SampleIdent,897C 33R-2 80-81,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,25-mar-1993 14:52,/ DataAngleRange, 2.0000, 34.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 62, 96, 69, 74, 74, 90, 72, 79 64, 62, 62, 77, 76, 81, 67, 71 62, 61, 77, 62, 62, 62, 67, 79 83, 83, 72, 79, 86, 85, 71, 67 59, 71, 72, 74, 55, 76, 77, 76 62, 79, 76, 66, 67, 66, 86, 72 66, 64, 66, 77, 76, 79, 72, 76 72, 72, 67, 77, 76, 77, 85, 71 69, 76, 66, 67, 71, 66, 85, 74 66, 71, 90, 76, 86, 94, 59, 67 74, 76, 72, 79, 64, 83, 77, 85 76, 77, 88, 62, 85, 79, 85, 77 76, 85, 85, 85, 88, 77, 72, 67 67, 76, 74, 66, 79, 79, 81, 88 76, 86, 96, 77, 88, 72, 85, 77 79, 79, 88, 67, 98, 86, 90, 81 76, 77, 74, 67, 92, 76, 86, 66 74, 85, 77, 83, 92, 72, 76, 104 96, 83, 90, 72, 90, 76, 104, 88 106, 102, 88, 100, 76, 96, 90, 88 96, 100, 112, 86, 112, 90, 104, 88 90, 104, 110, 100, 92, 106, 112, 96 92, 96, 96, 77, 94, 123, 92, 96 106, 94, 86, 112, 100, 96, 114, 94 128, 125, 92, 104, 104, 98, 117, 102 110, 123, 102, 110, 114, 102, 106, 106 404, 125, 121, 108, 92, 117, 94, 117 110, 114, 125, 130, 144, 106, 117, 125 121, 104, 117, 128, 117, 142, 400, 117 112, 121, 125, 130, 117, 132, 139, 128 125, 100, 151, 123, 121, 135, 137, 119 146, 142, 154, 125, 151, 132, 132, 154 119, 142, 149, 135, 139, 123, 137, 132 154, 123, 154, 135, 137, 139, 149, 151 154, 164, 149, 128, 154, 139, 177, 144 137, 130, 149, 174, 139, 174, 169, 159 132, 169, 154, 161, 159, 151, 177, 139 166, 164, 164, 161, 177, 174, 159, 177 172, 174, 159, 180, 169, 169, 166, 172 149, 177, 185, 166, 164, 172, 172, 185 185, 185, 177, 185, 182, 156, 185, 196 177, 180, 204, 166, 193, 202, 156, 207 196, 196, 174, 182, 196, 196, 190, 182 185, 190, 196, 174, 185, 219, 210, 207 213, 199, 231, 196, 196, 204, 210, 188 190, 216, 202, 216, 177, 202, 216, 231 213, 216, 216, 222, 219, 190, 219, 240 219, 210, 231, 202, 204, 216, 210, 207 216, 250, 219, 216, 219, 216, 225, 219 222, 225, 231, 216, 240, 202, 237, 222 234, 240, 243, 225, 279, 246, 225, 222 246, 262, 262, 240, 240, 222, 234, 256 225, 234, 256, 256, 266, 246, 272, 272 256, 243, 266, 246, 234, 279, 243, 269 266, 253, 259, 266, 256, 269, 243, 253 256, 269, 243, 259, 276, 269, 276, 246 279, 269, 276, 259, 269, 256, 253, 276 262, 279, 262, 250, 250, 259, 279, 253 266, 256, 272, 253, 292, 279, 237, 269 237, 250, 279, 256, 269, 246, 250, 246 228, 250, 243, 240, 259, 276, 272, 272 289, 276, 299, 234, 279, 282, 250, 250 272, 286, 266, 276, 199, 243, 259, 262 262, 250, 262, 259, 266, 219, 243, 272 266, 253, 243, 253, 253, 240, 262, 256 256, 237, 262, 266, 253, 262, 240, 250 266, 272, 269, 246, 262, 204, 237, 225 228, 246, 250, 246, 228, 259, 243, 262 243, 231, 272, 237, 240, 