SampleIdent,897C 31R-1 93-94 GLY,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,29-apr-1993 4:18,/ DataAngleRange, 2.0000, 34.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 77, 83, 76, 90, 83, 74, 88, 79 74, 72, 77, 77, 69, 76, 86, 85 72, 76, 286, 76, 86, 76, 71, 79 92, 71, 85, 64, 85, 94, 72, 67 72, 79, 66, 98, 71, 81, 67, 74 85, 85, 77, 85, 94, 76, 79, 74 85, 86, 66, 86, 98, 88, 77, 77 77, 53, 71, 81, 79, 66, 76, 90 79, 71, 66, 66, 77, 71, 90, 83 79, 59, 79, 90, 62, 85, 100, 86 74, 76, 90, 85, 72, 69, 88, 71 66, 79, 69, 77, 71, 69, 72, 69 74, 71, 83, 76, 86, 79, 71, 76 71, 76, 81, 102, 74, 79, 86, 79 79, 77, 72, 110, 83, 81, 88, 66 96, 85, 76, 74, 79, 85, 79, 79 88, 79, 77, 83, 71, 90, 72, 90 85, 88, 79, 83, 83, 83, 90, 94 76, 88, 77, 92, 79, 299, 98, 85 90, 94, 79, 88, 92, 94, 79, 100 88, 88, 81, 94, 102, 88, 121, 104 110, 112, 92, 100, 119, 137, 102, 106 112, 104, 92, 121, 98, 96, 125, 104 132, 117, 117, 121, 132, 112, 108, 130 117, 137, 130, 121, 125, 137, 135, 139 144, 137, 130, 146, 137, 123, 149, 112 151, 142, 144, 130, 144, 161, 130, 146 151, 144, 149, 156, 159, 166, 164, 169 169, 166, 169, 161, 156, 177, 164, 166 169, 180, 164, 169, 188, 185, 174, 196 188, 190, 188, 196, 188, 202, 185, 207 190, 210, 210, 182, 193, 199, 204, 210 228, 237, 210, 216, 225, 231, 222, 207 225, 237, 207, 228, 272, 234, 250, 259 240, 243, 231, 237, 250, 246, 253, 237 256, 253, 282, 246, 253, 262, 276, 262 286, 292, 296, 253, 269, 276, 256, 250 296, 234, 269, 299, 313, 296, 310, 299 299, 306, 313, 313, 320, 289, 286, 299 313, 289, 317, 313, 310, 335, 310, 310 342, 313, 320, 303, 306, 317, 320, 306 299, 282, 310, 320, 303, 306, 328, 292 286, 289, 331, 335, 342, 328, 320, 320 296, 306, 328, 328, 299, 313, 292, 335 313, 310, 303, 292, 289, 313, 303, 292 272, 296, 282, 276, 303, 303, 253, 286 246, 292, 279, 282, 292, 303, 306, 269 299, 250, 253, 292, 259, 276, 296, 272 328, 259, 243, 269, 262, 286, 292, 266 256, 303, 279, 279, 266, 289, 276, 256 259, 246, 276, 256, 269, 262, 266, 266 256, 225, 219, 243, 246, 228, 253, 228 225, 240, 259, 228, 228, 253, 259, 259 256, 246, 259, 225, 237, 234, 234, 204 231, 219, 234, 213, 231, 216, 231, 237 213, 231, 228, 246, 225, 231, 234, 234 231, 222, 231, 250, 231, 216, 222, 234 228, 240, 228, 213, 219, 231, 253, 228 222, 216, 231, 228, 210, 246, 246, 219 213, 207, 196, 207, 204, 228, 225, 213 204, 207, 196, 216, 240, 222, 237, 219 269, 219, 222, 213, 193, 174, 243, 204 225, 196, 210, 216, 188, 234, 202, 228 190, 216, 190, 196, 199, 196, 234, 219 228, 219, 222, 202, 210, 216, 231, 231 174, 196, 219, 177, 199, 213, 202, 219 207, 228, 196, 210, 207, 216, 219, 231 190, 207, 225, 204, 207, 216, 188, 210 202, 199, 190, 219, 210, 210, 185, 196 234, 207, 222, 204, 202, 202, 207, 207 190, 234, 180, 196, 213, 188, 216, 225 