SampleIdent,897C 3R-1 59-60 GLY,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,28-apr-1993 13:26,/ DataAngleRange, 2.0000, 34.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 74, 76, 74, 79, 61, 76, 71, 74 77, 67, 53, 69, 92, 71, 72, 67 67, 79, 88, 72, 81, 72, 72, 69 72, 77, 74, 67, 66, 79, 62, 67 85, 76, 72, 55, 67, 72, 72, 74 71, 56, 56, 69, 71, 76, 79, 61 79, 83, 66, 74, 83, 64, 62, 67 86, 71, 71, 71, 77, 66, 69, 85 72, 61, 56, 56, 77, 66, 59, 66 79, 76, 72, 62, 79, 69, 77, 64 55, 56, 79, 72, 67, 69, 74, 81 79, 50, 76, 56, 71, 53, 67, 71 71, 66, 74, 59, 66, 79, 72, 59 76, 59, 67, 71, 62, 71, 58, 86 55, 77, 50, 66, 72, 61, 72, 58 58, 74, 67, 62, 76, 69, 76, 50 67, 71, 67, 79, 62, 56, 62, 56 67, 48, 67, 53, 72, 64, 71, 58 72, 71, 72, 56, 59, 77, 71, 86 71, 66, 59, 67, 67, 72, 83, 72 62, 83, 77, 62, 92, 79, 66, 67 72, 74, 79, 86, 88, 71, 85, 83 64, 96, 81, 76, 86, 72, 92, 77 74, 74, 76, 76, 76, 81, 77, 86 92, 77, 88, 92, 92, 108, 90, 92 96, 67, 85, 90, 86, 100, 108, 83 92, 98, 102, 96, 88, 104, 98, 117 110, 102, 110, 98, 98, 83, 112, 110 96, 114, 114, 112, 104, 112, 114, 144 121, 137, 117, 114, 130, 130, 142, 135 146, 135, 144, 123, 149, 130, 139, 132 154, 144, 144, 154, 144, 161, 146, 149 135, 146, 159, 164, 159, 154, 159, 182 180, 164, 177, 193, 169, 159, 169, 164 139, 164, 166, 196, 193, 188, 159, 190 222, 182, 185, 204, 190, 193, 213, 210 188, 177, 199, 228, 199, 193, 222, 243 202, 231, 225, 204, 250, 219, 222, 243 269, 253, 246, 228, 240, 228, 259, 256 228, 219, 228, 269, 228, 272, 250, 269 262, 279, 286, 282, 259, 250, 272, 279 269, 253, 266, 272, 240, 317, 282, 289 246, 276, 269, 253, 272, 303, 296, 289 266, 246, 306, 276, 289, 266, 282, 313 286, 276, 272, 286, 303, 299, 279, 296 272, 276, 269, 276, 586, 289, 266, 296 286, 276, 266, 262, 292, 279, 286, 262 262, 286, 296, 272, 282, 276, 246, 296 282, 234, 292, 279, 289, 279, 279, 276 279, 289, 299, 276, 243, 246, 262, 276 256, 289, 276, 269, 286, 259, 266, 269 279, 253, 299, 276, 276, 299, 259, 282 276, 292, 299, 303, 279, 286, 282, 262 269, 299, 303, 279, 272, 266, 279, 276 286, 237, 276, 243, 286, 282, 266, 262 256, 269, 259, 262, 250, 250, 259, 250 276, 250, 292, 262, 286, 246, 282, 250 237, 259, 269, 266, 246, 262, 272, 282 259, 256, 231, 253, 256, 282, 262, 240 234, 262, 262, 259, 266, 259, 234, 225 231, 240, 256, 253, 272, 228, 256, 259 225, 231, 234, 262, 243, 289, 250, 243 234, 228, 256, 237, 243, 256, 246, 222 246, 250, 259, 262, 246, 262, 262, 246 243, 240, 231, 243, 240, 231, 250, 228 243, 250, 240, 228, 246, 246, 237, 222 219, 253, 234, 225, 246, 228, 237, 246 243, 269, 228, 234, 243, 222, 222, 237 231, 276, 243, 240, 228, 207, 231, 237 231, 243, 228, 