246, 228, 243 231, 234, 231, 213, 228, 256, 234, 213 253, 262, 216, 243, 222, 216, 216, 216 246, 234, 250, 240, 228, 237, 231, 225 253, 243, 240, 216, 228, 243, 228, 256 210, 222, 237, 237, 228, 240, 231, 213 222, 210, 219, 240, 222, 228, 207, 243 243, 216, 225, 253, 262, 259, 272, 228 234, 250, 250, 272, 234, 240, 225, 228 259, 243, 266, 262, 256, 228, 259, 272 276, 266, 259, 259, 292, 256, 282, 266 292, 289, 310, 303, 324, 313, 320, 286 313, 292, 335, 296, 328, 313, 286, 595 339, 350, 372, 380, 372, 342, 357, 376 404, 458, 428, 458, 462, 502, 511, 538 576, 600, 625, 666, 676, 773, 801, 751 713, 734, 751, 778, 773, 692, 697, 655 620, 534, 529, 488, 433, 449, 357, 353 313, 310, 306, 259, 269, 225, 246, 234 219, 250, 240, 219, 228, 199, 213, 243 190, 240, 216, 177, 216, 207, 188, 199 169, 169, 190, 185, 180, 185, 174, 159 177, 190, 182, 225, 166, 166, 188, 146 149, 182, 151, 154, 185, 177, 177, 174 164, 151, 156, 177, 161, 169, 161, 154 169, 172, 164, 161, 159, 185, 151, 174 144, 149, 180, 169, 151, 149, 137, 149 172, 156, 135, 130, 144, 149, 156, 164 125, 142, 154, 144, 154, 146, 151, 149 172, 169, 154, 149, 164, 172, 154, 169 128, 137, 166, 142, 169, 123, 137, 142 144, 151, 139, 142, 142, 128, 142, 137 117, 142, 121, 137, 137, 144, 135, 123 156, 146, 146, 151, 144, 144, 139, 149 139, 151, 146, 144, 154, 142, 132, 125 156, 135, 149, 121, 144, 137, 132, 130 132, 123, 142, 132, 149, 142, 130, 132 142, 142, 144, 135, 135, 149, 149, 142 128, 144, 125, 164, 130, 128, 123, 154 142, 130, 137, 114, 146, 151, 161, 132 149, 132, 121, 137, 151, 146, 188, 161 154, 164, 161, 161, 166, 164, 166, 149 130, 146, 154, 164, 149, 164, 161, 132 154, 151, 164, 180, 154, 142, 154, 154 174, 169, 161, 180, 190, 164, 196, 172 193, 182, 159, 161, 185, 149, 166, 172 182, 177, 188, 172, 164, 172, 156, 144 144, 142, 154, 161, 159, 190, 151, 164 156, 199, 156, 156, 130, 159, 142, 154 166, 144, 146, 199, 156, 149, 149, 149 166, 180, 174, 182, 154, 161, 185, 156 164, 172, 161, 164, 169, 174, 174, 161 151, 182, 188, 156, 169, 190, 169, 193 172, 169, 177, 164, 196, 177, 196, 202 199, 216, 199, 174, 213, 219, 202, 219 246, 222, 228, 228, 240, 253, 228, 231 246, 259, 259, 266, 286, 292, 279, 253 289, 289, 269, 313, 357, 331, 320, 350 361, 350, 353, 424, 372, 445, 416, 441 475, 441, 506, 480, 467, 520, 497, 566 515, 538, 484, 529, 511, 502, 520, 484 462, 520, 480, 462, 458, 445, 420, 388 400, 365, 380, 350, 306, 306, 292, 289 266, 269, 253, 266, 266, 253, 250, 237 196, 188, 202, 213, 202, 196, 156, 177 207, 166, 185, 159, 182, 142, 161, 154 164, 142, 182, 172, 161, 144, 169, 137 144, 159, 137, 137, 137, 117, 164, 135 146, 135, 121, 119, 121, 125, 146, 146 149, 121, 128, 139, 