SampleIdent,897C 40R-3 6-7 GLY,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,29-apr-1993 9:54,/ DataAngleRange, 2.0000, 34.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 106, 90, 100, 90, 79, 85, 88, 112 92, 85, 88, 90, 77, 104, 76, 86 88, 108, 83, 86, 104, 86, 96, 77 102, 83, 86, 96, 94, 88, 102, 90 81, 85, 102, 83, 86, 98, 92, 98 108, 86, 92, 90, 90, 72, 94, 90 96, 88, 77, 86, 98, 86, 74, 90 72, 94, 90, 88, 106, 86, 88, 90 86, 76, 85, 117, 72, 94, 81, 90 88, 90, 98, 86, 86, 90, 86, 100 94, 90, 96, 92, 94, 77, 85, 88 85, 102, 86, 79, 104, 98, 85, 96 92, 104, 77, 83, 106, 85, 94, 83 79, 108, 100, 104, 104, 102, 98, 121 85, 365, 102, 106, 90, 94, 94, 121 102, 106, 86, 130, 102, 102, 110, 110 104, 119, 90, 110, 106, 114, 110, 139 137, 119, 132, 125, 128, 100, 121, 125 104, 142, 121, 132, 137, 132, 119, 142 144, 154, 144, 117, 132, 151, 132, 154 149, 144, 154, 174, 156, 156, 159, 161 144, 151, 151, 164, 177, 159, 188, 161 154, 196, 172, 177, 182, 182, 188, 172 213, 185, 196, 210, 213, 225, 185, 210 193, 213, 222, 213, 219, 240, 234, 228 231, 228, 237, 240, 228, 234, 225, 246 225, 256, 259, 259, 282, 276, 259, 253 286, 276, 276, 282, 266, 289, 324, 292 286, 303, 296, 292, 313, 286, 331, 328 331, 339, 346, 353, 331, 369, 396, 372 335, 404, 342, 361, 380, 357, 384, 400 404, 420, 449, 424, 433, 433, 441, 462 441, 441, 462, 502, 488, 454, 433, 437 480, 441, 529, 445, 529, 515, 538, 552 557, 506, 506, 538, 538, 520, 557, 529 529, 581, 566, 595, 581, 615, 625, 586 557, 586, 625, 615, 635, 600, 630, 650 615, 692, 635, 660, 686, 650, 645, 718 702, 692, 676, 708, 692, 625, 713, 681 686, 671, 660, 650, 671, 650, 713, 724 655, 692, 660, 692, 708, 686, 708, 630 655, 630, 660, 686, 620, 640, 671, 655 600, 615, 630, 660, 615, 595, 640, 620 610, 557, 576, 595, 552, 605, 562, 557 581, 600, 571, 557, 543, 562, 571, 557 529, 534, 493, 511, 484, 529, 502, 493 497, 458, 480, 493, 471, 488, 502, 437 484, 462, 454, 462, 462, 445, 445, 437 471, 467, 458, 454, 441, 428, 416, 454 416, 428, 424, 441, 424, 412, 365, 388 400, 408, 380, 384, 365, 365, 380, 384 331, 372, 388, 384, 376, 342, 357, 350 331, 331, 369, 361, 384, 384, 376, 350 350, 353, 339, 335, 310, 357, 320, 350 324, 331, 292, 310, 299, 310, 361, 320 303, 335, 310, 303, 269, 306, 328, 306 303, 289, 331, 310, 286, 289, 306, 320 306, 310, 306, 289, 282, 292, 259, 306 303, 262, 286, 279, 299, 313, 299, 317 269, 276, 276, 286, 266, 266, 289, 276 292, 276, 262, 276, 282, 262, 276, 286 279, 269, 289, 286, 269, 292, 272, 269 266, 276, 262, 276, 282, 269, 272, 250 262, 292, 276, 231, 250, 282, 262, 269 253, 279, 282, 246, 246, 289, 253, 250 269, 269, 262, 276, 292, 234, 259, 246 240, 279, 231, 256, 250, 250, 259, 289 253, 