SampleIdent,897C 31R-3 119-121,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,25-mar-1993 12:57,/ DataAngleRange, 2.0000, 34.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 92, 90, 92, 79, 72, 67, 77, 85 83, 71, 69, 72, 77, 81, 98, 92 76, 72, 83, 94, 62, 72, 72, 83 81, 72, 76, 76, 62, 86, 83, 79 72, 67, 77, 92, 94, 86, 53, 90 67, 77, 98, 71, 72, 100, 71, 90 67, 83, 79, 83, 76, 67, 88, 71 76, 77, 67, 79, 86, 92, 86, 88 72, 69, 88, 71, 72, 76, 76, 77 86, 81, 77, 77, 85, 83, 85, 79 88, 86, 98, 86, 76, 71, 86, 83 92, 76, 85, 83, 88, 81, 86, 79 72, 74, 90, 64, 83, 67, 98, 76 72, 69, 72, 77, 67, 100, 85, 88 79, 83, 85, 79, 92, 83, 77, 66 79, 76, 92, 98, 81, 81, 77, 76 83, 92, 92, 61, 76, 81, 74, 72 85, 77, 81, 90, 98, 94, 77, 72 85, 76, 77, 79, 94, 79, 79, 83 98, 64, 88, 90, 69, 76, 76, 79 71, 86, 88, 67, 90, 104, 77, 94 86, 81, 83, 66, 83, 92, 77, 83 76, 83, 72, 85, 77, 85, 81, 98 81, 85, 94, 98, 96, 83, 85, 102 74, 92, 66, 81, 96, 76, 96, 85 90, 83, 83, 86, 88, 94, 74, 86 108, 74, 90, 102, 88, 92, 96, 94 86, 88, 83, 108, 88, 67, 83, 77 79, 86, 85, 88, 100, 74, 83, 76 74, 85, 96, 83, 86, 76, 79, 98 86, 83, 92, 88, 106, 94, 86, 88 85, 100, 90, 79, 71, 88, 96, 100 90, 86, 96, 71, 79, 85, 100, 71 100, 77, 79, 85, 92, 88, 98, 104 90, 98, 106, 94, 98, 83, 100, 90 119, 88, 83, 79, 96, 92, 88, 88 83, 108, 90, 90, 100, 85, 100, 104 100, 92, 76, 81, 92, 90, 96, 102 106, 92, 85, 100, 100, 86, 104, 104 108, 94, 88, 96, 110, 94, 100, 102 104, 110, 114, 100, 102, 94, 106, 90 79, 112, 92, 100, 96, 94, 88, 110 102, 98, 96, 81, 94, 98, 92, 106 112, 112, 106, 79, 96, 96, 104, 123 106, 94, 108, 90, 94, 102, 98, 110 104, 88, 94, 106, 96, 92, 104, 104 104, 86, 94, 104, 106, 96, 123, 104 100, 102, 112, 98, 123, 88, 114, 96 102, 98, 106, 123, 106, 94, 98, 114 92, 121, 110, 96, 114, 94, 108, 108 110, 119, 110, 110, 110, 114, 112, 102 128, 137, 112, 102, 108, 121, 128, 119 106, 108, 94, 121, 104, 104, 94, 125 104, 137, 108, 108, 102, 110, 114, 137 114, 108, 114, 119, 132, 433, 110, 112 104, 106, 119, 112, 110, 98, 90, 96 121, 102, 119, 121, 121, 102, 98, 104 106, 119, 121, 123, 121, 121, 110, 135 110, 106, 117, 128, 112, 119, 88, 119 110, 117, 119, 125, 106, 98, 114, 132 125, 102, 119, 125, 117, 128, 137, 94 96, 114, 121, 114, 125, 114, 112, 139 117, 117, 112, 132, 117, 123, 104, 100 121, 119, 119, 98, 112, 94, 108, 121 92, 146, 114, 110, 92, 119, 90, 144 125, 121, 121, 108, 132, 102, 112, 125 98, 135, 119, 98, 128, 117, 102, 100 104, 108, 117, 117, 117, 108, 100, 110 125, 135, 106, 130, 94, 119, 117, 110 137, 125, 117, 96, 100, 125, 128, 117 121, 128, 117, 125, 100, 108, 117, 104 108, 108, 