128, 132, 137, 144 123, 139, 139, 128, 125, 112, 149, 132 149, 123, 112, 121, 117, 117, 128, 144 119, 125, 114, 112, 132, 123, 130, 108 119, 119, 119, 102, 117, 117, 132, 135 137, 121, 102, 123, 112, 104, 110, 114 132, 119, 104, 117, 110, 112, 130, 130 128, 112, 108, 117, 130, 130, 104, 110 108, 128, 114, 142, 112, 112, 110, 114 135, 121, 123, 125, 121, 119, 110, 119 121, 125, 114, 119, 114, 110, 125, 119 121, 139, 112, 128, 139, 137, 112, 128 135, 121, 121, 121, 139, 132, 128, 135 117, 121, 117, 135, 102, 121, 119, 121 114, 135, 117, 137, 130, 128, 114, 123 123, 114, 96, 121, 119, 104, 98, 106 110, 112, 132, 123, 117, 128, 130, 132 121, 106, 117, 119, 92, 106, 104, 142 151, 102, 117, 117, 119, 112, 123, 108 132, 92, 142, 128, 110, 108, 137, 123 135, 128, 102, 112, 125, 102, 90, 117 117, 102, 137, 110, 119, 121, 121, 100 119, 102, 119, 104, 119, 108, 130, 117 121, 117, 125, 102, 121, 112, 125, 121 121, 117, 104, 110, 123, 121, 98, 110 100, 132, 112, 119, 130, 108, 108, 106 125, 117, 135, 100, 114, 108, 132, 76 125, 102, 132, 96, 108, 104, 121, 125 125, 83, 142, 110, 112, 112, 106, 128 98, 102, 119, 119, 119, 112, 130, 104 112, 108, 110, 119, 108, 112, 114, 114 132, 125, 121, 104, 112, 121, 108, 123 110, 117, 121, 110, 110, 114, 104, 114 110, 128, 123, 94, 125, 102, 125, 94 112, 144, 130, 128, 108, 108, 108, 112 114, 102, 125, 117, 125, 108, 121, 117 117, 121, 125, 114, 121, 121, 119, 121 100, 117, 110, 121, 114, 123, 125, 128 117, 114, 110, 94, 117, 130, 121, 130 128, 125, 121, 114, 112, 135, 130, 119 108, 128, 121, 135, 142, 119, 114, 114 132, 117, 117, 146, 139, 121, 128, 121 106, 132, 104, 123, 123, 137, 128, 132 130, 135, 125, 110, 128, 154, 132, 132 119, 130, 137, 137, 130, 137, 125, 112 130, 144, 117, 123, 121, 117, 144, 139 149, 130, 121, 121, 130, 159, 121, 139 119, 121, 128, 146, 128, 139, 132, 125 121, 137, 130, 137, 144, 123, 130, 149 144, 135, 125, 142, 146, 149, 420, 146 151, 132, 132, 121, 144, 159, 151, 149 132, 149, 146, 125, 166, 149, 159, 159 164, 154, 137, 166, 174, 164, 142, 159 151, 142, 161, 177, 159, 137, 177, 154 154, 146, 188, 164, 169, 177, 159, 174 172, 202, 213, 188, 193, 207, 228, 213 219, 246, 225, 228, 253, 310, 299, 317 357, 388, 365, 416, 437, 458, 493, 484 552, 520, 581, 562, 576, 543, 586, 595 566, 586, 571, 548, 467, 552, 493, 462 416, 412, 369, 346, 350, 282, 276, 282 219, 222, 213, 204, 204, 202, 228, 199 216, 196, 180, 172, 180, 196, 193, 196 174, 174, 164, 196, 190, 190, 193, 185 169, 159, 185, 185, 159, 174, 159, 180 190, 193, 177, 156, 202, 185, 204, 185 182, 185, 161, 188, 169, 174, 182, 169 188, 193, 185, 182, 169, 174, 190, 188 177, 180, 193, 172, 177, 193, 182, 174 177, 180, 199, 166, 193, 161, 