SampleIdent,897C 40R-3 6-8,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,26-mar-1993 18:59,/ DataAngleRange, 2.0000, 34.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 96, 71, 86, 86, 79, 76, 72, 94 88, 81, 94, 77, 81, 77, 66, 74 77, 74, 74, 76, 85, 71, 67, 71 72, 61, 72, 86, 86, 72, 69, 76 88, 76, 90, 67, 76, 86, 79, 77 92, 74, 100, 74, 79, 85, 86, 85 83, 114, 98, 77, 83, 98, 77, 96 98, 110, 86, 106, 92, 77, 202, 98 94, 100, 102, 92, 88, 96, 98, 98 121, 102, 94, 110, 102, 114, 98, 117 100, 112, 119, 112, 114, 98, 112, 108 94, 114, 106, 102, 119, 98, 100, 119 102, 123, 112, 117, 121, 90, 121, 110 130, 112, 123, 121, 121, 108, 102, 117 112, 123, 121, 112, 123, 123, 106, 121 104, 135, 110, 121, 117, 149, 119, 128 121, 121, 90, 130, 125, 130, 137, 117 125, 121, 144, 137, 156, 144, 132, 137 128, 119, 142, 137, 130, 121, 137, 156 159, 172, 156, 182, 154, 146, 149, 142 161, 151, 166, 161, 154, 166, 154, 182 151, 137, 166, 159, 172, 164, 142, 164 156, 169, 142, 156, 169, 166, 196, 161 151, 188, 166, 166, 169, 182, 193, 154 182, 188, 199, 161, 202, 196, 193, 188 169, 164, 199, 185, 193, 202, 185, 185 180, 185, 190, 182, 172, 190, 185, 193 188, 177, 190, 207, 202, 219, 193, 219 196, 207, 199, 199, 213, 213, 196, 207 225, 216, 213, 219, 219, 240, 228, 225 234, 237, 225, 202, 207, 240, 225, 213 231, 250, 240, 219, 222, 210, 259, 216 240, 240, 207, 256, 228, 228, 259, 253 253, 225, 240, 237, 269, 237, 237, 234 246, 231, 237, 228, 231, 259, 279, 276 276, 276, 272, 246, 243, 269, 266, 289 256, 243, 253, 269, 240, 262, 272, 253 269, 272, 266, 306, 292, 303, 292, 282 256, 259, 276, 272, 296, 286, 266, 324 266, 282, 272, 286, 328, 286, 317, 292 269, 272, 276, 320, 272, 279, 299, 292 306, 286, 303, 303, 331, 324, 296, 296 306, 320, 276, 306, 292, 310, 328, 289 317, 299, 317, 306, 324, 313, 324, 303 339, 276, 335, 313, 303, 331, 328, 324 331, 310, 331, 328, 346, 313, 296, 313 335, 303, 320, 310, 328, 339, 339, 335 335, 353, 331, 324, 306, 303, 324, 331 313, 346, 317, 328, 357, 384, 361, 335 353, 306, 335, 306, 350, 353, 335, 320 335, 335, 335, 339, 342, 350, 342, 339 339, 396, 313, 346, 335, 342, 361, 346 357, 350, 557, 342, 317, 361, 331, 339 335, 335, 384, 310, 324, 353, 320, 350 331, 353, 324, 324, 365, 350, 335, 353 331, 331, 346, 342, 342, 328, 310, 346 317, 310, 324, 310, 369, 320, 346, 372 303, 317, 353, 342, 339, 313, 357, 369 317, 317, 342, 320, 331, 361, 296, 365 331, 342, 331, 310, 296, 346, 328, 328 335, 331, 313, 350, 317, 342, 317, 328 331, 331, 320, 339, 357, 335, 346, 313 320, 342, 361, 310, 317, 313, 317, 317 317, 289, 313, 306, 306, 328, 313, 317 320, 306, 339, 303, 306, 310, 317, 303 317, 328, 303, 292, 296, 320, 313, 313 286, 292, 306, 