SampleIdent,897C 41R-1 53-54 GLY,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,29-apr-1993 7:52,/ DataAngleRange, 2.0000, 34.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 90, 86, 92, 102, 90, 100, 117, 83 112, 98, 86, 96, 85, 76, 90, 92 90, 85, 85, 90, 114, 92, 85, 88 71, 86, 88, 85, 98, 104, 110, 92 83, 76, 90, 96, 96, 86, 98, 79 98, 81, 85, 96, 86, 98, 104, 85 88, 92, 86, 86, 96, 85, 92, 85 96, 77, 98, 98, 79, 81, 79, 74 85, 58, 79, 72, 96, 83, 74, 69 90, 67, 77, 85, 85, 85, 98, 90 98, 85, 92, 88, 81, 90, 72, 83 66, 85, 62, 86, 92, 90, 83, 98 106, 98, 81, 77, 94, 85, 104, 94 79, 92, 85, 104, 96, 85, 77, 100 119, 108, 119, 114, 121, 102, 112, 130 121, 132, 112, 123, 125, 137, 114, 119 117, 135, 137, 137, 130, 112, 121, 139 128, 149, 149, 144, 108, 174, 142, 137 142, 142, 130, 154, 174, 159, 174, 164 156, 151, 164, 169, 185, 174, 156, 182 174, 174, 180, 193, 185, 180, 180, 182 182, 228, 193, 196, 210, 202, 228, 216 243, 219, 216, 219, 228, 262, 222, 243 276, 225, 259, 253, 276, 243, 276, 279 272, 262, 259, 310, 306, 299, 276, 276 282, 269, 306, 324, 324, 306, 320, 313 361, 350, 342, 324, 372, 339, 372, 328 342, 350, 346, 372, 372, 412, 396, 396 412, 404, 380, 449, 475, 437, 404, 416 424, 449, 467, 502, 462, 493, 462, 497 497, 529, 511, 590, 484, 557, 562, 586 576, 534, 562, 605, 576, 571, 615, 610 610, 630, 645, 620, 645, 615, 660, 686 729, 718, 692, 686, 734, 745, 773, 734 751, 756, 767, 790, 729, 762, 829, 778 812, 812, 864, 888, 853, 835, 847, 882 829, 882, 882, 864, 894, 930, 912, 912 961, 870, 999, 906, 949, 973, 949, 942 992, 986, 961, 986, 961, 980, 942, 912 942, 967, 961, 949, 949, 918, 912, 1005 924, 961, 912, 980, 924, 900, 801, 906 942, 900, 882, 864, 858, 900, 829, 807 835, 812, 812, 818, 801, 853, 762, 745 762, 795, 729, 756, 724, 729, 713, 740 718, 702, 692, 681, 702, 681, 681, 666 666, 640, 635, 666, 655, 655, 660, 640 595, 590, 595, 543, 586, 576, 600, 581 576, 571, 576, 529, 493, 562, 543, 548 557, 511, 497, 471, 488, 515, 484, 488 475, 462, 454, 493, 467, 441, 475, 458 433, 475, 420, 400, 445, 424, 404, 416 424, 416, 428, 441, 424, 420, 428, 380 380, 392, 384, 380, 420, 416, 380, 384 372, 346, 369, 380, 376, 361, 357, 369 335, 372, 357, 350, 365, 320, 320, 306 365, 324, 339, 339, 317, 339, 339, 361 353, 313, 331, 310, 339, 350, 306, 346 320, 320, 279, 324, 306, 317, 282, 313 286, 320, 303, 279, 299, 299, 306, 296 310, 296, 313, 272, 328, 279, 320, 317 299, 231, 282, 286, 272, 266, 292, 303 279, 310, 292, 282, 313, 289, 276, 289 313, 276, 289, 272, 282, 266, 276, 299 246, 266, 272, 246, 292, 262, 296, 262 266, 246, 286, 282, 253, 292, 272, 262 292, 259, 262, 262, 289, 240, 256, 246 266, 253, 276, 282, 272, 256, 250, 279 240, 