174, 174 204, 188, 196, 196, 185, 174, 193, 182 196, 207, 210, 207, 174, 193, 188, 213 177, 182, 193, 185, 193, 182, 164, 166 185, 199, 161, 182, 166, 185, 169, 188 146, 156, 139, 166, 159, 172, 161, 159 125, 166, 159, 146, 154, 151, 149, 123 156, 132, 149, 149, 154, 144, 154, 139 142, 161, 137, 130, 164, 149, 151, 130 125, 154, 146, 159, 149, 154, 154, 139 144, 135, 125, 151, 159, 139, 154, 142 154, 144, 149, 137, 137, 142, 144, 144 180, 139, 154, 149, 142, 130, 142, 164 144, 151, 151, 149, 164, 144, 130, 146 135, 137, 149, 164, 135, 146, 156, 164 172, 166, 154, 154, 161, 161, 154, 154 144, 154, 159, 146, 156, 130, 146, 142 166, 130, 156, 151, 172, 142, 172, 144 172, 154, 156, 185, 151, 161, 144, 135 156, 142, 164, 159, 151, 164, 128, 142 166, 149, 164, 144, 151, 156, 146, 142 144, 144, 166, 169, 177, 149, 151, 130 154, 159, 125, 159, 159, 132, 130, 149 139, 154, 182, 154, 164, 144, 151, 149 151, 144, 146, 151, 182, 177, 154, 172 169, 159, 142, 182, 161, 164, 156, 164 159, 196, 156, 146, 202, 161, 177, 180 188, 164, 180, 216, 213, 204, 210, 213 207, 240, 240, 240, 240, 240, 225, 276 237, 237, 222, 262, 204, 225, 219, 180 193, 188, 193, 188, 169, 174, 190, 164 159, 188, 164, 182, 193, 154, 164, 149 180, 164, 174, 164, 164, 169, 164, 169 161, 154, 185, 169, 174, 166, 161, 180 164, 177, 149, 196, 154, 161, 188, 169 202, 174, 154, 159, 164, 180, 182, 172 166, 174, 180, 159, 172, 188, 174, 177 169, 166, 164, 166, 161, 164, 159, 185 154, 182, 166, 174, 190, 164, 164, 174 144, 172, 154, 174, 169, 156, 177, 159 174, 190, 174, 182, 172, 180, 172, 149 174, 154, 180, 174, 169, 177, 164, 185 196, 177, 174, 177, 180, 188, 185, 177 193, 196, 193, 182, 196, 180, 182, 188 177, 185, 182, 199, 188, 190, 188, 172 169, 185, 193, 193, 185, 177, 169, 169 213, 185, 185, 182, 219, 210, 222, 219 225, 228, 196, 204, 199, 266, 234, 228 231, 207, 253, 204, 225, 240, 237, 216 225, 207, 210, 199, 228, 210, 219, 202 174, 204, 188, 180, 190, 199, 182, 196 169, 190, 180, 193, 172, 185, 193, 185 196, 193, 180, 196, 225, 193, 185, 193 185, 204, 174, 204, 182, 202, 210, 185 190, 193, 177, 207, 180, 182, 193, 188 207, 196, 190, 202, 177, 204, 172, 185 199, 193, 188, 219, 172, 196, 204, 216 204, 174, 182, 196, 185, 177, 190, 182 199, 196, 180, 216, 182, 190, 193, 219 204, 222, 177, 188, 190, 193, 188, 199 193, 182, 202, 182, 202, 193, 228, 213 180, 222, 213, 188, 213, 193, 213, 207 193, 210, 193, 228, 213, 231, 219, 213 231, 196, 204, 237, 237, 219, 202, 199 213, 216, 216, 216, 202, 234, 219, 228 216, 207, 219, 202, 219, 207, 237, 225 207, 228, 213, 210, 219, 219, 262, 210 216, 219, 199, 219, 196, 240, 216, 237 213, 216, 231, 234, 246, 237, 256, 237 250, 256, 237, 243, 253, 