357, 317, 296, 320, 266 313, 310, 306, 296, 306, 346, 292, 286 306, 282, 292, 289, 328, 331, 303, 306 303, 282, 328, 313, 289, 279, 310, 306 350, 339, 289, 289, 324, 310, 317, 296 331, 313, 286, 299, 310, 299, 328, 328 335, 299, 310, 317, 299, 339, 320, 272 286, 303, 306, 350, 310, 296, 286, 299 296, 324, 324, 346, 310, 299, 342, 339 306, 353, 342, 299, 324, 320, 339, 331 328, 342, 296, 328, 331, 324, 331, 292 339, 306, 357, 320, 353, 339, 331, 369 376, 365, 331, 365, 353, 376, 412, 372 388, 365, 396, 396, 408, 433, 467, 428 437, 428, 441, 484, 454, 437, 493, 484 484, 502, 562, 511, 524, 562, 600, 625 600, 620, 615, 686, 671, 660, 734, 751 708, 713, 697, 686, 697, 666, 676, 595 566, 520, 566, 484, 511, 484, 437, 376 404, 357, 346, 365, 313, 320, 313, 328 292, 286, 282, 279, 262, 289, 276, 262 256, 228, 243, 256, 222, 234, 266, 231 210, 240, 228, 228, 216, 225, 231, 207 202, 262, 228, 204, 216, 213, 210, 216 190, 185, 207, 202, 202, 193, 182, 202 204, 213, 199, 199, 196, 199, 213, 188 225, 196, 199, 190, 213, 199, 166, 204 169, 204, 190, 172, 185, 188, 199, 169 190, 174, 156, 193, 164, 166, 164, 166 185, 174, 177, 180, 174, 174, 151, 177 174, 164, 166, 154, 172, 193, 166, 177 174, 149, 174, 174, 159, 169, 161, 159 164, 174, 128, 172, 144, 154, 166, 428 149, 151, 159, 177, 154, 144, 156, 174 159, 154, 159, 142, 154, 154, 146, 135 151, 142, 154, 159, 139, 135, 130, 149 139, 151, 161, 144, 135, 128, 164, 132 154, 154, 144, 132, 174, 139, 151, 156 169, 146, 156, 123, 182, 149, 146, 121 125, 149, 144, 149, 164, 149, 137, 151 135, 135, 142, 123, 144, 159, 137, 154 154, 130, 151, 132, 139, 154, 149, 137 172, 139, 144, 142, 123, 146, 146, 128 151, 123, 174, 130, 142, 149, 139, 172 159, 146, 130, 159, 164, 159, 144, 151 149, 132, 142, 121, 128, 112, 146, 156 166, 142, 166, 154, 135, 169, 149, 137 166, 132, 144, 154, 139, 135, 161, 130 144, 149, 156, 159, 146, 128, 125, 142 161, 139, 130, 144, 142, 156, 144, 137 164, 125, 144, 149, 137, 182, 142, 149 156, 146, 149, 149, 166, 172, 185, 151 154, 161, 174, 164, 177, 164, 182, 159 161, 172, 161, 169, 207, 151, 182, 174 199, 188, 169, 159, 166, 174, 202, 193 210, 216, 219, 196, 196, 193, 219, 204 216, 213, 216, 225, 228, 228, 240, 250 237, 253, 262, 289, 276, 292, 289, 286 292, 306, 320, 350, 306, 346, 388, 392 372, 365, 412, 433, 392, 484, 462, 462 493, 493, 502, 515, 576, 484, 534, 524 529, 548, 552, 543, 538, 548, 566, 502 502, 511, 511, 462, 441, 433, 462, 454 396, 408, 365, 416, 335, 372, 353, 346 331, 282, 276, 276, 272, 237, 231, 234 219, 225, 196, 207, 207, 219, 190, 199 180, 177, 188, 174, 182, 161, 169, 156 135, 166, 142, 166, 146, 154, 159, 164 149, 146, 154, 146, 154, 149, 154, 151 139, 137, 144, 130, 128, 