125, 119, 125, 125, 125, 121 135, 108, 112, 139, 104, 119, 128, 100 108, 130, 112, 114, 98, 114, 119, 121 128, 104, 100, 137, 119, 98, 128, 121 112, 130, 121, 112, 123, 117, 130, 130 128, 135, 146, 137, 123, 128, 132, 121 112, 121, 132, 104, 135, 137, 114, 121 149, 154, 119, 139, 137, 159, 154, 154 159, 154, 172, 188, 174, 174, 190, 161 169, 177, 137, 149, 149, 161, 164, 104 137, 117, 128, 132, 128, 114, 110, 104 121, 104, 123, 114, 108, 110, 125, 119 121, 132, 110, 117, 108, 110, 128, 117 123, 100, 112, 121, 106, 125, 119, 130 104, 108, 108, 83, 117, 117, 108, 121 128, 100, 125, 98, 121, 108, 117, 119 96, 104, 108, 117, 86, 123, 112, 117 96, 110, 100, 119, 88, 110, 108, 112 92, 117, 114, 119, 98, 117, 108, 100 125, 128, 114, 112, 114, 114, 121, 114 102, 108, 121, 104, 112, 119, 114, 123 128, 117, 94, 130, 86, 110, 125, 117 106, 100, 110, 92, 123, 98, 98, 110 108, 96, 85, 77, 92, 121, 121, 90 94, 96, 112, 100, 94, 108, 112, 106 106, 96, 110, 110, 112, 104, 86, 98 102, 108, 117, 114, 104, 119, 104, 108 125, 108, 114, 128, 110, 114, 121, 119 104, 110, 119, 121, 112, 94, 106, 117 128, 88, 92, 90, 100, 106, 112, 104 112, 96, 106, 90, 121, 110, 96, 104 100, 106, 104, 92, 117, 92, 106, 117 104, 112, 108, 114, 110, 100, 108, 121 98, 96, 104, 110, 102, 121, 114, 114 94, 83, 100, 96, 92, 92, 125, 117 96, 102, 98, 104, 102, 114, 102, 114 121, 108, 112, 100, 117, 102, 86, 100 117, 110, 104, 123, 104, 108, 117, 100 102, 94, 125, 110, 106, 110, 104, 106 114, 96, 108, 123, 94, 128, 110, 110 104, 88, 90, 106, 119, 108, 92, 108 104, 112, 88, 106, 92, 121, 102, 114 88, 110, 104, 100, 123, 125, 108, 117 88, 102, 112, 112, 100, 114, 102, 96 83, 110, 108, 117, 119, 94, 117, 108 98, 96, 86, 110, 112, 90, 100, 110 102, 112, 100, 110, 121, 94, 114, 114 104, 114, 90, 125, 119, 119, 128, 104 98, 112, 114, 121, 132, 94, 112, 100 100, 117, 123, 121, 137, 112, 117, 125 104, 121, 117, 121, 117, 121, 121, 125 121, 142, 137, 137, 144, 146, 135, 135 139, 123, 144, 149, 132, 164, 144, 164 149, 139, 151, 151, 130, 161, 156, 132 135, 154, 142, 169, 146, 149, 159, 164 144, 177, 130, 144, 144, 112, 117, 137 119, 135, 121, 121, 117, 123, 90, 130 117, 135, 117, 102, 137, 100, 102, 86 108, 112, 119, 106, 117, 112, 114, 117 98, 104, 106, 117, 92, 128, 92, 96 123, 110, 102, 83, 96, 119, 100, 104 114, 88, 96, 125, 112, 114, 106, 100 94, 96, 96, 130, 110, 108, 86, 108 106, 92, 98, 104, 110, 112, 86, 94 102, 85, 98, 108, 92, 100, 119, 86 96, 108, 88, 96, 112, 104, 96, 110 102, 77, 108, 106, 98, 108, 86, 125 98, 112, 117, 108, 114, 100, 102, 108 102, 96, 102, 106, 110, 102, 90, 102 104, 108, 142, 102, 108, 110, 96, 108 100, 