SampleIdent,897C 60R-3 42-3 HEAT,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,29-apr-1993 16:17,/ DataAngleRange, 2.0000, 34.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 92, 71, 71, 77, 66, 76, 77, 56 85, 79, 66, 83, 71, 72, 67, 72 76, 69, 72, 85, 58, 59, 71, 76 67, 69, 66, 72, 66, 81, 71, 61 76, 66, 66, 53, 66, 83, 56, 59 62, 71, 66, 69, 71, 83, 64, 48 71, 376, 67, 61, 67, 81, 67, 71 71, 72, 53, 56, 71, 66, 62, 56 53, 53, 44, 76, 76, 58, 79, 64 64, 56, 52, 71, 64, 59, 69, 49 52, 72, 59, 67, 62, 58, 66, 50 55, 59, 72, 66, 71, 56, 64, 74 61, 58, 69, 76, 56, 66, 67, 67 56, 83, 62, 59, 66, 52, 66, 76 72, 66, 50, 56, 56, 61, 56, 64 59, 58, 76, 74, 50, 50, 62, 69 72, 67, 62, 46, 62, 64, 59, 62 64, 62, 72, 62, 83, 41, 66, 69 62, 62, 74, 62, 77, 64, 83, 69 71, 58, 71, 66, 76, 85, 64, 62 72, 72, 61, 59, 81, 62, 58, 67 62, 58, 71, 56, 72, 64, 59, 69 67, 67, 76, 71, 62, 72, 71, 92 62, 62, 71, 76, 66, 71, 74, 77 67, 62, 79, 58, 71, 74, 56, 59 83, 61, 55, 66, 76, 67, 66, 85 66, 76, 71, 76, 71, 76, 77, 61 76, 62, 67, 69, 77, 77, 72, 62 66, 69, 76, 64, 74, 69, 76, 83 76, 83, 83, 76, 83, 66, 69, 94 59, 81, 79, 83, 85, 79, 71, 71 67, 56, 79, 67, 86, 79, 85, 85 71, 76, 61, 81, 79, 83, 76, 85 83, 77, 77, 106, 86, 96, 77, 74 64, 83, 76, 86, 72, 86, 98, 77 86, 88, 88, 90, 92, 72, 77, 92 83, 92, 92, 77, 100, 85, 96, 96 90, 85, 106, 88, 119, 104, 96, 79 79, 92, 96, 104, 108, 88, 108, 125 96, 86, 98, 92, 119, 106, 112, 117 114, 98, 108, 100, 121, 114, 137, 94 119, 108, 112, 144, 125, 132, 135, 117 142, 117, 117, 130, 108, 137, 149, 149 121, 123, 135, 154, 156, 156, 144, 139 161, 144, 137, 146, 154, 149, 144, 137 137, 151, 154, 151, 146, 149, 135, 177 159, 149, 159, 169, 161, 166, 164, 156 174, 144, 185, 154, 182, 182, 169, 190 182, 188, 188, 154, 196, 202, 185, 196 228, 204, 188, 185, 177, 219, 159, 196 213, 207, 207, 196, 204, 216, 199, 210 193, 213, 231, 190, 207, 210, 237, 231 234, 250, 228, 259, 231, 246, 243, 231 266, 269, 253, 286, 256, 266, 279, 269 262, 279, 289, 282, 286, 299, 279, 286 279, 296, 317, 289, 292, 299, 276, 313 299, 279, 262, 310, 320, 286, 272, 282 289, 299, 320, 282, 317, 286, 259, 253 296, 266, 289, 256, 269, 256, 286, 286 282, 299, 292, 306, 276, 289, 303, 246 299, 292, 299, 269, 276, 296, 243, 324 269, 276, 286, 269, 272, 289, 276, 306 320, 292, 286, 324, 266, 292, 276, 272 292, 282, 299, 299, 282, 299, 303, 306 335, 286, 331, 310, 292, 286, 282, 286 313, 299, 306, 306, 313, 342, 306, 299 328, 279, 313, 313, 286, 353, 296, 328 317, 320, 350, 313, 346, 296, 346, 324 320, 339, 299, 299, 313, 310, 331, 331 306, 313, 331, 353, 320, 339, 335, 339 342, 365, 339, 353, 346, 335, 365, 350 392, 350, 350, 369, 350, 317, 