240, 246, 213 219, 246, 225, 250, 262, 266, 246, 256 222, 250, 276, 266, 266, 266, 262, 266 272, 282, 292, 269, 299, 276, 276, 320 259, 320, 279, 286, 289, 286, 324, 320 306, 289, 331, 324, 324, 296, 331, 339 335, 346, 339, 342, 350, 369, 350, 392 441, 400, 433, 404, 420, 462, 488, 475 488, 511, 511, 543, 548, 557, 610, 566 600, 729, 718, 718, 692, 778, 708, 724 756, 756, 773, 756, 801, 784, 784, 740 751, 778, 676, 734, 645, 713, 655, 590 600, 650, 586, 610, 562, 576, 548, 548 552, 538, 552, 548, 552, 511, 590, 571 538, 493, 515, 511, 515, 462, 493, 488 475, 458, 484, 471, 475, 484, 454, 497 408, 441, 471, 428, 428, 400, 428, 441 412, 428, 396, 400, 412, 404, 416, 392 408, 400, 420, 404, 408, 384, 392, 404 445, 408, 420, 433, 404, 388, 384, 412 388, 384, 400, 420, 384, 412, 404, 380 424, 408, 357, 384, 388, 392, 396, 388 376, 365, 361, 372, 408, 396, 372, 357 380, 350, 350, 317, 392, 353, 357, 376 350, 353, 361, 380, 328, 388, 400, 380 328, 388, 353, 408, 350, 384, 384, 376 388, 380, 380, 392, 408, 380, 388, 372 384, 424, 441, 437, 424, 424, 433, 458 404, 388, 437, 449, 480, 458, 445, 488 493, 506, 515, 502, 576, 605, 676, 625 615, 686, 660, 676, 751, 853, 918, 961 1005, 1129, 1170, 1183, 1303, 1362, 1421, 1521 1576, 1568, 1739, 1798, 1892, 1875, 1901, 1892 1971, 2034, 2070, 2070, 2079, 2007, 1936, 1884 1823, 1806, 1798, 1697, 1600, 1576, 1444, 1362 1362, 1253, 1136, 1069, 961, 924, 870, 876 790, 724, 671, 660, 620, 635, 625, 562 566, 538, 515, 480, 566, 480, 454, 506 433, 467, 480, 467, 445, 428, 433, 458 412, 420, 412, 412, 404, 369, 400, 416 428, 416, 420, 408, 392, 420, 400, 433 416, 420, 420, 384, 437, 433, 437, 404 449, 428, 441, 428, 424, 437, 428, 449 475, 424, 424, 420, 416, 416, 392, 388 437, 384, 433, 428, 454, 404, 392, 388 353, 388, 357, 388, 346, 361, 365, 372 384, 392, 376, 350, 357, 412, 392, 384 396, 392, 342, 392, 420, 420, 416, 388 376, 412, 365, 396, 384, 404, 369, 404 416, 384, 372, 388, 376, 328, 350, 328 350, 392, 361, 328, 339, 339, 320, 317 346, 342, 313, 286, 306, 313, 335, 350 306, 484, 324, 289, 310, 313, 324, 299 289, 303, 328, 324, 313, 299, 313, 282 310, 286, 313, 303, 276, 306, 324, 282 320, 320, 306, 292, 292, 289, 299, 324 282, 282, 282, 279, 346, 292, 276, 320 269, 262, 289, 279, 250, 282, 276, 299 279, 306, 289, 292, 306, 246, 279, 262 296, 279, 292, 276, 276, 289, 313, 266 296, 289, 303, 276, 299, 292, 272, 279 269, 276, 279, 292, 259, 306, 289, 279 292, 310, 286, 286, 279, 292, 279, 286 269, 289, 313, 276, 299, 296, 256, 262 266, 296, 276, 259, 262, 269, 276, 279 259, 256, 272, 240, 269, 272, 296, 269 259, 276, 272, 262, 259, 279, 240, 243 246, 246, 272, 276, 266, 269, 240, 246 213, 243, 272, 259, 