250, 259, 240, 256, 266, 253, 299 240, 259, 228, 237, 269, 269, 259, 256 234, 266, 262, 256, 272, 292, 240, 243 231, 262, 269, 266, 250, 262, 222, 240 272, 269, 272, 253, 259, 289, 250, 237 253, 216, 259, 256, 253, 253, 262, 246 259, 266, 237, 272, 282, 276, 282, 272 253, 269, 269, 250, 250, 259, 266, 272 253, 246, 262, 262, 259, 292, 296, 286 289, 266, 253, 286, 306, 299, 286, 269 276, 306, 595, 279, 317, 335, 292, 289 306, 289, 282, 272, 317, 335, 320, 313 313, 306, 331, 313, 296, 346, 320, 346 342, 357, 361, 353, 335, 357, 339, 353 372, 376, 353, 372, 342, 380, 357, 416 392, 590, 420, 424, 428, 471, 449, 437 493, 497, 493, 484, 529, 571, 576, 586 600, 645, 650, 650, 655, 650, 660, 666 660, 655, 620, 610, 595, 576, 562, 529 502, 484, 488, 433, 437, 471, 424, 462 424, 408, 428, 392, 412, 384, 376, 346 361, 372, 328, 361, 342, 365, 372, 313 353, 353, 331, 331, 376, 335, 331, 317 328, 324, 306, 331, 328, 331, 303, 350 320, 313, 320, 328, 324, 590, 310, 310 335, 353, 286, 286, 296, 286, 299, 339 299, 317, 292, 306, 299, 303, 292, 289 299, 292, 324, 320, 320, 286, 299, 296 279, 324, 310, 328, 292, 292, 279, 306 292, 289, 303, 313, 313, 286, 299, 279 313, 320, 299, 292, 331, 310, 289, 279 296, 276, 313, 310, 320, 317, 292, 342 272, 286, 303, 303, 269, 296, 299, 296 299, 299, 279, 292, 272, 289, 262, 266 286, 296, 256, 292, 289, 276, 272, 276 262, 269, 282, 276, 262, 289, 324, 286 243, 269, 269, 296, 253, 256, 262, 289 262, 276, 272, 306, 269, 250, 246, 262 234, 225, 276, 246, 253, 259, 234, 279 237, 262, 250, 246, 243, 250, 231, 231 253, 246, 246, 204, 240, 237, 231, 228 228, 207, 222, 213, 185, 219, 231, 228 174, 177, 204, 210, 193, 193, 219, 216 219, 180, 231, 207, 207, 188, 213, 177 177, 207, 234, 196, 219, 182, 199, 202 196, 174, 182, 182, 182, 185, 182, 199 196, 202, 190, 190, 196, 188, 213, 182 185, 174, 172, 180, 193, 196, 182, 202 177, 207, 188, 188, 188, 196, 216, 216 188, 180, 188, 193, 185, 188, 180, 204 180, 188, 202, 190, 210, 196, 196, 216 185, 199, 188, 225, 204, 210, 199, 202 216, 231, 199, 182, 185, 213, 202, 207 225, 204, 207, 231, 225, 231, 225, 246 219, 213, 231, 225, 237, 243, 228, 259 262, 272, 266, 262, 272, 272, 289, 276 269, 310, 289, 292, 328, 320, 339, 361 335, 320, 335, 365, 372, 361, 361, 372 416, 396, 404, 404, 408, 424, 449, 424 467, 497, 515, 529, 524, 538, 605, 610 605, 620, 620, 650, 745, 708, 740, 729 756, 756, 740, 812, 824, 795, 756, 767 718, 718, 762, 702, 630, 640, 620, 610 548, 502, 497, 462, 484, 493, 437, 449 396, 357, 361, 331, 346, 306, 303, 306 324, 282, 289, 276, 262, 259, 259, 272 225, 269, 213, 216, 207, 190, 213, 202 228, 207, 185, 199, 182, 207, 185, 180 196, 182, 169, 199, 185, 210, 204, 154 159, 161, 166, 156, 159, 