SampleIdent,907A-3-2/98,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 8-aug-1993 23:05,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 92, 88, 86, 92, 77, 86, 98, 77 86, 90, 104, 90, 90, 96, 94, 74 71, 102, 98, 90, 100, 102, 119, 100 77, 104, 86, 96, 94, 94, 110, 100 98, 110, 102, 92, 98, 98, 102, 114 114, 106, 94, 90, 119, 112, 117, 98 96, 108, 121, 100, 85, 112, 119, 112 106, 104, 121, 117, 123, 123, 104, 100 117, 112, 108, 104, 121, 121, 108, 102 139, 130, 100, 119, 110, 121, 137, 110 125, 121, 119, 121, 119, 121, 125, 104 108, 139, 112, 121, 137, 114, 123, 128 123, 135, 117, 121, 128, 108, 128, 130 132, 112, 130, 117, 125, 121, 125, 128 121, 114, 119, 112, 102, 123, 119, 130 123, 104, 121, 130, 117, 128, 125, 110 130, 372, 112, 112, 125, 132, 135, 117 135, 119, 128, 100, 96, 110, 119, 106 125, 114, 110, 130, 117, 112, 130, 112 92, 100, 130, 130, 106, 137, 121, 106 121, 132, 106, 117, 110, 149, 100, 79 119, 110, 128, 119, 121, 117, 104, 121 119, 132, 149, 130, 119, 135, 139, 151 139, 128, 135, 139, 151, 149, 123, 139 132, 128, 130, 132, 132, 106, 112, 117 123, 130, 106, 112, 100, 110, 112, 83 92, 88, 132, 342, 94, 110, 102, 135 117, 104, 98, 102, 98, 100, 108, 108 92, 104, 100, 92, 100, 98, 85, 88 112, 104, 94, 100, 83, 79, 106, 94 100, 85, 90, 88, 117, 90, 94, 85 92, 88, 79, 92, 86, 108, 96, 100 98, 69, 81, 90, 106, 88, 88, 74 81, 108, 104, 96, 96, 104, 117, 88 98, 88, 92, 102, 83, 85, 102, 86 79, 94, 96, 106, 77, 92, 85, 90 74, 106, 69, 83, 106, 100, 110, 81 76, 94, 90, 94, 112, 98, 76, 76 83, 88, 110, 88, 96, 76, 86, 88 90, 86, 77, 100, 102, 96, 86, 86 94, 106, 85, 85, 79, 83, 98, 110 83, 83, 88, 92, 83, 110, 83, 86 79, 96, 96, 90, 88, 104, 86, 88 88, 100, 94, 92, 106, 110, 92, 110 114, 106, 96, 98, 121, 94, 88, 104 130, 139, 128, 128, 139, 130, 110, 130 135, 161, 125, 114, 149, 149, 139, 125 119, 139, 132, 114, 83, 104, 88, 86 98, 92, 90, 83, 98, 86, 90, 79 90, 102, 94, 88, 86, 76, 83, 77 71, 85, 88, 92, 83, 90, 104, 90 88, 77, 86, 98, 92, 92, 69, 88 94, 90, 85, 79, 83, 92, 79, 86 90, 77, 86, 83, 106, 83, 92, 88 92, 108, 96, 94, 90, 67, 96, 86 85, 102, 86, 100, 94, 106, 85, 98 71, 90, 85, 102, 62, 79, 79, 71 83, 79, 88, 83, 72, 77, 76, 85 94, 77, 77, 83, 72, 77, 90, 71 88, 94, 71, 83, 79, 83, 79, 79 77, 81, 74, 74, 90, 72, 67, 77 86, 86, 88, 71, 76, 66, 83, 98 96, 92, 92, 85, 94, 92, 74, 100 81, 96, 74, 64, 76, 72, 94, 76 67, 71, 102, 88, 83, 79, 64, 79 72, 62, 66, 83, 62, 74, 72, 52 71, 76, 85, 85, 76, 71, 76, 85 85, 79, 79, 76, 