SampleIdent,897C 19R-3 95-95,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,25-mar-1993 17:45,/ DataAngleRange, 2.0000, 34.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 86, 94, 67, 86, 85, 62, 64, 86 76, 71, 79, 86, 71, 72, 88, 69 71, 72, 76, 77, 72, 64, 85, 72 71, 71, 71, 79, 72, 83, 76, 79 90, 86, 71, 72, 98, 83, 88, 64 72, 90, 76, 86, 85, 88, 72, 88 72, 83, 76, 79, 83, 86, 100, 83 69, 72, 92, 72, 62, 62, 100, 86 94, 67, 90, 67, 77, 77, 71, 77 85, 67, 67, 71, 90, 81, 72, 77 71, 76, 59, 79, 79, 71, 74, 81 72, 81, 76, 76, 85, 77, 71, 76 79, 83, 79, 88, 71, 79, 79, 77 79, 67, 83, 81, 83, 90, 86, 86 55, 74, 86, 79, 77, 83, 67, 86 71, 71, 102, 79, 77, 72, 85, 83 96, 74, 85, 76, 88, 79, 67, 76 90, 86, 69, 72, 79, 88, 81, 67 90, 85, 102, 76, 81, 88, 83, 85 92, 74, 90, 67, 88, 85, 77, 86 83, 76, 85, 90, 102, 86, 86, 98 92, 86, 90, 85, 90, 72, 90, 88 92, 96, 96, 85, 88, 92, 104, 112 92, 106, 110, 102, 83, 90, 96, 98 98, 81, 100, 114, 119, 83, 117, 92 88, 86, 94, 85, 66, 100, 98, 86 98, 90, 102, 125, 117, 106, 94, 102 100, 96, 121, 112, 96, 98, 100, 104 108, 114, 102, 114, 114, 110, 108, 90 112, 128, 117, 112, 112, 132, 121, 108 102, 121, 100, 117, 114, 121, 128, 117 117, 106, 112, 121, 128, 100, 106, 102 106, 119, 130, 123, 137, 266, 135, 130 110, 125, 123, 125, 128, 121, 114, 137 128, 121, 121, 112, 130, 123, 166, 128 135, 139, 123, 137, 112, 112, 128, 142 123, 137, 130, 149, 137, 166, 142, 130 121, 137, 154, 144, 137, 137, 142, 142 130, 154, 130, 159, 132, 130, 132, 144 146, 142, 146, 137, 146, 144, 159, 139 154, 125, 132, 135, 139, 159, 125, 130 144, 151, 135, 172, 139, 144, 169, 130 169, 161, 156, 144, 137, 151, 169, 159 146, 151, 159, 182, 139, 149, 149, 146 159, 154, 154, 151, 149, 156, 172, 172 125, 164, 174, 172, 161, 159, 146, 151 144, 154, 144, 161, 149, 149, 156, 139 154, 159, 149, 154, 154, 166, 169, 161 169, 166, 156, 174, 169, 172, 159, 169 156, 182, 159, 151, 159, 156, 172, 182 146, 164, 164, 156, 174, 172, 139, 180 172, 174, 172, 146, 149, 166, 161, 154 172, 180, 166, 149, 199, 190, 164, 188 188, 182, 193, 154, 188, 161, 149, 177 156, 154, 156, 151, 185, 169, 164, 149 159, 154, 161, 164, 172, 149, 166, 149 164, 169, 161, 154, 159, 177, 161, 159 172, 154, 164, 172, 146, 154, 142, 156 164, 169, 149, 149, 169, 169, 159, 154 146, 180, 154, 154, 190, 159, 169, 154 161, 144, 161, 166, 154, 139, 164, 161 182, 174, 169, 164, 156, 172, 156, 159 169, 169, 149, 159, 166, 180, 166, 151 139, 149, 161, 166, 166, 159, 180, 177 146, 161, 161, 144, 177, 174, 154, 154 169, 182, 166, 156, 139, 154, 156, 161 151, 169, 149, 159, 159, 144, 182, 164 177, 185, 166, 156, 166, 154, 166, 137 164, 156, 144, 139, 159, 149, 154, 156 164, 