SampleIdent,907A-2-4/24,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 8-aug-1993 19:22,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 104, 98, 96, 96, 114, 104, 86, 104 100, 108, 117, 119, 112, 112, 98, 92 121, 110, 94, 117, 100, 106, 96, 94 92, 104, 112, 108, 85, 104, 88, 104 119, 104, 114, 100, 98, 102, 102, 110 100, 117, 94, 110, 128, 106, 88, 117 128, 114, 125, 96, 94, 100, 108, 130 125, 100, 114, 123, 112, 121, 149, 92 117, 128, 123, 117, 96, 110, 123, 135 121, 114, 139, 119, 132, 119, 104, 128 137, 121, 110, 125, 119, 137, 106, 139 110, 135, 117, 121, 130, 139, 125, 130 121, 125, 137, 119, 123, 128, 110, 135 128, 144, 125, 119, 114, 137, 135, 139 125, 146, 135, 123, 123, 121, 123, 132 137, 144, 132, 128, 135, 130, 121, 123 125, 130, 125, 128, 130, 114, 121, 119 123, 110, 102, 128, 132, 130, 123, 104 117, 106, 121, 106, 159, 121, 130, 146 130, 121, 130, 128, 117, 114, 117, 132 123, 125, 137, 137, 135, 119, 154, 121 154, 132, 117, 121, 132, 128, 117, 137 130, 130, 146, 139, 139, 146, 146, 132 137, 144, 164, 149, 149, 139, 128, 117 125, 121, 119, 119, 108, 112, 119, 108 110, 112, 112, 96, 110, 108, 100, 117 106, 108, 100, 125, 104, 112, 110, 110 102, 123, 90, 106, 108, 96, 123, 117 102, 104, 121, 106, 112, 123, 123, 96 112, 121, 100, 94, 102, 112, 79, 90 88, 83, 117, 106, 94, 114, 98, 106 108, 100, 102, 108, 98, 85, 90, 125 96, 100, 90, 100, 114, 88, 110, 104 90, 96, 98, 112, 114, 98, 100, 106 92, 106, 98, 98, 98, 100, 94, 90 72, 92, 83, 94, 92, 94, 96, 94 86, 85, 112, 98, 108, 79, 100, 88 92, 88, 77, 79, 98, 86, 108, 102 106, 106, 104, 94, 88, 119, 96, 106 94, 100, 100, 94, 96, 86, 100, 102 86, 102, 110, 121, 104, 98, 94, 96 86, 86, 102, 102, 86, 108, 90, 94 92, 96, 83, 86, 96, 96, 88, 90 112, 104, 98, 90, 100, 108, 96, 108 112, 119, 121, 123, 128, 98, 121, 135 123, 154, 142, 156, 161, 137, 142, 121 121, 123, 125, 144, 144, 121, 114, 125 100, 108, 108, 100, 121, 100, 83, 90 79, 86, 100, 98, 85, 86, 85, 86 106, 90, 94, 98, 85, 76, 79, 85 81, 94, 96, 83, 88, 72, 79, 85 90, 83, 98, 86, 83, 81, 110, 77 76, 79, 106, 94, 72, 76, 88, 86 96, 92, 96, 102, 74, 94, 102, 96 96, 88, 85, 77, 88, 77, 90, 112 92, 94, 96, 69, 98, 88, 79, 83 96, 98, 81, 72, 69, 76, 77, 98 76, 67, 90, 72, 72, 85, 79, 85 81, 72, 79, 76, 79, 81, 90, 86 74, 88, 79, 71, 67, 83, 79, 76 83, 77, 92, 72, 76, 76, 72, 72 62, 86, 102, 76, 67, 96, 102, 76 108, 94, 85, 76, 96, 79, 81, 71 85, 76, 71, 94, 88, 86, 92, 74 79, 81, 94, 76, 85, 77, 76, 79 86, 83, 86, 88, 88, 88, 77, 85 88, 66, 59, 72, 85, 72, 86, 66 98, 83, 