76, 88, 85, 77 72, 72, 74, 77, 66, 76, 85, 62 66, 72, 72, 62, 96, 76, 71, 66 86, 77, 62, 79, 58, 76, 55, 88 83, 86, 71, 81, 66, 62, 66, 64 77, 62, 76, 58, 71, 62, 67, 66 83, 86, 85, 77, 74, 85, 74, 77 83, 72, 79, 72, 67, 62, 86, 59 62, 71, 83, 72, 76, 77, 77, 88 72, 59, 76, 83, 72, 66, 76, 64 94, 83, 81, 72, 74, 77, 86, 81 77, 59, 81, 94, 96, 83, 98, 102 94, 94, 112, 94, 100, 110, 100, 100 100, 86, 92, 88, 86, 86, 74, 85 81, 67, 85, 85, 100, 74, 76, 62 77, 83, 79, 90, 90, 83, 96, 88 69, 71, 72, 85, 66, 81, 86, 66 74, 72, 69, 92, 79, 85, 83, 98 69, 108, 92, 86, 90, 102, 108, 85 110, 96, 102, 94, 98, 92, 98, 100 83, 112, 86, 85, 90, 88, 81, 94 102, 76, 72, 108, 98, 98, 128, 96 94, 110, 110, 108, 98, 135, 130, 119 106, 119, 130, 119, 132, 151, 151, 146 177, 149, 154, 166, 185, 210, 213, 190 199, 193, 213, 240, 213, 210, 204, 199 185, 213, 202, 185, 161, 151, 151, 164 130, 123, 161, 151, 139, 137, 142, 149 132, 139, 130, 128, 137, 130, 135, 130 123, 125, 117, 130, 121, 121, 139, 144 137, 139, 123, 146, 146, 156, 182, 213 225, 272, 246, 335, 350, 361, 346, 369 357, 376, 320, 335, 253, 243, 161, 164 182, 135, 144, 137, 114, 112, 119, 108 96, 125, 112, 125, 306, 92, 98, 108 96, 119, 102, 96, 94, 108, 112, 98 121, 112, 108, 119, 100, 110, 102, 114 110, 445, 102, 102, 98, 98, 125, 102 98, 125, 114, 123, 146, 164, 139, 177 177, 193, 199, 193, 196, 190, 159, 172 151, 130, 114, 114, 121, 114, 90, 85 94, 88, 88, 98, 108, 88, 102, 102 104, 98, 94, 108, 104, 108, 106, 112 96, 94, 94, 102, 110, 104, 104, 104 100, 110, 114, 98, 128, 114, 128, 117 135, 119, 130, 132, 121, 128, 149, 121 94, 110, 106, 119, 114, 102, 117, 112 92, 125, 96, 100, 119, 110, 110, 121 142, 142, 142, 154, 151, 207, 240, 228 237, 256, 188, 228, 180, 159, 188, 159 149, 144, 144, 146, 142, 121, 135, 135 121, 119, 132, 137, 108, 125, 159, 144 159, 137, 144, 154, 169, 164, 177, 161 204, 182, 190, 182, 213, 185, 202, 169 159, 169, 135, 128, 123, 104, 130, 117 117, 110, 125, 104, 114, 112, 121, 128 117, 132, 132, 135, 154, 121, 121, 132 137, 132, 154, 151, 380, 130, 135, 144 137, 132, 154, 164, 177, 159, 193, 180 199, 196, 196, 190, 180, 177, 182, 182 188, 185, 202, 199, 174, 196, 180, 174 159, 180, 185, 196, 172, 166, 142, 159 164, 154, 159, 166, 117, 128, 144, 144 137, 128, 123, 125, 123, 125, 125, 154 149, 128, 106, 135, 114, 117, 276, 137 154, 146, 144, 149, 151, 166, 174, 174 196, 207, 207, 266, 324, 392, 445, 524 610, 724, 900, 967, 1183, 1406, 1640, 1815 1918, 2061, 2134, 2256, 2098, 1927, 1521, 