106, 121, 90, 96, 94, 110, 102 90, 96, 96, 100, 92, 96, 110, 100 108, 100, 98, 81, 94, 88, 90, 117 98, 104, 86, 108, 88, 96, 94, 110 112, 102, 90, 112, 108, 117, 100, 114 79, 98, 125, 100, 102, 106, 104, 86 102, 119, 92, 108, 94, 88, 88, 128 96, 108, 286, 106, 102, 110, 108, 130 114, 110, 81, 100, 86, 100, 121, 104 108, 98, 108, 92, 117, 112, 108, 117 104, 106, 96, 92, 94, 96, 86, 83 112, 100, 90, 100, 100, 102, 96, 112 86, 100, 106, 106, 112, 90, 94, 102 112, 100, 110, 94, 110, 112, 92, 94 100, 104, 106, 102, 128, 100, 104, 108 110, 112, 85, 110, 106, 102, 102, 88 119, 130, 83, 106, 110, 104, 104, 114 110, 96, 98, 114, 104, 104, 108, 92 114, 110, 88, 102, 114, 102, 106, 102 94, 92, 98, 96, 104, 125, 102, 100 104, 83, 94, 106, 117, 112, 102, 108 123, 85, 108, 96, 117, 119, 108, 106 104, 106, 86, 98, 110, 100, 108, 96 117, 102, 130, 104, 112, 125, 98, 128 110, 88, 128, 128, 108, 128, 132, 108 98, 100, 106, 102, 108, 100, 92, 121 96, 125, 117, 102, 106, 104, 123, 112 86, 102, 119, 117, 108, 128, 114, 102 110, 106, 121, 88, 123, 114, 83, 119 92, 100, 123, 90, 98, 108, 102, 102 86, 121, 96, 102, 108, 88, 112, 100 123, 102, 100, 112, 125, 108, 100, 83 110, 104, 106, 130, 98, 106, 110, 114 98, 104, 121, 125, 85, 137, 128, 114 102, 110, 110, 123, 123, 121, 114, 112 94, 128, 104, 108, 108, 114, 117, 96 104, 106, 108, 104, 100, 114, 104, 135 114, 108, 114, 108, 130, 112, 114, 121 119, 102, 92, 102, 117, 94, 106, 108 121, 125, 114, 119, 112, 104, 106, 108 119, 139, 106, 121, 110, 106, 123, 110 128, 110, 117, 117, 110, 125, 121, 104 119, 144, 123, 128, 102, 114, 117, 130 108, 104, 128, 110, 108, 114, 110, 128 121, 121, 125, 123, 102, 135, 106, 123 117, 128, 139, 114, 132, 96, 128, 94 123, 146, 142, 128, 142, 128, 119, 125 132, 132, 135, 132, 100, 144, 135, 137 161, 166, 159, 149, 182, 166, 164, 188 193, 213, 250, 210, 219, 243, 231, 234 272, 240, 253, 225, 231, 219, 210, 180 182, 154, 156, 177, 149, 137, 151, 151 137, 139, 146, 142, 123, 112, 139, 149 137, 132, 135, 128, 119, 149, 135, 154 130, 121, 114, 125, 144, 112, 137, 121 123, 117, 130, 119, 117, 119, 137, 137 123, 169, 128, 128, 119, 139, 149, 130 125, 142, 144, 156, 128, 121, 135, 137 144, 121, 135, 132, 125, 132, 128, 137 146, 128, 128, 135, 123, 144, 130, 104 114, 132, 154, 139, 125, 135, 128, 144 146, 132, 114, 149, 137, 112, 130, 149 159, 130, 132, 144, 132, 144, 156, 149 164, 121, 139, 137, 135, 144, 149, 154 137, 149, 149, 135, 144, 123, 137, 144 135, 121, 123, 125, 128, 121, 123, 139 130, 135, 144, 149, 137, 139, 151, 149 135, 154, 142, 137, 125, 117, 146, 132 119, 135, 146, 135, 119, 123, 132, 137 130, 130, 149, 125, 135, 