SampleIdent,907A-2-2,69,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 6-aug-1993 13:23,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 94, 86, 104, 102, 96, 106, 92, 102 96, 98, 96, 110, 117, 102, 88, 121 98, 104, 108, 94, 110, 96, 110, 90 112, 104, 83, 112, 108, 123, 88, 104 96, 86, 112, 83, 112, 104, 85, 117 125, 112, 104, 106, 125, 142, 106, 110 130, 130, 121, 108, 135, 117, 112, 130 130, 154, 110, 121, 137, 144, 125, 121 125, 100, 104, 121, 117, 117, 128, 123 123, 110, 135, 110, 110, 135, 102, 104 114, 117, 121, 132, 104, 112, 123, 104 121, 104, 114, 106, 117, 128, 92, 132 135, 123, 104, 114, 112, 121, 132, 128 117, 125, 119, 112, 114, 119, 137, 121 132, 96, 125, 98, 121, 104, 137, 110 123, 119, 121, 117, 98, 110, 117, 104 132, 144, 121, 137, 125, 121, 142, 130 125, 123, 106, 125, 121, 128, 137, 125 119, 119, 117, 130, 146, 135, 128, 139 139, 144, 137, 164, 121, 139, 156, 130 169, 132, 132, 142, 142, 164, 151, 144 151, 164, 159, 142, 177, 172, 177, 137 177, 154, 166, 159, 156, 164, 151, 196 190, 177, 196, 185, 225, 180, 202, 169 199, 149, 154, 135, 123, 121, 123, 112 132, 114, 121, 112, 98, 102, 100, 110 104, 100, 108, 112, 85, 108, 108, 104 110, 92, 102, 88, 106, 98, 102, 92 81, 90, 98, 77, 90, 106, 85, 98 96, 106, 86, 88, 100, 106, 106, 104 88, 90, 85, 108, 112, 88, 102, 98 88, 86, 102, 96, 98, 98, 96, 94 102, 86, 110, 104, 108, 94, 77, 86 100, 94, 108, 92, 77, 96, 83, 90 104, 86, 90, 83, 85, 102, 90, 108 88, 90, 86, 86, 79, 86, 108, 77 106, 104, 94, 92, 92, 92, 86, 85 74, 100, 96, 98, 79, 81, 85, 85 83, 98, 86, 86, 85, 104, 104, 88 88, 104, 104, 77, 92, 79, 96, 94 98, 96, 100, 100, 92, 96, 96, 100 94, 88, 85, 96, 100, 104, 86, 106 88, 86, 96, 100, 98, 100, 102, 125 112, 112, 112, 88, 102, 106, 125, 130 139, 112, 130, 139, 135, 146, 128, 149 177, 169, 159, 180, 185, 196, 231, 240 250, 262, 276, 269, 253, 259, 225, 190 174, 142, 144, 149, 125, 106, 108, 119 102, 114, 92, 108, 104, 100, 86, 102 117, 81, 88, 86, 88, 85, 98, 79 104, 88, 94, 88, 92, 92, 94, 79 96, 90, 83, 86, 98, 98, 102, 100 108, 86, 88, 88, 72, 100, 83, 83 86, 86, 77, 92, 96, 76, 94, 88 102, 106, 76, 94, 104, 108, 85, 114 85, 88, 86, 92, 92, 85, 77, 79 114, 86, 98, 81, 83, 79, 90, 81 86, 62, 90, 79, 83, 92, 83, 69 71, 94, 110, 85, 85, 92, 72, 98 72, 83, 77, 85, 76, 94, 88, 67 77, 98, 92, 94, 196, 74, 88, 90 77, 83, 85, 72, 88, 90, 100, 92 85, 81, 66, 96, 85, 90, 86, 71 90, 79, 67, 76, 72, 92, 94, 74 102, 79, 71, 76, 83, 88, 67, 94 81, 71, 52, 90, 79, 79, 90, 94 71, 72, 94, 76, 74, 76, 69, 77 79, 