174, 154, 149, 164, 166, 149, 149 161, 166, 151, 174, 166, 154, 144, 156 151, 149, 132, 142, 182, 137, 159, 164 142, 154, 159, 166, 164, 172, 174, 177 144, 144, 156, 174, 156, 161, 164, 161 174, 159, 177, 164, 169, 154, 172, 174 169, 164, 166, 154, 159, 172, 161, 154 159, 151, 159, 172, 164, 144, 156, 396 172, 169, 174, 188, 166, 166, 182, 182 159, 172, 188, 196, 172, 193, 180, 156 182, 196, 151, 188, 188, 193, 182, 202 166, 180, 196, 166, 196, 188, 164, 190 182, 199, 193, 219, 202, 207, 207, 207 204, 213, 213, 222, 210, 237, 250, 213 228, 246, 237, 282, 279, 250, 310, 299 346, 328, 328, 380, 388, 437, 445, 471 488, 488, 520, 484, 506, 493, 511, 534 497, 445, 408, 384, 346, 286, 253, 282 237, 246, 228, 219, 225, 204, 231, 213 207, 188, 193, 188, 190, 174, 177, 177 193, 180, 169, 177, 182, 177, 177, 182 180, 164, 156, 190, 182, 159, 177, 164 164, 182, 154, 164, 159, 169, 144, 154 156, 174, 144, 156, 164, 159, 172, 159 185, 156, 130, 166, 132, 182, 149, 156 154, 144, 149, 144, 149, 154, 159, 188 137, 164, 146, 149, 132, 142, 137, 146 139, 164, 146, 128, 149, 149, 164, 128 149, 149, 130, 135, 139, 121, 130, 172 125, 135, 139, 132, 130, 130, 156, 144 142, 128, 128, 121, 117, 144, 130, 128 276, 149, 114, 135, 154, 142, 137, 142 125, 130, 159, 135, 154, 121, 142, 130 149, 130, 128, 135, 130, 125, 137, 110 159, 139, 119, 149, 132, 144, 119, 125 139, 135, 144, 121, 130, 121, 119, 114 130, 137, 149, 123, 132, 130, 108, 130 128, 106, 135, 114, 135, 142, 135, 117 137, 117, 114, 130, 114, 128, 123, 119 132, 128, 121, 132, 108, 123, 121, 121 121, 130, 123, 114, 146, 146, 154, 132 121, 128, 110, 125, 119, 132, 151, 119 139, 137, 117, 142, 125, 132, 135, 104 137, 125, 137, 130, 114, 125, 119, 132 137, 114, 121, 132, 125, 112, 123, 117 121, 117, 139, 137, 144, 137, 135, 117 121, 151, 139, 130, 139, 119, 114, 98 139, 139, 128, 125, 142, 139, 125, 130 135, 130, 132, 137, 121, 130, 137, 121 142, 128, 135, 128, 125, 130, 151, 144 144, 135, 130, 149, 130, 130, 125, 130 128, 139, 144, 151, 121, 149, 114, 154 146, 130, 137, 137, 137, 132, 142, 132 151, 144, 177, 164, 146, 159, 132, 159 149, 128, 146, 169, 159, 154, 146, 154 161, 161, 156, 174, 164, 164, 190, 161 172, 182, 177, 182, 185, 174, 172, 188 193, 204, 172, 180, 207, 219, 222, 246 210, 246, 253, 276, 234, 256, 272, 253 276, 313, 286, 320, 320, 313, 324, 331 342, 353, 380, 581, 380, 365, 369, 380 376, 380, 400, 380, 376, 380, 365, 369 353, 384, 384, 353, 342, 350, 365, 313 357, 292, 350, 272, 269, 219, 210, 196 193, 185, 207, 166, 166, 142, 149, 172 146, 159, 135, 151, 154, 149, 125, 125 135, 146, 123, 144, 123, 130, 128, 128 125, 132, 132, 121, 149, 149, 104, 117 125, 104, 117, 121, 119, 125, 