139, 139, 121 132, 128, 104, 128, 106, 106, 123, 128 123, 142, 114, 154, 123, 142, 121, 117 130, 125, 128, 121, 128, 144, 139, 123 114, 112, 121, 121, 114, 119, 106, 121 135, 112, 132, 121, 112, 123, 119, 128 119, 110, 92, 108, 117, 100, 114, 110 110, 130, 112, 121, 121, 130, 121, 100 121, 106, 108, 110, 128, 137, 119, 94 112, 125, 108, 142, 92, 102, 112, 104 102, 130, 106, 123, 123, 104, 128, 121 154, 108, 144, 119, 94, 119, 119, 102 317, 110, 119, 114, 117, 117, 102, 125 108, 104, 112, 123, 130, 117, 142, 104 108, 121, 106, 135, 117, 121, 112, 112 125, 102, 121, 119, 117, 114, 117, 92 108, 104, 119, 112, 98, 110, 114, 112 110, 112, 121, 112, 121, 128, 106, 121 121, 94, 114, 106, 112, 119, 112, 106 112, 112, 117, 96, 100, 108, 102, 121 123, 94, 96, 119, 114, 100, 114, 96 108, 114, 110, 88, 110, 114, 108, 110 114, 121, 108, 94, 85, 110, 110, 98 114, 125, 112, 112, 108, 108, 90, 110 104, 112, 112, 104, 108, 108, 121, 110 119, 104, 121, 102, 114, 100, 114, 104 110, 98, 108, 114, 117, 104, 100, 100 106, 110, 119, 130, 104, 108, 96, 121 112, 114, 98, 110, 112, 114, 100, 94 130, 114, 100, 117, 121, 117, 112, 108 112, 96, 108, 98, 90, 123, 102, 121 123, 119, 117, 132, 112, 110, 125, 121 106, 114, 110, 117, 100, 123, 100, 117 125, 94, 100, 110, 125, 86, 108, 119 112, 104, 104, 106, 106, 98, 117, 104 119, 121, 112, 117, 121, 114, 104, 130 100, 121, 92, 104, 125, 123, 125, 96 108, 112, 114, 112, 114, 119, 102, 104 106, 119, 119, 114, 119, 130, 110, 108 121, 102, 106, 106, 142, 108, 123, 128 112, 114, 108, 117, 104, 123, 121, 96 121, 135, 135, 137, 119, 130, 125, 106 139, 121, 114, 119, 104, 125, 119, 121 132, 108, 112, 128, 110, 119, 100, 130 149, 149, 132, 132, 125, 121, 135, 142 135, 137, 132, 125, 125, 132, 125, 146 135, 125, 135, 125, 112, 137, 128, 112 144, 132, 146, 142, 117, 128, 139, 132 146, 154, 142, 139, 164, 110, 130, 130 137, 114, 156, 144, 137, 164, 132, 166 159, 139, 151, 130, 144, 128, 154, 146 142, 161, 144, 132, 128, 146, 384, 149 169, 156, 154, 139, 164, 142, 135, 159 161, 172, 172, 139, 164, 159, 144, 174 174, 139, 169, 190, 185, 169, 151, 185 188, 172, 180, 177, 213, 174, 193, 222 222, 219, 213, 199, 222, 225, 193, 228 240, 253, 246, 306, 272, 231, 286, 353 353, 339, 372, 416, 400, 471, 449, 454 511, 506, 515, 557, 543, 571, 571, 493 529, 529, 480, 471, 462, 462, 441, 388 339, 331, 303, 303, 324, 289, 266, 237 234, 250, 240, 207, 228, 237, 202, 185 196, 182, 196, 199, 182, 188, 210, 207 182, 196, 190, 182, 216, 190, 166, 185 166, 182, 177, 177, 188, 177, 188, 174 169, 199, 180, 182, 169, 174, 180, 185 164, 177, 156, 174, 164, 174, 164, 196 144, 196, 172, 164, 180, 164, 174, 172 149, 156, 166, 169, 174, 185, 177, 182 156, 180, 151, 156, 166, 