250, 219, 262, 237, 237 231, 234, 234, 237, 240, 234, 243, 228 213, 234, 246, 243, 253, 225, 243, 279 196, 231, 216, 256, 246, 234, 213, 234 219, 234, 210, 259, 243, 216, 262, 246 231, 259, 240, 272, 246, 246, 225, 234 262, 234, 279, 272, 246, 246, 266, 253 228, 246, 253, 269, 253, 262, 246, 296 262, 266, 266, 296, 262, 269, 243, 243 240, 276, 262, 266, 269, 282, 256, 256 262, 276, 335, 289, 246, 269, 279, 310 306, 279, 303, 299, 289, 303, 317, 303 296, 286, 303, 324, 306, 313, 303, 342 324, 342, 346, 313, 331, 357, 404, 400 357, 369, 376, 404, 400, 412, 424, 420 454, 437, 462, 506, 475, 458, 520, 502 515, 538, 543, 524, 515, 520, 445, 529 458, 467, 437, 441, 412, 388, 392, 388 424, 357, 357, 365, 324, 335, 384, 339 320, 335, 313, 376, 320, 299, 296, 296 317, 306, 303, 306, 269, 272, 303, 289 289, 289, 269, 269, 286, 292, 266, 250 256, 262, 292, 262, 289, 276, 256, 286 276, 253, 259, 237, 266, 246, 243, 234 250, 250, 231, 234, 207, 216, 240, 250 225, 199, 269, 259, 246, 246, 228, 225 246, 250, 243, 246, 269, 185, 231, 237 228, 222, 210, 231, 243, 188, 222, 210 228, 216, 219, 213, 228, 202, 202, 210 216, 204, 210, 225, 213, 216, 185, 225 222, 237, 210, 193, 202, 225, 207, 216 199, 216, 174, 193, 204, 204, 202, 188 204, 177, 219, 207, 180, 213, 188, 185 204, 196, 193, 164, 190, 177, 156, 182 174, 180, 196, 177, 188, 185, 185, 188 156, 193, 177, 182, 169, 144, 169, 164 174, 169, 169, 174, 174, 154, 172, 193 188, 166, 159, 180, 161, 166, 177, 188 169, 177, 199, 164, 174, 172, 177, 164 154, 164, 199, 169, 164, 144, 154, 159 159, 142, 149, 174, 182, 146, 169, 174 164, 169, 166, 164, 156, 144, 149, 159 154, 142, 172, 128, 159, 154, 169, 130 156, 154, 172, 172, 159, 142, 149, 146 161, 135, 151, 159, 161, 156, 154, 149 142, 149, 149, 151, 169, 166, 144, 159 139, 146, 172, 164, 156, 169, 161, 154 149, 154, 185, 177, 159, 137, 144, 166 149, 137, 164, 172, 196, 161, 169, 177 161, 151, 172, 156, 159, 156, 177, 174 164, 177, 166, 196, 174, 151, 151, 172 154, 182, 169, 174, 180, 154, 188, 164 149, 193, 169, 169, 180, 185, 210, 193 169, 177, 196, 182, 180, 190, 193, 188 196, 210, 188, 188, 193, 216, 213, 219 202, 222, 188, 225, 199, 234, 210, 231 225, 253, 231, 243, 240, 240, 243, 253 231, 253, 262, 292, 256, 262, 292, 313 299, 313, 339, 328, 335, 328, 361, 380 353, 388, 380, 404, 412, 416, 416, 404 449, 488, 433, 416, 408, 458, 428, 428 384, 384, 400, 392, 335, 331, 346, 353 320, 538, 324, 296, 286, 276, 282, 246 259, 272, 231, 196, 216, 202, 190, 182 190, 210, 180, 161, 174, 161, 161, 188 156, 177, 174, 174, 159, 164, 154, 159 159, 154, 156, 146, 161, 144, 159, 166 139, 161, 149, 149, 149, 154, 130, 117 130, 144, 117, 119, 139, 119, 182, 123 