231, 299, 282, 259, 231, 234, 246 259, 228, 243, 250, 256, 243, 237, 240 262, 262, 266, 259, 269, 253, 240, 259 266, 228, 250, 282, 259, 259, 266, 243 262, 246, 243, 253, 259, 259, 222, 253 266, 256, 256, 256, 231, 262, 240, 256 243, 266, 253, 246, 250, 272, 259, 262 259, 266, 266, 250, 269, 256, 276, 262 279, 259, 282, 269, 279, 276, 266, 282 279, 259, 266, 289, 292, 262, 303, 276 282, 272, 342, 279, 286, 320, 317, 296 320, 331, 292, 313, 317, 313, 320, 286 286, 339, 328, 335, 342, 313, 306, 353 342, 306, 376, 372, 376, 361, 331, 392 342, 376, 408, 384, 408, 372, 437, 454 437, 462, 497, 458, 488, 462, 538, 534 552, 529, 615, 605, 650, 666, 708, 676 778, 751, 795, 773, 740, 734, 660, 666 625, 571, 630, 538, 502, 520, 458, 458 445, 392, 388, 424, 400, 380, 365, 376 392, 396, 357, 372, 357, 369, 384, 369 320, 313, 324, 306, 361, 324, 331, 296 320, 339, 296, 313, 328, 292, 313, 299 306, 286, 317, 303, 328, 324, 299, 320 279, 339, 303, 320, 282, 286, 310, 313 320, 279, 296, 299, 306, 282, 286, 292 286, 282, 303, 299, 269, 331, 331, 292 534, 286, 350, 296, 272, 346, 320, 299 296, 292, 324, 306, 303, 272, 331, 292 303, 313, 310, 286, 342, 310, 289, 292 303, 320, 313, 324, 320, 313, 303, 303 317, 335, 306, 306, 324, 339, 306, 331 331, 328, 320, 317, 303, 339, 292, 279 335, 310, 328, 335, 306, 282, 317, 313 289, 313, 328, 320, 342, 296, 299, 313 282, 313, 282, 286, 286, 240, 296, 306 313, 303, 303, 310, 303, 269, 310, 282 250, 282, 282, 306, 259, 279, 279, 282 259, 262, 259, 279, 250, 289, 240, 231 269, 246, 225, 240, 256, 237, 222, 228 219, 216, 222, 190, 237, 228, 234, 228 222, 228, 222, 172, 185, 216, 202, 177 193, 185, 190, 188, 210, 185, 182, 164 199, 182, 202, 213, 182, 180, 199, 193 193, 182, 174, 185, 196, 164, 174, 164 185, 193, 177, 169, 182, 177, 149, 156 166, 177, 177, 161, 190, 172, 174, 174 172, 182, 159, 164, 146, 149, 188, 166 188, 164, 159, 180, 193, 185, 188, 180 182, 172, 182, 182, 177, 164, 193, 185 156, 169, 166, 193, 166, 161, 159, 177 164, 204, 196, 177, 190, 164, 166, 207 180, 196, 193, 196, 156, 193, 172, 177 185, 188, 207, 193, 182, 193, 199, 190 169, 202, 204, 177, 199, 210, 196, 207 196, 216, 210, 193, 204, 213, 237, 185 222, 222, 225, 228, 237, 204, 240, 256 225, 240, 250, 262, 234, 269, 250, 256 320, 296, 306, 303, 313, 342, 299, 331 328, 392, 365, 365, 372, 388, 392, 404 441, 458, 471, 441, 449, 502, 449, 502 462, 529, 502, 441, 480, 502, 462, 433 441, 458, 424, 404, 408, 372, 376, 339 313, 353, 310, 269, 306, 299, 286, 262 269, 282, 240, 219, 243, 204, 202, 182 207, 202, 193, 193, 180, 177, 182, 169 174, 172, 154, 159, 174, 185, 164, 146 159, 142, 159, 130, 154, 151, 151, 137 177, 149, 144, 128, 146, 159, 128, 166 154, 144, 142, 135, 