1239 973, 697, 511, 384, 299, 286, 289, 250 246, 216, 216, 228, 196, 199, 188, 199 180, 159, 169, 169, 151, 174, 159, 151 144, 151, 177, 172, 207, 210, 210, 199 185, 228, 246, 219, 219, 219, 210, 250 219, 317, 317, 292, 296, 339, 365, 353 380, 433, 445, 445, 467, 441, 576, 630 686, 692, 702, 713, 645, 625, 449, 441 380, 346, 306, 256, 216, 228, 202, 204 210, 164, 193, 146, 174, 177, 139, 164 149, 135, 149, 123, 154, 151, 154, 151 154, 137, 137, 128, 114, 123, 110, 102 110, 112, 83, 112, 106, 88, 96, 98 106, 110, 94, 119, 98, 137, 86, 114 108, 125, 96, 112, 128, 106, 108, 108 85, 106, 98, 123, 108, 90, 121, 77 102, 94, 100, 110, 102, 117, 104, 96 112, 96, 106, 106, 104, 100, 128, 139 128, 130, 149, 132, 142, 146, 144, 174 161, 177, 172, 159, 174, 172, 130, 166 121, 156, 130, 135, 149, 142, 146, 159 156, 149, 135, 144, 137, 132, 149, 139 135, 159, 169, 164, 154, 159, 154, 146 190, 166, 139, 156, 164, 156, 123, 137 128, 128, 121, 132, 128, 117, 110, 142 130, 164, 159, 210, 188, 228, 228, 237 262, 317, 365, 400, 380, 372, 276, 310 253, 207, 169, 154, 149, 125, 139, 142 137, 154, 132, 142, 135, 154, 144, 130 164, 135, 121, 121, 144, 159, 123, 139 166, 182, 207, 193, 225, 219, 234, 234 216, 243, 207, 202, 172, 156, 144, 137 132, 112, 106, 106, 117, 110, 94, 114 92, 117, 100, 100, 92, 85, 90, 98 94, 98, 94, 79, 76, 90, 76, 96 92, 98, 94, 77, 83, 83, 77, 86 85, 90, 72, 77, 79, 76, 81, 72 71, 67, 62, 58, 71, 71, 67, 83 72, 76, 72, 69, 86, 92, 76, 83 90, 88, 85, 85, 83, 67, 88, 71 72, 83, 96, 72, 74, 79, 90, 96 83, 98, 96, 94, 90, 100, 96, 100 92, 94, 90, 96, 98, 102, 102, 94 106, 100, 94, 92, 98, 104, 90, 86 104, 125, 96, 121, 121, 135, 121, 108 112, 110, 102, 114, 112, 125, 110, 132 125, 102, 121, 114, 112, 123, 135, 137 156, 166, 149, 154, 185, 180, 196, 193 202, 213, 216, 213, 182, 228, 199, 222 213, 234, 210, 231, 231, 276, 250, 256 246, 279, 266, 259, 250, 282, 286, 324 303, 282, 317, 317, 299, 296, 292, 296 292, 269, 250, 250, 210, 219, 182, 225 199, 185, 156, 174, 190, 172, 185, 204 222, 222, 193, 151, 177, 177, 149, 159 135, 128, 137, 137, 149, 139, 142, 130 125, 144, 146, 123, 130, 137, 132, 149 135, 132, 142, 123, 132, 151, 166, 123 137, 128, 144, 137, 135, 114, 128, 104 117, 117, 130, 159, 119, 159, 156, 169 177, 185, 216, 228, 262, 292, 269, 331 320, 357, 324, 328, 276, 272, 279, 262 243, 234, 207, 180, 169, 199, 204, 137 172, 174, 144, 166, 169, 151, 185, 154 169, 154, 172, 174, 188, 164, 174, 146 159, 154, 151, 121, 169, 137, 146, 166 161, 166, 177, 