SampleIdent,897C 65R1 41-43,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,13-apr-1993 14:33,/ DataAngleRange, 2.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 90, 79, 92, 85, 64, 74, 62, 74 72, 62, 69, 72, 74, 83, 85, 76 61, 62, 72, 71, 71, 86, 66, 69 72, 69, 76, 69, 58, 72, 67, 58 71, 76, 66, 50, 62, 71, 66, 67 85, 85, 53, 72, 74, 53, 79, 56 83, 81, 85, 79, 83, 64, 77, 62 76, 81, 55, 66, 62, 72, 88, 66 67, 58, 88, 81, 62, 76, 52, 67 76, 67, 79, 62, 74, 77, 86, 72 86, 81, 58, 86, 94, 90, 71, 94 72, 71, 81, 72, 59, 71, 76, 72 85, 86, 86, 76, 77, 67, 74, 85 72, 86, 79, 85, 71, 76, 67, 85 85, 71, 90, 86, 76, 72, 88, 77 83, 88, 85, 53, 85, 90, 77, 90 62, 62, 86, 96, 88, 74, 81, 90 96, 96, 86, 112, 85, 86, 92, 90 88, 85, 83, 86, 117, 94, 88, 86 88, 88, 94, 98, 117, 110, 110, 102 100, 98, 104, 114, 96, 83, 92, 98 130, 102, 104, 100, 98, 119, 102, 110 125, 100, 119, 106, 100, 102, 123, 100 98, 106, 121, 96, 106, 119, 119, 114 108, 117, 94, 108, 123, 142, 117, 104 106, 117, 117, 144, 114, 137, 110, 125 130, 125, 92, 137, 149, 128, 146, 123 117, 128, 125, 119, 132, 119, 139, 132 144, 166, 130, 128, 139, 110, 144, 135 135, 151, 135, 154, 142, 159, 149, 121 130, 125, 137, 123, 137, 137, 161, 123 139, 132, 142, 132, 139, 146, 135, 130 156, 149, 135, 121, 123, 125, 137, 130 149, 125, 123, 142, 128, 123, 154, 125 112, 144, 139, 128, 117, 137, 112, 142 132, 102, 123, 121, 125, 125, 128, 139 110, 110, 149, 108, 121, 123, 121, 114 114, 108, 119, 125, 121, 98, 96, 125 121, 112, 128, 137, 112, 117, 121, 110 119, 117, 117, 102, 121, 123, 146, 114 114, 112, 110, 121, 106, 104, 108, 104 114, 117, 135, 110, 117, 110, 108, 132 125, 114, 100, 112, 108, 108, 100, 106 110, 104, 102, 106, 104, 98, 102, 110 106, 106, 90, 106, 96, 108, 119, 96 104, 102, 108, 102, 121, 114, 125, 98 108, 108, 90, 114, 106, 94, 125, 119 92, 90, 112, 94, 123, 100, 102, 119 106, 90, 106, 96, 90, 90, 79, 96 88, 92, 96, 86, 114, 106, 102, 96 110, 104, 102, 86, 94, 117, 110, 114 119, 98, 98, 98, 85, 92, 117, 96 100, 114, 106, 76, 100, 98, 114, 104 104, 108, 108, 114, 106, 98, 104, 100 104, 98, 96, 106, 102, 85, 130, 108 96, 102, 96, 86, 112, 108, 110, 119 106, 121, 108, 96, 98, 104, 125, 125 121, 100, 104, 123, 117, 121, 135, 114 117, 130, 137, 144, 142, 159, 144, 169 166, 174, 180, 190, 196, 216, 234, 243 259, 289, 286, 286, 296, 335, 320, 303 384, 396, 376, 437, 480, 497, 506, 506 586, 630, 630, 610, 650, 660, 660, 692 686, 576, 595, 548, 562, 520, 424, 424 365, 276, 276, 250, 182, 188, 166, 169 144, 149, 137, 121, 121, 114, 130, 108 96, 100, 112, 114, 114, 102, 112, 102 96, 83, 94, 96, 90, 86, 102, 88 106, 86, 86, 94, 90, 71, 92, 79 96, 92, 96, 85, 77, 86, 92, 100 