98, 98, 86, 83, 72, 83, 71 88, 79, 76, 96, 71, 74, 72, 81 86, 67, 72, 62, 86, 72, 96, 88 96, 86, 77, 71, 85, 83, 72, 76 83, 96, 86, 90, 81, 86, 86, 83 94, 74, 71, 86, 71, 72, 71, 66 71, 83, 96, 83, 81, 86, 67, 74 76, 66, 102, 81, 72, 98, 72, 90 96, 88, 106, 94, 92, 98, 112, 79 90, 71, 76, 88, 90, 85, 76, 86 88, 90, 88, 112, 96, 94, 96, 121 110, 108, 128, 123, 108, 128, 128, 130 130, 154, 142, 130, 156, 159, 151, 144 130, 114, 106, 125, 98, 106, 86, 119 100, 114, 77, 100, 114, 117, 102, 102 86, 92, 90, 94, 76, 96, 92, 88 98, 108, 117, 108, 106, 98, 123, 102 106, 86, 104, 98, 106, 123, 98, 154 112, 130, 142, 130, 135, 135, 123, 119 144, 119, 128, 121, 114, 104, 119, 98 121, 102, 94, 98, 110, 88, 119, 108 123, 128, 100, 102, 96, 114, 104, 104 74, 102, 98, 88, 114, 102, 106, 117 104, 108, 123, 125, 159, 154, 149, 174 166, 225, 234, 237, 228, 303, 266, 240 234, 256, 253, 213, 231, 202, 177, 193 174, 174, 144, 151, 159, 369, 146, 149 137, 142, 128, 135, 125, 132, 121, 139 123, 144, 135, 142, 130, 139, 137, 128 132, 123, 130, 94, 130, 106, 132, 125 123, 164, 151, 174, 180, 190, 196, 259 269, 289, 342, 384, 437, 475, 471, 441 400, 306, 237, 199, 144, 125, 128, 117 117, 117, 100, 110, 104, 85, 98, 98 114, 96, 114, 112, 94, 106, 106, 102 110, 92, 112, 92, 83, 98, 121, 102 104, 106, 96, 86, 106, 96, 119, 98 96, 102, 108, 117, 102, 94, 100, 123 117, 119, 121, 137, 142, 159, 182, 188 180, 199, 166, 196, 156, 139, 100, 100 106, 100, 92, 81, 98, 121, 86, 98 86, 96, 110, 88, 94, 71, 83, 88 102, 110, 90, 102, 94, 114, 90, 88 94, 94, 106, 121, 100, 117, 106, 135 110, 106, 119, 142, 128, 132, 121, 125 146, 110, 110, 121, 139, 132, 132, 96 108, 106, 104, 112, 112, 94, 114, 123 112, 94, 100, 112, 128, 100, 125, 121 125, 130, 154, 154, 180, 159, 188, 146 156, 166, 144, 130, 135, 128, 149, 139 130, 123, 123, 132, 144, 144, 144, 130 137, 130, 144, 166, 128, 151, 146, 182 196, 216, 196, 219, 185, 222, 222, 199 199, 231, 225, 204, 188, 166, 180, 161 146, 151, 135, 142, 154, 156, 125, 137 142, 146, 137, 146, 142, 151, 137, 132 159, 144, 169, 172, 159, 144, 169, 164 164, 180, 210, 213, 237, 213, 246, 262 279, 266, 289, 292, 317, 346, 306, 350 328, 292, 306, 259, 250, 282, 279, 256 253, 222, 243, 225, 225, 210, 204, 207 190, 172, 188, 161, 180, 149, 142, 154 128, 146, 142, 142, 154, 130, 144, 139 156, 159, 130, 132, 128, 144, 154, 130 146, 128, 132, 144, 166, 135, 132, 185 169, 161, 172, 172, 177, 190, 204, 210 207, 266, 299, 380, 388, 506, 581, 784 918, 1129, 1318, 1656, 1866, 2181, 2480, 2581 2391, 2107, 