92, 76, 94, 53, 76, 86 77, 92, 98, 72, 81, 72, 71, 67 81, 77, 71, 72, 79, 72, 85, 83 76, 64, 77, 69, 88, 59, 98, 100 79, 71, 88, 88, 71, 98, 72, 76 69, 69, 71, 85, 94, 67, 72, 66 83, 79, 72, 62, 79, 83, 71, 74 81, 67, 66, 92, 74, 71, 94, 67 59, 77, 85, 88, 96, 79, 86, 92 66, 83, 55, 77, 83, 83, 77, 76 79, 90, 77, 83, 74, 83, 90, 98 83, 96, 86, 104, 92, 83, 106, 106 110, 96, 96, 100, 88, 92, 100, 81 114, 94, 88, 83, 77, 86, 90, 85 76, 76, 79, 77, 86, 71, 90, 85 81, 102, 88, 94, 85, 79, 66, 77 98, 69, 96, 94, 98, 83, 98, 88 90, 77, 85, 112, 98, 104, 94, 88 85, 108, 85, 76, 81, 92, 117, 92 90, 112, 94, 88, 94, 104, 85, 94 110, 86, 100, 114, 110, 79, 106, 96 125, 102, 104, 104, 119, 110, 110, 117 104, 98, 110, 96, 135, 139, 125, 139 106, 137, 125, 169, 154, 149, 182, 161 199, 174, 188, 193, 228, 210, 237, 246 204, 222, 202, 231, 225, 213, 207, 213 185, 185, 180, 177, 151, 185, 164, 159 159, 156, 139, 144, 149, 123, 149, 159 159, 135, 154, 154, 139, 144, 146, 125 142, 144, 139, 135, 142, 149, 159, 137 161, 174, 151, 174, 164, 174, 190, 219 246, 262, 266, 299, 384, 484, 566, 605 488, 361, 331, 237, 207, 164, 151, 137 166, 142, 149, 125, 132, 132, 146, 104 114, 135, 125, 110, 112, 108, 112, 104 121, 108, 132, 110, 119, 106, 137, 132 123, 110, 117, 125, 104, 98, 106, 114 114, 123, 130, 139, 117, 121, 104, 137 146, 139, 156, 154, 144, 132, 139, 135 154, 142, 142, 164, 130, 121, 123, 135 102, 121, 108, 100, 83, 102, 106, 104 106, 100, 83, 125, 108, 112, 110, 102 114, 119, 117, 100, 104, 137, 96, 110 121, 119, 121, 125, 102, 128, 108, 121 112, 132, 125, 139, 137, 130, 114, 137 123, 154, 135, 125, 132, 142, 119, 137 112, 132, 114, 114, 110, 119, 123, 112 110, 110, 114, 125, 130, 130, 130, 121 121, 159, 151, 164, 146, 164, 166, 154 376, 144, 156, 159, 161, 135, 142, 132 132, 128, 121, 132, 137, 161, 128, 159 119, 119, 114, 137, 119, 125, 139, 139 164, 146, 135, 144, 149, 144, 146, 169 161, 172, 188, 156, 149, 144, 154, 123 119, 149, 139, 146, 106, 119, 130, 137 128, 128, 130, 117, 119, 128, 146, 128 135, 119, 149, 149, 149, 154, 177, 174 172, 210, 207, 164, 193, 159, 174, 151 142, 135, 172, 149, 174, 166, 156, 188 177, 180, 159, 188, 164, 164, 164, 182 164, 132, 156, 166, 182, 190, 185, 174 185, 166, 151, 185, 149, 156, 196, 190 188, 172, 164, 166, 151, 144, 132, 130 159, 161, 125, 142, 144, 123, 128, 144 142, 146, 121, 125, 121, 139, 128, 159 128, 166, 166, 164, 159, 190, 182, 216 225, 250, 289, 353, 404, 408, 506, 676 812, 888, 936, 1129, 1197, 1218, 1332, 1369 1384, 1218, 1089, 973, 870, 640, 