106, 100, 90, 85, 110, 90, 90, 98 92, 79, 85, 110, 79, 79, 85, 96 88, 88, 76, 92, 86, 86, 81, 85 98, 83, 94, 77, 67, 79, 94, 77 79, 90, 92, 79, 102, 76, 86, 88 90, 86, 86, 79, 102, 83, 86, 79 85, 85, 96, 76, 108, 86, 56, 79 86, 96, 104, 86, 86, 72, 90, 79 86, 76, 92, 88, 92, 88, 79, 79 92, 83, 72, 79, 74, 76, 92, 88 86, 86, 86, 71, 71, 86, 88, 72 77, 76, 88, 94, 74, 88, 76, 88 90, 81, 83, 76, 79, 90, 83, 74 77, 90, 90, 86, 79, 79, 94, 86 77, 72, 86, 79, 71, 83, 79, 67 67, 83, 76, 67, 81, 85, 88, 83 85, 83, 83, 79, 92, 79, 79, 59 79, 77, 76, 102, 86, 98, 77, 77 77, 92, 83, 92, 83, 98, 79, 79 71, 69, 72, 71, 71, 72, 79, 67 67, 69, 66, 72, 67, 83, 66, 86 83, 77, 77, 76, 71, 79, 86, 62 100, 77, 76, 83, 88, 72, 90, 83 76, 81, 77, 69, 86, 79, 85, 104 61, 67, 76, 79, 83, 86, 62, 98 85, 88, 83, 77, 77, 66, 85, 79 72, 81, 71, 69, 313, 67, 81, 90 56, 71, 83, 71, 106, 83, 67, 72 79, 76, 53, 83, 90, 90, 62, 71 72, 90, 76, 83, 83, 72, 90, 71 66, 72, 67, 77, 83, 79, 85, 72 86, 83, 77, 79, 79, 67, 85, 83 88, 71, 85, 92, 77, 85, 81, 79 79, 85, 100, 88, 86, 92, 94, 85 96, 67, 96, 106, 83, 90, 102, 79 85, 110, 85, 106, 94, 106, 112, 110 110, 128, 144, 166, 166, 188, 174, 207 222, 234, 292, 296, 292, 289, 317, 365 296, 339, 376, 350, 328, 342, 346, 328 346, 328, 320, 240, 303, 296, 306, 272 276, 272, 259, 279, 266, 259, 253, 240 213, 259, 219, 222, 216, 213, 202, 225 207, 225, 234, 177, 182, 225, 196, 190 180, 213, 216, 199, 213, 199, 182, 216 182, 166, 188, 185, 190, 185, 188, 164 174, 172, 174, 188, 188, 180, 146, 161 182, 182, 169, 182, 149, 174, 172, 182 172, 182, 182, 174, 164, 149, 177, 185 182, 188, 177, 154, 193, 164, 169, 172 161, 151, 154, 149, 166, 180, 154, 164 130, 154, 132, 169, 156, 146, 142, 144 139, 132, 154, 174, 154, 144, 139, 123 149, 135, 142, 139, 159, 142, 144, 146 151, 156, 135, 130, 161, 144, 137, 139 149, 174, 144, 144, 123, 130, 128, 142 149, 137, 119, 135, 149, 137, 132, 135 151, 139, 135, 144, 104, 151, 128, 128 146, 146, 135, 146, 137, 146, 146, 144 135, 135, 154, 125, 164, 169, 174, 154 177, 156, 174, 180, 182, 154, 156, 159 154, 188, 159, 166, 174, 164, 180, 177 193, 174, 151, 156, 166, 159, 166, 159 172, 161, 166, 182, 174, 185, 169, 142 166, 164, 172, 164, 149, 185, 169, 182 210, 185, 219, 164, 190, 207, 199, 188 210, 237, 219, 497, 237, 250, 216, 231 246, 237, 259, 282, 310, 272, 292, 324 296, 324, 324, 335, 339, 339, 369, 361 376, 400, 471, 484, 462, 502, 524, 534 566, 562, 581, 660, 635, 681, 740, 724 697, 692, 740, 697, 734, 724, 702, 635 600, 548, 566, 511, 420, 388, 365, 313 296, 279, 266, 253, 222, 219, 204, 199 196, 182, 207, 174, 193, 180, 146, 159 164, 164, 146, 146, 144, 164, 159, 144 146, 137, 144, 135, 