SampleIdent,907A-1-2/18,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 8-aug-1993 12:52,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 119, 90, 102, 100, 88, 98, 102, 102 85, 96, 94, 119, 98, 114, 121, 96 100, 94, 98, 83, 100, 100, 96, 94 90, 96, 96, 98, 85, 94, 79, 96 94, 117, 96, 100, 96, 94, 102, 117 102, 106, 100, 114, 112, 121, 104, 102 104, 114, 119, 123, 94, 117, 112, 96 102, 108, 108, 100, 112, 114, 117, 125 119, 117, 121, 96, 108, 106, 114, 108 110, 137, 130, 106, 104, 106, 125, 121 117, 128, 106, 130, 130, 117, 117, 123 102, 121, 146, 123, 123, 121, 130, 106 128, 112, 121, 121, 112, 119, 102, 121 130, 108, 117, 119, 123, 119, 117, 121 102, 123, 106, 102, 137, 108, 110, 121 121, 128, 121, 88, 130, 123, 130, 125 119, 110, 108, 114, 121, 108, 110, 102 121, 128, 128, 98, 121, 117, 106, 128 121, 110, 108, 112, 119, 112, 125, 128 119, 121, 119, 154, 128, 112, 119, 144 123, 108, 108, 112, 119, 117, 112, 110 121, 125, 108, 112, 117, 114, 121, 128 130, 98, 123, 149, 121, 137, 121, 114 130, 146, 142, 135, 139, 144, 161, 144 146, 135, 132, 119, 128, 121, 100, 137 117, 117, 114, 106, 117, 98, 100, 98 106, 135, 100, 108, 104, 100, 108, 102 121, 119, 114, 96, 112, 104, 92, 90 90, 100, 106, 104, 86, 92, 90, 96 98, 110, 94, 83, 106, 92, 72, 106 88, 114, 317, 90, 85, 104, 102, 90 96, 94, 98, 108, 85, 90, 92, 98 92, 92, 94, 71, 77, 90, 92, 83 96, 79, 85, 104, 77, 88, 86, 71 85, 92, 86, 92, 92, 81, 108, 86 100, 88, 67, 83, 81, 96, 94, 108 83, 100, 86, 72, 98, 74, 85, 94 86, 94, 85, 100, 88, 90, 88, 77 94, 104, 79, 83, 83, 72, 66, 94 79, 85, 90, 77, 108, 94, 92, 100 67, 59, 92, 79, 88, 81, 104, 77 94, 96, 88, 98, 79, 94, 96, 96 90, 90, 79, 88, 98, 96, 88, 106 86, 98, 96, 83, 92, 100, 88, 96 94, 98, 102, 90, 92, 96, 102, 104 102, 98, 104, 85, 108, 114, 108, 117 119, 132, 128, 119, 132, 114, 125, 149 137, 130, 128, 104, 102, 104, 110, 67 85, 94, 79, 94, 92, 79, 90, 88 94, 88, 83, 85, 83, 83, 85, 94 86, 86, 92, 253, 66, 76, 90, 76 71, 77, 81, 90, 74, 83, 100, 86 81, 110, 83, 88, 72, 79, 90, 77 86, 69, 83, 90, 81, 83, 98, 86 79, 100, 67, 88, 79, 94, 106, 100 96, 94, 98, 86, 94, 90, 88, 76 83, 77, 96, 76, 86, 86, 88, 88 83, 88, 86, 83, 90, 76, 76, 88 88, 69, 88, 83, 85, 79, 79, 77 74, 76, 67, 77, 83, 88, 77, 77 98, 81, 86, 72, 88, 94, 83, 76 69, 85, 88, 102, 79, 76, 76, 76 76, 71, 76, 90, 86, 72, 90, 79 76, 66, 83, 79, 81, 85, 88, 72 76, 86, 96, 88, 79, 71, 85, 86 79, 72, 72, 83, 81, 86, 74, 76 72, 77, 85, 69, 76, 61, 83, 81 64, 71, 71, 62, 92, 77, 