346, 380 384, 369, 353, 384, 365, 372, 342, 380 372, 384, 388, 388, 400, 339, 384, 380 396, 372, 369, 400, 376, 384, 400, 372 408, 342, 400, 412, 420, 433, 412, 408 458, 433, 437, 404, 433, 458, 488, 475 424, 408, 428, 471, 493, 441, 416, 488 511, 502, 488, 467, 524, 493, 484, 534 493, 571, 488, 511, 548, 520, 571, 534 581, 610, 571, 615, 534, 645, 625, 605 640, 640, 676, 655, 640, 660, 692, 686 713, 756, 756, 762, 751, 801, 818, 818 900, 894, 847, 918, 912, 955, 955, 973 1005, 1102, 1163, 1089, 1156, 1211, 1232, 1282 1332, 1332, 1296, 1253, 1303, 1303, 1232, 1136 1170, 1096, 1142, 1069, 1005, 986, 955, 992 888, 912, 847, 807, 778, 762, 745, 681 708, 692, 692, 681, 630, 605, 660, 600 571, 576, 534, 548, 562, 552, 515, 475 475, 511, 511, 488, 467, 458, 462, 433 404, 412, 454, 388, 412, 416, 416, 412 369, 353, 339, 369, 384, 320, 372, 331 331, 313, 372, 335, 346, 328, 320, 306 303, 286, 286, 276, 313, 272, 289, 276 276, 246, 269, 250, 262, 266, 237, 253 240, 262, 231, 259, 237, 240, 237, 222 237, 240, 199, 188, 182, 210, 190, 177 222, 204, 188, 196, 210, 196, 193, 207 164, 196, 174, 156, 156, 159, 161, 166 156, 174, 154, 156, 177, 172, 154, 151 154, 146, 174, 137, 156, 142, 144, 164 159, 149, 135, 139, 164, 139, 135, 137 137, 137, 130, 119, 139, 146, 132, 139 139, 128, 121, 121, 139, 128, 139, 144 144, 139, 117, 132, 139, 137, 142, 142 139, 130, 130, 128, 128, 128, 117, 110 121, 132, 135, 128, 139, 149, 139, 130 132, 123, 123, 102, 125, 135, 125, 130 130, 130, 112, 110, 102, 137, 112, 98 144, 112, 121, 119, 119, 128, 98, 110 130, 135, 137, 108, 121, 119, 112, 112 121, 110, 96, 144, 130, 130, 123, 123 114, 110, 125, 112, 114, 119, 96, 117 128, 114, 108, 117, 102, 130, 112, 117 123, 135, 102, 130, 128, 132, 106, 119 112, 119, 112, 121, 102, 102, 110, 117 96, 121, 106, 104, 77, 102, 100, 96 121, 108, 110, 112, 94, 106, 121, 121 100, 110, 114, 112, 123, 106, 100, 106 104, 276, 106, 106, 416, 112, 123, 102 106, 114, 114, 100, 108, 110, 92, 130 96, 110, 130, 112, 102, 121, 106, 104 121, 112, 117, 121, 92, 114, 108, 117 114, 132, 117, 100, 123, 100, 100, 112 114, 121, 100, 114, 121, 102, 100, 112 114, 96, 123, 88, 102, 86, 114, 123 114, 123, 106, 108, 98, 106, 100, 106 128, 110, 96, 119, 121, 114, 110, 123 108, 128, 142, 114, 132, 106, 121, 94 121, 114, 119, 114, 90, 132, 112, 119 104, 100, 121, 110, 123, 121, 137, 106 119, 106, 114, 114, 110, 123, 104, 112 110, 106, 83, 94, 112, 110, 106, 128 112, 98, 119, 110, 88, 104, 94, 102 123, 94, 104, 117, 119, 114, 92, 112 121, 123, 104, 92, 117, 123, 121, 98 125, 90, 137, 98, 104, 104, 98, 112 110, 110, 102, 94, 102, 102, 112, 119 94, 104, 110, 106, 114, 86, 132, 110 98, 119, 121, 104, 104, 119, 