146, 156, 164, 151 142, 117, 142, 146, 125, 139, 121, 119 114, 137, 117, 123, 112, 119, 121, 112 106, 119, 121, 114, 121, 137, 108, 119 114, 100, 94, 123, 106, 108, 94, 108 128, 121, 123, 128, 96, 135, 106, 121 100, 119, 106, 117, 112, 114, 114, 108 110, 114, 98, 128, 119, 104, 119, 90 137, 128, 102, 114, 108, 100, 119, 121 128, 108, 102, 110, 125, 123, 117, 110 119, 112, 114, 123, 114, 94, 112, 121 110, 104, 104, 112, 121, 112, 86, 112 114, 121, 125, 119, 104, 96, 130, 119 110, 104, 102, 102, 110, 117, 104, 114 114, 123, 114, 106, 123, 114, 96, 100 90, 121, 123, 92, 106, 108, 112, 125 123, 106, 104, 110, 94, 110, 114, 128 125, 119, 128, 135, 119, 135, 125, 125 132, 123, 119, 132, 119, 135, 132, 144 135, 121, 119, 121, 137, 139, 149, 132 142, 130, 139, 110, 114, 135, 114, 114 125, 135, 119, 114, 102, 123, 108, 128 104, 119, 106, 110, 108, 121, 130, 121 104, 110, 96, 94, 106, 110, 110, 110 121, 108, 119, 114, 146, 117, 117, 125 114, 146, 144, 139, 144, 177, 185, 210 276, 380, 566, 645, 620, 620, 600, 590 548, 380, 282, 282, 204, 169, 130, 142 119, 121, 121, 117, 104, 96, 104, 100 106, 98, 102, 94, 96, 96, 108, 100 88, 92, 88, 100, 96, 98, 92, 104 92, 92, 94, 102, 94, 85, 98, 108 104, 76, 92, 76, 94, 92, 76, 81 98, 74, 72, 88, 100, 94, 102, 119 88, 102, 79, 85, 76, 98, 66, 90 85, 98, 79, 110, 86, 94, 96, 112 83, 88, 108, 83, 96, 76, 102, 92 86, 92, 108, 88, 100, 114, 86, 110 114, 104, 92, 102, 112, 96, 98, 104 94, 108, 102, 110, 92, 123, 83, 110 102, 92, 90, 102, 92, 96, 98, 106 88, 85, 108, 76, 98, 76, 96, 86 88, 88, 98, 77, 86, 86, 88, 96 85, 62, 69, 110, 88, 83, 85, 77 90, 79, 85, 98, 83, 71, 90, 88 77, 88, 83, 90, 76, 77, 79, 92 76, 79, 86, 88, 83, 76, 85, 81 72, 96, 77, 85, 79, 79, 81, 100 85, 94, 100, 83, 88, 77, 96, 81 76, 81, 90, 83, 83, 86, 83, 76 83, 96, 90, 102, 106, 98, 94, 100 96, 102, 130, 110, 121, 128, 130, 144 137, 132, 156, 185, 188, 164, 169, 199 222, 219, 222, 210, 204, 246, 213, 231 225, 272, 246, 228, 259, 253, 237, 250 240, 243, 256, 292, 262, 250, 272, 276 286, 310, 289, 269, 269, 313, 289, 272 240, 279, 231, 279, 237, 256, 246, 253 296, 237, 253, 256, 272, 272, 269, 243 286, 269, 289, 269, 279, 256, 246, 296 282, 282, 289, 286, 310, 324, 320, 272 279, 296, 310, 296, 313, 306, 310, 324 313, 328, 350, 328, 335, 317, 350, 331 372, 372, 335, 328, 350, 331, 353, 365 380, 388, 396, 404, 424, 420, 392, 420 449, 467, 488, 529, 548, 534, 605, 605 666, 729, 767, 778, 824, 824, 807, 847 847, 835, 841, 756, 745, 773, 773, 692 660, 640, 666, 610, 600, 576, 590, 610 605, 562, 562, 557, 571, 605, 605, 581 620, 600, 586, 610, 625, 605, 620, 615 620, 630, 581, 615, 552, 581, 538, 520 515, 538, 524, 515, 480, 488, 458, 408 