132, 146, 149, 137 130, 132, 135, 119, 128, 144, 137, 125 130, 130, 119, 117, 132, 119, 112, 123 125, 142, 128, 112, 137, 128, 139, 135 132, 112, 137, 139, 130, 119, 117, 135 128, 130, 110, 102, 130, 119, 119, 130 135, 121, 132, 123, 110, 135, 128, 112 110, 137, 137, 123, 139, 114, 121, 117 125, 137, 112, 128, 132, 102, 135, 137 106, 121, 130, 130, 114, 139, 132, 123 137, 132, 130, 114, 161, 149, 128, 112 128, 119, 130, 154, 125, 149, 114, 119 121, 117, 121, 121, 139, 128, 139, 112 132, 117, 135, 123, 137, 121, 132, 123 119, 144, 142, 123, 130, 135, 144, 117 139, 128, 139, 114, 144, 130, 137, 117 130, 132, 139, 119, 144, 135, 125, 144 130, 135, 125, 130, 144, 112, 144, 125 135, 149, 132, 130, 151, 139, 137, 137 159, 123, 146, 159, 154, 125, 154, 156 149, 123, 161, 125, 132, 114, 149, 128 146, 130, 144, 164, 154, 137, 142, 164 154, 137, 149, 174, 159, 149, 146, 151 161, 149, 144, 161, 172, 437, 156, 159 161, 156, 159, 185, 161, 185, 159, 166 180, 156, 182, 180, 196, 190, 182, 172 166, 210, 196, 190, 188, 156, 196, 207 202, 182, 196, 188, 204, 202, 180, 240 213, 199, 204, 202, 193, 202, 225, 222 222, 237, 199, 228, 222, 210, 237, 228 228, 222, 222, 250, 231, 240, 225, 228 240, 256, 262, 231, 240, 243, 240, 246 250, 234, 286, 262, 262, 250, 256, 266 269, 299, 253, 272, 246, 276, 286, 286 269, 266, 262, 266, 292, 279, 243, 279 240, 246, 259, 286, 276, 299, 231, 289 246, 286, 250, 266, 292, 259, 272, 289 286, 256, 269, 269, 286, 237, 256, 253 259, 259, 246, 282, 256, 243, 246, 243 222, 240, 246, 243, 266, 259, 237, 243 240, 253, 222, 237, 246, 246, 225, 228 228, 228, 213, 222, 237, 231, 228, 259 219, 228, 219, 234, 228, 234, 216, 210 202, 225, 190, 228, 213, 231, 219, 202 234, 210, 228, 228, 210, 193, 219, 234 237, 210, 202, 207, 207, 219, 196, 185 210, 174, 207, 202, 193, 202, 204, 210 188, 185, 188, 196, 199, 219, 210, 164 210, 174, 193, 180, 182, 193, 196, 210 161, 210, 207, 196, 180, 182, 202, 180 207, 204, 185, 210, 204, 207, 185, 202 216, 193, 190, 222, 182, 210, 234, 222 216, 213, 185, 180, 219, 213, 204, 199 202, 166, 225, 202, 222, 213, 210, 228 216, 234, 219, 246, 225, 234, 234, 222 237, 253, 222, 202, 222, 246, 262, 243 250, 266, 237, 266, 279, 299, 289, 299 306, 320, 331, 350, 339, 396, 350, 404 384, 420, 428, 449, 462, 480, 467, 543 506, 534, 562, 529, 548, 595, 552, 484 520, 524, 515, 433, 404, 384, 384, 361 357, 292, 335, 296, 299, 276, 276, 231 256, 269, 243, 231, 256, 228, 225, 216 225, 240, 210, 207, 185, 210, 210, 193 185, 210, 204, 199, 193, 193, 213, 199 180, 202, 210, 193, 177, 196, 188, 177 174, 196, 166, 193, 174, 202, 177, 196 169, 185, 196, 180, 180, 180, 169, 185 182, 169, 161, 169, 213, 188, 204, 185 177, 164, 180, 185, 174, 185, 166, 193 