100, 102 110, 100, 92, 112, 128, 117, 110, 104 114, 100, 110, 125, 110, 119, 108, 96 121, 114, 112, 123, 106, 114, 114, 121 123, 121, 104, 112, 121, 112, 125, 130 114, 108, 121, 112, 112, 144, 119, 128 106, 149, 110, 114, 108, 114, 123, 125 110, 96, 102, 112, 110, 128, 123, 121 119, 121, 123, 117, 117, 130, 108, 94 121, 114, 125, 123, 142, 130, 112, 117 112, 132, 110, 123, 142, 139, 125, 132 125, 137, 119, 112, 125, 135, 132, 132 123, 123, 135, 132, 130, 123, 132, 121 137, 102, 117, 130, 128, 114, 130, 139 100, 110, 130, 117, 135, 110, 139, 125 121, 106, 142, 125, 121, 112, 117, 130 128, 117, 106, 128, 117, 106, 137, 128 132, 119, 119, 104, 119, 110, 114, 108 106, 123, 123, 110, 114, 117, 135, 123 130, 119, 114, 139, 112, 117, 121, 112 121, 112, 132, 114, 119, 119, 132, 106 121, 128, 117, 123, 114, 112, 137, 119 123, 125, 121, 149, 119, 121, 121, 114 137, 125, 114, 149, 123, 149, 110, 137 135, 146, 121, 130, 137, 137, 123, 144 159, 119, 130, 123, 121, 135, 132, 149 144, 121, 149, 151, 151, 135, 135, 144 130, 130, 117, 139, 139, 161, 149, 137 137, 135, 139, 128, 154, 161, 159, 161 174, 142, 137, 135, 149, 137, 164, 142 156, 166, 177, 144, 130, 169, 161, 137 154, 156, 166, 144, 146, 159, 154, 177 166, 154, 149, 130, 174, 172, 180, 177 156, 193, 169, 161, 177, 174, 174, 151 182, 177, 156, 159, 161, 159, 190, 188 185, 154, 188, 174, 196, 185, 169, 159 188, 161, 159, 159, 182, 156, 216, 190 182, 222, 202, 169, 161, 182, 190, 159 188, 204, 213, 177, 182, 196, 202, 216 202, 172, 207, 161, 166, 164, 185, 196 231, 196, 185, 219, 180, 207, 196, 193 210, 202, 231, 202, 225, 202, 199, 210 202, 207, 400, 213, 193, 213, 228, 219 234, 231, 228, 213, 216, 204, 210, 222 243, 210, 213, 246, 222, 213, 210, 246 228, 237, 237, 225, 207, 225, 240, 243 246, 228, 216, 222, 259, 240, 213, 231 259, 243, 246, 253, 246, 240, 266, 266 237, 246, 282, 259, 253, 222, 266, 276 269, 292, 286, 272, 299, 292, 296, 292 317, 286, 310, 292, 320, 310, 306, 342 361, 331, 303, 339, 353, 365, 365, 384 388, 380, 408, 420, 412, 441, 433, 428 458, 471, 497, 502, 538, 524, 511, 586 615, 645, 625, 671, 650, 734, 708, 762 790, 756, 829, 778, 812, 912, 876, 882 961, 924, 955, 961, 973, 961, 930, 853 894, 876, 812, 756, 784, 708, 692, 650 640, 581, 586, 595, 600, 548, 534, 520 484, 484, 471, 511, 471, 471, 488, 441 475, 437, 408, 424, 449, 392, 408, 416 400, 412, 412, 372, 400, 400, 376, 365 353, 350, 328, 357, 384, 357, 342, 369 346, 317, 372, 339, 324, 306, 324, 328 317, 306, 289, 299, 303, 286, 276, 266 303, 272, 306, 286, 272, 253, 292, 243 262, 266, 269, 253, 289, 231, 262, 240 234, 237, 246, 269, 253, 237, 272, 256 237, 222, 256, 253, 253, 243, 231, 237 253, 216, 225, 199, 