412, 441, 445, 400, 420, 369, 353, 353 408, 361, 342, 328, 324, 317, 331, 342 306, 320, 324, 299, 313, 320, 276, 262 279, 262, 272, 266, 256, 276, 231, 262 246, 240, 266, 243, 240, 250, 234, 225 240, 237, 204, 222, 199, 202, 210, 213 213, 204, 202, 196, 185, 196, 193, 182 202, 185, 213, 182, 199, 177, 190, 156 199, 174, 196, 196, 196, 222, 213, 199 210, 199, 234, 253, 210, 240, 207, 243 240, 228, 222, 246, 250, 237, 219, 256 222, 228, 222, 228, 190, 190, 216, 196 204, 188, 188, 185, 185, 182, 172, 193 172, 159, 204, 182, 166, 169, 177, 202 188, 151, 193, 228, 202, 190, 210, 199 213, 262, 193, 225, 246, 240, 299, 262 266, 253, 240, 216, 246, 213, 228, 177 190, 185, 193, 188, 182, 177, 172, 182 177, 169, 164, 182, 164, 164, 169, 177 159, 174, 169, 182, 151, 151, 174, 164 164, 177, 182, 172, 169, 130, 174, 180 164, 172, 135, 166, 146, 156, 185, 174 177, 149, 146, 130, 144, 161, 159, 146 169, 159, 161, 166, 151, 177, 149, 154 174, 159, 159, 164, 193, 159, 185, 190 164, 156, 149, 177, 159, 180, 164, 169 156, 190, 185, 172, 180, 182, 182, 174 149, 193, 172, 169, 174, 185, 164, 172 185, 177, 182, 174, 177, 207, 159, 190 182, 202, 272, 196, 202, 185, 216, 199 219, 216, 246, 216, 216, 219, 199, 228 240, 234, 262, 243, 286, 266, 286, 253 303, 276, 317, 286, 299, 276, 306, 306 262, 282, 286, 246, 272, 269, 259, 253 219, 234, 237, 253, 228, 207, 202, 225 219, 207, 204, 240, 222, 188, 219, 199 213, 237, 202, 222, 259, 219, 204, 202 213, 234, 204, 243, 222, 216, 243, 240 222, 246, 246, 243, 259, 213, 246, 269 259, 253, 246, 266, 222, 246, 222, 228 237, 188, 219, 207, 207, 207, 222, 196 213, 222, 182, 199, 182, 164, 174, 177 154, 193, 177, 159, 185, 144, 199, 161 177, 180, 177, 193, 177, 182, 190, 174 177, 166, 174, 182, 164, 172, 159, 144 149, 132, 121, 119, 121, 151, 142, 135 117, 146, 154, 161, 142, 154, 151, 169 185, 177, 219, 213, 202, 240, 253, 231 188, 177, 177, 182, 190, 159, 154, 130 132, 132, 130, 114, 142, 121, 123, 121 137, 132, 104, 137, 104, 121, 132, 130 112, 114, 132, 114, 104, 108, 110, 112 112, 102, 132, 123, 130, 123, 112, 130 121, 117, 125, 121, 108, 125, 130, 121 130, 123, 130, 130, 121, 102, 128, 130 119, 125, 119, 121, 144, 121, 135, 132 142, 119, 144, 132, 123, 149, 135, 144 169, 156, 149, 169, 188, 164, 182, 169 156, 166, 185, 188, 172, 210, 196, 207 188, 196, 190, 164, 182, 169, 172, 180 159, 149, 154, 174, 149, 130, 135, 144 144, 132, 132, 154, 110, 121, 119, 112 114, 110, 100, 117, 125, 108, 104, 106 112, 98, 123, 102, 110, 90, 130, 121 104, 102, 112, 123, 98, 108, 149, 108 121, 125, 117, 108, 106, 108, 112, 125 137, 144, 154, 137, 142, 135, 149, 169 154, 144, 159, 164, 137, 159, 144, 130 117, 119, 119, 135, 121, 