144, 144, 130, 128, 117, 104, 142, 144 144, 121, 125, 125, 123, 135, 132, 123 123, 125, 128, 123, 130, 114, 121, 119 142, 119, 130, 132, 121, 121, 137, 130 104, 132, 98, 123, 132, 119, 112, 121 135, 121, 119, 123, 102, 102, 104, 146 112, 125, 123, 112, 130, 114, 123, 130 139, 137, 128, 117, 121, 110, 112, 108 121, 104, 135, 108, 108, 121, 121, 128 128, 125, 100, 102, 104, 114, 121, 110 135, 128, 121, 130, 119, 117, 106, 299 121, 106, 117, 121, 108, 98, 112, 123 117, 128, 117, 128, 119, 98, 130, 130 123, 121, 102, 125, 112, 94, 139, 112 108, 106, 106, 112, 112, 132, 130, 121 130, 123, 121, 121, 110, 108, 98, 128 123, 135, 110, 130, 110, 132, 98, 104 104, 132, 132, 108, 110, 102, 100, 119 100, 121, 135, 130, 123, 119, 121, 110 119, 128, 130, 106, 121, 121, 108, 130 106, 137, 117, 108, 117, 106, 114, 106 146, 125, 137, 128, 108, 108, 137, 135 110, 106, 132, 112, 114, 123, 117, 110 114, 121, 130, 123, 130, 112, 137, 108 137, 123, 130, 123, 125, 119, 121, 159 151, 132, 128, 123, 114, 130, 121, 135 121, 130, 137, 128, 137, 130, 112, 146 119, 128, 130, 135, 144, 130, 121, 135 137, 156, 137, 135, 128, 110, 114, 121 128, 154, 137, 144, 112, 123, 154, 142 149, 130, 151, 135, 142, 128, 306, 132 139, 123, 142, 132, 121, 144, 130, 123 142, 137, 132, 123, 144, 149, 169, 146 146, 139, 137, 142, 139, 161, 164, 121 142, 130, 137, 159, 144, 146, 139, 132 149, 132, 156, 146, 132, 151, 149, 149 149, 164, 135, 146, 154, 144, 154, 146 142, 151, 142, 151, 142, 149, 164, 149 137, 139, 135, 161, 159, 149, 130, 146 154, 156, 149, 164, 156, 146, 146, 166 151, 130, 174, 164, 149, 156, 144, 137 156, 142, 156, 149, 154, 151, 177, 149 146, 156, 159, 151, 166, 156, 149, 156 159, 137, 159, 159, 169, 151, 144, 182 180, 156, 149, 172, 159, 177, 146, 161 151, 159, 154, 190, 164, 166, 164, 169 164, 169, 177, 166, 146, 166, 177, 137 169, 166, 177, 164, 156, 166, 182, 159 202, 172, 169, 151, 172, 151, 169, 151 169, 174, 159, 174, 199, 149, 177, 182 182, 182, 219, 196, 164, 169, 174, 180 172, 182, 161, 182, 196, 196, 188, 188 196, 204, 177, 174, 196, 190, 196, 196 210, 159, 190, 166, 204, 174, 207, 202 188, 210, 207, 196, 196, 204, 193, 210 216, 210, 243, 225, 225, 234, 222, 246 259, 231, 222, 286, 219, 276, 276, 276 310, 276, 303, 306, 292, 342, 346, 328 342, 350, 346, 350, 365, 324, 339, 310 320, 299, 313, 313, 306, 282, 286, 286 269, 246, 222, 262, 250, 228, 246, 250 240, 253, 210, 240, 222, 243, 204, 228 216, 213, 207, 213, 225, 210, 207, 207 199, 207, 207, 225, 210, 246, 185, 199 210, 210, 210, 222, 240, 225, 202, 210 202, 210, 222, 219, 193, 210, 204, 216 185, 202, 202, 196, 216, 196, 190, 213 207, 199, 202, 196, 204, 210, 219, 199 190, 193, 199, 216, 199, 196, 