538, 404 331, 292, 292, 269, 276, 237, 259, 237 182, 199, 225, 199, 185, 172, 185, 174 185, 164, 182, 164, 154, 202, 174, 190 210, 213, 207, 204, 210, 225, 234, 259 299, 279, 234, 259, 234, 259, 231, 262 243, 279, 246, 289, 279, 292, 286, 250 292, 317, 342, 324, 324, 335, 335, 346 357, 320, 299, 299, 279, 310, 253, 219 210, 204, 202, 185, 182, 188, 180, 159 177, 177, 174, 159, 169, 142, 169, 144 149, 139, 159, 112, 110, 137, 121, 130 98, 110, 121, 100, 119, 121, 98, 106 102, 106, 92, 108, 114, 94, 100, 104 117, 98, 106, 102, 119, 102, 102, 106 123, 125, 132, 112, 119, 132, 132, 154 142, 177, 146, 188, 219, 188, 196, 219 234, 231, 240, 253, 259, 253, 246, 231 204, 169, 174, 185, 121, 149, 139, 132 161, 139, 154, 156, 154, 159, 159, 180 174, 161, 166, 166, 164, 174, 161, 151 149, 149, 164, 142, 130, 172, 146, 130 151, 169, 142, 149, 159, 154, 149, 159 139, 154, 156, 130, 149, 144, 130, 149 154, 144, 132, 123, 132, 137, 114, 117 117, 137, 132, 139, 144, 159, 154, 169 174, 172, 164, 159, 213, 177, 213, 299 433, 538, 506, 388, 328, 350, 292, 222 185, 169, 130, 139, 135, 130, 149, 144 130, 149, 149, 142, 135, 130, 123, 132 137, 137, 154, 166, 164, 180, 196, 213 246, 240, 289, 272, 296, 299, 272, 269 243, 237, 199, 149, 161, 144, 159, 132 125, 123, 117, 104, 119, 137, 117, 102 117, 98, 123, 100, 94, 85, 79, 100 114, 100, 100, 92, 90, 88, 108, 96 72, 92, 86, 85, 100, 62, 83, 102 98, 110, 98, 77, 90, 100, 86, 79 88, 94, 74, 86, 92, 85, 77, 79 88, 94, 110, 96, 86, 331, 83, 94 100, 104, 98, 79, 96, 85, 112, 79 77, 100, 96, 100, 96, 112, 86, 79 108, 100, 96, 106, 106, 90, 110, 119 98, 106, 110, 86, 114, 110, 106, 102 106, 102, 114, 92, 104, 100, 119, 110 100, 110, 104, 125, 112, 121, 125, 117 142, 112, 121, 132, 110, 137, 125, 142 125, 146, 164, 172, 174, 137, 172, 185 180, 174, 196, 213, 207, 231, 234, 204 216, 207, 237, 246, 250, 216, 240, 240 225, 240, 262, 250, 225, 256, 259, 282 266, 282, 286, 282, 299, 286, 296, 289 269, 279, 262, 282, 253, 253, 253, 246 256, 210, 207, 266, 210, 190, 210, 185 202, 185, 193, 177, 182, 177, 174, 190 169, 182, 174, 182, 169, 204, 166, 172 166, 437, 177, 161, 169, 182, 130, 149 151, 154, 161, 154, 161, 146, 172, 169 151, 151, 144, 156, 164, 159, 135, 139 151, 144, 130, 144, 125, 142, 117, 146 132, 151, 139, 169, 196, 210, 199, 202 207, 243, 231, 240, 253, 256, 228, 259 240, 286, 272, 222, 231, 210, 190, 196 169, 188, 185, 161, 137, 196, 164, 177 146, 164, 137, 161, 151, 159, 144, 161 146, 139, 146, 135, 132, 132, 128, 174 164, 132, 154, 146, 154, 161, 149, 159 156, 