154, 182, 172 139, 151, 166, 142, 161, 159, 142, 132 132, 132, 125, 117, 149, 130, 137, 119 144, 144, 144, 132, 128, 123, 137, 144 130, 144, 144, 142, 144, 144, 139, 154 128, 128, 121, 135, 137, 151, 135, 135 121, 135, 130, 149, 135, 130, 139, 106 139, 125, 139, 123, 154, 149, 139, 110 144, 128, 137, 125, 125, 130, 112, 123 151, 156, 123, 144, 125, 144, 128, 156 135, 142, 142, 110, 142, 123, 137, 135 119, 112, 121, 144, 112, 139, 117, 130 121, 130, 125, 119, 130, 123, 117, 112 137, 125, 121, 132, 119, 149, 125, 130 117, 125, 106, 121, 151, 121, 132, 121 125, 121, 119, 135, 137, 137, 130, 121 135, 108, 108, 123, 125, 130, 121, 139 114, 135, 156, 137, 123, 146, 125, 128 128, 132, 121, 137, 125, 132, 117, 135 125, 144, 135, 149, 119, 149, 123, 117 142, 139, 142, 144, 137, 130, 144, 137 139, 146, 149, 142, 123, 161, 159, 144 123, 135, 139, 146, 121, 154, 146, 130 137, 151, 166, 128, 135, 130, 137, 149 164, 154, 146, 149, 144, 154, 174, 154 151, 151, 169, 154, 161, 166, 156, 156 166, 156, 149, 169, 164, 177, 164, 154 166, 172, 182, 164, 185, 177, 185, 172 174, 166, 180, 164, 199, 164, 169, 196 159, 193, 185, 174, 174, 188, 164, 188 188, 193, 222, 196, 182, 188, 166, 188 188, 216, 222, 222, 196, 237, 207, 207 207, 231, 210, 216, 213, 219, 253, 190 225, 234, 202, 213, 243, 210, 216, 222 210, 219, 243, 222, 196, 213, 237, 240 219, 243, 213, 237, 222, 213, 225, 449 202, 231, 228, 216, 222, 225, 234, 219 243, 219, 213, 240, 219, 231, 243, 204 174, 231, 231, 237, 216, 216, 222, 196 199, 219, 231, 213, 222, 193, 207, 225 231, 210, 222, 219, 213, 225, 207, 204 204, 196, 207, 219, 202, 202, 202, 210 193, 202, 180, 199, 193, 202, 188, 177 193, 193, 202, 210, 188, 196, 177, 193 193, 180, 182, 182, 182, 213, 182, 199 193, 199, 180, 188, 196, 204, 199, 188 204, 174, 196, 185, 180, 193, 199, 199 182, 207, 180, 182, 207, 199, 196, 199 185, 222, 172, 185, 196, 213, 193, 202 204, 196, 204, 177, 213, 182, 177, 193 188, 185, 185, 182, 190, 204, 204, 210 174, 202, 196, 182, 185, 196, 190, 222 177, 193, 180, 180, 207, 193, 180, 199 196, 196, 193, 213, 207, 210, 185, 219 222, 172, 204, 199, 193, 234, 234, 228 174, 199, 207, 222, 243, 228, 225, 276 246, 243, 259, 250, 250, 246, 289, 234 262, 246, 256, 272, 306, 289, 306, 259 331, 306, 328, 310, 353, 353, 380, 342 372, 408, 392, 408, 416, 412, 467, 433 449, 458, 433, 404, 534, 420, 404, 420 396, 416, 342, 342, 339, 328, 335, 279 289, 289, 262, 296, 259, 246, 246, 269 272, 246, 222, 259, 246, 240, 202, 234 213, 216, 225, 219, 225, 231, 180, 216 216, 219, 216, 202, 182, 222, 177, 199 219, 199, 182, 207, 193, 193, 185, 213 196, 202, 182, 177, 188, 213, 222, 193 182, 210, 193, 199, 210, 193, 185, 172 207, 188, 196, 177, 193, 182, 177, 193 