190, 202 210, 202, 190, 222, 193, 213, 199, 202 225, 216, 240, 207, 185, 196, 225, 225 190, 213, 210, 210, 199, 213, 199, 219 207, 213, 188, 204, 202, 188, 172, 207 213, 180, 177, 180, 185, 193, 185, 177 202, 185, 199, 164, 190, 193, 199, 193 182, 180, 180, 174, 202, 174, 188, 169 188, 190, 188, 182, 182, 182, 177, 177 185, 196, 177, 204, 199, 190, 193, 196 182, 202, 166, 174, 193, 190, 177, 174 174, 149, 161, 180, 213, 193, 188, 196 174, 182, 180, 182, 177, 166, 193, 210 180, 164, 169, 190, 185, 193, 172, 193 185, 199, 190, 213, 193, 182, 213, 196 190, 193, 182, 177, 185, 172, 213, 174 185, 202, 196, 185, 207, 177, 193, 185 188, 199, 213, 207, 202, 196, 204, 196 188, 199, 159, 196, 185, 185, 182, 177 177, 202, 190, 190, 207, 199, 199, 190 219, 219, 174, 182, 216, 188, 199, 188 193, 196, 210, 185, 199, 185, 234, 199 240, 199, 188, 185, 213, 196, 202, 185 196, 202, 193, 196, 182, 210, 196, 199 213, 216, 161, 193, 172, 193, 199, 196 190, 219, 199, 204, 196, 202, 219, 210 210, 228, 177, 185, 207, 204, 210, 190 190, 190, 199, 210, 202, 237, 174, 213 216, 222, 228, 213, 228, 207, 266, 213 219, 231, 234, 213, 213, 240, 243, 250 225, 228, 213, 222, 225, 185, 190, 196 222, 234, 219, 207, 210, 222, 234, 202 210, 177, 204, 196, 193, 202, 202, 228 193, 225, 207, 219, 222, 213, 222, 222 185, 185, 219, 240, 216, 222, 213, 213 196, 216, 199, 222, 196, 210, 202, 196 196, 196, 237, 204, 225, 231, 210, 225 210, 202, 213, 188, 204, 243, 204, 210 225, 193, 219, 193, 199, 199, 216, 219 240, 213, 222, 219, 216, 228, 213, 199 231, 225, 213, 219, 228, 225, 210, 210 243, 225, 243, 207, 196, 207, 202, 213 219, 231, 246, 219, 256, 204, 216, 213 240, 234, 225, 207, 219, 222, 234, 219 216, 199, 219, 246, 213, 253, 253, 190 253, 250, 231, 237, 204, 225, 231, 253 240, 216, 243, 219, 216, 228, 250, 246 216, 225, 222, 234, 237, 207, 250, 213 246, 231, 511, 243, 234, 237, 222, 219 228, 228, 240, 225, 246, 219, 207, 231 253, 222, 231, 231, 246, 246, 222, 237 225, 240, 262, 243, 240, 253, 256, 213 228, 259, 237, 240, 237, 225, 237, 240 276, 253, 259, 234, 262, 259, 256, 228 246, 246, 240, 240, 243, 231, 237, 237 213, 259, 256, 256, 292, 259, 222, 225 246, 250, 231, 253, 228, 237, 250, 253 234, 240, 269, 237, 246, 234, 262, 250 250, 243, 276, 259, 253, 243, 243, 246 272, 240, 240, 243, 272, 240, 246, 253 279, 272, 262, 246, 240, 250, 219, 253 262, 269, 253, 286, 272, 256, 243, 292 266, 246, 259, 237, 276, 259, 276, 262 256, 266, 269, 250, 250, 286, 259, 296 269, 269, 250, 266, 279, 289, 246, 269 253, 266, 276, 231, 250, 286, 292, 253 256, 282, 262, 272, 259, 306, 299, 262 250, 272, 282, 276, 240, 279, 262, 286 306, 310, 259, 262, 289, 292, 266, 296 279, 272, 320, 286, 