164, 156, 177, 156, 166, 177, 188 156, 166, 172, 185, 161, 185, 172, 193 161, 199, 174, 166, 166, 174, 159, 137 159, 123, 121, 119, 130, 154, 112, 128 121, 117, 135, 114, 92, 112, 106, 114 117, 117, 125, 130, 125, 114, 128, 117 128, 125, 114, 121, 128, 128, 125, 121 117, 110, 132, 104, 108, 108, 130, 104 100, 130, 123, 119, 94, 106, 121, 106 123, 112, 106, 112, 125, 90, 100, 112 85, 100, 104, 92, 98, 114, 108, 117 106, 100, 114, 144, 130, 137, 144, 137 159, 144, 182, 169, 199, 210, 219, 256 240, 454, 262, 246, 243, 190, 180, 185 166, 128, 144, 100, 112, 110, 128, 119 104, 119, 114, 102, 130, 121, 121, 121 108, 112, 125, 139, 117, 100, 132, 119 117, 151, 132, 154, 149, 139, 139, 149 182, 166, 177, 166, 177, 159, 123, 137 119, 137, 130, 128, 94, 121, 110, 104 104, 119, 119, 104, 108, 119, 119, 108 90, 96, 119, 121, 88, 100, 114, 119 119, 130, 110, 121, 114, 114, 119, 130 125, 130, 119, 119, 135, 114, 137, 135 121, 117, 130, 102, 104, 123, 130, 94 128, 112, 121, 114, 123, 90, 104, 106 121, 123, 110, 102, 117, 135, 114, 108 125, 123, 102, 130, 125, 90, 125, 132 130, 108, 123, 98, 114, 123, 128, 114 112, 102, 137, 121, 144, 106, 110, 125 130, 123, 137, 137, 139, 149, 177, 154 180, 199, 190, 213, 202, 216, 199, 216 210, 185, 185, 190, 169, 169, 172, 154 130, 144, 137, 119, 108, 112, 104, 102 112, 106, 98, 88, 112, 85, 88, 92 106, 128, 117, 86, 117, 119, 106, 130 149, 144, 137, 128, 151, 132, 119, 112 112, 117, 104, 104, 112, 100, 106, 104 94, 92, 114, 117, 100, 104, 98, 104 98, 79, 108, 85, 100, 102, 92, 117 96, 90, 92, 92, 108, 104, 121, 104 102, 106, 123, 104, 146, 110, 108, 128 108, 110, 108, 130, 106, 112, 110, 110 86, 100, 96, 98, 88, 100, 79, 86 94, 104, 90, 112, 100, 125, 121, 135 154, 142, 164, 161, 159, 174, 156, 151 139, 149, 144, 123, 137, 139, 121, 130 121, 130, 125, 135, 130, 130, 144, 142 119, 125, 142, 125, 137, 135, 156, 159 139, 144, 166, 199, 185, 207, 240, 243 259, 253, 266, 246, 262, 289, 253, 256 222, 237, 202, 204, 174, 202, 161, 216 204, 237, 216, 225, 207, 213, 199, 222 219, 213, 177, 144, 130, 119, 123, 139 123, 108, 108, 96, 98, 98, 104, 94 66, 83, 85, 106, 85, 104, 77, 85 79, 77, 79, 88, 83, 98, 94, 94 94, 106, 96, 77, 96, 85, 98, 100 85, 85, 81, 79, 88, 79, 88, 88 69, 85, 96, 88, 85, 69, 100, 85 88, 90, 79, 108, 86, 81, 92, 96 90, 88, 90, 102, 88, 94, 79, 88 106, 102, 102, 102, 98, 102, 102, 98 121, 130, 132, 114, 112, 112, 114, 106 117, 108, 88, 88, 106, 106, 104, 86 79, 79, 77, 98, 90, 79, 85, 90 88, 77, 100, 96, 81, 90, 92, 94 98, 79, 92, 96, 98, 85, 102, 90 88, 