117, 135 121, 132, 112, 112, 132, 121, 392, 102 106, 112, 108, 110, 106, 128, 119, 125 123, 123, 125, 125, 102, 110, 123, 96 112, 117, 108, 112, 104, 119, 121, 108 110, 100, 119, 108, 123, 104, 112, 110 94, 104, 108, 121, 102, 139, 121, 123 110, 94, 106, 104, 108, 119, 125, 123 102, 135, 130, 142, 108, 125, 108, 110 117, 121, 112, 125, 110, 114, 121, 96 108, 117, 117, 380, 123, 96, 108, 121 104, 117, 121, 119, 117, 135, 117, 121 121, 106, 106, 106, 94, 106, 98, 110 108, 119, 117, 119, 106, 110, 121, 110 110, 102, 121, 112, 117, 119, 114, 144 112, 121, 94, 123, 110, 100, 110, 108 132, 100, 96, 117, 144, 112, 121, 130 110, 125, 102, 104, 106, 114, 96, 90 128, 108, 108, 106, 100, 104, 121, 106 114, 96, 100, 117, 117, 119, 123, 108 110, 112, 90, 96, 114, 106, 92, 110 137, 108, 117, 112, 117, 132, 112, 102 128, 121, 130, 121, 104, 128, 114, 117 114, 98, 132, 130, 110, 121, 121, 117 114, 112, 121, 132, 112, 119, 94, 114 139, 130, 121, 117, 121, 125, 125, 119 132, 102, 130, 114, 146, 123, 125, 117 119, 121, 110, 108, 121, 132, 112, 132 108, 117, 137, 114, 137, 121, 104, 130 106, 114, 110, 96, 104, 112, 139, 104 135, 137, 121, 135, 125, 128, 119, 128 130, 130, 121, 117, 123, 128, 125, 125 112, 119, 137, 125, 128, 135, 110, 132 117, 123, 117, 125, 100, 128, 125, 149 102, 123, 117, 130, 112, 125, 117, 121 128, 125, 132, 119, 119, 117, 121, 125 130, 135, 112, 112, 125, 132, 121, 110 114, 114, 121, 132, 121, 123, 130, 149 117, 146, 112, 121, 130, 130, 121, 123 135, 121, 132, 128, 130, 144, 121, 135 121, 123, 114, 130, 128, 144, 137, 132 123, 130, 121, 119, 135, 119, 125, 117 135, 144, 130, 139, 142, 139, 135, 139 130, 130, 135, 128, 108, 128, 130, 119 128, 132, 135, 123, 149, 149, 135, 139 123, 154, 144, 137, 123, 128, 137, 151 137, 137, 132, 144, 128, 125, 123, 114 119, 146, 154, 132, 154, 149, 123, 139 135, 137, 137, 139, 130, 135, 146, 144 149, 151, 135, 154, 142, 100, 144, 144 149, 149, 154, 139, 125, 132, 174, 166 177, 137, 159, 132, 154, 144, 125, 154 159, 144, 142, 139, 144, 156, 149, 135 142, 159, 146, 166, 154, 154, 166, 174 144, 135, 154, 182, 137, 151, 156, 169 156, 164, 169, 164, 161, 177, 174, 185 164, 169, 193, 174, 180, 172, 182, 193 182, 185, 169, 166, 204, 199, 237, 213 240, 237, 256, 276, 289, 272, 266, 276 303, 328, 335, 342, 365, 449, 365, 449 424, 441, 441, 400, 400, 408, 392, 433 353, 357, 310, 303, 289, 250, 253, 222 243, 216, 210, 207, 185, 199, 188, 193 202, 199, 190, 188, 193, 188, 166, 159 177, 188, 182, 185, 207, 193, 169, 182 174, 182, 190, 185, 182, 188, 159, 188 159, 180, 177, 177, 177, 199, 185, 154 182, 172, 190, 177, 202, 174, 202, 159 172, 177, 185, 161, 188, 185, 164, 193 190, 190, 166, 182, 202, 204, 174, 