213, 222, 210, 228 240, 259, 207, 234, 262, 219, 210, 250 196, 185, 204, 202, 225, 199, 225, 210 182, 196, 231, 204, 207, 202, 207, 202 225, 231, 222, 202, 207, 196, 196, 207 225, 213, 213, 199, 219, 199, 199, 216 185, 182, 177, 172, 202, 185, 185, 196 166, 177, 188, 210, 193, 188, 182, 177 190, 196, 185, 193, 164, 199, 188, 199 169, 174, 199, 188, 190, 182, 207, 180 188, 199, 166, 180, 185, 180, 166, 156 180, 159, 188, 166, 188, 159, 169, 169 169, 185, 196, 190, 169, 177, 164, 172 180, 188, 185, 182, 172, 172, 185, 166 164, 177, 188, 174, 188, 185, 188, 177 177, 177, 193, 188, 199, 185, 210, 182 177, 185, 174, 166, 185, 161, 196, 164 185, 216, 180, 177, 174, 210, 185, 193 169, 188, 199, 188, 202, 154, 177, 172 185, 172, 174, 174, 164, 180, 164, 185 188, 193, 169, 199, 177, 188, 159, 180 193, 177, 193, 174, 196, 180, 182, 164 172, 185, 188, 164, 193, 172, 164, 169 182, 177, 177, 169, 172, 177, 180, 151 180, 161, 180, 166, 154, 174, 185, 188 174, 177, 177, 202, 180, 172, 172, 174 169, 196, 180, 182, 188, 174, 169, 172 196, 174, 202, 190, 190, 182, 193, 177 193, 199, 182, 185, 207, 172, 193, 196 177, 182, 169, 169, 164, 177, 210, 202 188, 188, 188, 190, 172, 207, 174, 196 182, 164, 193, 164, 177, 199, 196, 190 213, 185, 193, 169, 177, 174, 199, 177 202, 180, 182, 182, 196, 166, 193, 199 166, 177, 193, 193, 180, 169, 196, 169 164, 164, 190, 199, 172, 151, 174, 196 177, 202, 185, 169, 174, 177, 180, 169 166, 219, 207, 193, 193, 193, 190, 207 185, 207, 204, 196, 204, 188, 174, 182 188, 188, 182, 193, 199, 199, 196, 185 190, 172, 202, 199, 188, 188, 219, 185 188, 177, 210, 210, 185, 213, 188, 204 222, 210, 193, 204, 202, 207, 216, 204 182, 190, 196, 185, 190, 177, 185, 196 216, 185, 174, 182, 156, 216, 222, 204 196, 182, 219, 234, 222, 193, 190, 185 207, 231, 231, 222, 213, 222, 202, 196 199, 202, 190, 193, 188, 231, 219, 207 204, 204, 213, 204, 228, 213, 196, 228 225, 219, 213, 216, 231, 237, 185, 234 210, 213, 219, 207, 210, 207, 228, 216 225, 231, 219, 213, 237, 202, 216, 240 219, 225, 213, 196, 231, 219, 240, 228 216, 228, 228, 234, 222, 231, 231, 234 228, 237, 237, 225, 234, 272, 237, 250 228, 259, 246, 213, 246, 262, 228, 231 256, 259, 246, 207, 237, 237, 256, 237 253, 216, 240, 243, 266, 243, 266, 243 222, 225, 234, 272, 246, 240, 256, 250 250, 199, 279, 234, 240, 250, 237, 286 253, 269, 279, 240, 246, 262, 279, 269 276, 253, 269, 246, 256, 256, 269, 286 234, 259, 299, 292, 266, 262, 259, 269 286, 276, 253, 266, 262, 259, 266, 269 243, 253, 286, 259, 259, 296, 289, 246 299, 286, 299, 306, 262, 279, 313, 272 279, 306, 246, 292, 292, 286, 296, 299 303, 328, 262, 303, 289, 299, 276, 269 292, 328, 279, 328, 331, 276, 303, 299 256, 