262, 276, 228, 228 256, 269, 262, 225, 272, 234, 243, 279 250, 219, 234, 262, 266, 253, 269, 269 231, 262, 243, 246, 234, 243, 246, 228 240, 269, 243, 231, 259, 266, 243, 237 240, 266, 243, 246, 250, 259, 256, 222 231, 237, 246, 250, 219, 234, 246, 240 234, 253, 256, 250, 237, 199, 234, 256 262, 250, 222, 237, 253, 231, 225, 237 237, 234, 228, 213, 210, 219, 246, 225 231, 216, 225, 222, 210, 243, 253, 234 210, 225, 228, 225, 219, 219, 219, 250 225, 269, 234, 246, 213, 240, 222, 231 234, 253, 225, 234, 199, 222, 237, 250 213, 213, 225, 237, 225, 216, 240, 228 246, 216, 237, 225, 225, 234, 210, 240 225, 231, 202, 199, 228, 225, 243, 219 193, 219, 243, 237, 204, 207, 240, 225 188, 199, 216, 202, 222, 210, 237, 231 210, 225, 207, 216, 246, 204, 222, 213 219, 213, 228, 213, 231, 207, 253, 228 213, 210, 234, 222, 231, 225, 213, 234 219, 222, 207, 231, 222, 234, 240, 204 193, 207, 213, 216, 243, 246, 234, 253 228, 213, 237, 213, 210, 219, 222, 196 243, 222, 266, 225, 259, 228, 225, 240 246, 243, 237, 250, 276, 246, 253, 276 228, 246, 225, 250, 216, 237, 225, 225 228, 237, 213, 225, 234, 225, 213, 204 234, 216, 202, 188, 225, 219, 231, 216 216, 210, 256, 225, 204, 216, 207, 237 213, 213, 225, 202, 225, 216, 202, 219 207, 219, 216, 210, 196, 204, 219, 185 202, 196, 196, 213, 196, 196, 193, 207 210, 225, 193, 199, 222, 180, 193, 193 193, 188, 193, 202, 199, 180, 231, 185 193, 190, 199, 193, 188, 190, 185, 177 199, 188, 190, 196, 172, 199, 185, 213 199, 196, 202, 204, 188, 210, 213, 190 196, 188, 188, 193, 199, 185, 182, 185 185, 180, 193, 207, 193, 185, 193, 180 213, 222, 207, 202, 204, 190, 216, 190 199, 193, 204, 213, 174, 185, 166, 169 196, 196, 177, 196, 169, 193, 196, 213 204, 216, 185, 169, 225, 182, 180, 169 196, 196, 166, 180, 188, 182, 190, 182 188, 177, 216, 185, 169, 193, 190, 202 177, 182, 196, 193, 172, 188, 196, 207 193, 182, 182, 199, 190, 185, 185, 177 188, 199, 174, 169, 180, 149, 196, 169 180, 169, 169, 172, 177, 199, 164, 188 177, 190, 190, 185, 180, 199, 174, 196 188, 174, 156, 174, 185, 188, 177, 169 174, 188, 164, 180, 164, 166, 177, 149 199, 202, 166, 161, 180, 196, 169, 169 188, 182, 159, 182, 193, 202, 199, 172 169, 188, 188, 182, 182, 166, 193, 172 166, 172, 180, 169, 185, 172, 172, 169 164, 149, 164, 159, 159, 161, 174, 166 156, 193, 174, 169, 161, 164, 188, 164 188, 177, 149, 154, 177, 172, 185, 210 154, 177, 169, 180, 177, 202, 154, 190 185, 174, 169, 190, 185, 188, 137, 199 164, 196, 146, 193, 177, 154, 177, 188 182, 169, 185, 204, 185, 182, 174, 199 161, 174, 182, 182, 169, 193, 177, 190 185, 169, 190, 174, 182, 182, 159, 190 180, 177, 210, 174, 188, 177, 188, 185 185, 137, 193, 172, 207, 174, 188, 169 177, 180, 169,/