1815, 1414, 1109, 853, 660, 524 471, 458, 424, 392, 384, 361, 310, 317 259, 276, 262, 219, 240, 225, 222, 231 207, 202, 210, 199, 190, 210, 196, 182 172, 169, 188, 169, 156, 161, 172, 185 207, 172, 188, 161, 180, 159, 196, 172 216, 228, 225, 253, 299, 262, 317, 328 324, 357, 404, 369, 441, 433, 441, 471 467, 449, 416, 388, 346, 306, 246, 216 237, 231, 225, 199, 231, 213, 204, 188 196, 177, 159, 161, 137, 234, 142, 159 142, 151, 137, 154, 130, 132, 128, 121 137, 117, 119, 135, 108, 139, 135, 132 117, 137, 137, 125, 110, 130, 135, 135 132, 149, 128, 142, 128, 108, 114, 146 137, 174, 144, 144, 154, 144, 144, 151 130, 142, 137, 169, 139, 142, 119, 139 121, 156, 132, 128, 123, 132, 142, 144 128, 130, 149, 135, 154, 139, 142, 149 146, 137, 159, 139, 180, 164, 164, 185 166, 196, 169, 172, 144, 159, 193, 166 164, 180, 151, 161, 166, 164, 154, 137 137, 159, 159, 139, 132, 144, 132, 156 159, 144, 177, 164, 174, 174, 185, 177 182, 174, 159, 130, 135, 132, 137, 121 121, 125, 130, 104, 102, 121, 112, 128 114, 121, 92, 121, 106, 128, 121, 119 142, 102, 123, 137, 137, 130, 132, 154 139, 130, 144, 172, 172, 159, 169, 169 174, 174, 166, 130, 135, 130, 146, 139 142, 159, 144, 125, 139, 137, 137, 114 149, 114, 119, 119, 132, 106, 125, 100 108, 128, 117, 104, 130, 108, 142, 135 114, 132, 137, 123, 130, 137, 128, 119 114, 139, 110, 104, 110, 108, 98, 117 117, 94, 102, 102, 104, 100, 96, 72 90, 299, 74, 79, 96, 83, 83, 92 79, 86, 88, 98, 77, 85, 86, 77 90, 98, 102, 74, 83, 81, 90, 96 81, 88, 86, 86, 72, 92, 88, 104 96, 102, 102, 76, 98, 85, 85, 92 125, 106, 100, 85, 96, 100, 102, 104 106, 110, 102, 104, 121, 100, 123, 92 108, 106, 108, 119, 114, 125, 86, 104 121, 121, 135, 121, 102, 104, 100, 110 100, 123, 117, 106, 96, 110, 112, 117 92, 121, 106, 90, 102, 86, 79, 114 112, 139, 119, 108, 110, 132, 123, 110 144, 139, 177, 151, 202, 177, 207, 196 207, 250, 250, 234, 266, 231, 282, 272 262, 262, 299, 262, 299, 269, 299, 296 310, 317, 310, 365, 372, 353, 353, 324 350, 357, 331, 339, 317, 306, 259, 286 276, 253, 225, 222, 190, 199, 182, 182 149, 166, 164, 130, 164, 144, 123, 130 149, 123, 117, 139, 114, 123, 119, 130 114, 128, 119, 132, 119, 121, 110, 146 119, 137, 142, 151, 164, 137, 142, 137 139, 137, 132, 151, 142, 139, 121, 149 154, 142, 112, 149, 154, 137, 123, 128 151, 151, 164, 154, 159, 190, 222, 246 228, 272, 279, 306, 353, 376, 396, 380 357, 339, 299, 320, 262, 225, 228, 210 172, 180, 185, 196, 172, 161, 182, 164 180, 164, 149, 159, 161, 164, 164, 169 154, 144, 112, 146, 172, 149, 166, 161 161, 