174, 177, 164 151, 182, 159, 177, 161, 159, 166, 156 202, 185, 202, 199, 188, 193, 169, 204 190, 190, 188, 169, 174, 204, 172, 156 159, 166, 159, 144, 169, 180, 130, 149 130, 146, 132, 154, 146, 130, 144, 149 125, 135, 146, 123, 142, 135, 128, 128 149, 123, 128, 132, 130, 137, 139, 128 139, 130, 125, 123, 137, 130, 119, 128 130, 135, 135, 135, 137, 139, 139, 135 114, 149, 151, 100, 119, 135, 135, 123 121, 135, 130, 135, 132, 146, 128, 135 161, 144, 132, 137, 135, 125, 132, 130 149, 117, 151, 154, 144, 151, 144, 156 149, 174, 180, 180, 164, 154, 174, 164 142, 166, 130, 144, 142, 177, 161, 164 142, 154, 169, 177, 166, 154, 161, 169 154, 149, 156, 154, 154, 159, 151, 174 154, 159, 132, 169, 151, 135, 142, 137 142, 146, 139, 121, 151, 164, 144, 132 135, 123, 161, 132, 151, 142, 166, 137 130, 132, 132, 151, 149, 123, 130, 125 132, 119, 137, 128, 132, 144, 149, 130 132, 121, 139, 146, 137, 139, 112, 132 135, 125, 123, 137, 125, 119, 164, 132 144, 125, 154, 149, 142, 130, 146, 149 130, 144, 135, 151, 130, 154, 151, 193 182, 174, 177, 177, 182, 193, 216, 202 185, 213, 222, 269, 246, 243, 253, 256 262, 262, 237, 225, 216, 237, 193, 202 182, 180, 172, 174, 177, 161, 164, 159 123, 119, 142, 119, 137, 144, 146, 130 114, 144, 149, 139, 130, 117, 128, 117 125, 137, 139, 114, 146, 119, 130, 137 123, 146, 142, 137, 142, 125, 135, 135 125, 130, 146, 142, 130, 123, 128, 135 125, 121, 128, 137, 135, 132, 137, 121 137, 121, 130, 130, 144, 132, 130, 132 125, 119, 132, 123, 125, 121, 139, 117 137, 121, 135, 110, 123, 121, 123, 128 125, 112, 135, 144, 117, 125, 137, 137 132, 137, 112, 123, 156, 149, 146, 144 125, 123, 159, 137, 139, 123, 142, 137 156, 169, 161, 151, 144, 128, 137, 144 151, 144, 151, 128, 154, 132, 123, 121 121, 128, 130, 142, 125, 130, 110, 142 146, 125, 135, 139, 156, 137, 142, 154 128, 128, 135, 135, 132, 137, 156, 154 166, 159, 139, 123, 156, 137, 125, 110 164, 135, 132, 142, 117, 144, 137, 159 119, 144, 137, 144, 142, 121, 154, 130 151, 137, 159, 142, 146, 130, 114, 139 114, 137, 139, 146, 151, 123, 137, 128 144, 154, 146, 146, 130, 149, 144, 161 146, 142, 169, 149, 182, 142, 121, 125 135, 125, 159, 154, 132, 151, 117, 151 144, 154, 164, 144, 154, 144, 128, 151 151, 144, 144, 156, 144, 137, 130, 154 149, 164, 156, 130, 142, 154, 154, 151 172, 137, 137, 149, 166, 174, 174, 149 149, 159, 164, 159, 139, 146, 149, 166 146, 154, 156, 164, 164, 164, 172, 177 169, 154, 164, 207, 182, 174, 174, 166 185, 188, 177, 174, 169, 169, 174, 159 188, 166, 159, 164, 172, 172, 188, 188 169, 169, 182, 196, 174, 166, 180, 182 180, 196, 193, 177, 193, 188, 164, 169 188, 169, 196, 193, 188, 196, 174, 190 174, 193, 177, 188, 213, 188, 174, 210 222, 185, 199, 166, 193, 199, 193, 