121, 121, 146 149, 149, 110, 135, 144, 149, 130, 139 128, 121, 151, 121, 144, 130, 142, 149 154, 156, 174, 154, 159, 144, 146, 139 146, 159, 139, 144, 144, 123, 128, 164 137, 142, 151, 135, 149, 164, 128, 119 139, 151, 161, 166, 151, 174, 161, 144 156, 156, 154, 154, 151, 164, 156, 151 177, 172, 169, 156, 166, 151, 144, 408 159, 144, 142, 149, 135, 149, 156, 146 142, 154, 146, 144, 174, 146, 146, 164 156, 137, 172, 154, 144, 159, 151, 123 177, 149, 149, 154, 137, 159, 135, 151 154, 146, 151, 149, 128, 151, 169, 154 144, 156, 137, 161, 135, 154, 144, 154 161, 149, 164, 149, 149, 166, 161, 154 151, 142, 159, 151, 144, 164, 154, 137 164, 174, 139, 151, 154, 159, 169, 137 180, 161, 164, 164, 164, 159, 188, 177 151, 193, 166, 190, 180, 202, 180, 199 174, 210, 219, 202, 154, 199, 202, 182 174, 169, 166, 161, 166, 169, 139, 169 156, 146, 177, 144, 146, 172, 174, 146 166, 159, 164, 154, 172, 177, 177, 164 142, 156, 161, 164, 159, 177, 177, 174 164, 146, 169, 172, 146, 177, 159, 149 169, 185, 174, 159, 166, 154, 164, 159 154, 164, 149, 149, 154, 149, 177, 151 169, 159, 159, 182, 164, 166, 161, 144 161, 154, 159, 156, 154, 193, 144, 177 156, 180, 159, 166, 156, 193, 166, 177 154, 159, 154, 151, 144, 159, 137, 182 164, 156, 177, 164, 146, 146, 180, 128 156, 169, 177, 199, 166, 174, 159, 166 161, 151, 177, 169, 190, 190, 177, 193 151, 177, 159, 166, 161, 174, 154, 190 151, 151, 177, 174, 169, 169, 159, 156 177, 182, 182, 172, 151, 185, 177, 169 185, 174, 177, 182, 164, 161, 169, 166 156, 190, 172, 164, 185, 161, 166, 164 180, 164, 174, 164, 182, 174, 169, 169 159, 207, 166, 188, 185, 177, 193, 182 199, 177, 185, 188, 188, 164, 177, 185 156, 193, 185, 216, 164, 182, 182, 196 164, 169, 172, 177, 174, 182, 174, 161 177, 177, 182, 169, 164, 193, 159, 188 207, 196, 210, 204, 234, 240, 199, 259 237, 243, 256, 246, 228, 234, 210, 243 222, 202, 182, 196, 199, 193, 190, 213 204, 180, 193, 196, 182, 159, 149, 169 169, 190, 185, 185, 199, 159, 185, 182 190, 169, 188, 172, 202, 188, 182, 188 196, 161, 164, 188, 188, 164, 180, 174 193, 193, 180, 154, 169, 202, 174, 196 177, 182, 196, 193, 144, 174, 174, 188 166, 196, 164, 166, 185, 174, 166, 169 174, 177, 156, 185, 185, 174, 222, 177 216, 207, 199, 188, 174, 188, 185, 190 210, 172, 180, 188, 180, 169, 202, 193 159, 193, 196, 193, 196, 196, 177, 188 174, 193, 219, 204, 188, 196, 172, 185 228, 199, 188, 204, 207, 188, 196, 177 216, 216, 185, 193, 182, 204, 202, 193 213, 199, 204, 190, 210, 190, 182, 177 216, 172, 196, 199, 207, 190, 188, 185 182, 196, 228, 202, 207, 199, 210, 216 216, 219, 193, 207, 213, 216, 213, 188 225, 228, 196, 228, 222, 225, 210, 