213, 172, 185, 166, 193, 190, 182, 172 188, 216, 164, 199, 204, 177, 204, 185 204, 177, 177, 180, 196, 188, 185, 172 188, 180, 164, 204, 151, 213, 185, 182 166, 193, 199, 177, 174, 199, 151, 196 188, 177, 190, 177, 207, 172, 199, 207 149, 174, 164, 177, 177, 174, 180, 166 177, 185, 164, 185, 164, 177, 154, 180 169, 172, 169, 196, 193, 174, 159, 180 182, 164, 185, 185, 164, 169, 185, 177 164, 202, 185, 180, 161, 169, 182, 174 185, 174, 169, 166, 174, 174, 164, 182 169, 182, 188, 180, 156, 174, 180, 190 174, 154, 166, 185, 177, 190, 154, 202 180, 188, 180, 196, 185, 169, 199, 193 190, 182, 185, 185, 190, 169, 196, 172 188, 190, 204, 188, 190, 188, 185, 231 172, 182, 193, 216, 185, 182, 174, 185 210, 188, 182, 202, 188, 188, 190, 204 188, 210, 193, 193, 204, 202, 164, 169 202, 185, 193, 207, 185, 204, 188, 174 177, 182, 202, 199, 196, 202, 210, 196 185, 207, 193, 199, 199, 199, 202, 222 207, 210, 188, 204, 188, 188, 199, 164 204, 199, 193, 159, 196, 169, 174, 180 196, 172, 182, 193, 213, 182, 199, 202 182, 207, 177, 193, 196, 180, 185, 202 190, 193, 199, 196, 204, 199, 204, 193 199, 199, 180, 188, 207, 196, 213, 202 222, 216, 228, 225, 216, 213, 219, 202 196, 210, 193, 193, 234, 210, 193, 204 188, 199, 199, 174, 202, 188, 174, 164 161, 169, 216, 196, 199, 188, 193, 199 169, 169, 185, 177, 210, 166, 213, 207 161, 204, 193, 193, 196, 188, 174, 169 172, 196, 185, 177, 180, 177, 172, 207 190, 185, 169, 177, 177, 196, 177, 188 161, 196, 177, 174, 164, 193, 166, 172 177, 149, 204, 174, 166, 159, 188, 193 182, 161, 174, 166, 166, 182, 137, 182 164, 174, 169, 188, 166, 190, 164, 161 177, 169, 164, 169, 149, 164, 164, 169 196, 185, 182, 154, 177, 188, 204, 159 164, 164, 177, 182, 190, 174, 164, 193 151, 154, 172, 156, 188, 174, 164, 174 180, 190, 177, 156, 177, 164, 169, 164 144, 202, 202, 169, 164, 177, 174, 174 174, 169, 172, 204, 166, 174, 188, 177 190, 182, 166, 166, 177, 188, 172, 190 169, 182, 180, 202, 177, 188, 177, 159 169, 154, 182, 188, 174, 185, 196, 174 196, 188, 185, 213, 199, 177, 182, 199 199, 169, 190, 185, 182, 164, 196, 174 169, 182, 188, 188, 190, 196, 174, 207 180, 185, 222, 190, 188, 169, 177, 213 219, 190, 222, 207, 202, 185, 207, 204 228, 222, 225, 222, 190, 164, 213, 180 182, 202, 180, 182, 180, 222, 174, 207 207, 193, 210, 216, 177, 199, 190, 172 202, 182, 166, 182, 207, 216, 213, 193 231, 207, 222, 196, 216, 182, 216, 228 204, 213, 188, 196, 190, 222, 219, 196 204, 222, 237, 231, 225, 216, 231, 216 196, 240, 231, 225, 219, 240, 219, 225 234, 237, 207, 228, 266, 202, 234, 237 225, 219, 259, 234, 240, 243, 216, 216 240, 243, 237, 231, 259, 243, 231, 240 246, 225, 243, 243, 272, 250, 246, 243 240, 250, 259, 488, 256, 228, 272, 266 246, 276, 303, 276, 