282, 256, 259, 272 299, 306, 276, 279, 296, 282, 289, 299 324, 299, 299, 313, 306, 317, 313, 286 306, 346, 335, 289, 286, 310, 320, 320 306, 317, 306, 303, 303, 331, 320, 350 328, 331, 331, 320, 320, 328, 342, 350 346, 339, 342, 342, 353, 342, 342, 372 310, 384, 365, 404, 372, 392, 655, 392 428, 424, 458, 376, 441, 437, 493, 511 506, 467, 475, 534, 524, 557, 520, 520 566, 581, 590, 615, 620, 686, 635, 655 671, 650, 666, 635, 660, 640, 625, 590 576, 557, 615, 595, 548, 520, 586, 480 576, 529, 520, 502, 529, 506, 520, 493 529, 506, 471, 511, 520, 520, 493, 497 515, 502, 475, 524, 520, 520, 529, 437 458, 428, 475, 462, 445, 424, 408, 420 441, 449, 449, 424, 420, 404, 424, 428 428, 408, 437, 400, 428, 396, 412, 416 404, 445, 428, 416, 424, 433, 420, 437 449, 412, 420, 449, 437, 392, 449, 484 404, 441, 445, 454, 475, 449, 416, 488 445, 396, 404, 449, 420, 433, 471, 445 441, 441, 416, 445, 454, 437, 462, 420 475, 484, 471, 462, 475, 449, 520, 458 458, 467, 462, 524, 458, 475, 493, 488 480, 515, 534, 475, 511, 480, 529, 511 524, 557, 520, 520, 557, 552, 548, 529 524, 557, 557, 600, 548, 557, 571, 590 562, 605, 620, 635, 655, 610, 645, 676 645, 660, 718, 686, 702, 713, 734, 729 751, 790, 745, 751, 818, 841, 853, 841 864, 930, 949, 986, 961, 1011, 973, 1018 1011, 1037, 1096, 1096, 1056, 1122, 1050, 1050 1129, 1050, 1037, 1069, 1050, 1011, 1018, 973 936, 930, 906, 942, 835, 801, 767, 734 740, 762, 740, 724, 666, 655, 625, 605 645, 610, 595, 576, 600, 543, 538, 515 590, 538, 506, 529, 552, 538, 552, 511 484, 506, 520, 467, 493, 520, 475, 475 454, 445, 515, 449, 449, 420, 493, 433 471, 445, 454, 428, 424, 428, 420, 392 433, 433, 424, 392, 404, 420, 420, 388 420, 365, 396, 433, 462, 408, 400, 396 416, 384, 392, 384, 365, 380, 392, 384 404, 396, 328, 372, 392, 365, 365, 380 384, 365, 369, 361, 342, 396, 361, 384 339, 365, 361, 350, 324, 388, 369, 350 342, 328, 346, 346, 313, 346, 331, 339 342, 346, 365, 353, 320, 320, 331, 339 335, 350, 331, 306, 303, 292, 313, 303 335, 353, 317, 289, 306, 324, 320, 286 303, 282, 317, 303, 303, 320, 317, 306 292, 296, 313, 286, 286, 286, 310, 279 276, 317, 286, 296, 279, 276, 282, 276 299, 292, 286, 292, 320, 286, 296, 299 272, 296, 313, 289, 289, 262, 320, 286 279, 276, 306, 282, 306, 266, 269, 266 269, 272, 299, 286, 286, 286, 259, 282 310, 262, 276, 276, 289, 279, 259, 266 246, 269, 296, 253, 266, 259, 289, 289 279, 502, 282, 272, 269, 276, 276, 289 282, 266, 276, 272, 303, 279, 282, 282 262, 256, 250, 259, 246, 269, 266, 262 282, 240, 289, 292, 299, 266, 237, 246 282, 246, 272, 250, 262, 286, 250, 272 279, 272, 243, 262, 279, 292, 269, 269 266, 276, 256, 306, 253, 259, 256, 289 256, 246, 272, 292, 225, 250, 