174, 149, 180, 172, 193, 188, 193 166, 164, 202, 193, 202, 172, 216, 213 182, 202, 219, 193, 196, 213, 219, 202 204, 213, 207, 202, 180, 196, 177, 180 149, 177, 164, 159, 166, 159, 130, 110 125, 125, 130, 125, 121, 112, 98, 112 83, 96, 104, 102, 92, 119, 96, 100 112, 108, 117, 98, 98, 110, 104, 104 94, 106, 88, 83, 102, 108, 90, 86 83, 83, 77, 88, 76, 88, 90, 85 92, 92, 85, 85, 104, 92, 100, 92 92, 69, 79, 72, 90, 85, 86, 92 83, 72, 92, 88, 102, 112, 119, 96 114, 132, 164, 174, 213, 219, 253, 262 289, 259, 266, 231, 213, 169, 177, 174 139, 117, 102, 130, 102, 98, 110, 114 108, 90, 110, 121, 121, 119, 117, 128 128, 128, 117, 108, 135, 128, 135, 144 139, 130, 137, 139, 132, 159, 151, 199 180, 210, 196, 202, 159, 154, 132, 144 137, 114, 106, 106, 102, 88, 123, 98 100, 92, 94, 100, 88, 83, 86, 110 102, 83, 119, 98, 104, 125, 123, 110 121, 94, 137, 104, 85, 119, 108, 104 123, 102, 106, 137, 123, 112, 128, 146 114, 96, 121, 125, 112, 100, 88, 102 106, 98, 119, 96, 104, 100, 117, 119 88, 79, 98, 114, 94, 94, 98, 104 85, 98, 104, 117, 108, 119, 123, 132 132, 108, 104, 121, 128, 149, 121, 137 137, 114, 137, 137, 130, 135, 142, 119 144, 144, 135, 142, 169, 185, 182, 199 216, 222, 286, 320, 282, 303, 306, 279 266, 246, 202, 213, 202, 174, 164, 130 106, 119, 110, 139, 119, 132, 121, 125 110, 108, 117, 108, 114, 106, 121, 104 98, 117, 92, 123, 98, 110, 114, 100 100, 108, 94, 108, 104, 88, 102, 112 112, 108, 125, 100, 102, 114, 90, 96 83, 114, 90, 106, 98, 92, 88, 98 96, 106, 90, 106, 100, 90, 98, 96 102, 110, 96, 88, 128, 106, 112, 137 121, 128, 121, 125, 114, 112, 142, 144 125, 123, 102, 112, 119, 114, 114, 117 102, 114, 137, 102, 98, 112, 110, 100 106, 106, 137, 130, 137, 146, 154, 180 190, 196, 213, 204, 196, 199, 190, 161 177, 169, 156, 164, 161, 159, 151, 154 169, 174, 159, 169, 190, 166, 188, 154 196, 174, 193, 169, 182, 199, 188, 196 196, 199, 216, 193, 234, 222, 216, 259 222, 225, 225, 243, 202, 250, 228, 222 213, 193, 222, 199, 210, 219, 199, 266 219, 204, 240, 256, 269, 243, 250, 228 216, 202, 190, 202, 177, 149, 132, 149 108, 128, 123, 128, 98, 130, 98, 110 117, 114, 112, 108, 108, 100, 106, 112 114, 94, 104, 119, 102, 92, 88, 98 100, 88, 117, 92, 117, 85, 76, 98 94, 79, 98, 86, 79, 90, 86, 94 90, 83, 86, 88, 85, 85, 77, 85 98, 77, 108, 77, 74, 76, 77, 71 71, 66, 81, 71, 64, 86, 67, 72 62, 59, 79, 59, 69, 69, 67, 62 69, 72, 62, 76, 61, 76, 61, 66 77, 83, 71, 83, 76, 71, 66, 76 81, 76, 96, 102, 83, 106, 100, 86 88, 104, 110, 117, 102, 102, 106, 119 117, 98, 94, 104, 139, 110, 102, 