SampleIdent,907A-1-3/21,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 8-aug-1993 14:44,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 98, 90, 90, 102, 90, 106, 83, 79 88, 114, 83, 86, 90, 88, 106, 108 98, 72, 108, 92, 102, 96, 86, 108 85, 90, 100, 100, 83, 121, 102, 90 96, 106, 90, 94, 100, 86, 92, 102 114, 86, 90, 104, 114, 114, 92, 100 79, 110, 94, 106, 108, 104, 102, 108 104, 106, 96, 102, 114, 85, 96, 108 92, 121, 96, 121, 98, 106, 110, 112 132, 110, 96, 132, 98, 125, 108, 110 132, 121, 125, 100, 128, 137, 110, 130 125, 104, 128, 112, 125, 123, 110, 117 112, 121, 119, 119, 121, 106, 110, 108 135, 123, 125, 110, 128, 108, 98, 137 112, 106, 96, 119, 130, 102, 102, 104 121, 110, 108, 114, 102, 112, 106, 121 121, 117, 119, 110, 100, 135, 137, 102 128, 92, 119, 125, 98, 112, 98, 135 112, 106, 108, 119, 86, 119, 112, 108 128, 104, 100, 110, 117, 121, 106, 100 128, 128, 123, 114, 108, 130, 104, 92 104, 96, 114, 121, 114, 104, 117, 98 117, 123, 132, 144, 92, 119, 112, 130 94, 128, 117, 142, 151, 125, 156, 123 123, 130, 142, 125, 130, 117, 98, 106 102, 106, 123, 98, 104, 108, 117, 108 112, 102, 117, 112, 104, 96, 88, 110 94, 104, 96, 98, 110, 110, 108, 92 102, 94, 88, 108, 92, 83, 100, 85 110, 100, 79, 102, 92, 102, 94, 94 92, 94, 110, 85, 96, 83, 104, 108 85, 81, 108, 92, 85, 104, 90, 85 104, 100, 104, 88, 94, 100, 92, 92 76, 77, 96, 112, 92, 88, 92, 94 71, 106, 100, 90, 94, 98, 86, 83 88, 79, 83, 88, 76, 85, 83, 88 79, 96, 90, 94, 108, 104, 100, 92 86, 90, 86, 88, 86, 74, 96, 96 88, 86, 83, 79, 76, 90, 79, 92 320, 92, 76, 86, 90, 85, 98, 96 76, 100, 76, 83, 77, 92, 86, 90 90, 104, 92, 86, 83, 94, 94, 92 106, 86, 100, 76, 94, 96, 81, 106 110, 96, 88, 88, 112, 98, 98, 92 86, 104, 90, 110, 94, 106, 108, 114 106, 117, 108, 119, 142, 112, 135, 117 117, 119, 142, 121, 135, 112, 137, 114 100, 108, 110, 119, 104, 96, 85, 81 100, 98, 96, 76, 98, 90, 85, 104 100, 92, 85, 86, 86, 74, 85, 79 77, 96, 96, 72, 77, 98, 102, 83 79, 85, 90, 98, 83, 61, 86, 79 83, 83, 83, 79, 102, 86, 72, 72 85, 76, 94, 76, 94, 83, 94, 100 85, 92, 83, 94, 83, 106, 90, 88 83, 90, 90, 104, 98, 98, 86, 92 77, 77, 90, 83, 94, 66, 71, 72 74, 96, 83, 72, 90, 81, 72, 66 86, 77, 69, 92, 55, 79, 77, 79 72, 90, 61, 83, 72, 74, 71, 62 90, 86, 83, 76, 74, 67, 69, 76 79, 86, 76, 67, 76, 92, 76, 76 100, 66, 94, 86, 72, 67, 86, 74 81, 67, 71, 77, 94, 77, 88, 86 64, 86, 66, 56, 76, 85, 77, 72 72, 79, 81, 71, 83, 81, 88, 71 83, 69, 71, 77, 67, 90, 79, 64 85, 76, 