86, 266 77, 86, 85, 86, 56, 64, 64, 72 59, 71, 67, 83, 67, 71, 77, 74 86, 77, 88, 61, 72, 85, 71, 67 71, 64, 69, 76, 76, 79, 72, 71 83, 62, 72, 66, 92, 79, 71, 76 55, 71, 59, 66, 72, 62, 86, 62 77, 67, 67, 76, 83, 67, 72, 90 69, 59, 100, 71, 88, 79, 79, 71 76, 76, 62, 79, 69, 83, 71, 79 67, 74, 66, 67, 76, 86, 88, 76 81, 85, 67, 81, 67, 96, 90, 90 76, 77, 79, 100, 86, 96, 108, 94 108, 102, 102, 104, 110, 100, 106, 94 83, 83, 85, 98, 76, 81, 71, 72 85, 74, 88, 67, 90, 71, 72, 71 83, 79, 102, 86, 76, 72, 81, 74 72, 88, 64, 81, 83, 96, 83, 90 94, 92, 88, 90, 76, 77, 86, 92 90, 86, 102, 104, 90, 100, 86, 86 110, 72, 85, 86, 72, 85, 86, 76 83, 83, 85, 79, 92, 92, 83, 92 74, 100, 92, 92, 100, 94, 96, 102 90, 117, 121, 110, 112, 110, 117, 146 139, 110, 130, 128, 156, 156, 159, 156 196, 193, 159, 172, 172, 202, 188, 177 161, 172, 164, 188, 156, 174, 159, 139 135, 123, 114, 132, 100, 144, 110, 112 98, 117, 137, 137, 128, 117, 114, 114 96, 139, 119, 108, 125, 139, 119, 108 92, 121, 123, 125, 149, 114, 119, 154 149, 182, 185, 199, 237, 246, 259, 299 282, 306, 310, 339, 331, 289, 289, 279 250, 154, 149, 139, 146, 135, 106, 102 125, 110, 119, 121, 108, 86, 106, 114 108, 108, 85, 98, 114, 83, 98, 100 96, 125, 98, 121, 100, 100, 102, 114 112, 83, 90, 96, 106, 104, 108, 96 90, 96, 104, 119, 100, 125, 117, 137 149, 132, 149, 151, 156, 161, 159, 151 149, 166, 130, 149, 130, 117, 114, 108 108, 96, 108, 92, 90, 92, 117, 90 83, 79, 77, 79, 96, 119, 96, 102 102, 94, 83, 85, 90, 98, 106, 102 104, 96, 104, 104, 100, 104, 132, 112 130, 130, 123, 112, 125, 135, 130, 146 137, 130, 125, 108, 121, 102, 108, 102 104, 114, 108, 92, 94, 128, 104, 104 108, 100, 108, 144, 135, 130, 144, 161 146, 156, 161, 137, 159, 161, 177, 188 204, 185, 164, 142, 130, 135, 121, 144 139, 130, 137, 123, 121, 110, 121, 117 114, 114, 121, 139, 125, 154, 137, 139 172, 159, 146, 185, 142, 166, 166, 144 144, 151, 130, 156, 137, 121, 210, 135 119, 121, 110, 117, 110, 110, 119, 112 104, 96, 112, 112, 102, 128, 117, 123 110, 144, 121, 128, 125, 119, 130, 117 123, 144, 142, 139, 121, 149, 149, 156 151, 161, 159, 166, 196, 154, 174, 172 156, 177, 146, 144, 172, 169, 142, 166 146, 154, 161, 149, 142, 177, 144, 154 151, 164, 137, 151, 137, 137, 142, 146 130, 110, 121, 112, 104, 117, 123, 142 110, 144, 119, 121, 125, 110, 128, 159 128, 139, 121, 146, 137, 154, 144, 174 159, 166, 172, 188, 177, 219, 202, 234 262, 339, 404, 502, 718, 853, 1183, 1204 1246, 1369, 1429, 1436, 1568, 1592, 1592, 1436 1318, 1056, 835, 620, 