98, 110, 123 121, 88, 94, 121, 98, 117, 112, 110 104, 94, 106, 102, 119, 104, 90, 92 110, 94, 114, 104, 119, 130, 123, 135 154, 169, 174, 177, 164, 193, 164, 185 190, 182, 180, 166, 149, 172, 149, 149 135, 114, 123, 104, 123, 121, 100, 108 135, 112, 85, 123, 106, 104, 102, 117 96, 121, 92, 100, 108, 117, 117, 142 110, 114, 123, 123, 100, 128, 121, 130 98, 106, 137, 110, 112, 104, 121, 121 142, 139, 121, 121, 117, 110, 110, 121 121, 117, 117, 119, 130, 135, 135, 139 128, 132, 149, 139, 142, 119, 128, 137 146, 130, 146, 142, 130, 114, 144, 154 144, 139, 151, 169, 169, 166, 142, 142 130, 154, 144, 139, 149, 114, 132, 135 142, 137, 156, 139, 144, 135, 154, 154 128, 174, 166, 151, 144, 159, 182, 151 164, 161, 164, 188, 172, 180, 177, 202 188, 185, 202, 193, 196, 182, 185, 199 216, 172, 196, 159, 188, 166, 180, 177 161, 169, 204, 193, 159, 172, 154, 164 149, 177, 159, 149, 146, 164, 156, 177 169, 149, 149, 151, 139, 156, 161, 174 154, 159, 159, 159, 142, 159, 172, 193 174, 166, 169, 159, 156, 161, 151, 185 193, 213, 172, 196, 169, 190, 169, 196 204, 202, 213, 228, 202, 199, 225, 243 240, 219, 266, 216, 231, 266, 262, 246 266, 240, 276, 246, 246, 240, 259, 256 234, 269, 250, 240, 240, 237, 219, 231 243, 243, 234, 193, 210, 213, 225, 222 196, 199, 256, 213, 174, 207, 190, 185 182, 156, 164, 172, 166, 188, 166, 174 180, 188, 185, 180, 169, 166, 174, 185 177, 188, 177, 182, 149, 177, 169, 182 149, 164, 149, 159, 174, 174, 161, 164 149, 149, 146, 166, 161, 185, 169, 159 149, 164, 151, 174, 188, 166, 146, 144 146, 156, 159, 146, 144, 135, 159, 149 151, 156, 125, 149, 139, 139, 132, 135 142, 154, 137, 123, 139, 146, 132, 132 137, 144, 154, 137, 130, 121, 135, 164 137, 159, 137, 137, 154, 144, 135, 130 144, 121, 130, 137, 144, 128, 137, 130 117, 142, 135, 144, 137, 121, 149, 125 110, 142, 146, 130, 125, 132, 125, 117 132, 128, 139, 142, 119, 121, 139, 112 130, 132, 135, 144, 121, 130, 119, 144 144, 123, 125, 130, 137, 151, 125, 144 128, 135, 123, 146, 137, 149, 151, 164 166, 137, 161, 169, 177, 169, 172, 180 180, 156, 137, 166, 146, 161, 154, 177 182, 172, 172, 161, 151, 151, 164, 169 149, 149, 182, 159, 164, 144, 154, 154 130, 151, 125, 144, 146, 130, 142, 142 130, 123, 128, 135, 130, 112, 137, 123 123, 121, 106, 114, 98, 137, 102, 130 117, 123, 112, 121, 132, 114, 128, 119 137, 139, 142, 121, 117, 144, 130, 125 137, 144, 142, 139, 130, 132, 130, 142 137, 112, 135, 130, 119, 132, 121, 130 130, 121, 137, 123, 135, 130, 146, 151 151, 132, 130, 123, 156, 132, 146, 128 139, 130, 125, 121, 146, 154, 154, 159 135, 149, 119, 123, 137, 146, 114, 151 110, 139, 135, 123, 142, 139, 132, 142 125, 146, 144, 139, 154, 135, 156, 161 149, 142, 130, 142, 156, 