67, 71, 79, 86, 88, 66 76, 76, 71, 92, 83, 62, 59, 77 76, 67, 76, 69, 83, 66, 92, 79 76, 85, 58, 77, 85, 76, 66, 62 72, 61, 71, 76, 66, 98, 67, 69 66, 71, 77, 56, 74, 83, 50, 86 77, 69, 66, 66, 58, 62, 52, 77 76, 71, 92, 64, 66, 74, 72, 67 79, 76, 86, 90, 74, 71, 83, 71 79, 72, 86, 71, 77, 79, 71, 71 56, 77, 69, 66, 92, 64, 77, 83 83, 66, 64, 85, 72, 77, 74, 83 77, 86, 92, 92, 90, 104, 98, 100 96, 96, 90, 108, 81, 77, 100, 71 71, 83, 69, 83, 64, 62, 106, 85 79, 64, 86, 79, 69, 76, 86, 85 88, 81, 86, 77, 66, 79, 67, 96 85, 88, 92, 72, 85, 86, 83, 76 67, 81, 92, 77, 74, 76, 94, 79 85, 88, 85, 83, 86, 102, 88, 76 66, 85, 77, 85, 86, 76, 76, 67 79, 83, 90, 86, 88, 102, 100, 85 112, 96, 104, 88, 86, 104, 96, 96 112, 112, 90, 112, 121, 125, 110, 117 121, 114, 144, 125, 137, 166, 159, 169 159, 166, 185, 164, 174, 172, 174, 190 180, 177, 174, 169, 135, 144, 139, 139 114, 121, 121, 154, 112, 128, 154, 125 102, 119, 110, 121, 119, 130, 108, 96 94, 110, 117, 114, 104, 92, 117, 123 121, 125, 128, 114, 117, 137, 137, 154 196, 219, 243, 262, 317, 256, 289, 289 299, 331, 361, 396, 372, 320, 266, 207 156, 161, 130, 119, 117, 123, 110, 104 110, 110, 104, 106, 104, 98, 112, 76 106, 94, 104, 98, 90, 102, 104, 92 92, 90, 121, 119, 104, 102, 121, 94 104, 92, 102, 106, 92, 90, 92, 110 102, 112, 121, 125, 128, 130, 128, 142 139, 159, 166, 142, 149, 144, 144, 112 119, 125, 117, 100, 92, 86, 94, 92 102, 102, 90, 100, 88, 104, 100, 106 106, 100, 72, 86, 112, 81, 92, 110 96, 108, 92, 102, 88, 108, 106, 112 92, 88, 98, 125, 117, 98, 132, 125 112, 132, 137, 146, 164, 130, 149, 132 144, 144, 149, 146, 128, 112, 132, 100 110, 108, 108, 102, 104, 98, 100, 114 117, 130, 121, 139, 144, 164, 177, 146 172, 174, 172, 172, 164, 146, 161, 164 137, 146, 117, 130, 104, 108, 130, 102 128, 135, 128, 119, 98, 106, 135, 112 123, 128, 142, 112, 119, 142, 151, 149 121, 151, 135, 166, 144, 112, 130, 128 119, 149, 130, 117, 132, 156, 137, 121 117, 114, 119, 110, 106, 71, 100, 114 110, 125, 112, 114, 132, 114, 94, 106 121, 125, 142, 135, 132, 117, 112, 123 144, 135, 125, 139, 135, 137, 154, 135 137, 151, 151, 132, 185, 149, 123, 144 154, 156, 180, 149, 156, 135, 149, 151 182, 166, 159, 177, 169, 154, 149, 149 169, 117, 135, 144, 166, 114, 137, 125 132, 121, 119, 112, 121, 117, 110, 135 137, 121, 94, 100, 125, 119, 135, 123 135, 130, 125, 123, 137, 154, 146, 137 156, 185, 174, 169, 199, 240, 286, 310 380, 441, 511, 645, 835, 1050, 1218, 1406 1798, 2043, 2401, 2809, 3170, 