199, 210, 225, 202, 216, 222, 207, 213 231, 243, 199, 222, 193, 202, 237, 219 207, 202, 213, 207, 237, 240, 237, 222 219, 204, 243, 237, 222, 243, 231, 185 207, 237, 240, 228, 246, 250, 246, 243 228, 256, 243, 216, 253, 262, 259, 219 259, 250, 246, 225, 253, 256, 234, 262 240, 259, 269, 262, 256, 256, 266, 256 299, 266, 276, 276, 256, 299, 286, 262 253, 320, 306, 286, 320, 342, 299, 317 346, 313, 306, 342, 350, 331, 331, 361 357, 392, 392, 392, 392, 400, 433, 433 471, 462, 437, 467, 449, 467, 515, 467 524, 445, 454, 449, 506, 480, 428, 458 454, 441, 404, 392, 384, 388, 400, 342 342, 324, 350, 361, 328, 328, 331, 303 335, 310, 317, 276, 306, 292, 296, 272 299, 269, 279, 259, 266, 272, 253, 279 259, 262, 259, 240, 266, 250, 279, 269 225, 234, 234, 216, 246, 240, 243, 222 246, 240, 266, 213, 231, 228, 202, 225 225, 228, 216, 219, 234, 204, 216, 222 246, 219, 228, 216, 222, 216, 222, 199 228, 234, 216, 207, 204, 225, 234, 219 256, 210, 228, 199, 219, 222, 193, 216 222, 202, 246, 222, 182, 253, 222, 231 216, 222, 234, 199, 204, 196, 216, 199 196, 216, 207, 202, 237, 193, 210, 210 213, 210, 177, 237, 207, 199, 193, 199 207, 222, 182, 202, 207, 196, 219, 196 196, 174, 199, 219, 207, 188, 210, 210 231, 231, 199, 182, 182, 210, 193, 204 196, 207, 202, 190, 172, 196, 202, 188 177, 190, 164, 161, 202, 180, 182, 169 193, 185, 161, 169, 188, 185, 188, 188 204, 180, 188, 172, 169, 172, 177, 161 185, 161, 159, 164, 174, 177, 180, 182 161, 169, 154, 149, 172, 151, 174, 174 172, 164, 169, 166, 174, 169, 151, 177 161, 164, 156, 172, 365, 177, 161, 164 182, 169, 161, 164, 164, 132, 166, 169 164, 188, 159, 174, 159, 159, 169, 164 154, 149, 137, 159, 164, 180, 177, 164 151, 154, 149, 172, 156, 164, 182, 169 174, 166, 151, 169, 164, 156, 174, 154 164, 159, 161, 149, 172, 154, 149, 174 174, 188, 151, 193, 159, 169, 164, 515 177, 164, 174, 149, 174, 185, 182, 172 196, 180, 182, 182, 161, 182, 177, 174 169, 196, 164, 166, 185, 174, 207, 177 225, 204, 174, 210, 196, 204, 210, 213 202, 199, 222, 219, 231, 225, 222, 243 237, 222, 253, 256, 272, 259, 259, 276 269, 272, 259, 269, 310, 292, 279, 299 286, 306, 299, 313, 310, 331, 384, 365 357, 404, 369, 384, 369, 408, 404, 396 454, 449, 480, 445, 458, 502, 475, 488 445, 449, 441, 445, 412, 471, 412, 396 412, 412, 392, 380, 372, 342, 339, 310 369, 276, 299, 306, 292, 299, 289, 237 231, 237, 246, 256, 228, 216, 225, 210 210, 219, 196, 190, 196, 161, 196, 174 172, 185, 182, 172, 142, 159, 182, 156 166, 177, 156, 139, 164, 161, 156, 139 149, 164, 139, 146, 151, 144, 132, 151 146, 112, 164, 144, 137, 144, 130, 149 123, 137, 125, 137, 132, 132, 114, 125 125, 114, 132, 117, 130, 144, 119, 130 112, 128, 137, 121, 132, 106, 149, 128 121, 112, 117, 135, 130, 130, 144, 137 125, 125, 110, 110, 128, 125, 119, 123 108, 125, 110, 123, 130, 