282, 276, 331, 296, 292, 282, 306 306, 299, 266, 292, 296, 299, 324, 292 339, 272, 328, 289, 310, 292, 328, 299 292, 313, 299, 303, 317, 324, 328, 317 317, 292, 286, 296, 306, 292, 306, 272 320, 292, 320, 328, 342, 292, 296, 299 328, 306, 320, 328, 317, 328, 339, 289 331, 328, 328, 328, 350, 306, 331, 313 286, 310, 357, 339, 353, 328, 331, 331 357, 342, 335, 346, 299, 313, 353, 369 331, 369, 317, 331, 369, 369, 384, 339 339, 372, 342, 346, 365, 365, 392, 357 384, 328, 388, 412, 369, 412, 392, 400 424, 404, 380, 396, 392, 408, 376, 380 346, 408, 441, 392, 396, 424, 384, 400 388, 408, 412, 384, 428, 433, 412, 396 376, 369, 441, 420, 445, 404, 437, 396 433, 404, 400, 392, 396, 412, 458, 454 420, 445, 428, 467, 424, 408, 408, 412 424, 454, 467, 424, 454, 467, 480, 437 449, 484, 475, 480, 475, 502, 480, 480 506, 458, 484, 484, 529, 506, 520, 566 488, 548, 502, 562, 576, 543, 562, 590 586, 600, 635, 625, 595, 625, 600, 625 640, 640, 697, 713, 692, 729, 734, 756 745, 751, 818, 864, 847, 888, 876, 924 967, 973, 1037, 973, 1102, 1136, 1204, 1267 1274, 1303, 1318, 1452, 1482, 1529, 1648, 1665 1781, 1823, 1901, 1936, 2116, 2172, 2294, 2275 2440, 2470, 2673, 2591, 2809, 2642, 2798, 2830 2959, 3058, 2927, 3047, 3147, 2970, 3091, 3102 3272, 3014, 3069, 2959, 2852, 2841, 2841, 2735 2632, 2550, 2480, 2333, 2372, 2314, 2162, 2125 2153, 1971, 1954, 1849, 1781, 1764, 1798, 1689 1739, 1656, 1656, 1632, 1560, 1560, 1521, 1632 1537, 1498, 1421, 1521, 1429, 1513, 1384, 1414 1421, 1391, 1391, 1354, 1354, 1421, 1310, 1362 1289, 1260, 1332, 1289, 1303, 1282, 1296, 1218 1246, 1253, 1303, 1218, 1218, 1232, 1253, 1211 1183, 1225, 1142, 1225, 1129, 1116, 1102, 1142 1069, 1122, 1102, 1076, 1089, 1109, 1056, 1005 986, 1267, 973, 999, 1005, 967, 961, 1011 961, 924, 961, 912, 955, 900, 894, 906 824, 876, 858, 801, 888, 835, 812, 784 847, 841, 751, 767, 835, 784, 790, 767 756, 745, 740, 767, 756, 718, 718, 697 702, 692, 702, 671, 681, 697, 681, 655 630, 702, 625, 605, 600, 620, 605, 590 610, 571, 562, 600, 600, 610, 571, 586 595, 586, 543, 562, 534, 615, 543, 543 538, 548, 524, 520, 538, 529, 502, 502 488, 534, 548, 515, 488, 506, 502, 502 467, 493, 484, 441, 480, 502, 467, 454 488, 484, 433, 458, 475, 484, 428, 484 462, 445, 437, 462, 462, 433, 441, 441 428, 437, 424, 471, 408, 424, 408, 433 416, 412, 416, 428, 416, 449, 412, 424 408, 396, 408, 416, 376, 361, 428, 372 380, 437, 392, 380, 376, 404, 388, 384 388, 384, 365, 420, 376, 372, 357, 380 369, 357, 372, 346, 346, 357, 369, 357 339, 376, 357, 339, 380, 339, 361, 335 388, 380, 335, 361, 392, 350, 339, 342 335, 339, 292, 328, 328, 320, 313, 331 331, 339, 313, 310, 266, 384, 339, 328 313, 320, 346, 335, 324, 310, 