276, 279, 276, 262 306, 269, 306, 266, 253, 299, 289, 313 289, 286, 353, 320, 282, 292, 303, 306 331, 299, 313, 328, 328, 369, 372, 303 350, 357, 342, 384, 396, 416, 384, 408 369, 404, 400, 449, 376, 416, 441, 462 416, 454, 458, 467, 493, 462, 534, 557 543, 538, 557, 581, 645, 605, 671, 645 697, 751, 745, 762, 795, 858, 807, 858 906, 942, 986, 961, 1050, 1056, 1011, 1109 1156, 1183, 1170, 1190, 1149, 1232, 1149, 1218 1183, 1190, 1211, 1076, 1116, 1050, 1102, 967 961, 955, 930, 918, 894, 847, 835, 841 801, 807, 807, 790, 767, 713, 697, 724 756, 676, 697, 686, 751, 666, 640, 655 660, 615, 671, 635, 590, 635, 655, 625 625, 640, 586, 600, 635, 615, 586, 600 620, 595, 620, 566, 625, 620, 620, 576 610, 600, 640, 557, 571, 562, 666, 576 605, 610, 581, 630, 600, 581, 576, 630 615, 615, 586, 676, 645, 595, 645, 686 671, 635, 686, 681, 660, 686, 660, 702 697, 718, 671, 697, 718, 708, 718, 702 724, 702, 713, 718, 708, 692, 718, 745 756, 745, 795, 756, 812, 767, 745, 801 767, 790, 795, 773, 829, 858, 784, 835 824, 841, 847, 818, 841, 824, 882, 864 870, 924, 918, 942, 924, 949, 936, 912 961, 894, 930, 967, 1043, 924, 986, 1030 986, 1063, 1050, 999, 1050, 1076, 1102, 1102 1043, 1096, 1116, 1176, 1156, 1218, 1190, 1204 1211, 1267, 1347, 1414, 1406, 1384, 1414, 1429 1544, 1505, 1608, 1706, 1689, 1772, 1764, 1731 1739, 1739, 1832, 1815, 1731, 1798, 1772, 1731 1747, 1714, 1640, 1640, 1584, 1498, 1529, 1436 1421, 1325, 1340, 1225, 1163, 1156, 1089, 1076 1030, 1005, 906, 924, 888, 841, 795, 784 778, 784, 790, 745, 713, 729, 718, 645 697, 645, 645, 590, 630, 595, 645, 600 576, 605, 576, 511, 620, 595, 543, 529 548, 520, 538, 515, 548, 534, 488, 467 497, 529, 502, 467, 506, 506, 488, 471 515, 497, 502, 458, 458, 488, 458, 488 462, 433, 437, 497, 441, 458, 467, 420 441, 441, 433, 424, 433, 416, 424, 369 396, 412, 416, 380, 454, 380, 396, 372 376, 388, 392, 388, 342, 372, 376, 380 384, 365, 372, 369, 357, 350, 380, 357 324, 388, 313, 369, 376, 353, 335, 335 392, 350, 353, 376, 331, 335, 320, 306 320, 339, 353, 320, 324, 320, 313, 313 317, 320, 303, 289, 299, 303, 320, 335 292, 276, 292, 303, 256, 303, 292, 299 303, 306, 272, 306, 269, 253, 286, 328 253, 259, 272, 276, 282, 320, 286, 306 299, 262, 320, 240, 289, 306, 310, 292 313, 276, 256, 269, 299, 269, 286, 289 324, 269, 262, 272, 269, 282, 262, 289 286, 269, 282, 266, 262, 262, 286, 289 272, 256, 286, 246, 246, 292, 240, 272 282, 276, 253, 276, 250, 289, 256, 299 243, 269, 313, 259, 272, 272, 279, 272 253, 246, 279, 282, 299, 272, 272, 266 256, 272, 292, 286, 262, 272, 286, 259 292, 262, 272, 259, 243, 306, 279, 279 246, 286, 262, 250, 279, 256, 292, 237 250, 269, 286, 243, 225, 269, 266, 282 256, 282, 259, 262, 237, 259, 253, 