114 110, 96, 92, 96, 100, 72, 100, 77 72, 85, 86, 72, 76, 72, 67, 62 76, 72, 72, 64, 66, 83, 77, 58 76, 69, 62, 59, 67, 66, 56, 72 64, 64, 71, 71, 72, 76, 85, 72 72, 76, 86, 76, 86, 62, 88, 96 77, 96, 106, 100, 86, 102, 92, 79 86, 71, 85, 76, 86, 72, 85, 85 88, 66, 81, 79, 94, 86, 98, 104 100, 96, 110, 110, 106, 135, 123, 132 100, 130, 154, 146, 139, 185, 210, 262 331, 361, 400, 480, 480, 529, 471, 480 408, 396, 331, 313, 292, 259, 237, 159 130, 108, 88, 81, 81, 90, 85, 79 77, 72, 79, 104, 94, 79, 86, 102 88, 88, 96, 106, 94, 88, 81, 92 71, 81, 62, 71, 76, 58, 71, 71 77, 69, 66, 79, 86, 88, 83, 88 98, 92, 100, 106, 96, 108, 96, 96 96, 88, 83, 66, 71, 77, 83, 71 72, 71, 69, 71, 66, 69, 66, 69 79, 59, 76, 66, 71, 69, 83, 72 46, 71, 61, 59, 69, 67, 74, 66 90, 90, 67, 62, 62, 81, 77, 79 85, 77, 90, 86, 83, 85, 90, 85 102, 104, 106, 85, 94, 76, 92, 110 90, 92, 94, 77, 85, 67, 90, 98 106, 76, 92, 96, 83, 77, 96, 79 102, 110, 108, 92, 110, 102, 98, 106 119, 108, 119, 100, 94, 104, 108, 119 100, 130, 96, 90, 92, 117, 117, 123 108, 102, 119, 106, 110, 106, 94, 102 125, 112, 112, 85, 100, 123, 125, 121 110, 119, 108, 121, 108, 96, 130, 106 108, 139, 119, 96, 128, 121, 114, 137 149, 130, 144, 112, 146, 139, 125, 117 128, 132, 125, 121, 132, 149, 146, 139 142, 128, 121, 114, 135, 123, 125, 144 139, 132, 132, 125, 130, 128, 121, 142 130, 128, 132, 144, 130, 121, 142, 108 128, 154, 159, 149, 185, 219, 188, 228 243, 246, 303, 262, 234, 246, 256, 219 240, 246, 237, 231, 216, 202, 216, 196 182, 213, 207, 388, 246, 213, 216, 231 250, 240, 213, 210, 185, 210, 188, 202 159, 196, 193, 190, 172, 180, 159, 159 166, 164, 166, 174, 159, 193, 180, 177 207, 166, 207, 180, 174, 185, 177, 188 149, 159, 185, 188, 154, 154, 149, 174 154, 144, 156, 161, 125, 161, 144, 146 159, 137, 144, 125, 125, 128, 125, 137 125, 137, 137, 125, 130, 135, 142, 119 142, 130, 128, 121, 123, 108, 117, 119 121, 98, 125, 114, 154, 102, 121, 112 108, 117, 110, 117, 110, 108, 106, 114 112, 114, 110, 110, 106, 117, 117, 117 102, 137, 100, 110, 94, 112, 86, 100 117, 119, 106, 104, 117, 90, 108, 106 106, 110, 102, 106, 119, 119, 106, 121 106, 104, 104, 106, 108, 96, 108, 102 108, 112, 106, 102, 110, 86, 117, 119 96, 96, 117, 98, 121, 92, 104, 90 100, 90, 76, 110, 119, 98, 114, 90 102, 90, 106, 114, 104, 104, 88, 106 130, 85, 90, 128, 88, 117, 130, 121 144, 125, 130, 119, 121, 112, 135, 130 123, 100, 114, 123, 135, 139, 121, 125 117, 137, 112, 112, 139, 123, 121, 142 110, 121, 125, 149, 137, 142, 123, 137 123, 130, 137, 149, 119, 132, 