119, 104, 144 135, 130, 156, 132, 106, 114, 92, 151 123, 125, 137, 146, 112, 132, 108, 117 137, 144, 121, 144, 121, 110, 128, 130 130, 110, 112, 110, 128, 123, 123, 130 117, 135, 108, 102, 100, 130, 123, 132 112, 108, 137, 119, 142, 125, 137, 128 130, 114, 128, 119, 144, 110, 123, 149 119, 130, 102, 128, 123, 128, 102, 139 132, 121, 121, 142, 119, 130, 125, 117 121, 121, 132, 110, 135, 114, 130, 144 108, 112, 123, 121, 130, 121, 117, 123 135, 110, 106, 121, 123, 121, 121, 130 117, 121, 139, 146, 117, 137, 149, 139 117, 135, 128, 132, 144, 130, 128, 137 121, 146, 132, 119, 125, 130, 128, 137 137, 125, 130, 154, 117, 149, 117, 142 161, 139, 112, 132, 144, 146, 130, 132 159, 144, 151, 156, 128, 128, 137, 142 135, 164, 137, 139, 135, 121, 154, 144 135, 139, 149, 142, 144, 135, 154, 156 149, 149, 149, 137, 135, 137, 172 164, 146, 174, 182, 154, 154, 146, 169 172, 180, 151, 159, 169, 166, 172, 174 172, 174, 202, 182, 172, 154, 174, 204 169, 185, 190, 159, 188, 135, 174, 164 174, 174, 154, 164, 161, 166, 154, 164 159, 159, 199, 164, 180, 177, 142, 172 177, 164, 174, 159, 149, 156, 149, 146 164, 151, 166, 174, 180, 154, 172, 146 182, 149, 169, 161, 174, 174, 180, 151 164, 169, 139, 169, 161, 185, 169, 164 146, 164, 159, 164, 169, 172, 154, 156 156, 174, 156, 161, 146, 154, 154, 154 166, 161, 169, 151, 172, 159, 161, 161 180, 161, 156, 202, 166, 154, 190, 177 177, 164, 166, 142, 193, 172, 182, 169 166, 169, 169, 172, 188, 177, 154, 177 177, 174, 172, 174, 151, 161, 174, 174 159, 151, 146, 154, 164, 149, 149, 151 156, 164, 149, 154, 156, 156, 149, 149 151, 156, 135, 144, 149, 159, 146, 177 123, 156, 174, 161, 142, 132, 164, 156 159, 130, 149, 154, 156, 164, 169, 149 159, 137, 139, 137, 144, 174, 164, 135 137, 182, 135, 151, 161, 180, 172, 146 169, 149, 156, 154, 144, 142, 154, 172 156, 164, 166, 166, 144, 151, 146, 142 149, 149, 151, 146, 166, 128, 177, 146 149, 139, 149, 137, 123, 154, 149, 142 137, 154, 149, 177, 164, 166, 177, 142 161, 169, 159, 149, 137, 139, 172, 156 159, 159, 161, 156, 142, 164, 149, 142 164, 169, 154, 166, 159, 151, 180, 164 161, 156, 144, 144, 169, 172, 156, 154 182, 144, 161, 149, 159, 159, 172, 161 169, 149, 177, 169, 151, 172, 180, 149 149, 174, 154, 161, 174, 169, 154, 154 174, 169, 166, 172, 172, 164, 149, 161 135, 166, 169, 164, 177, 177, 137, 182 142, 164, 164, 164, 154, 174, 149, 172 149, 188, 144, 149, 199, 169, 154, 174 154, 166, 159, 164, 164, 202, 164, 156 139, 172, 164, 149, 154, 174, 161, 185 172, 164, 182, 132, 161, 177, 154, 180 180, 156, 193, 166, 169, 169, 185, 166 164, 185, 180, 185, 182, 169, 196, 174 213, 164, 172, 166, 185, 190, 185, 188 188, 169, 169, 193, 174, 177, 182, 213 174, 182, 188, 174, 180, 182, 188, 161 193, 177, 172, 166, 182, 210, 204, 182 182, 213, 185, 185, 177, 196, 207, 199 204, 188, 188, 