2820, 2362, 1840 1482, 1063, 681, 445, 384, 296, 262, 250 253, 207, 193, 210, 202, 193, 188, 174 188, 196, 164, 159, 161, 149, 166, 154 161, 159, 182, 190, 199, 246, 225, 222 256, 266, 299, 276, 286, 266, 289, 237 202, 216, 204, 231, 219, 240, 259, 306 279, 310, 282, 306, 335, 328, 313, 350 353, 392, 380, 392, 396, 581, 384, 353 296, 272, 266, 231, 228, 164, 177, 164 174, 151, 156, 137, 139, 159, 135, 137 146, 144, 121, 142, 114, 98, 121, 112 132, 119, 112, 123, 119, 117, 85, 110 106, 96, 92, 110, 94, 123, 102, 100 100, 94, 106, 98, 104, 292, 96, 96 110, 123, 108, 137, 125, 117, 149, 146 174, 193, 253, 259, 310, 400, 449, 581 650, 734, 795, 930, 961, 992, 999, 894 801, 681, 538, 449, 357, 262, 202, 190 169, 159, 151, 164, 159, 172, 151, 169 164, 146, 137, 166, 154, 154, 149, 144 137, 146, 128, 166, 121, 146, 139, 164 146, 137, 154, 164, 137, 156, 154, 135 142, 164, 128, 159, 128, 156, 139, 137 146, 125, 137, 125, 156, 121, 144, 110 130, 130, 104, 121, 135, 112, 135, 130 128, 159, 132, 128, 156, 130, 142, 139 139, 154, 114, 132, 130, 102, 146, 125 106, 117, 135, 121, 121, 108, 132, 117 139, 117, 121, 130, 125, 137, 125, 161 144, 166, 164, 190, 154, 166, 172, 182 182, 169, 169, 188, 185, 210, 225, 237 253, 213, 240, 219, 210, 169, 166, 149 121, 142, 86, 119, 123, 96, 100, 98 114, 90, 100, 92, 90, 86, 94, 83 90, 92, 79, 81, 81, 79, 86, 92 88, 79, 77, 86, 83, 85, 85, 71 81, 88, 79, 85, 85, 83, 74, 77 90, 90, 79, 88, 85, 62, 76, 74 76, 77, 88, 77, 76, 67, 72, 77 85, 72, 92, 83, 88, 81, 83, 88 72, 74, 83, 98, 74, 92, 71, 104 92, 96, 94, 98, 81, 76, 71, 71 85, 88, 110, 108, 114, 96, 77, 96 86, 98, 88, 83, 94, 77, 85, 88 90, 81, 96, 104, 96, 102, 96, 96 98, 102, 98, 121, 86, 102, 106, 104 114, 98, 104, 121, 104, 108, 117, 135 137, 144, 139, 112, 132, 159, 135, 149 149, 161, 164, 159, 169, 172, 174, 182 166, 177, 213, 182, 182, 185, 174, 190 199, 207, 216, 243, 202, 216, 243, 243 213, 237, 216, 237, 240, 219, 234, 225 250, 231, 185, 202, 202, 169, 182, 182 169, 190, 177, 172, 164, 169, 172, 151 149, 146, 151, 123, 177, 137, 154, 137 159, 154, 164, 139, 135, 130, 159, 174 169, 149, 151, 172, 144, 151, 177, 193 182, 202, 185, 213, 182, 185, 193, 204 213, 174, 144, 154, 142, 144, 132, 121 137, 112, 123, 135, 114, 117, 135, 137 121, 142, 149, 193, 182, 240, 231, 262 253, 269, 269, 324, 269, 282, 262, 222 216, 225, 190, 202, 169, 161, 151, 156 139, 130, 128, 159, 132, 110, 130, 130 130, 132, 121, 121, 144, 132, 110, 112 108, 130, 132, 