119, 151 154, 159, 137, 151, 137, 154, 159, 169 159, 172, 199, 169, 174, 202, 182, 210 210, 243, 299, 299, 335, 388, 445, 458 480, 515, 515, 420, 380, 361, 342, 331 310, 303, 289, 246, 204, 210, 164, 144 139, 154, 149, 151, 144, 149, 117, 112 106, 137, 128, 139, 112, 121, 102, 110 132, 114, 130, 139, 135, 139, 125, 144 149, 142, 121, 108, 142, 132, 119, 125 130, 137, 128, 135, 132, 130, 149, 149 142, 144, 149, 161, 159, 108, 154, 156 149, 151, 182, 151, 151, 210, 177, 174 190, 185, 177, 188, 185, 237, 231, 222 213, 228, 243, 234, 259, 292, 279, 276 303, 266, 225, 282, 279, 282, 282, 250 272, 256, 250, 246, 234, 213, 225, 228 210, 193, 185, 172, 182, 159, 185, 139 132, 149, 159, 139, 142, 137, 114, 123 123, 110, 130, 117, 123, 135, 121, 119 130, 128, 137, 106, 110, 144, 114, 106 149, 139, 121, 121, 119, 128, 106, 83 128, 108, 130, 121, 108, 121, 110, 100 119, 106, 119, 92, 125, 112, 100, 85 96, 104, 108, 104, 108, 102, 92, 92 112, 106, 98, 117, 121, 108, 94, 119 106, 128, 114, 117, 119, 108, 125, 125 125, 123, 123, 119, 117, 130, 104, 104 112, 117, 119, 125, 112, 137, 117, 146 146, 161, 130, 161, 149, 174, 156, 159 151, 132, 125, 146, 130, 142, 135, 110 94, 100, 117, 102, 92, 76, 98, 94 85, 90, 85, 98, 94, 106, 77, 79 85, 83, 96, 96, 83, 92, 94, 90 98, 86, 90, 94, 114, 110, 98, 88 90, 77, 92, 119, 114, 108, 117, 117 117, 106, 112, 108, 104, 123, 112, 100 119, 114, 104, 114, 119, 119, 121, 106 137, 98, 128, 130, 98, 112, 132, 121 130, 100, 108, 121, 102, 128, 117, 135 104, 110, 121, 125, 121, 123, 108, 110 119, 125, 117, 121, 130, 114, 132, 110 117, 112, 108, 123, 135, 108, 119, 110 98, 94, 108, 104, 106, 90, 98, 88 94, 104, 110, 110, 96, 88, 90, 88 96, 110, 85, 90, 92, 86, 86, 104 76, 106, 85, 86, 86, 98, 104, 92 88, 85, 85, 119, 125, 102, 100, 92 96, 119, 110, 121, 108, 96, 117, 125 125, 114, 112, 104, 121, 130, 110, 123 106, 104, 121, 137, 114, 114, 102, 100 130, 132, 125, 117, 144, 123, 151, 174 174, 240, 253, 266, 282, 299, 313, 292 286, 276, 231, 262, 234, 269, 266, 256 266, 286, 234, 253, 250, 256, 310, 313 339, 384, 433, 392, 369, 369, 331, 369 376, 416, 433, 433, 388, 388, 303, 292 222, 234, 222, 222, 250, 204, 185, 188 172, 144, 117, 142, 123, 135, 135, 132 139, 142, 125, 130, 121, 132, 117, 114 125, 132, 144, 125, 139, 159, 106, 117 123, 119, 114, 130, 132, 149, 146, 149 121, 135, 151, 161, 146, 156, 137, 159 159, 174, 169, 156, 185, 174, 169, 164 149, 177, 159, 169, 164, 149, 169, 172 164, 146, 144, 166, 185, 161, 161, 172 132, 151, 174, 174, 174, 149, 177, 149 151,/