164, 174, 159, 156, 159 199, 182, 188, 185, 196, 177, 172, 190 207, 185, 188, 164, 177, 219, 159, 182 169, 159, 161, 169, 161, 154, 137, 128 125, 121, 106, 94, 114, 130, 119, 108 96, 88, 110, 112, 135, 112, 100, 128 125, 125, 146, 130, 128, 114, 123, 130 112, 94, 139, 96, 88, 108, 96, 96 102, 119, 102, 100, 114, 88, 106, 96 102, 102, 110, 112, 114, 117, 117, 108 92, 92, 96, 94, 106, 119, 96, 98 86, 102, 98, 85, 104, 104, 106, 94 117, 149, 135, 182, 172, 202, 222, 199 269, 272, 276, 320, 276, 272, 240, 259 190, 172, 182, 146, 139, 110, 119, 121 98, 114, 110, 110, 117, 90, 117, 92 106, 108, 96, 117, 121, 135, 108, 119 112, 123, 128, 149, 128, 142, 132, 132 164, 164, 182, 177, 164, 182, 172, 154 169, 164, 151, 123, 117, 121, 110, 104 112, 98, 92, 88, 96, 85, 106, 96 108, 85, 94, 100, 98, 90, 96, 117 112, 96, 130, 96, 108, 100, 117, 114 114, 106, 123, 117, 121, 135, 123, 142 114, 130, 106, 104, 121, 121, 112, 94 110, 119, 106, 92, 98, 88, 108, 104 88, 90, 114, 108, 94, 117, 123, 106 119, 130, 119, 137, 117, 108, 119, 102 110, 117, 114, 114, 119, 114, 112, 108 121, 110, 128, 132, 123, 130, 128, 137 137, 112, 135, 130, 137, 125, 144, 154 182, 177, 237, 237, 262, 262, 272, 279 289, 259, 276, 276, 240, 210, 213, 177 185, 144, 130, 125, 123, 108, 114, 112 128, 144, 100, 119, 106, 112, 121, 151 130, 182, 164, 130, 121, 130, 123, 125 151, 96, 112, 94, 85, 88, 86, 104 92, 94, 88, 77, 86, 94, 102, 100 90, 100, 98, 100, 94, 90, 110, 100 104, 117, 102, 98, 108, 104, 125, 94 104, 106, 100, 94, 98, 117, 117, 106 128, 130, 132, 144, 128, 119, 125, 123 123, 130, 130, 106, 106, 119, 112, 94 96, 100, 92, 88, 92, 98, 100, 100 90, 96, 128, 144, 130, 154, 128, 154 151, 149, 137, 180, 149, 151, 149, 135 144, 135, 128, 117, 132, 125, 106, 137 146, 146, 137, 154, 169, 132, 135, 166 164, 159, 159, 156, 130, 132, 128, 182 164, 144, 149, 169, 156, 188, 172, 202 210, 222, 225, 246, 282, 262, 262, 259 276, 222, 259, 225, 246, 172, 216, 210 219, 222, 256, 243, 213, 250, 204, 196 243, 196, 216, 193, 193, 177, 164, 151 125, 137, 114, 106, 92, 98, 98, 106 104, 77, 100, 90, 81, 81, 76, 74 85, 86, 94, 85, 69, 77, 85, 76 88, 74, 81, 79, 62, 90, 79, 67 85, 77, 83, 83, 76, 71, 76, 76 71, 62, 81, 77, 79, 81, 79, 67 74, 66, 85, 108, 86, 72, 94, 71 90, 92, 77, 77, 83, 53, 72, 71 77, 71, 61, 62, 71, 67, 77, 83 77, 74, 79, 71, 64, 61, 79, 66 92, 85, 74, 64, 77, 66, 59, 69 83, 77, 59, 77, 86, 88, 77, 79 90, 76, 98, 104, 90, 86, 94, 100 121, 90, 106, 121, 98, 102, 104, 114 106, 106, 96, 112, 96, 108, 