289, 279 259, 276, 262, 292, 272, 299, 253, 266 253, 259, 250, 282, 276, 276, 299, 272 262, 289, 279, 282, 246, 279, 266, 237 276, 240, 279, 292, 246, 299, 240, 259 272, 240, 272, 269, 240, 276, 276, 272 292, 276, 262, 256, 269, 259, 243, 272 262, 317, 269, 269, 259, 259, 253, 303 250, 246, 269, 272, 269, 237, 279, 250 259, 228, 292, 246, 282, 262, 256, 262 269, 259, 276, 279, 243, 279, 272, 256 259, 231, 237, 234, 272, 266, 276, 266 246, 259, 292, 259, 266, 266, 282, 272 276, 262, 282, 266, 269, 246, 276, 243 256, 234, 259, 272, 250, 259, 259, 276 256, 246, 262, 240, 289, 256, 282, 262 266, 276, 269, 228, 259, 262, 256, 246 269, 259, 246, 234, 237, 237, 292, 256 276, 243, 256, 250, 299, 259, 259, 250 259, 243, 256, 276, 266, 279, 259, 262 256, 237, 282, 276, 259, 253, 269, 253 282, 250, 282, 253, 276, 272, 269, 250 250, 279, 259, 262, 292, 253, 256, 259 246, 259, 243, 225, 266, 286, 272, 262 262, 246, 256, 259, 272, 276, 246, 262 246, 262, 256, 262, 269, 262, 237, 279 266, 292, 276, 269, 269, 286, 296, 250 286, 272, 256, 262, 296, 256, 256, 276 250, 256, 262, 289, 276, 266, 279, 240 269, 262, 253, 246, 253, 256, 272, 276 250, 262, 231, 246, 279, 243, 259, 256 266, 243, 240, 262, 262, 262, 246, 279 253, 253, 250, 272, 243, 250, 266, 228 253, 240, 243, 276, 250, 266, 231, 286 246, 240, 240, 228, 240, 253, 237, 240 237, 256, 234, 228, 213, 250, 266, 240 234, 234, 210, 256, 243, 243, 219, 250 262, 259, 243, 231, 240, 199, 269, 256 262, 219, 262, 225, 240, 240, 228, 228 276, 237, 246, 222, 228, 266, 234, 237 207, 246, 240, 259, 250, 266, 228, 237 237, 231, 210, 231, 269, 222, 225, 228 237, 228, 210, 253, 240, 234, 234, 237 234, 240, 216, 243, 219, 234, 228, 234 228, 231, 246, 231, 234, 204, 210, 225 216, 225, 225, 225, 228, 231, 246, 225 222, 213, 204, 228, 210, 207, 222, 234 237, 225, 219, 225, 228, 246, 210, 210 210, 225, 213, 219, 213, 202, 231, 219 210, 225, 237, 210, 225, 219, 240, 243 193, 237, 219, 199, 231, 216, 213, 188 225, 231, 234, 210, 204, 213, 240, 219 213, 228, 210, 213, 202, 231, 231, 222 462, 216, 219, 193, 193, 202, 234, 231 188, 225, 216, 228, 188, 207, 225, 207 207, 182, 246, 234, 225, 234, 237, 225 199, 202, 219, 219, 234, 202, 219, 219 190, 202, 202, 207, 225, 210, 177, 199 202, 216, 196, 213, 216, 210, 219, 216 196, 202, 207, 219, 204, 202, 231, 199 196, 193, 193, 199, 222, 234, 219, 228 188, 199, 207, 213, 177, 196, 185, 219 228, 204, 185, 199, 228, 207, 210, 219 202, 222, 202, 188, 219, 246, 222, 202 207, 219, 231, 228, 213, 196, 210, 177 202, 213, 210, 210, 237, 182, 202, 204 225, 185, 199, 213, 190, 213, 204, 228 207, 188, 190, 188, 204, 210, 202, 202 219, 210, 210, 225, 196, 210, 180, 213 185, 219, 216,/