121, 123, 151, 139, 142 121, 132, 154, 139, 135, 137, 159, 137 144, 156, 121, 137, 139, 149, 142, 149 144, 154, 149, 130, 137, 137, 142, 154 146, 128, 117, 137, 110, 117, 117, 119 98, 119, 85, 112, 121, 90, 90, 100 102, 106, 85, 98, 114, 100, 90, 112 110, 98, 106, 110, 88, 102, 98, 88 98, 94, 92, 79, 96, 88, 128, 94 90, 88, 94, 92, 81, 79, 98, 85 96, 86, 94, 100, 85, 98, 106, 110 108, 104, 86, 86, 96, 94, 88, 83 92, 96, 102, 83, 102, 114, 119, 112 144, 151, 164, 159, 196, 246, 253, 286 320, 335, 357, 412, 396, 353, 328, 259 253, 225, 213, 161, 159, 146, 142, 121 94, 83, 98, 110, 85, 85, 106, 110 90, 104, 102, 94, 112, 72, 108, 117 96, 96, 110, 119, 104, 98, 128, 125 125, 125, 159, 161, 174, 188, 188, 180 185, 161, 151, 114, 137, 117, 102, 88 110, 94, 85, 108, 85, 90, 90, 90 92, 79, 96, 76, 104, 81, 81, 88 88, 108, 98, 90, 88, 85, 104, 110 102, 106, 86, 102, 83, 108, 104, 88 123, 98, 102, 106, 125, 110, 100, 146 112, 98, 102, 96, 77, 86, 79, 69 77, 90, 92, 83, 79, 104, 104, 72 106, 92, 104, 108, 108, 130, 108, 100 104, 125, 112, 121, 102, 90, 106, 104 98, 86, 121, 102, 104, 88, 106, 96 112, 86, 108, 102, 117, 125, 177, 190 216, 266, 185, 190, 202, 243, 243, 253 234, 262, 196, 225, 240, 207, 177, 166 166, 139, 159, 132, 137, 112, 102, 90 104, 98, 90, 108, 112, 88, 100, 106 112, 96, 100, 106, 130, 132, 137, 164 154, 193, 210, 196, 213, 190, 190, 166 188, 139, 159, 135, 139, 114, 112, 81 90, 85, 86, 83, 67, 92, 85, 108 94, 108, 88, 94, 104, 88, 102, 102 96, 96, 96, 88, 123, 114, 123, 117 119, 108, 102, 110, 92, 108, 110, 90 98, 79, 86, 96, 77, 83, 77, 92 94, 85, 88, 98, 88, 86, 96, 106 108, 117, 125, 144, 159, 142, 154, 156 154, 166, 177, 159, 159, 144, 135, 169 137, 137, 104, 108, 102, 100, 98, 102 102, 104, 117, 114, 110, 132, 117, 125 114, 110, 112, 144, 128, 117, 125, 108 142, 144, 149, 137, 135, 130, 144, 185 172, 177, 193, 237, 243, 243, 243, 262 234, 253, 237, 225, 207, 196, 199, 190 185, 149, 151, 164, 154, 159, 149, 164 169, 188, 169, 177, 161, 149, 125, 121 130, 132, 121, 110, 128, 98, 100, 98 83, 96, 86, 67, 86, 104, 92, 88 92, 74, 83, 79, 86, 88, 85, 90 59, 88, 86, 77, 66, 79, 90, 94 67, 76, 86, 76, 66, 67, 71, 77 76, 86, 83, 79, 98, 85, 98, 79 92, 92, 110, 112, 114, 104, 149, 146 132, 137, 149, 164, 144, 161, 142, 159 142, 142, 139, 149, 188, 169, 240, 228 289, 313, 380, 441, 449, 445, 445, 471 408, 404, 376, 339, 262, 276, 246, 190 177, 161, 137, 102, 96, 104, 102, 90 90, 88, 92, 102, 77, 112, 106, 83 77, 83, 96, 