454, 400, 313, 276 272, 246, 222, 225, 202, 199, 219, 166 164, 193, 185, 166, 177, 154, 182, 204 146, 164, 156, 185, 177, 182, 182, 185 190, 231, 210, 266, 228, 250, 279, 279 276, 234, 269, 269, 276, 276, 269, 272 313, 296, 357, 365, 437, 428, 388, 445 493, 515, 428, 458, 458, 412, 328, 317 313, 306, 279, 282, 246, 231, 177, 204 202, 159, 166, 180, 182, 246, 279, 289 234, 177, 222, 190, 159, 110, 128, 137 119, 110, 114, 404, 114, 108, 106, 104 132, 161, 146, 154, 142, 128, 128, 106 110, 92, 104, 112, 104, 106, 94, 100 100, 90, 110, 100, 142, 128, 108, 119 139, 135, 149, 180, 185, 240, 282, 342 361, 433, 524, 713, 666, 650, 645, 708 671, 576, 471, 454, 441, 346, 303, 266 240, 204, 199, 204, 180, 172, 166, 193 172, 182, 182, 177, 185, 216, 228, 172 213, 193, 169, 154, 161, 154, 128, 149 144, 130, 156, 146, 142, 151, 144, 137 154, 139, 151, 144, 156, 130, 164, 144 159, 154, 130, 154, 142, 151, 159, 156 137, 128, 164, 130, 144, 130, 154, 151 172, 164, 159, 177, 182, 182, 174, 190 180, 169, 174, 185, 156, 169, 182, 172 146, 142, 142, 130, 135, 128, 130, 123 149, 130, 119, 137, 106, 128, 144, 146 156, 151, 154, 130, 151, 151, 151, 144 135, 188, 188, 190, 204, 228, 222, 240 240, 225, 243, 234, 225, 199, 210, 177 174, 142, 137, 114, 121, 114, 104, 106 104, 108, 110, 94, 90, 81, 77, 104 104, 90, 106, 83, 90, 85, 85, 100 83, 94, 94, 79, 92, 98, 69, 88 72, 74, 85, 71, 94, 76, 88, 81 85, 86, 85, 88, 83, 76, 71, 71 77, 81, 79, 76, 72, 77, 92, 86 88, 100, 83, 98, 100, 88, 100, 98 104, 102, 119, 104, 92, 98, 85, 86 96, 90, 86, 85, 71, 88, 98, 69 74, 71, 94, 85, 94, 96, 92, 94 104, 96, 88, 90, 102, 108, 114, 79 83, 108, 102, 96, 102, 100, 100, 94 137, 92, 112, 114, 114, 117, 94, 98 114, 117, 117, 121, 112, 110, 139, 135 128, 144, 149, 149, 159, 144, 182, 144 149, 149, 149, 177, 172, 182, 154, 199 199, 193, 180, 182, 196, 204, 190, 207 213, 202, 204, 219, 202, 202, 222, 256 243, 210, 262, 253, 266, 262, 262, 262 240, 250, 279, 266, 250, 231, 228, 228 243, 204, 182, 185, 185, 172, 169, 172 180, 174, 142, 159, 154, 146, 166, 159 146, 149, 154, 159, 169, 174, 137, 172 159, 154, 161, 142, 149, 151, 196, 172 185, 164, 199, 199, 185, 169, 188, 190 177, 185, 193, 151, 159, 144, 149, 146 144, 146, 114, 135, 130, 149, 123, 121 123, 188, 177, 166, 190, 210, 240, 243 269, 269, 279, 289, 269, 286, 299, 279 222, 225, 228, 199, 177, 166, 154, 128 164, 146, 146, 130, 119, 137, 137, 154 130, 130, 130, 119, 149, 142, 119, 139 174, 172, 144, 146, 135, 108, 137, 149 132, 139, 137, 