231, 190, 185, 190, 199 219, 174, 204, 193, 225, 204, 199, 204 190, 207, 213, 222, 225, 231, 199, 219 196, 228, 202, 219, 454, 199, 204, 243 228, 219, 213, 222, 219, 196, 222, 204 207, 259, 246, 222, 222, 246, 269, 216 256, 250, 246, 234, 234, 279, 246, 225 262, 256, 253, 253, 276, 279, 286, 296 317, 292, 299, 292, 286, 299, 282, 269 296, 282, 299, 310, 296, 303, 365, 299 339, 353, 350, 353, 361, 369, 369, 384 372, 365, 372, 420, 420, 420, 428, 458 433, 467, 488, 502, 493, 543, 520, 552 581, 566, 630, 620, 620, 660, 630, 650 718, 681, 660, 729, 740, 729, 778, 751 773, 729, 790, 807, 745, 756, 784, 767 790, 756, 790, 729, 734, 702, 610, 676 708, 676, 671, 635, 635, 625, 586, 620 571, 562, 605, 590, 581, 562, 548, 566 534, 529, 562, 586, 475, 557, 493, 557 480, 511, 534, 502, 467, 497, 497, 497 475, 493, 493, 428, 524, 484, 484, 488 462, 441, 480, 462, 471, 458, 488, 454 467, 471, 497, 475, 493, 467, 480, 449 480, 462, 480, 511, 488, 475, 471, 493 506, 497, 506, 515, 484, 548, 543, 524 497, 534, 529, 488, 543, 497, 506, 534 543, 488, 538, 502, 484, 566, 595, 562 548, 562, 534, 562, 590, 586, 590, 610 581, 538, 600, 605, 610, 595, 586, 557 595, 615, 595, 595, 630, 600, 620, 713 697, 640, 702, 640, 692, 671, 708, 681 640, 734, 729, 745, 756, 756, 734, 734 778, 818, 829, 801, 847, 858, 818, 876 847, 924, 894, 900, 906, 918, 961, 1018 961, 1096, 1063, 1129, 1176, 1142, 1197, 1253 1310, 1369, 1303, 1303, 1436, 1369, 1475, 1482 1521, 1560, 1584, 1513, 1673, 1592, 1673, 1624 1624, 1681, 1552, 1624, 1592, 1552, 1608, 1608 1560, 1467, 1436, 1354, 1347, 1282, 1253, 1289 1197, 1136, 1089, 1037, 1056, 1024, 949, 870 870, 824, 858, 795, 864, 795, 745, 724 692, 692, 635, 702, 635, 600, 655, 635 635, 581, 615, 562, 557, 590, 576, 538 566, 538, 506, 534, 548, 493, 515, 520 538, 488, 502, 502, 538, 520, 462, 471 445, 458, 506, 424, 493, 484, 454, 458 449, 445, 408, 441, 437, 449, 412, 462 392, 449, 437, 400, 424, 396, 396, 441 424, 384, 384, 384, 353, 380, 388, 350 331, 416, 353, 361, 331, 376, 346, 372 350, 353, 372, 342, 346, 380, 320, 328 350, 342, 306, 331, 339, 361, 313, 342 331, 310, 306, 306, 342, 303, 299, 306 313, 317, 292, 317, 335, 324, 272, 296 310, 292, 243, 313, 272, 266, 296, 296 286, 286, 269, 269, 292, 250, 246, 276 286, 282, 269, 276, 243, 259, 299, 262 272, 262, 272, 262, 286, 253, 253, 259 240, 259, 282, 243, 266, 262, 272, 502 276, 269, 282, 246, 234, 240, 259, 234 262, 259, 286, 256, 225, 216, 256, 240 269, 253, 266, 269, 243, 234, 253, 231 231, 228, 237, 234, 222, 243, 250, 219 276, 213, 231, 259, 246, 259, 246, 250 276, 240, 231, 253, 246, 234, 222, 262 250, 231, 219, 240, 216, 243, 250, 256 259, 231, 259, 228, 240, 222, 253, 237 231, 237, 240, 246, 243, 234, 240, 246 234, 269, 237, 237, 234, 237, 250, 246 225, 234, 243, 213, 240, 219, 