177 202, 199, 202, 177, 193, 204, 188, 177 185, 199, 188, 219, 172, 210, 213, 231 190, 204, 193, 234, 237, 207, 240, 231 219, 222, 231, 253, 225, 237, 246, 228 240, 237, 219, 213, 199, 199, 199, 213 185, 177, 207, 151, 182, 174, 213, 177 166, 177, 174, 156, 193, 169, 156, 190 172, 151, 172, 177, 182, 166, 149, 164 174, 169, 169, 182, 164, 193, 174, 159 190, 172, 182, 164, 185, 166, 202, 156 177, 210, 188, 174, 199, 169, 190, 185 177, 185, 193, 169, 199, 182, 172, 196 166, 185, 190, 188, 159, 174, 164, 199 182, 177, 190, 164, 174, 188, 185, 185 216, 169, 193, 182, 172, 188, 207, 202 182, 185, 188, 182, 213, 202, 193, 202 202, 196, 182, 188, 190, 231, 225, 174 199, 204, 199, 207, 207, 196, 207, 188 213, 234, 237, 174, 193, 196, 196, 177 222, 216, 182, 188, 174, 185, 210, 182 216, 177, 190, 174, 202, 193, 207, 210 216, 193, 180, 196, 237, 196, 207, 219 193, 169, 202, 204, 180, 204, 213, 216 180, 213, 177, 199, 199, 196, 202, 172 219, 190, 213, 185, 193, 196, 204, 193 207, 216, 193, 207, 213, 196, 204, 202 216, 185, 199, 216, 204, 225, 210, 210 246, 234, 240, 199, 210, 237, 243, 246 266, 243, 253, 259, 262, 259, 289, 282 262, 276, 250, 262, 256, 256, 262, 231 250, 222, 234, 234, 210, 219, 243, 250 228, 213, 225, 207, 225, 190, 240, 216 199, 216, 240, 204, 210, 216, 222, 240 219, 237, 207, 216, 213, 234, 222, 216 213, 199, 222, 207, 222, 225, 202, 222 222, 225, 210, 222, 228, 199, 210, 222 231, 216, 219, 222, 225, 225, 196, 416 222, 222, 225, 216, 228, 219, 240, 243 228, 204, 213, 237, 246, 222, 207, 222 246, 207, 216, 216, 234, 210, 222, 228 222, 196, 253, 213, 219, 250, 240, 219 210, 216, 228, 234, 286, 204, 231, 225 454, 240, 240, 219, 207, 222, 216, 256 237, 228, 250, 237, 225, 202, 246, 240 222, 250, 216, 237, 204, 237, 246, 253 199, 219, 210, 216, 246, 243, 216, 272 219, 234, 253, 231, 207, 231, 250, 240 253, 219, 269, 204, 289, 266, 237, 246 246, 213, 234, 237, 246, 250, 246, 231 240, 225, 253, 253, 207, 237, 231, 234 243, 231, 256, 259, 289, 234, 228, 219 240, 234, 228, 228, 231, 231, 246, 266 259, 262, 253, 256, 253, 253, 228, 234 231, 225, 253, 259, 262, 231, 253, 231 234, 250, 253, 234, 240, 262, 253, 246 228, 262, 259, 237, 259, 237, 256, 234 266, 256, 253, 207, 231, 266, 272, 228 266, 279, 276, 262, 240, 253, 243, 253 253, 240, 222, 292, 228, 256, 250, 234 276, 259, 246, 228, 228, 256, 253, 253 250, 231, 266, 272, 286, 240, 253, 282 256, 286, 231, 266, 243, 246, 272, 256 259, 250, 286, 289, 269, 253, 262, 262 276, 266, 234, 253, 234, 286, 256, 246 279, 246, 276, 262, 256, 250, 253, 276 256, 262, 266, 253, 286, 266, 262, 303 256, 306, 269, 289, 286, 272, 256, 286 276, 276, 272, 282, 269, 256, 272, 269 266, 272, 303, 266, 286, 