190, 185, 166, 166, 182, 180, 185, 177 166, 159, 188, 213, 182, 190, 196, 204 199, 190, 180, 207, 159, 207, 199, 216 169, 182, 210, 174, 169, 204, 199, 193 190, 164, 154, 177, 174, 159, 188, 174 142, 156, 174, 174, 161, 159, 182, 177 174, 159, 169, 154, 172, 174, 172, 151 180, 166, 166, 164, 161, 180, 128, 156 166, 177, 180, 156, 159, 166, 164, 164 172, 188, 164, 190, 161, 164, 180, 199 169, 169, 177, 164, 166, 166, 169, 177 182, 159, 180, 161, 193, 182, 159, 182 180, 174, 182, 144, 185, 216, 174, 164 174, 185, 193, 174, 177, 174, 182, 182 182, 172, 216, 156, 190, 185, 196, 177 177, 166, 154, 169, 174, 190, 185, 196 177, 193, 154, 151, 164, 174, 185, 159 172, 185, 190, 188, 207, 169, 188, 188 182, 174, 164, 174, 182, 185, 199, 185 188, 180, 207, 199, 185, 185, 199, 219 193, 202, 188, 177, 188, 202, 193, 174 188, 166, 210, 199, 190, 177, 216, 202 174, 202, 202, 207, 219, 188, 204, 164 207, 222, 193, 193, 202, 204, 196, 196 196, 196, 213, 188, 196, 188, 213, 213 202, 188, 202, 210, 188, 193, 185, 177 199, 202, 190, 190, 204, 196, 193, 213 213, 225, 188, 180, 213, 202, 225, 228 202, 222, 207, 225, 225, 213, 202, 213 225, 190, 202, 225, 199, 204, 174, 196 202, 159, 199, 172, 169, 188, 180, 159 166, 185, 180, 182, 139, 154, 177, 182 151, 182, 172, 172, 151, 154, 159, 177 190, 149, 159, 174, 151, 166, 169, 159 151, 164, 144, 156, 166, 156, 159, 166 142, 139, 177, 177, 164, 169, 159, 159 169, 169, 144, 154, 151, 154, 149, 144 125, 128, 146, 137, 156, 169, 135, 159 164, 159, 156, 132, 149, 169, 156, 144 149, 130, 164, 146, 154, 149, 135, 139 149, 151, 125, 137, 149, 177, 151, 151 137, 139, 177, 128, 159, 146, 156, 144 137, 149, 142, 159, 149, 159, 177, 169 151, 130, 130, 154, 154, 144, 159, 149 135, 164, 142, 161, 137, 128, 164, 144 149, 119, 156, 121, 177, 169, 159, 159 164, 156, 149, 166, 154, 159, 137, 146 121, 151, 142, 149, 172, 146, 159, 159 156, 144, 144, 130, 149, 156, 144, 154 159, 149, 164, 169, 146, 149, 169, 156 142, 159, 164, 164, 159, 159, 159, 185 159, 154, 154, 142, 154, 159, 130, 151 149, 169, 142, 151, 139, 161, 142, 146 174, 177, 154, 172, 151, 151, 161, 159 154, 204, 177, 154, 196, 161, 164, 156 172, 135, 188, 177, 154, 169, 161, 164 182, 177, 161, 174, 144, 166, 149, 156 169, 149, 146, 185, 149, 139, 193, 202 164, 144, 146, 174, 166, 161, 161, 161 188, 154, 164, 180, 174, 149, 172, 166 177, 177, 174, 182, 169, 193, 182, 161 177, 188, 154, 210, 199, 182, 177, 188 193, 177, 193, 190, 199, 177, 182, 193 193, 188, 199, 169, 166, 199, 213, 202 204, 182, 210, 185, 190, 210, 193, 202 196, 199, 219, 207, 225, 199, 193, 204 204, 196, 193, 213, 204, 204, 185, 222 219, 199, 216, 216, 213, 210, 219, 210 207, 210, 216, 193, 240, 228, 234, 250 207, 234, 216, 