 128, 139, 144, 121, 125, 112, 121 137, 121, 121, 137, 119, 125, 137, 125 128, 139, 128, 130, 125, 132, 123, 135 125, 117, 130, 137, 130, 108, 135, 119 144, 144, 132, 130, 121, 121, 132, 119 117, 128, 121, 135, 123, 121, 121, 139 130, 128, 121, 132, 139, 117, 125, 130 106, 102, 117, 135, 112, 128, 119, 139 123, 119, 123, 137, 119, 108, 135, 125 142, 139, 125, 154, 144, 144, 130, 144 142, 149, 174, 132, 154, 169, 164, 180 180, 174, 180, 177, 190, 182, 188, 196 185, 204, 219, 228, 216, 190, 204, 219 185, 202, 180, 185, 172, 161, 182, 146 149, 142, 137, 119, 156, 121, 132, 137 119, 123, 144, 132, 130, 137, 123, 110 96, 106, 121, 112, 100, 125, 299, 114 128, 110, 102, 112, 125, 119, 128, 123 114, 114, 119, 130, 112, 121, 104, 117 119, 125, 114, 114, 135, 123, 119, 102 110, 114, 142, 119, 121, 144, 112, 130 132, 137, 137, 125, 121, 139, 132, 135 156, 135, 146, 149, 172, 149, 156, 185 207, 219, 213, 237, 240, 276, 292, 324 339, 324, 376, 428, 400, 392, 365, 404 335, 365, 320, 269, 250, 256, 216, 202 190, 151, 180, 151, 144, 128, 146, 125 130, 130, 123, 128, 142, 119, 121, 117 144, 139, 125, 108, 128, 112, 135, 128 137, 144, 130, 146, 128, 130, 123, 154 139, 119, 128, 146, 114, 121, 149, 142 146, 146, 159, 149, 132, 130, 149, 137 123, 128, 144, 149, 121, 125, 144, 135 156, 135, 121, 132, 132, 135, 132, 144 139, 144, 135, 151, 135, 151, 177, 151 202, 202, 202, 180, 190, 154, 185, 177 196, 180, 180, 196, 180, 204, 182, 161 164, 169, 182, 169, 132, 146, 159, 132 166, 130, 132, 123, 146, 121, 144, 130 123, 125, 130, 130, 132, 151, 125, 132 108, 142, 159, 128, 149, 135, 114, 132 135, 154, 117, 166, 154, 159, 135, 185 185, 177, 196, 219, 182, 202, 199, 204 190, 182, 202, 207, 219, 202, 243, 262 243, 543, 228, 262, 266, 282, 286, 310 320, 328, 346, 331, 328, 369, 424, 412 428, 458, 433, 437, 424, 428, 380, 372 317, 306, 320, 296, 250, 231, 228, 207 182, 182, 154, 156, 188, 139, 144, 156 154, 169, 149, 190, 169, 164, 149, 172 /