299, 266, 286 303, 292, 292, 282, 303, 299, 269, 292 299, 276, 279, 286, 289, 269, 286, 286 282, 276, 286, 262, 282, 289, 256, 313 286, 292, 299, 286, 292, 303, 286, 266 306, 289, 289, 299, 317, 320, 320, 328 289, 346, 299, 313, 303, 292, 331, 292 331, 313, 328, 324, 335, 350, 328, 328 335, 335, 339, 380, 365, 376, 372, 376 365, 380, 412, 424, 380, 433, 437, 467 424, 471, 502, 506, 529, 488, 529, 488 529, 552, 515, 515, 571, 562, 548, 548 511, 497, 454, 497, 484, 475, 515, 475 454, 437, 454, 493, 471, 480, 484, 520 467, 524, 449, 493, 511, 524, 520, 571 529, 552, 534, 538, 562, 548, 543, 511 520, 538, 538, 475, 497, 449, 441, 420 433, 424, 392, 372, 361, 380, 380, 342 365, 372, 339, 376, 404, 357, 372, 331 365, 369, 400, 357, 361, 388, 357, 339 342, 353, 353, 346, 392, 328, 328, 384 342, 372, 310, 328, 342, 328, 324, 342 376, 317, 346, 339, 350, 357, 331, 331 320, 299, 342, 324, 346, 353, 350, 361 306, 303, 331, 376, 350, 361, 342, 357 361, 331, 376, 365, 342, 376, 317, 335 299, 357, 350, 361, 331, 365, 353, 380 384, 376, 353, 384, 384, 372, 369, 404 357, 372, 392, 376, 396, 408, 408, 420 400, 384, 408, 428, 404, 449, 437, 420 449, 445, 449, 454, 506, 471, 480, 506 520, 506, 506, 548, 557, 625, 615, 686 718, 756, 778, 812, 853, 847, 853, 930 949, 1018, 1076, 1149, 1096, 1156, 1204, 1211 1274, 1289, 1239, 1246, 1318, 1211, 1310, 1310 1310, 1296, 1239, 1197, 1183, 1183, 1109, 1030 973, 876, 773, 778, 745, 671, 605, 610 552, 524, 511, 502, 471, 480, 449, 392 392, 369, 400, 372, 408, 404, 384, 372 369, 408, 357, 335, 361, 353, 357, 342 324, 350, 324, 350, 320, 353, 328, 331 299, 353, 303, 342, 328, 353, 335, 342 328, 342, 369, 331, 365, 353, 357, 357 400, 380, 384, 384, 342, 400, 361, 376 331, 384, 335, 350, 380, 339, 350, 372 365, 320, 324, 339, 328, 317, 310, 303 296, 279, 313, 299, 328, 353, 286, 299 286, 331, 313, 306, 320, 292, 310, 328 320, 346, 328, 324, 331, 342, 342, 306 335, 306, 324, 353, 313, 328, 335, 328 369, 324, 335, 324, 350, 328, 313, 324 310, 317, 286, 313, 269, 289, 306, 306 303, 306, 289, 276, 282, 272, 276, 250 279, 286, 259, 299, 279, 303, 272, 299 276, 259, 286, 262, 276, 282, 272, 282 269, 262, 259, 299, 237, 272, 292, 250 289, 262, 276, 269, 276, 272, 276, 269 282, 253, 240, 289, 240, 289, 282, 296 279, 243, 266, 272, 250, 253, 299, 237 262, 253, 276, 246, 253, 276, 256, 266 231, 269, 250, 266, 299, 256, 272, 262 262, 269, 256, 282, 256, 276, 269, 259 256, 219, 269, 262, 231, 262, 292, 269 237, 259, 266, 269, 289, 256, 246, 276 286, 282, 262, 272, 276, 269, 286, 246 253, 262, 296, 266, 246, 276, 250, 246 262, 237, 250, 237, 289, 262, 279, 320 282, 269, 313, 303, 276, 269, 246, 272 253, 276, 282, 279, 256, 