199 231, 207, 202, 219, 222, 259, 228, 213 243, 243, 225, 213, 250, 222, 228, 234 234, 240, 237, 250, 225, 240, 259, 256 231, 262, 246, 256, 272, 256, 269, 256 269, 272, 282, 266, 310, 279, 331, 317 335, 331, 342, 342, 350, 342, 357, 372 396, 408, 408, 420, 449, 449, 493, 454 524, 534, 529, 534, 625, 576, 605, 590 625, 692, 708, 734, 681, 718, 745, 729 724, 729, 824, 756, 773, 740, 762, 718 729, 773, 713, 676, 660, 660, 660, 660 635, 586, 595, 566, 571, 538, 571, 562 571, 571, 590, 571, 543, 520, 511, 534 502, 511, 506, 497, 511, 462, 497, 480 467, 449, 467, 404, 396, 412, 400, 404 384, 412, 372, 350, 361, 372, 357, 357 350, 346, 339, 357, 353, 339, 361, 369 335, 331, 376, 376, 365, 350, 342, 335 376, 342, 372, 369, 331, 339, 324, 313 357, 317, 306, 324, 328, 346, 328, 339 331, 317, 339, 346, 350, 317, 292, 328 339, 342, 324, 328, 324, 342, 310, 346 328, 339, 299, 339, 313, 335, 313, 335 310, 313, 320, 306, 365, 328, 331, 320 372, 369, 353, 303, 361, 365, 317, 350 335, 357, 365, 331, 376, 339, 380, 342 372, 408, 392, 392, 408, 396, 437, 424 392, 412, 412, 454, 462, 467, 458, 480 475, 515, 548, 548, 600, 534, 620, 625 681, 702, 756, 824, 829, 912, 992, 1050 1089, 1204, 1267, 1436, 1467, 1576, 1673, 1756 1772, 1781, 1875, 1936, 2098, 2070, 2107, 2107 2079, 2107, 2162, 2153, 2144, 1980, 1971, 1884 1884, 1832, 1714, 1616, 1584, 1459, 1376, 1362 1289, 1204, 1082, 1024, 1050, 942, 835, 801 824, 724, 745, 702, 708, 655, 625, 615 635, 586, 576, 610, 548, 534, 543, 548 484, 529, 515, 534, 520, 520, 529, 529 502, 529, 475, 493, 471, 480, 475, 480 502, 454, 529, 467, 412, 449, 471, 428 462, 462, 471, 484, 462, 475, 484, 488 502, 493, 458, 449, 502, 493, 480, 445 458, 454, 484, 488, 433, 493, 433, 449 433, 416, 462, 420, 408, 400, 433, 437 408, 420, 416, 412, 420, 420, 420, 433 392, 392, 412, 441, 400, 462, 420, 449 437, 433, 445, 441, 437, 462, 458, 445 458, 424, 420, 396, 420, 408, 416, 445 400, 404, 424, 388, 388, 380, 380, 376 361, 372, 361, 361, 384, 376, 365, 328 372, 365, 369, 313, 328, 310, 346, 310 350, 361, 331, 310, 342, 320, 310, 324 339, 313, 346, 339, 320, 331, 331, 320 289, 306, 331, 313, 310, 299, 292, 282 328, 286, 320, 289, 276, 299, 324, 292 266, 292, 296, 306, 289, 289, 292, 303 310, 331, 253, 286, 279, 276, 276, 292 286, 286, 269, 266, 269, 276, 289, 266 289, 317, 282, 266, 286, 289, 279, 259 303, 262, 276, 256, 306, 237, 243, 279 276, 262, 272, 246, 289, 253, 262, 279 289, 279, 269, 269, 299, 272, 310, 313 299, 253, 282, 262, 282, 276, 256, 286 286, 256, 259, 269, 259, 246, 246, 234 262, 253, 250, 234, 246, 240, 222, 234 216, 246, 262, 222, 210, 237, 234, 207 196, 213, 262, 213, 240, 237, 219, 231 253, 219, 219, 231, 199, 237, 225, 216 243, 