161, 128, 137, 146, 149 154, 154, 135, 159, 137, 156, 159, 161 164, 169, 172, 135, 151, 154, 149, 128 164, 159, 164, 159, 161, 132, 149, 151 154, 119, 123, 125, 102, 114, 112, 299 114, 85, 100, 94, 96, 88, 108, 100 112, 79, 112, 98, 108, 98, 98, 100 92, 121, 106, 114, 98, 72, 104, 96 104, 102, 106, 85, 110, 112, 114, 96 102, 98, 100, 96, 102, 92, 90, 90 98, 98, 86, 83, 85, 100, 86, 96 85, 98, 106, 100, 100, 85, 98, 106 121, 117, 159, 154, 164, 177, 222, 202 253, 253, 272, 296, 269, 299, 286, 269 276, 219, 237, 180, 146, 159, 151, 123 121, 94, 110, 86, 110, 90, 96, 106 108, 100, 81, 106, 98, 100, 110, 100 108, 88, 117, 102, 104, 106, 110, 135 135, 142, 139, 164, 139, 164, 139, 177 154, 132, 130, 137, 117, 117, 114, 121 108, 102, 81, 92, 86, 90, 100, 117 94, 110, 94, 81, 86, 112, 86, 114 114, 90, 104, 119, 85, 123, 121, 94 108, 114, 119, 119, 121, 108, 125, 128 125, 119, 123, 123, 117, 130, 110, 137 106, 110, 104, 112, 121, 112, 112, 96 94, 100, 94, 92, 83, 102, 83, 96 90, 104, 94, 94, 121, 125, 114, 102 108, 121, 108, 112, 98, 102, 106, 86 106, 106, 125, 119, 119, 110, 119, 90 119, 100, 125, 121, 117, 121, 117, 144 132, 144, 142, 132, 154, 193, 202, 216 237, 253, 250, 246, 250, 213, 216, 177 202, 169, 180, 154, 139, 114, 121, 125 102, 102, 121, 98, 119, 112, 119, 106 106, 96, 108, 128, 106, 104, 114, 110 125, 123, 149, 132, 156, 161, 177, 185 185, 193, 172, 156, 151, 132, 123, 121 121, 114, 128, 85, 85, 79, 102, 81 83, 90, 88, 92, 88, 83, 88, 98 83, 92, 66, 83, 98, 90, 94, 88 98, 114, 121, 90, 83, 114, 96, 112 83, 88, 117, 86, 104, 114, 77, 88 98, 81, 92, 79, 86, 83, 79, 83 90, 77, 98, 104, 106, 114, 130, 139 125, 149, 159, 156, 130, 144, 142, 159 137, 139, 130, 108, 112, 125, 110, 125 135, 123, 128, 121, 144, 112, 125, 125 125, 137, 128, 137, 139, 112, 149, 119 146, 128, 119, 137, 144, 142, 156, 151 172, 166, 204, 202, 219, 231, 246, 237 272, 262, 243, 250, 246, 243, 216, 190 228, 234, 222, 207, 174, 164, 199, 213 207, 216, 202, 228, 172, 185, 177, 182 149, 139, 144, 144, 125, 130, 108, 98 102, 104, 92, 94, 86, 98, 92, 88 96, 79, 92, 88, 79, 74, 72, 86 96, 83, 74, 71, 77, 76, 79, 71 86, 83, 86, 77, 86, 67, 72, 90 79, 90, 72, 74, 71, 79, 86, 79 72, 76, 90, 94, 94, 96, 94, 125 108, 135, 128, 112, 123, 132, 114, 114 110, 119, 106, 104, 128, 100, 142, 130 161, 177, 207, 207, 231, 234, 256, 269 269, 240, 250, 262, 222, 185, 164, 156 164, 128, 128, 110, 108, 98, 90, 90 83, 102, 86, 94, 104, 88, 96, 94 94, 104, 98, 102, 104, 94, 92, 102 106, 121, 98, 96, 112, 