262 213, 262, 266, 266, 262, 243, 269, 279 246, 246, 250, 259, 276, 240, 289, 276 256, 276, 246, 279, 262, 262, 240, 282 269, 272, 237, 246, 269, 289, 269, 262 259, 262, 259, 243, 262, 250, 286, 262 276, 276, 262, 286, 262, 276, 266, 269 286, 276, 253, 246, 303, 269, 253, 256 259, 259, 243, 253, 228, 253, 276, 240 250, 253, 279, 246, 253, 279, 259, 276 289, 250, 266, 262, 262, 269, 246, 282 303, 262, 306, 266, 279, 299, 286, 266 259, 269, 269, 282, 262, 292, 292, 276 246, 269, 282, 296, 282, 286, 266, 269 262, 310, 272, 266, 276, 303, 286, 272 286, 269, 292, 299, 299, 279, 303, 289 296, 282, 231, 296, 320, 276, 320, 282 299, 296, 292, 320, 282, 313, 259, 286 303, 324, 299, 303, 303, 292, 313, 303 289, 306, 269, 299, 266, 317, 317, 299 306, 306, 313, 299, 292, 299, 272, 299 313, 292, 328, 272, 310, 282, 342, 279 328, 292, 289, 306, 313, 339, 324, 324 320, 328, 313, 335, 335, 286, 299, 324 342, 353, 324, 310, 279, 306, 317, 369 299, 306, 317, 313, 313, 306, 317, 342 335, 342, 313, 342, 331, 317, 320, 324 320, 328, 350, 342, 365, 335, 339, 328 342, 339, 346, 320, 310, 317, 306, 324 324, 342, 357, 310, 342, 320, 286, 296 331, 296, 303, 350, 286, 328, 320, 299 262, 262, 306, 276, 299, 317, 296, 313 296, 286, 276, 272, 286, 250, 296, 259 286, 253, 299, 286, 279, 250, 276, 276 250, 276, 282, 276, 282, 256, 250, 240 272, 272, 269, 246, 234, 259, 231, 262 256, 219, 228, 240, 237, 272, 246, 246 234, 246, 237, 228, 216, 243, 246, 243 210, 228, 256, 222, 210, 234, 219, 266 225, 243, 222, 228, 213, 225, 216, 216 225, 207, 237, 207, 204, 207, 204, 213 213, 202, 199, 219, 228, 231, 222, 219 210, 216, 234, 219, 219, 204, 210, 213 237, 199, 196, 210, 213, 185, 210, 219 216, 199, 213, 207, 213, 207, 213, 219 216, 204, 204, 177, 222, 228, 177, 207 180, 216, 190, 228, 199, 219, 207, 196 225, 228, 231, 210, 210, 196, 213, 188 182, 219, 190, 199, 207, 196, 202, 193 210, 177, 182, 182, 210, 199, 177, 210 202, 177, 199, 204, 196, 199, 180, 185 190, 202, 193, 193, 196, 188, 199, 180 188, 210, 188, 180, 213, 185, 188, 210 193, 196, 196, 199, 193, 213, 190, 161 166, 164, 182, 177, 177, 193, 188, 154 182, 199, 177, 196, 185, 180, 199, 193 177, 159, 216, 164, 185, 177, 188, 188 169, 169, 185, 182, 182, 169, 164, 190 169, 190, 182, 196, 180, 164, 161, 182 177, 188, 182, 210, 188, 196, 182, 177 164, 185, 161, 166, 177, 159, 177, 207 188, 174, 188, 139, 180, 174, 172, 199 190, 174, 182, 177, 188, 174, 199, 172 161, 169, 174, 177, 196, 190, 169, 151 177, 199, 196, 185, 164, 172, 172, 188 185, 182, 177, 202, 177, 174, 174, 169 177, 177, 182, 161, 164, 182, 193, 166 161, 149, 204, 188, 190, 144, 172, 185 154, 172, 174, 182, 180, 164, 159, 193 169, 172, 174, 190, 177, 149, 202, 193 190, 177, 182,/