72, 67 100, 102, 102, 88, 92, 72, 86, 74 90, 83, 85, 96, 71, 86, 71, 90 86, 71, 85, 85, 66, 100, 86, 74 85, 74, 69, 79, 83, 81, 76, 76 88, 86, 90, 86, 83, 100, 92, 104 90, 110, 102, 94, 96, 83, 117, 94 94, 88, 94, 77, 88, 88, 86, 83 104, 90, 98, 85, 88, 96, 86, 108 102, 98, 98, 92, 119, 119, 137, 142 102, 137, 130, 172, 154, 164, 190, 210 202, 219, 296, 331, 365, 404, 424, 467 420, 454, 458, 412, 404, 350, 266, 276 231, 228, 177, 154, 137, 149, 123, 108 110, 106, 102, 110, 119, 135, 119, 121 137, 125, 144, 125, 123, 114, 117, 104 123, 104, 100, 119, 96, 86, 76, 94 98, 92, 102, 102, 92, 114, 117, 98 104, 125, 110, 117, 123, 108, 112, 102 104, 90, 104, 76, 90, 83, 85, 77 92, 67, 86, 85, 90, 86, 76, 79 72, 67, 59, 58, 66, 62, 67, 67 76, 67, 71, 74, 62, 64, 67, 69 56, 67, 71, 66, 71, 66, 71, 92 66, 77, 71, 66, 79, 85, 86, 88 79, 85, 62, 74, 85, 83, 90, 83 86, 98, 96, 85, 79, 110, 92, 76 71, 83, 79, 92, 83, 102, 85, 92 98, 92, 86, 79, 77, 88, 72, 88 102, 96, 104, 76, 100, 96, 98, 117 86, 90, 104, 100, 85, 117, 110, 117 98, 132, 121, 128, 121, 130, 128, 137 125, 125, 121, 90, 112, 130, 104, 102 119, 92, 100, 88, 112, 104, 117, 108 102, 88, 123, 106, 123, 125, 112, 119 119, 128, 128, 117, 125, 110, 125, 106 106, 154, 119, 98, 128, 132, 104, 106 125, 108, 132, 106, 119, 119, 128, 130 130, 139, 121, 121, 117, 117, 119, 114 114, 117, 123, 137, 128, 121, 108, 130 121, 144, 125, 132, 128, 144, 144, 146 202, 216, 210, 207, 246, 250, 246, 243 246, 222, 228, 219, 213, 204, 177, 210 174, 174, 172, 164, 174, 174, 188, 156 188, 172, 156, 185, 216, 188, 188, 177 151, 151, 137, 151, 149, 164, 172, 146 142, 132, 142, 132, 137, 159, 121, 137 112, 130, 144, 130, 146, 123, 132, 137 121, 139, 137, 132, 137, 130, 144, 151 132, 106, 121, 137, 108, 130, 119, 114 132, 114, 119, 130, 135, 112, 146, 132 121, 139, 149, 139, 159, 164, 182, 166 144, 144, 146, 128, 144, 142, 112, 123 135, 112, 108, 114, 98, 114, 94, 110 102, 96, 90, 88, 106, 94, 102, 117 112, 98, 112, 86, 96, 98, 96, 106 110, 108, 98, 96, 102, 102, 94, 104 102, 114, 112, 96, 117, 110, 83, 96 96, 106, 106, 86, 94, 108, 121, 117 92, 110, 114, 96, 110, 114, 96, 108 112, 112, 100, 106, 102, 92, 100, 102 96, 92, 96, 86, 98, 104, 86, 96 104, 83, 106, 98, 77, 106, 104, 94 104, 98, 94, 88, 96, 114, 76, 83 96, 90, 96, 88, 106, 102, 96, 119 110, 121, 108, 108, 139, 110, 137, 94 121, 112, 121, 128, 96, 121, 114, 114 128, 102, 90, 112, 112, 104, 112, 102 106, 90, 112, 88, 110, 123, 100, 112 121, 100, 102, 121, 132, 102, 108, 119 