213 202, 219, 177, 210, 219, 231, 237, 199 222, 207, 210, 243, 228, 272, 250, 243 256, 269, 246, 243, 262, 279, 250, 276 243, 246, 266, 240, 228, 243, 231, 253 210, 269, 207, 246, 216, 237, 253, 246 240, 216, 266, 228, 262, 262, 272, 243 272, 266, 246, 269, 250, 250, 243, 246 250, 240, 246, 253, 237, 234, 222, 207 250, 237, 210, 222, 228, 246, 243, 237 237, 237, 228, 225, 237, 234, 196, 240 219, 225, 253, 185, 231, 237, 231, 222 225, 228, 222, 237, 204, 204, 240, 185 246, 231, 234, 219, 228, 222, 207, 228 234, 237, 231, 228, 219, 225, 234, 231 210, 222, 213, 210, 234, 219, 240, 219 207, 231, 231, 190, 228, 213, 225, 225 202, 237, 196, 213, 188, 237, 199, 204 207, 193, 219, 222, 219, 199, 219, 216 177, 207, 225, 207, 246, 185, 222, 219 204, 225, 204, 225, 231, 237, 243, 228 225, 231, 246, 210, 231, 246, 231, 246 243, 253, 228, 286, 262, 243, 246, 225 279, 272, 262, 276, 306, 303, 331, 342 346, 342, 380, 404, 408, 475, 484, 506 467, 566, 548, 610, 576, 630, 620, 615 600, 610, 630, 660, 650, 630, 630, 590 615, 610, 538, 467, 467, 458, 437, 412 420, 350, 320, 317, 310, 292, 306, 282 286, 272, 256, 272, 250, 256, 269, 246 234, 250, 246, 222, 228, 240, 243, 231 231, 207, 243, 213, 204, 237, 240, 246 202, 253, 231, 400, 216, 225, 213, 213 196, 210, 222, 240, 210, 246, 231, 231 243, 243, 231, 228, 216, 222, 256, 246 240, 282, 243, 266, 276, 246, 240, 240 216, 222, 246, 259, 240, 213, 240, 228 228, 207, 240, 207, 216, 216, 199, 231 228, 202, 243, 216, 207, 234, 259, 228 243, 225, 204, 213, 202, 253, 231, 243 193, 237, 202, 210, 207, 222, 225, 231 250, 225, 240, 237, 216, 237, 246, 222 237, 228, 222, 207, 234, 207, 216, 222 213, 210, 222, 228, 222, 207, 202, 225 222, 219, 199, 185, 216, 202, 204, 190 225, 188, 216, 222, 231, 228, 204, 219 210, 210, 188, 210, 199, 190, 222, 225 202, 193, 199, 190, 219, 185, 193, 193 219, 199, 213, 219, 188, 202, 202, 231 216, 199, 207, 202, 219, 202, 199, 204 182, 199, 161, 177, 196, 185, 177, 213 234, 216, 202, 222, 182, 204, 199, 196 199, 210, 166, 250, 231, 216, 188, 219 196, 219, 199, 219, 222, 216, 204, 216 204, 207, 222, 207, 196, 213, 196, 219 222, 207, 204, 204, 196, 222, 231, 225 213, 216, 240, 243, 216, 240, 196, 246 250, 269, 272, 259, 282, 289, 310, 262 292, 361, 392, 412, 502, 506, 600, 666 734, 751, 835, 864, 930, 961, 949, 888 949, 876, 745, 778, 686, 645, 625, 630 524, 493, 384, 353, 353, 286, 292, 279 286, 256, 222, 253, 243, 228, 207, 216 231, 216, 240, 253, 225, 234, 253, 199 207, 216, 199, 213, 185, 237, 213, 234 228, 199, 222, 225, 196, 213, 199, 213 196, 207, 199, 182, 225, 225, 231, 213 216, 199, 202, 213, 202, 213, 169, 207 202, 