102, 98, 102, 104, 117, 110, 119 96, 96, 108, 114, 100, 121, 128, 104 108, 130, 121, 388, 106, 94, 100, 96 85, 92, 81, 67, 72, 69, 71, 92 83, 77, 76, 69, 67, 74, 88, 90 83, 85, 100, 88, 83, 88, 92, 81 102, 86, 74, 106, 114, 96, 85, 86 100, 74, 83, 72, 94, 72, 83, 88 92, 81, 92, 108, 67, 88, 83, 92 100, 110, 98, 123, 86, 104, 85, 117 139, 110, 112, 164, 137, 174, 169, 210 216, 266, 256, 335, 299, 306, 320, 313 317, 346, 286, 231, 225, 193, 188, 172 193, 119, 119, 119, 114, 90, 110, 102 102, 121, 92, 102, 94, 125, 100, 121 130, 128, 106, 106, 98, 117, 121, 90 108, 86, 90, 106, 90, 94, 106, 100 110, 100, 106, 110, 114, 125, 112, 114 119, 104, 96, 88, 104, 96, 85, 102 100, 94, 88, 98, 102, 90, 85, 85 79, 86, 77, 90, 88, 77, 85, 85 83, 88, 79, 71, 83, 61, 66, 67 77, 61, 71, 64, 74, 59, 77, 53 74, 83, 76, 67, 59, 74, 88, 83 62, 77, 86, 85, 88, 79, 100, 106 96, 83, 94, 88, 98, 74, 369, 96 85, 114, 104, 76, 231, 76, 69, 92 90, 96, 98, 62, 100, 88, 85, 94 90, 76, 117, 79, 86, 90, 86, 110 92, 92, 100, 114, 88, 104, 88, 112 110, 117, 123, 130, 125, 119, 98, 108 94, 106, 104, 96, 88, 125, 98, 88 119, 110, 110, 94, 100, 108, 117, 102 104, 119, 88, 106, 100, 94, 114, 108 123, 114, 135, 146, 117, 121, 110, 125 137, 125, 139, 137, 125, 132, 139, 125 132, 132, 125, 130, 114, 112, 110, 130 144, 117, 137, 130, 123, 121, 130, 142 135, 137, 132, 130, 144, 139, 119, 114 117, 119, 128, 144, 125, 130, 130, 149 137, 139, 154, 149, 166, 172, 146, 199 190, 177, 193, 213, 210, 210, 172, 207 174, 180, 166, 185, 161, 180, 169, 154 154, 174, 172, 151, 164, 156, 174, 193 185, 169, 185, 164, 174, 199, 130, 142 146, 161, 142, 151, 137, 161, 154, 149 139, 151, 139, 139, 149, 142, 125, 123 137, 146, 142, 146, 166, 156, 161, 137 132, 130, 130, 142, 104, 135, 123, 130 119, 104, 135, 121, 128, 137, 130, 144 123, 132, 137, 144, 146, 144, 139, 166 190, 159, 149, 190, 172, 164, 172, 172 159, 169, 142, 172, 156, 149, 146, 128 132, 128, 137, 108, 125, 121, 112, 128 114, 121, 102, 106, 108, 114, 117, 92 119, 92, 117, 114, 117, 117, 100, 123 110, 112, 106, 125, 114, 142, 128, 132 121, 117, 104, 117, 121, 130, 142, 121 112, 125, 119, 100, 110, 90, 121, 94 96, 106, 117, 110, 104, 114, 110, 110 108, 98, 83, 98, 102, 102, 88, 104 102, 98, 100, 102, 106, 94, 96, 86 114, 98, 83, 112, 108, 94, 98, 98 92, 96, 125, 108, 106, 104, 96, 100 94, 114, 104, 94, 90, 108, 102, 123 112, 98, 117, 106, 108, 102, 104, 104 96, 117, 98, 112, 106, 125, 90, 90 98, 104, 104, 86, 92, 110, 112, 121 108, 128, 125, 96, 121, 114, 114, 104 121, 98, 100, 123, 110, 