262, 256, 259 246, 259, 299, 292, 262, 246, 272, 246 266, 246, 240, 269, 296, 269, 276, 234 246, 253, 256, 262, 282, 259, 272, 250 246, 286, 266, 286, 240, 253, 237, 276 262, 276, 259, 269, 269, 256, 272, 259 243, 272, 279, 276, 266, 272, 266, 246 286, 266, 272, 234, 289, 246, 272, 276 228, 253, 246, 276, 237, 262, 266, 279 259, 237, 292, 279, 250, 289, 256, 237 256, 276, 266, 256, 286, 262, 234, 256 250, 243, 253, 237, 240, 253, 266, 253 246, 262, 246, 272, 250, 246, 246, 276 253, 237, 246, 243, 253, 237, 240, 262 269, 282, 237, 240, 246, 256, 250, 234 231, 269, 240, 259, 259, 253, 246, 237 256, 276, 282, 259, 262, 262, 234, 272 282, 272, 259, 266, 286, 299, 292, 262 279, 292, 276, 272, 266, 299, 250, 272 253, 276, 250, 266, 303, 253, 266, 279 289, 259, 259, 259, 279, 276, 262, 262 231, 262, 228, 279, 246, 266, 262, 237 253, 246, 289, 240, 269, 240, 259, 259 259, 276, 269, 246, 256, 262, 262, 266 240, 243, 282, 269, 256, 266, 272, 266 243, 279, 286, 272, 256, 262, 262, 259 272, 296, 279, 259, 279, 324, 286, 299 272, 306, 306, 289, 282, 276, 279, 303 292, 262, 296, 240, 292, 266, 289, 256 253, 266, 240, 266, 234, 243, 269, 253 269, 250, 234, 256, 256, 240, 237, 272 269, 266, 228, 250, 259, 253, 243, 250 243, 243, 262, 269, 231, 240, 256, 228 269, 237, 250, 237, 246, 237, 234, 256 234, 213, 246, 237, 256, 243, 246, 213 240, 253, 269, 234, 210, 219, 225, 246 231, 231, 237, 234, 231, 234, 250, 222 213, 243, 216, 240, 243, 213, 250, 237 234, 216, 234, 234, 202, 250, 240, 243 234, 228, 237, 193, 222, 237, 234, 243 225, 222, 282, 250, 204, 225, 222, 228 225, 228, 219, 237, 207, 204, 222, 225 222, 237, 225, 216, 266, 207, 240, 202 246, 219, 222, 196, 213, 219, 246, 228 207, 228, 196, 240, 210, 222, 222, 210 225, 222, 219, 237, 213, 228, 225, 234 213, 222, 231, 228, 204, 207, 240, 213 216, 234, 237, 216, 222, 190, 225, 207 210, 240, 219, 225, 207, 228, 243, 219 228, 196, 231, 210, 225, 216, 240, 222 228, 207, 225, 213, 202, 202, 207, 259 243, 210, 234, 188, 216, 207, 207, 246 207, 228, 240, 204, 199, 210, 190, 216 216, 250, 207, 202, 216, 207, 188, 250 207, 204, 231, 204, 202, 210, 213, 213 240, 199, 204, 219, 213, 182, 210, 213 222, 188, 213, 199, 228, 213, 199, 213 231, 193, 202, 210, 210, 225, 202, 202 196, 196, 207, 190, 222, 207, 193, 202 210, 222, 219, 213, 207, 210, 225, 207 216, 210, 202, 193, 188, 207, 225, 196 166, 213, 216, 196, 207, 188, 210, 204 222, 199, 190, 216, 231, 237, 210, 199 210, 196, 204, 199, 237, 199, 210, 216 193, 222, 207, 204, 202, 202, 234, 210 216, 210, 234, 207, 185, 216, 213, 210 188, 207, 228, 210, 225, 188, 190, 210 210, 210, 202, 202, 199, 207, 225, 222 196, 196, 188, 213, 193, 204, 207, 228 196, 219, 216,/