216, 240 246, 219, 237, 246, 231, 250, 228, 246 216, 225, 225, 266, 237, 250, 231, 231 253, 228, 250, 219, 207, 256, 240, 231 213, 243, 243, 222, 231, 243, 228, 219 256, 228, 193, 246, 219, 266, 228, 222 240, 256, 219, 243, 213, 253, 262, 250 259, 231, 250, 225, 213, 246, 240, 228 231, 237, 234, 219, 207, 256, 234, 253 234, 219, 237, 231, 234, 216, 237, 240 228, 234, 237, 240, 196, 210, 199, 216 216, 243, 204, 202, 222, 240, 240, 210 253, 228, 228, 228, 231, 246, 210, 196 228, 240, 240, 213, 231, 231, 213, 228 199, 228, 234, 228, 243, 228, 225, 234 240, 210, 253, 216, 231, 246, 266, 231 231, 228, 243, 256, 219, 266, 219, 246 210, 234, 253, 231, 216, 240, 219, 231 225, 199, 219, 256, 231, 266, 237, 256 272, 243, 237, 210, 240, 225, 250, 222 269, 234, 216, 219, 234, 237, 243, 234 262, 259, 246, 234, 237, 228, 243, 228 262, 256, 228, 250, 259, 256, 250, 243 269, 246, 266, 266, 250, 246, 253, 240 243, 234, 246, 240, 225, 222, 259, 237 246, 282, 276, 243, 237, 289, 262, 237 262, 262, 256, 259, 266, 292, 269, 234 292, 243, 243, 276, 276, 253, 279, 246 250, 256, 286, 266, 259, 276, 259, 259 243, 240, 256, 262, 266, 292, 262, 276 262, 292, 253, 266, 282, 279, 246, 246 259, 246, 282, 276, 234, 253, 246, 250 237, 259, 276, 228, 240, 259, 246, 231 272, 228, 231, 240, 253, 225, 262, 228 279, 276, 259, 243, 250, 246, 228, 234 269, 231, 228, 250, 207, 210, 219, 269 256, 228, 219, 222, 237, 225, 210, 231 219, 228, 225, 237, 216, 243, 237, 228 225, 228, 213, 210, 231, 246, 216, 196 210, 213, 204, 210, 234, 240, 199, 216 216, 204, 210, 207, 204, 207, 213, 199 193, 202, 199, 222, 207, 234, 196, 180 204, 172, 228, 188, 204, 204, 196, 188 216, 213, 228, 210, 182, 202, 196, 210 204, 185, 210, 169, 210, 188, 204, 193 204, 190, 225, 166, 231, 188, 207, 193 177, 169, 185, 174, 180, 207, 204, 172 204, 180, 188, 156, 190, 188, 149, 185 166, 172, 188, 169, 202, 185, 166, 202 202, 199, 177, 185, 193, 177, 169, 169 164, 180, 193, 196, 185, 185, 177, 164 144, 204, 177, 180, 196, 199, 202, 172 164, 161, 169, 177, 174, 166, 188, 177 199, 177, 164, 180, 164, 159, 174, 159 166, 174, 182, 180, 180, 169, 169, 185 174, 174, 159, 182, 174, 156, 146, 174 185, 174, 161, 161, 169, 154, 137, 174 174, 159, 213, 161, 177, 169, 154, 180 180, 151, 149, 172, 144, 164, 166, 159 177, 193, 144, 177, 169, 169, 161, 164 177, 164, 151, 174, 166, 144, 164, 185 159, 144, 174, 169, 169, 177, 161, 193 146, 159, 151, 161, 142, 161, 204, 174 161, 166, 177, 159, 185, 169, 169, 180 161, 142, 161, 159, 164, 166, 156, 174 185, 180, 172, 149, 149, 164, 185, 144 161, 193, 190, 159, 156, 164, 166, 169 169, 154, 142, 159, 172, 154, 172, 149 177, 144, 151, 149, 169, 161, 169, 161 169, 177, 174, 164, 154, 174, 185, 146 164, 159, 156, 169, 172, 161, 193, 185 159, 154, 166, 177, 185, 174, 151, 188 149, 172, 182,/