146, 172, 132 149, 151, 169, 164, 139, 156, 154, 154 151, 161, 166, 169, 199, 164, 166, 149 210, 174, 190, 207, 222, 193, 216, 182 202, 207, 246, 216, 202, 243, 228, 246 237, 286, 279, 286, 320, 328, 328, 320 346, 365, 412, 433, 458, 462, 515, 506 615, 615, 640, 724, 686, 713, 847, 835 912, 888, 980, 1005, 992, 980, 1011, 992 973, 942, 888, 847, 801, 818, 818, 824 751, 718, 724, 645, 666, 595, 571, 538 534, 515, 467, 511, 515, 433, 497, 467 433, 420, 392, 376, 404, 404, 353, 350 331, 369, 384, 335, 357, 313, 313, 328 353, 335, 303, 331, 328, 331, 324, 317 342, 310, 310, 376, 384, 339, 339, 396 384, 376, 376, 408, 428, 400, 404, 400 449, 412, 458, 471, 433, 445, 449, 404 433, 408, 400, 372, 420, 408, 396, 433 384, 350, 372, 339, 365, 303, 292, 286 289, 292, 259, 225, 246, 231, 231, 219 219, 243, 196, 210, 193, 202, 199, 185 193, 174, 193, 172, 185, 185, 164, 156 182, 156, 159, 164, 137, 159, 154, 159 125, 154, 137, 156, 149, 144, 151, 159 144, 159, 142, 137, 139, 154, 149, 121 112, 159, 139, 130, 154, 154, 132, 154 159, 146, 159, 154, 161, 177, 199, 182 174, 174, 161, 154, 174, 151, 156, 137 185, 151, 154, 135, 132, 132, 154, 142 149, 135, 135, 151, 139, 112, 154, 149 137, 159, 144, 123, 146, 144, 142, 146 123, 137, 144, 142, 125, 137, 135, 130 159, 106, 154, 121, 125, 128, 117, 137 135, 146, 146, 123, 128, 130, 110, 128 128, 146, 100, 125, 132, 110, 142, 130 142, 139, 119, 121, 125, 117, 128, 132 146, 137, 149, 137, 164, 121, 130, 137 123, 139, 144, 108, 128, 154, 128, 110 149, 135, 125, 128, 119, 149, 135, 100 130, 117, 104, 132, 123, 130, 128, 121 146, 146, 139, 119, 128, 139, 123, 128 119, 182, 144, 161, 142, 130, 159, 159 166, 164, 185, 180, 180, 182, 177, 180 199, 174, 169, 182, 207, 185, 188, 177 185, 180, 182, 164, 159, 182, 177, 177 169, 156, 159, 159, 159, 166, 125, 135 135, 151, 125, 125, 130, 123, 149, 117 130, 123, 125, 114, 121, 130, 121, 137 132, 110, 106, 92, 117, 125, 130, 130 137, 108, 108, 117, 112, 121, 119, 110 102, 117, 110, 102, 98, 110, 102, 135 112, 114, 119, 108, 90, 117, 106, 98 106, 108, 121, 98, 121, 110, 114, 96 92, 106, 114, 117, 102, 110, 114, 90 114, 114, 125, 125, 102, 125, 108, 102 106, 100, 132, 92, 110, 130, 106, 125 121, 130, 106, 146, 110, 104, 119, 119 119, 110, 130, 117, 121, 139, 106, 128 117, 117, 100, 123, 121, 98, 121, 94 114, 104, 104, 110, 92, 108, 108, 94 112, 102, 114, 98, 108, 100, 130, 108 112, 88, 108, 92, 92, 108, 108, 90 81, 94, 96, 94, 106, 119, 96, 98 104, 96, 114, 106, 108, 117, 98, 100 128, 102, 112, 110, 102, 121, 119, 114 110, 108, 112, 108, 112, 96, 119, 106 110, 114, 117, 108, 112, 100, 114, 110 112, 106, 106, 108, 130, 112, 98, 146 114, 125, 144, 110, 117, 123, 121,/