346, 317 320, 313, 313, 310, 317, 303, 342, 365 342, 282, 342, 306, 320, 324, 346, 342 317, 269, 324, 299, 320, 306, 320, 331 346, 324, 310, 313, 320, 328, 292, 317 303, 331, 317, 286, 353, 292, 306, 328 279, 339, 269, 324, 299, 313, 272, 303 292, 276, 299, 299, 328, 328, 299, 310 279, 299, 296, 282, 328, 313, 296, 299 286, 289, 310, 292, 292, 310, 289, 310 276, 339, 282, 328, 331, 296, 335, 328 279, 286, 296, 335, 279, 299, 317, 324 310, 262, 303, 296, 317, 266, 296, 335 328, 292, 286, 299, 306, 313, 317, 310 292, 328, 296, 331, 313, 306, 259, 276 289, 266, 306, 299, 259, 266, 289, 292 272, 286, 313, 299, 269, 276, 269, 320 266, 279, 262, 282, 276, 276, 262, 266 292, 292, 269, 279, 243, 269, 269, 253 266, 262, 279, 269, 279, 269, 276, 259 262, 276, 256, 259, 276, 266, 262, 253 286, 269, 246, 243, 250, 346, 256, 262 253, 259, 262, 246, 262, 276, 250, 262 266, 262, 282, 259, 259, 279, 243, 296 262, 266, 269, 256, 250, 266, 250, 262 289, 259, 256, 276, 282, 272, 299, 256 256, 240, 253, 259, 272, 282, 303, 269 262, 262, 269, 262, 246, 272, 272, 272 250, 272, 234, 259, 269, 276, 276, 272 266, 276, 289, 269, 256, 253, 262, 259 259, 246, 276, 246, 286, 253, 237, 269 250, 276, 243, 228, 250, 272, 228, 256 250, 269, 262, 303, 231, 256, 240, 228 250, 292, 240, 253, 250, 259, 259, 216 234, 250, 276, 250, 259, 276, 253, 250 237, 237, 253, 222, 243, 237, 266, 246 246, 250, 225, 237, 237, 269, 243, 240 231, 210, 253, 234, 228, 240, 219, 234 246, 216, 228, 237, 225, 250, 240, 250 225, 231, 269, 246, 237, 237, 234, 246 246, 222, 228, 225, 243, 256, 213, 228 202, 213, 231, 231, 240, 243, 250, 234 237, 202, 234, 240, 253, 204, 259, 225 234, 243, 237, 234, 237, 240, 219, 231 237, 243, 234, 231, 246, 225, 250, 222 253, 231, 216, 219, 210, 234, 246, 231 246, 253, 213, 225, 243, 240, 237, 240 234, 225, 256, 219, 216, 250, 231, 234 237, 246, 219, 231, 237, 213, 202, 231 240, 207, 216, 228, 216, 231, 237, 246 237, 253, 234, 213, 259, 204, 207, 213 225, 213, 234, 216, 207, 234, 225, 228 250, 216, 207, 210, 231, 196, 246, 199 213, 213, 185, 216, 213, 213, 185, 213 193, 216, 213, 225, 210, 219, 216, 222 188, 231, 243, 216, 225, 216, 216, 202 216, 193, 199, 190, 210, 202, 237, 225 231, 225, 216, 182, 193, 180, 210, 199 237, 185, 193, 213, 182, 188, 199, 190 193, 219, 216, 202, 202, 199, 202, 196 190, 204, 188, 199, 216, 182, 204, 213 207, 199, 199, 213, 213, 188, 193, 202 188, 219, 199, 190, 193, 185, 190, 213 190, 202, 185, 188, 213, 222, 216, 216 216, 196, 202, 193, 199, 202, 202, 174 199, 185, 225, 188, 199, 199, 161, 204 202, 216, 177, 207, 185, 182, 210, 199 216, 213, 199, 199, 207, 188, 169, 193 188, 193, 204, 213, 199, 193, 193, 213 193, 199, 234,/