225, 216, 222, 276, 219 225, 228, 246, 222, 234, 243, 272, 246 269, 228, 266, 234, 266, 246, 266, 256 272, 286, 246, 282, 269, 266, 292, 292 286, 310, 303, 272, 282, 296, 361, 342 328, 365, 320, 357, 335, 335, 369, 342 357, 369, 350, 412, 428, 376, 424, 454 437, 449, 412, 449, 458, 475, 524, 484 586, 538, 600, 620, 681, 660, 676, 671 708, 692, 767, 812, 778, 778, 818, 847 835, 818, 801, 847, 801, 801, 790, 784 740, 751, 734, 713, 708, 650, 625, 681 635, 610, 610, 671, 595, 620, 586, 590 640, 576, 586, 620, 562, 581, 566, 511 605, 581, 586, 581, 576, 640, 566, 566 557, 557, 548, 571, 548, 511, 524, 576 529, 543, 524, 543, 538, 581, 538, 548 520, 538, 520, 562, 529, 543, 493, 581 605, 529, 581, 600, 610, 562, 590, 548 640, 625, 605, 576, 610, 620, 581, 600 645, 620, 645, 610, 666, 645, 645, 655 650, 645, 718, 702, 692, 697, 724, 686 713, 729, 784, 734, 724, 784, 751, 745 795, 818, 807, 812, 756, 853, 790, 807 829, 818, 841, 807, 829, 864, 824, 818 841, 894, 835, 992, 912, 906, 942, 906 888, 999, 912, 980, 942, 936, 1024, 1018 980, 1011, 992, 1005, 1063, 1089, 1109, 1024 1050, 1043, 1037, 1197, 1129, 1246, 1225, 1232 1149, 1232, 1253, 1274, 1274, 1296, 1376, 1376 1369, 1459, 1421, 1537, 1475, 1537, 1665, 1681 1756, 1739, 1798, 1980, 1927, 1971, 2125, 2144 2144, 2237, 2372, 2391, 2430, 2460, 2421, 2601 2460, 2460, 2381, 2323, 2323, 2256, 2153, 2172 2043, 1901, 1875, 1747, 1632, 1584, 1475, 1354 1318, 1318, 1176, 1170, 1129, 1096, 986, 1018 955, 955, 900, 858, 864, 858, 790, 812 784, 734, 708, 906, 729, 713, 676, 686 671, 630, 666, 600, 640, 635, 630, 600 590, 581, 571, 548, 538, 610, 557, 511 552, 581, 543, 538, 511, 488, 524, 502 502, 471, 520, 471, 534, 475, 488, 493 471, 515, 493, 484, 493, 471, 480, 502 441, 484, 445, 400, 454, 428, 462, 441 433, 441, 384, 433, 420, 400, 384, 392 372, 416, 400, 369, 376, 408, 365, 376 400, 404, 357, 392, 388, 372, 384, 376 335, 365, 365, 350, 335, 353, 353, 335 339, 346, 339, 346, 353, 346, 328, 317 335, 324, 331, 296, 320, 306, 292, 289 292, 303, 320, 320, 256, 276, 331, 310 272, 292, 310, 310, 272, 299, 279, 266 272, 289, 289, 282, 497, 276, 310, 269 286, 259, 292, 253, 292, 282, 272, 269 253, 272, 272, 269, 269, 282, 266, 246 246, 246, 250, 269, 272, 253, 240, 250 286, 272, 256, 286, 269, 250, 256, 256 262, 269, 262, 262, 250, 231, 237, 259 246, 253, 286, 253, 250, 276, 256, 256 269, 237, 256, 269, 231, 262, 250, 246 243, 269, 269, 282, 262, 246, 256, 246 240, 286, 262, 243, 272, 262, 240, 253 262, 286, 259, 272, 262, 256, 266, 262 259, 276, 250, 282, 250, 256, 231, 243 266, 250, 269, 243, 262, 243, 231, 256 262, 231, 259, 256, 202, 210, 246, 210 228, 228, 210, 253, 292, 262, 262, 196 262, 240, 237, 250, 246, 243, 228, 237 