204, 216, 182, 207, 228, 193, 213 210, 202, 185, 199, 188, 202, 188, 193 188, 188, 210, 177, 196, 207, 204, 196 199, 196, 228, 210, 219, 196, 202, 177 166, 199, 174, 177, 182, 213, 216, 202 196, 188, 210, 199, 188, 185, 210, 188 196, 213, 190, 216, 207, 177, 193, 210 204, 185, 199, 213, 190, 196, 199, 193 188, 193, 190, 190, 202, 199, 202, 193 199, 199, 154, 180, 207, 196, 204, 188 177, 216, 172, 172, 193, 210, 204, 202 199, 182, 199, 185, 177, 210, 219, 196 210, 193, 210, 185, 199, 180, 210, 213 182, 166, 177, 188, 188, 225, 204, 199 202, 188, 199, 180, 222, 204, 207, 193 210, 188, 219, 207, 185, 174, 210, 199 219, 188, 216, 202, 228, 216, 225, 228 222, 219, 222, 243, 266, 231, 222, 216 262, 213, 228, 237, 234, 213, 219, 199 216, 196, 246, 213, 228, 225, 240, 228 237, 246, 259, 246, 207, 219, 228, 253 250, 240, 222, 243, 219, 213, 196, 196 243, 222, 207, 207, 196, 196, 188, 199 199, 188, 190, 199, 185, 180, 169, 199 210, 185, 185, 182, 188, 199, 180, 204 199, 177, 174, 188, 169, 172, 166, 185 182, 190, 188, 193, 182, 177, 196, 190 144, 174, 180, 188, 177, 164, 177, 190 180, 199, 182, 172, 172, 146, 174, 182 182, 174, 146, 185, 185, 196, 182, 182 185, 174, 161, 182, 180, 151, 185, 188 169, 169, 169, 164, 159, 156, 199, 174 151, 182, 193, 174, 193, 149, 154, 166 185, 169, 177, 177, 159, 139, 174, 174 180, 188, 177, 182, 172, 164, 182, 161 182, 151, 174, 156, 182, 177, 161, 166 169, 182, 166, 174, 172, 151, 182, 420 164, 164, 169, 177, 177, 164, 177, 190 161, 357, 151, 149, 161, 190, 161, 331 169, 164, 166, 177, 172, 166, 169, 149 199, 169, 164, 164, 164, 164, 161, 172 159, 159, 164, 182, 188, 159, 154, 146 144, 166, 182, 169, 151, 166, 180, 159 142, 149, 169, 149, 172, 169, 156, 185 196, 174, 164, 190, 166, 156, 166, 193 142, 156, 169, 156, 188, 174, 169, 154 174, 154, 166, 169, 169, 154, 159, 161 193, 154, 154, 166, 159, 182, 154, 169 159, 154, 169, 154, 169, 137, 159, 169 172, 169, 146, 154, 151, 169, 174, 154 159, 142, 151, 159, 146, 164, 177, 156 174, 146, 164, 172, 149, 174, 144, 151 154, 146, 164, 174, 154, 144, 174, 161 139, 161, 169, 193, 159, 149, 169, 164 177, 174, 146, 159, 174, 132, 164, 166 159, 142, 169, 185, 154, 166, 156, 166 182, 156, 154, 135, 169, 159, 159, 159 146, 159, 161, 156, 166, 154, 144, 151 172, 169, 161, 204, 164, 166, 151, 196 159, 151, 154, 164, 135, 174, 166, 185 169, 166, 182, 188, 166, 164, 159, 142 151, 156, 169, 166, 161, 174, 151, 182 177, 172, 169, 161, 169, 177, 146, 149 182, 185, 190, 159, 149, 154, 137, 161 166, 151, 159, 164, 164, 149, 166, 137 144, 172, 146, 188, 142, 159, 144, 161 144, 149, 161, 139, 156, 154, 146, 177 154, 149, 156,/