108, 125, 114 102, 119, 106, 121, 104, 121, 123, 137 125, 135, 137, 146, 130, 139, 159, 196 174, 216, 216, 246, 259, 250, 317, 299 317, 339, 350, 310, 339, 339, 279, 276 243, 269, 225, 225, 207, 204, 164, 164 139, 154, 142, 130, 142, 121, 139, 104 149, 135, 142, 137, 144, 121, 137, 123 146, 142, 132, 154, 161, 144, 137, 146 177, 149, 128, 149, 151, 146, 169, 144 151, 139, 169, 174, 159, 146, 172, 144 151, 172, 135, 154, 166, 177, 130, 156 180, 156, 190, 174, 169, 154, 204, 188 182, 196, 193, 202, 207, 219, 222, 199 219, 240, 188, 237, 202, 237, 222, 219 237, 216, 216, 231, 225, 199, 231, 222 196, 199, 202, 196, 188, 196, 213, 161 161, 164, 159, 182, 188, 177, 161, 161 177, 169, 188, 164, 130, 161, 174, 159 161, 146, 166, 137, 144, 142, 144, 142 149, 146, 130, 128, 142, 128, 135, 137 121, 132, 125, 119, 130, 104, 110, 121 98, 123, 128, 106, 130, 112, 104, 108 104, 106, 112, 108, 110, 112, 102, 121 130, 112, 121, 114, 110, 104, 104, 123 106, 92, 88, 100, 94, 102, 104, 108 94, 90, 106, 92, 106, 92, 121, 108 110, 104, 123, 106, 96, 110, 119, 137 119, 125, 125, 108, 108, 114, 130, 114 132, 132, 161, 169, 132, 117, 139, 144 142, 137, 117, 108, 110, 112, 119, 114 112, 110, 94, 114, 112, 117, 96, 92 77, 90, 108, 102, 117, 88, 104, 106 90, 112, 106, 96, 106, 108, 125, 106 123, 121, 94, 102, 112, 100, 79, 104 106, 106, 123, 112, 102, 98, 100, 108 94, 98, 121, 106, 130, 108, 94, 114 123, 114, 96, 114, 106, 112, 108, 102 112, 102, 108, 92, 98, 88, 92, 94 86, 98, 104, 102, 106, 110, 98, 119 117, 79, 110, 132, 117, 132, 121, 102 98, 130, 137, 128, 108, 112, 104, 104 121, 128, 108, 128, 110, 123, 119, 106 121, 125, 114, 100, 100, 121, 106, 112 106, 108, 112, 104, 104, 119, 108, 100 100, 86, 85, 102, 98, 100, 94, 81 72, 90, 85, 98, 71, 85, 66, 81 102, 83, 106, 92, 96, 77, 88, 110 106, 106, 90, 98, 96, 121, 88, 108 102, 100, 104, 104, 112, 125, 119, 119 119, 108, 130, 104, 117, 110, 125, 117 110, 121, 110, 119, 106, 132, 121, 149 135, 149, 180, 196, 213, 222, 228, 213 231, 231, 219, 222, 204, 174, 151, 185 188, 190, 180, 202, 202, 225, 225, 219 240, 282, 259, 279, 342, 289, 282, 282 262, 282, 262, 272, 272, 282, 250, 225 216, 196, 207, 164, 164, 149, 182, 161 132, 121, 117, 110, 119, 114, 83, 106 104, 100, 112, 110, 102, 106, 112, 106 90, 117, 98, 108, 108, 117, 90, 108 106, 108, 94, 102, 119, 108, 110, 123 96, 121, 110, 123, 132, 125, 121, 117 130, 139, 123, 119, 128, 132, 106, 121 137, 139, 123, 121, 112, 132, 114, 137 114, 110, 112, 112, 151, 114, 132, 142 125, 123, 139, 128, 108, 123, 117, 117 125,/