119, 110, 125 132, 151, 164, 159, 180, 207, 240, 213 219, 231, 219, 234, 185, 199, 177, 188 149, 156, 159, 139, 100, 106, 83, 100 96, 86, 86, 90, 83, 83, 71, 98 77, 76, 86, 74, 92, 94, 85, 85 86, 94, 104, 90, 98, 106, 81, 92 98, 96, 88, 98, 79, 94, 76, 88 98, 79, 92, 100, 83, 92, 94, 85 81, 104, 96, 92, 86, 76, 110, 112 112, 104, 100, 90, 125, 130, 119, 128 142, 146, 188, 180, 204, 234, 246, 269 317, 320, 372, 331, 376, 350, 335, 292 276, 225, 222, 228, 182, 182, 104, 139 132, 130, 121, 108, 110, 130, 121, 117 144, 142, 137, 123, 144, 137, 123, 130 119, 110, 110, 102, 106, 119, 104, 106 110, 98, 102, 104, 102, 104, 110, 110 119, 123, 106, 108, 104, 108, 112, 128 106, 112, 90, 81, 108, 102, 92, 92 112, 88, 71, 90, 90, 85, 81, 90 86, 72, 83, 88, 86, 67, 67, 67 67, 66, 72, 66, 62, 64, 72, 55 71, 72, 62, 66, 71, 81, 67, 61 58, 71, 66, 72, 66, 71, 92, 71 67, 77, 79, 81, 83, 96, 86, 79 86, 79, 92, 94, 106, 86, 86, 83 88, 106, 90, 86, 88, 100, 81, 86 88, 92, 100, 88, 85, 92, 83, 76 86, 74, 92, 96, 104, 96, 108, 100 98, 110, 102, 106, 104, 81, 88, 90 121, 96, 114, 92, 98, 94, 114, 96 100, 110, 92, 119, 102, 90, 98, 110 112, 102, 98, 100, 92, 104, 119, 108 102, 114, 102, 117, 110, 102, 110, 112 96, 114, 96, 98, 108, 114, 121, 108 106, 137, 114, 88, 102, 114, 110, 98 117, 117, 110, 86, 106, 88, 106, 114 102, 96, 112, 112, 119, 119, 119, 112 108, 108, 106, 112, 112, 108, 110, 102 125, 108, 123, 112, 123, 108, 123, 125 142, 130, 161, 151, 164, 182, 182, 169 159, 174, 219, 174, 193, 154, 161, 177 169, 169, 142, 149, 135, 149, 130, 132 149, 149, 137, 139, 164, 164, 161, 144 144, 142, 130, 146, 154, 142, 125, 130 123, 121, 151, 110, 123, 110, 117, 123 123, 102, 137, 128, 121, 110, 123, 132 121, 125, 117, 121, 121, 110, 100, 119 121, 119, 121, 137, 121, 102, 114, 125 108, 92, 123, 106, 119, 119, 104, 125 135, 142, 132, 132, 130, 164, 161, 156 151, 154, 174, 156, 142, 151, 164, 135 128, 142, 106, 117, 130, 104, 106, 108 106, 110, 90, 92, 108, 106, 92, 83 90, 98, 125, 92, 96, 98, 85, 110 88, 94, 98, 123, 79, 121, 108, 130 139, 135, 149, 139, 166, 161, 159, 144 149, 154, 135, 144, 121, 119, 137, 142 100, 142, 108, 112, 100, 94, 104, 77 106, 96, 102, 100, 112, 104, 96, 96 123, 92, 92, 117, 96, 104, 104, 108 110, 83, 110, 102, 92, 102, 106, 76 86, 102, 88, 83, 81, 102, 85, 90 86, 104, 92, 96, 76, 90, 106, 96 94, 79, 92, 85, 92, 110, 135, 100 119, 104, 110, 86, 121, 86, 98, 114 92, 100, 100, 104, 96, 86, 98, 90 98, 104, 94, 108, 86, 92, 119, 100 100, 88, 100, 121, 98, 