114, 121, 106, 137, 130, 139, 135, 142 128, 132, 135, 151, 137, 149, 144, 164 161, 180, 188, 210, 250, 289, 289, 365 445, 493, 462, 488, 520, 493, 557, 502 449, 416, 369, 331, 339, 339, 310, 292 237, 196, 172, 128, 130, 128, 132, 144 121, 132, 144, 108, 125, 125, 137, 110 142, 139, 114, 137, 119, 108, 142, 128 130, 130, 144, 125, 146, 137, 139, 130 130, 154, 139, 146, 121, 149, 123, 139 149, 151, 146, 146, 174, 125, 146, 156 174, 139, 196, 159, 164, 156, 161, 174 180, 164, 188, 174, 196, 196, 190, 199 213, 190, 228, 185, 225, 234, 207, 231 237, 216, 240, 202, 231, 237, 228, 237 234, 231, 210, 202, 222, 199, 166, 193 196, 204, 177, 172, 172, 154, 169, 169 151, 161, 180, 169, 164, 166, 159, 180 144, 139, 151, 149, 144, 146, 125, 135 110, 130, 128, 132, 144, 125, 130, 108 130, 114, 106, 135, 125, 106, 125, 114 114, 110, 108, 94, 125, 106, 92, 90 112, 112, 74, 106, 114, 104, 100, 85 110, 106, 121, 92, 94, 110, 114, 100 94, 102, 96, 98, 102, 102, 110, 94 86, 88, 94, 106, 114, 86, 121, 117 102, 114, 121, 100, 106, 100, 100, 117 119, 125, 100, 119, 94, 110, 98, 154 159, 139, 139, 161, 151, 164, 177, 193 216, 222, 216, 190, 156, 154, 128, 137 149, 146, 154, 164, 144, 92, 117, 96 110, 108, 92, 86, 83, 106, 100, 88 92, 100, 92, 114, 96, 104, 81, 88 90, 81, 86, 114, 94, 85, 100, 114 117, 100, 98, 114, 119, 104, 121, 108 96, 110, 125, 110, 112, 112, 117, 108 117, 102, 117, 98, 108, 130, 106, 114 88, 108, 110, 125, 112, 102, 108, 106 108, 94, 121, 106, 110, 96, 102, 94 102, 104, 119, 108, 104, 121, 106, 121 123, 110, 98, 102, 108, 96, 104, 106 110, 85, 102, 128, 114, 112, 135, 110 114, 108, 119, 110, 108, 121, 106, 125 110, 112, 88, 98, 114, 102, 102, 108 104, 98, 85, 85, 108, 79, 88, 106 72, 98, 83, 88, 88, 100, 108, 79 81, 94, 79, 94, 90, 94, 79, 94 96, 104, 98, 102, 92, 96, 83, 96 86, 100, 94, 119, 96, 104, 108, 104 106, 114, 108, 102, 119, 114, 98, 98 132, 112, 121, 137, 110, 112, 139, 119 149, 172, 180, 202, 219, 234, 282, 282 313, 317, 331, 292, 303, 225, 246, 216 219, 262, 282, 231, 243, 237, 282, 237 289, 289, 310, 346, 353, 369, 369, 392 350, 365, 380, 369, 384, 412, 365, 400 392, 339, 279, 279, 240, 219, 213, 204 210, 204, 182, 169, 142, 144, 125, 128 94, 106, 125, 92, 110, 114, 114, 86 86, 100, 94, 123, 100, 100, 123, 296 112, 128, 114, 102, 119, 144, 106, 114 125, 128, 119, 132, 142, 132, 123, 135 117, 144, 164, 125, 146, 142, 135, 151 156, 137, 139, 144, 135, 149, 117, 125 130, 144, 144, 125, 114, 114, 108, 92 92, 125, 119, 121, 121, 137, 128, 106 114,/