219, 210, 193, 213, 231, 228, 207 253, 225, 219, 219, 237, 243, 240, 234 228, 213, 237, 225, 243, 228, 243, 259 256, 243, 234, 231, 246, 204, 256, 237 234, 219, 207, 216, 222, 225, 216, 234 210, 213, 219, 225, 213, 225, 199, 182 240, 188, 190, 222, 207, 213, 222, 190 207, 202, 193, 207, 222, 213, 199, 216 219, 204, 219, 193, 196, 225, 213, 213 202, 199, 193, 196, 202, 204, 219, 180 219, 219, 202, 207, 196, 177, 196, 210 213, 216, 202, 207, 199, 199, 199, 185 219, 213, 188, 207, 185, 202, 185, 222 216, 202, 182, 185, 180, 199, 204, 213 199, 207, 204, 199, 213, 228, 190, 231 188, 222, 188, 225, 202, 193, 237, 213 190, 210, 222, 222, 216, 246, 225, 204 202, 210, 228, 199, 193, 199, 185, 193 225, 190, 219, 213, 222, 204, 193, 199 202, 199, 207, 188, 222, 204, 182, 188 213, 222, 196, 219, 188, 196, 185, 169 196, 202, 188, 199, 213, 210, 193, 202 177, 210, 216, 182, 193, 213, 185, 185 182, 182, 219, 202, 202, 193, 190, 188 185, 185, 196, 185, 185, 193, 185, 216 182, 219, 188, 207, 193, 207, 193, 180 196, 237, 185, 185, 210, 190, 182, 188 180, 159, 151, 182, 185, 193, 174, 182 156, 199, 174, 193, 199, 188, 202, 174 180, 159, 180, 151, 159, 193, 174, 188 169, 202, 180, 210, 172, 161, 193, 207 188, 172, 174, 161, 164, 169, 166, 156 166, 159, 172, 164, 144, 161, 161, 164 177, 166, 151, 177, 156, 159, 137, 172 164, 144, 169, 142, 161, 169, 174, 142 174, 151, 151, 144, 151, 177, 172, 161 137, 159, 166, 149, 169, 164, 149, 149 151, 164, 142, 161, 151, 146, 151, 164 154, 146, 172, 164, 156, 149, 146, 146 130, 159, 161, 149, 146, 144, 142, 151 164, 117, 137, 174, 156, 142, 128, 174 142, 144, 149, 149, 154, 151, 139, 164 156, 159, 159, 137, 137, 149, 146, 161 161, 151, 169, 151, 137, 142, 161, 149 159, 151, 159, 144, 142, 142, 156, 151 166, 144, 154, 142, 146, 182, 156, 149 137, 137, 137, 151, 137, 137, 166, 151 149, 172, 174, 135, 144, 146, 156, 166 149, 146, 161, 144, 151, 144, 149, 130 132, 161, 159, 130, 149, 164, 137, 151 146, 130, 130, 146, 121, 137, 128, 151 154, 123, 149, 151, 96, 151, 137, 121 137, 128, 159, 149, 144, 142, 137, 132 130, 161, 149, 144, 159, 130, 149, 149 137, 149, 142, 142, 137, 149, 149, 142 130, 132, 128, 121, 154, 135, 146, 144 123, 156, 132, 154, 146, 130, 144, 149 132, 144, 137, 159, 125, 146, 149, 135 132, 149, 154, 149, 135, 142, 161, 161 142, 139, 142, 151, 156, 130, 149, 144 137, 177, 169, 135, 146, 125, 146, 144 169, 166, 164, 174, 169, 159, 180, 172 164, 172, 149, 174, 164, 188, 174, 177 154, 161, 177, 161, 137, 146, 159, 169 156, 182, 172, 154, 188, 164, 193, 166 182, 172, 196, 164, 177, 180, 169, 182 177, 182, 182, 210, 210, 177, 196, 199 202, 159, 199, 190, 182, 202, 180, 177 188, 193, 185, 193, 169, 177, 169, 159 180, 169, 159,/