90, 128, 102, 88, 98 117, 117, 100, 117, 123, 121, 149, 159 166, 190, 210, 256, 289, 276, 286, 303 339, 310, 279, 276, 256, 204, 216, 196 169, 169, 128, 110, 85, 98, 90, 86 92, 86, 86, 85, 88, 83, 83, 83 77, 88, 74, 79, 85, 88, 81, 90 77, 88, 83, 90, 83, 76, 86, 79 85, 94, 86, 69, 88, 85, 79, 88 83, 67, 77, 85, 72, 83, 90, 85 106, 83, 94, 85, 92, 85, 81, 98 85, 98, 106, 112, 77, 108, 121, 128 144, 144, 166, 199, 269, 259, 303, 350 396, 365, 428, 424, 428, 342, 335, 303 228, 222, 234, 204, 166, 137, 112, 88 94, 88, 98, 96, 98, 100, 108, 112 98, 117, 104, 102, 106, 135, 94, 108 90, 98, 100, 119, 102, 106, 92, 83 83, 86, 85, 94, 92, 85, 102, 83 106, 98, 86, 94, 376, 100, 88, 96 102, 88, 77, 86, 100, 83, 86, 74 79, 72, 86, 77, 86, 67, 72, 66 66, 74, 49, 61, 62, 61, 59, 62 53, 64, 79, 50, 50, 62, 53, 59 71, 66, 56, 66, 66, 58, 59, 88 62, 69, 58, 62, 59, 62, 59, 92 72, 94, 67, 85, 72, 76, 92, 76 77, 85, 76, 77, 85, 67, 71, 71 72, 59, 72, 69, 76, 79, 79, 71 72, 88, 88, 77, 85, 72, 77, 88 79, 83, 76, 77, 71, 72, 79, 90 83, 100, 76, 94, 88, 106, 74, 85 92, 112, 104, 90, 96, 102, 85, 94 86, 94, 104, 96, 112, 88, 108, 92 90, 85, 94, 94, 90, 94, 86, 88 92, 110, 76, 83, 96, 112, 98, 102 98, 104, 100, 112, 104, 94, 104, 114 110, 98, 112, 112, 104, 94, 137, 96 104, 96, 104, 100, 123, 112, 110, 102 112, 110, 114, 100, 100, 110, 123, 96 96, 121, 102, 114, 110, 114, 96, 112 106, 121, 121, 135, 123, 123, 125, 144 156, 169, 180, 174, 213, 269, 299, 306 286, 246, 207, 196, 180, 216, 213, 210 202, 164, 137, 142, 154, 142, 128, 144 154, 144, 149, 149, 135, 146, 142, 174 151, 149, 159, 142, 130, 121, 128, 144 130, 117, 132, 114, 123, 112, 121, 119 90, 106, 114, 128, 104, 114, 128, 121 98, 100, 110, 135, 117, 88, 110, 110 110, 108, 98, 112, 114, 108, 102, 132 114, 100, 104, 94, 119, 125, 137, 135 137, 135, 121, 137, 172, 144, 149, 151 159, 159, 154, 164, 128, 164, 164, 142 121, 130, 108, 142, 128, 117, 100, 114 94, 94, 108, 85, 83, 114, 79, 74 96, 81, 104, 96, 98, 86, 98, 98 88, 88, 123, 108, 117, 142, 132, 137 144, 166, 156, 154, 169, 199, 154, 219 190, 182, 156, 132, 139, 137, 144, 110 125, 132, 112, 102, 85, 94, 90, 88 83, 117, 79, 98, 92, 112, 88, 96 100, 96, 112, 104, 130, 100, 100, 119 121, 98, 98, 98, 98, 81, 96, 90 83, 96, 86, 79, 74, 110, 92, 83 79, 74, 86, 83, 94, 79, 83, 88 96, 102, 110, 83, 110, 96, 90, 92 98, 92, 94, 100, 88, 108, 110, 104 85, 98, 88, 100, 76, 96, 88, 88 92, 81, 88, 100, 79, 90, 112, 88 114, 102, 100, 92, 85, 83, 