240, 240, 250, 246, 237, 253, 237, 262 243, 250, 259, 279, 243, 272, 266, 262 259, 228, 231, 266, 231, 259, 276, 246 282, 237, 234, 237, 276, 243, 234, 213 256, 246, 269, 243, 234, 262, 246, 253 237, 216, 256, 266, 259, 276, 240, 259 253, 225, 240, 262, 246, 253, 225, 240 225, 259, 234, 243, 234, 240, 243, 286 292, 253, 256, 240, 246, 256, 256, 286 256, 282, 240, 237, 250, 240, 250, 269 272, 272, 234, 228, 276, 243, 272, 246 276, 237, 266, 262, 256, 262, 296, 276 269, 243, 234, 256, 286, 289, 237, 276 286, 253, 272, 262, 286, 299, 266, 259 269, 250, 276, 269, 279, 259, 262, 289 286, 269, 282, 266, 282, 282, 279, 289 276, 269, 286, 292, 303, 276, 310, 313 313, 313, 313, 256, 299, 320, 292, 276 313, 306, 313, 279, 296, 286, 328, 306 317, 289, 299, 286, 299, 299, 320, 317 350, 317, 306, 286, 324, 317, 292, 339 303, 320, 286, 310, 346, 317, 310, 320 331, 313, 335, 339, 339, 346, 317, 320 346, 342, 350, 331, 335, 331, 317, 353 342, 328, 342, 361, 361, 320, 331, 361 342, 306, 317, 320, 342, 357, 346, 320 350, 346, 339, 342, 342, 324, 350, 331 353, 365, 342, 339, 357, 313, 331, 317 299, 350, 342, 320, 350, 342, 313, 306 313, 328, 296, 335, 289, 328, 296, 310 306, 310, 299, 296, 289, 303, 286, 286 292, 299, 313, 276, 320, 262, 286, 303 276, 266, 289, 292, 279, 279, 266, 266 458, 262, 246, 256, 253, 259, 262, 243 262, 286, 262, 262, 237, 250, 250, 246 231, 234, 262, 237, 237, 222, 246, 216 202, 219, 222, 225, 210, 216, 213, 234 240, 225, 250, 207, 225, 202, 213, 207 210, 234, 213, 204, 190, 207, 210, 210 213, 228, 225, 213, 231, 188, 199, 202 196, 196, 182, 202, 207, 202, 188, 196 204, 196, 193, 180, 190, 182, 185, 199 193, 199, 193, 196, 190, 199, 185, 177 180, 172, 193, 180, 180, 196, 199, 180 190, 207, 199, 188, 202, 193, 193, 159 182, 172, 199, 174, 177, 193, 164, 169 196, 146, 199, 193, 196, 177, 188, 182 156, 199, 185, 159, 190, 169, 182, 177 177, 182, 188, 202, 161, 185, 159, 169 169, 182, 193, 177, 174, 169, 156, 149 156, 172, 188, 164, 156, 164, 156, 182 172, 180, 182, 202, 159, 144, 149, 164 166, 193, 164, 164, 174, 164, 166, 169 164, 164, 159, 164, 159, 164, 156, 182 177, 169, 156, 159, 128, 164, 164, 174 149, 161, 169, 185, 166, 161, 166, 174 142, 169, 169, 144, 144, 174, 164, 161 161, 166, 180, 146, 137, 204, 159, 166 164, 172, 151, 161, 151, 180, 159, 164 182, 166, 159, 164, 154, 177, 142, 182 156, 164, 174, 185, 149, 161, 159, 154 182, 169, 164, 164, 149, 166, 177, 166 151, 161, 164, 199, 166, 169, 161, 139 164, 151, 188, 154, 154, 172, 151, 166 164, 169, 144, 156, 164, 149, 169, 164 164, 177, 172, 149, 169, 174, 193, 159 146, 169, 169, 182, 169, 161, 169, 154 164, 169, 185, 149, 161, 159, 146, 159 164, 180, 161, 156, 177, 128, 193, 144 161, 353, 156,/