112, 106, 88 102, 88, 121, 112, 112, 94, 106, 106 110, 128, 114, 100, 121, 114, 104, 112 142, 142, 146, 185, 159, 190, 216, 279 306, 353, 331, 317, 369, 335, 357, 369 380, 392, 372, 310, 253, 243, 243, 246 234, 213, 196, 169, 177, 144, 137, 132 130, 130, 132, 117, 132, 117, 130, 132 125, 130, 146, 146, 142, 125, 142, 151 132, 139, 139, 185, 159, 164, 149, 144 132, 146, 142, 164, 137, 125, 144, 161 156, 130, 137, 159, 164, 142, 146, 156 139, 146, 121, 146, 154, 142, 149, 159 174, 169, 172, 174, 174, 188, 193, 185 202, 169, 202, 177, 196, 174, 196, 199 182, 185, 185, 193, 210, 190, 210, 182 169, 188, 202, 169, 172, 172, 159, 161 174, 174, 159, 169, 137, 132, 164, 137 154, 139, 128, 149, 137, 117, 137, 139 125, 94, 135, 130, 137, 137, 142, 117 132, 137, 114, 114, 123, 100, 108, 104 123, 98, 110, 83, 117, 121, 88, 94 110, 98, 119, 102, 121, 121, 90, 104 98, 100, 106, 94, 90, 119, 112, 90 117, 96, 92, 108, 108, 86, 94, 85 117, 86, 88, 117, 96, 102, 81, 114 102, 117, 104, 121, 92, 108, 112, 102 98, 92, 100, 102, 88, 112, 108, 420 90, 110, 119, 88, 104, 110, 104, 94 117, 125, 128, 144, 135, 130, 142, 161 159, 177, 185, 196, 172, 159, 142, 144 135, 137, 130, 130, 121, 137, 112, 112 104, 119, 90, 96, 72, 86, 106, 112 108, 108, 100, 125, 100, 117, 137, 137 154, 139, 149, 146, 132, 128, 123, 114 121, 125, 130, 123, 100, 112, 102, 94 132, 100, 106, 98, 106, 96, 100, 117 128, 77, 125, 114, 110, 114, 108, 94 96, 106, 104, 96, 100, 108, 110, 114 102, 117, 132, 123, 121, 142, 144, 137 166, 169, 137, 172, 159, 166, 151, 144 151, 149, 174, 144, 132, 137, 132, 102 110, 125, 121, 104, 104, 104, 106, 108 112, 132, 102, 119, 123, 117, 130, 104 117, 106, 96, 108, 125, 106, 98, 108 79, 88, 92, 83, 96, 94, 77, 110 94, 85, 94, 76, 98, 77, 71, 86 77, 86, 69, 83, 88, 72, 71, 88 72, 77, 77, 92, 88, 83, 102, 96 86, 110, 100, 92, 85, 98, 98, 102 112, 110, 98, 83, 98, 100, 94, 96 98, 100, 117, 104, 125, 92, 110, 121 121, 142, 137, 123, 156, 156, 177, 207 222, 234, 213, 225, 269, 262, 262, 234 207, 213, 204, 228, 207, 216, 225, 219 234, 216, 246, 276, 286, 346, 365, 324 357, 328, 331, 289, 299, 310, 350, 306 335, 292, 269, 289, 234, 237, 188, 188 169, 185, 151, 151, 125, 139, 117, 112 106, 98, 98, 92, 106, 86, 90, 94 100, 96, 106, 108, 81, 96, 96, 104 112, 94, 100, 112, 123, 114, 92, 79 114, 128, 104, 117, 117, 128, 108, 119 112, 128, 119, 135, 104, 119, 135, 106 128, 119, 100, 130, 114, 135, 130, 108 130, 130, 132, 128, 128, 144, 123, 114 104, 114, 108, 85, 121, 104, 110, 100 112,/