108, 79 88, 90, 102, 104, 72, 92, 96, 92 90, 96, 112, 121, 114, 102, 112, 123 114, 146, 128, 169, 166, 164, 199, 269 269, 335, 324, 365, 380, 404, 339, 320 289, 299, 259, 246, 246, 259, 199, 207 174, 166, 144, 121, 135, 135, 123, 128 125, 108, 130, 108, 121, 110, 132, 123 130, 117, 139, 149, 154, 182, 151, 139 161, 164, 166, 159, 161, 154, 139, 159 156, 149, 169, 159, 121, 149, 149, 161 146, 149, 166, 164, 135, 151, 151, 154 144, 123, 156, 182, 130, 174, 159, 156 196, 193, 180, 204, 193, 207, 225, 188 185, 182, 177, 188, 210, 188, 204, 174 188, 204, 169, 185, 169, 177, 161, 172 185, 144, 177, 199, 154, 159, 164, 144 130, 151, 128, 169, 144, 146, 135, 135 128, 142, 137, 119, 125, 142, 112, 114 128, 110, 144, 130, 137, 106, 121, 110 106, 123, 114, 108, 110, 117, 114, 114 102, 106, 132, 121, 88, 106, 94, 100 92, 92, 94, 110, 106, 96, 90, 83 98, 96, 102, 100, 94, 88, 123, 102 114, 85, 108, 117, 117, 104, 92, 106 102, 90, 110, 94, 114, 94, 104, 108 108, 98, 114, 104, 90, 110, 112, 94 85, 128, 106, 104, 96, 88, 77, 92 94, 100, 110, 100, 96, 104, 119, 106 112, 108, 110, 114, 132, 149, 177, 154 169, 164, 139, 139, 142, 110, 151, 117 110, 96, 128, 108, 114, 102, 86, 92 102, 92, 88, 90, 98, 88, 100, 110 104, 100, 114, 117, 137, 121, 117, 128 149, 144, 174, 149, 156, 112, 123, 139 106, 146, 144, 128, 108, 102, 100, 121 88, 104, 114, 102, 102, 102, 102, 77 92, 102, 110, 106, 106, 108, 104, 108 108, 108, 88, 112, 119, 94, 112, 149 149, 144, 154, 182, 210, 177, 213, 228 213, 182, 193, 174, 185, 166, 177, 193 132, 146, 159, 146, 135, 121, 110, 121 104, 96, 114, 106, 88, 110, 100, 108 98, 114, 96, 114, 108, 102, 106, 112 104, 100, 121, 96, 90, 100, 106, 76 92, 77, 79, 74, 79, 85, 79, 67 62, 81, 72, 62, 85, 81, 86, 56 61, 90, 77, 66, 64, 85, 88, 83 77, 85, 66, 83, 86, 81, 98, 106 88, 90, 108, 110, 86, 104, 76, 102 104, 104, 88, 90, 92, 83, 110, 106 100, 102, 94, 102, 88, 106, 104, 94 123, 125, 156, 161, 164, 234, 250, 286 306, 303, 339, 320, 292, 259, 222, 210 190, 240, 222, 237, 231, 216, 196, 222 185, 228, 234, 276, 320, 331, 357, 335 369, 328, 331, 328, 353, 339, 320, 317 306, 296, 243, 228, 234, 190, 202, 182 174, 142, 142, 154, 112, 123, 100, 100 104, 94, 112, 79, 96, 76, 100, 110 98, 98, 96, 83, 86, 94, 102, 92 104, 117, 98, 83, 106, 106, 90, 92 119, 110, 119, 110, 100, 128, 100, 102 108, 114, 114, 121, 106, 130, 125, 144 130, 132, 104, 94, 88, 114, 117, 114 110, 112, 104, 108, 88, 119, 128, 102 106, 102, 88, 92, 108, 98, 119, 86 100,/