SampleIdent,907A-3-6/97,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 9-aug-1993 0:01,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 79, 112, 90, 83, 79, 104, 92, 96 94, 100, 90, 88, 106, 74, 96, 106 96, 104, 98, 92, 83, 100, 100, 102 94, 106, 98, 92, 77, 104, 98, 83 85, 94, 92, 90, 106, 102, 102, 106 114, 110, 94, 117, 98, 110, 83, 86 94, 108, 108, 100, 125, 112, 98, 90 88, 94, 66, 102, 96, 94, 110, 102 98, 130, 112, 108, 123, 121, 117, 100 114, 121, 112, 128, 130, 94, 108, 119 106, 117, 90, 102, 104, 108, 100, 104 94, 96, 121, 102, 119, 123, 114, 137 128, 100, 114, 104, 119, 128, 106, 119 110, 108, 346, 110, 112, 121, 119, 98 117, 128, 90, 112, 117, 98, 117, 121 119, 102, 125, 96, 117, 110, 88, 117 108, 114, 121, 132, 96, 117, 110, 123 121, 119, 119, 88, 112, 112, 104, 106 96, 123, 94, 88, 104, 114, 121, 121 180, 123, 94, 110, 114, 108, 130, 110 128, 128, 112, 102, 130, 104, 117, 110 121, 104, 112, 139, 128, 114, 112, 132 119, 144, 144, 121, 130, 130, 144, 112 117, 144, 125, 137, 132, 125, 139, 137 119, 119, 144, 121, 90, 119, 132, 110 114, 117, 117, 108, 272, 110, 106, 108 114, 100, 98, 114, 106, 108, 110, 96 114, 100, 94, 108, 102, 79, 98, 112 108, 102, 90, 96, 102, 106, 112, 112 114, 86, 96, 94, 104, 86, 100, 114 86, 85, 94, 100, 119, 88, 92, 88 98, 114, 96, 83, 86, 108, 98, 98 86, 108, 88, 83, 112, 100, 98, 112 94, 92, 100, 96, 96, 86, 98, 96 86, 100, 86, 108, 98, 104, 106, 100 83, 94, 96, 94, 88, 106, 92, 102 98, 106, 77, 96, 86, 92, 88, 79 96, 90, 104, 92, 96, 102, 94, 76 102, 92, 85, 85, 83, 83, 98, 92 85, 86, 88, 83, 86, 79, 86, 86 104, 88, 106, 106, 92, 86, 92, 86 85, 88, 92, 77, 81, 98, 98, 96 88, 100, 94, 90, 102, 85, 102, 67 102, 92, 83, 90, 104, 108, 98, 108 104, 96, 114, 104, 88, 104, 132, 130 112, 123, 135, 119, 110, 149, 121, 149 119, 135, 139, 146, 130, 146, 149, 137 132, 130, 144, 114, 117, 94, 110, 90 85, 98, 86, 94, 86, 90, 79, 86 72, 83, 98, 77, 83, 94, 79, 92 76, 83, 106, 74, 77, 86, 67, 77 77, 81, 86, 86, 76, 77, 92, 74 86, 85, 92, 83, 67, 72, 96, 85 81, 85, 90, 66, 98, 96, 104, 88 90, 81, 96, 100, 88, 96, 79, 86 88, 88, 79, 104, 90, 85, 90, 81 92, 79, 81, 86, 71, 77, 72, 79 72, 76, 72, 77, 81, 77, 83, 79 106, 67, 96, 85, 67, 85, 83, 79 66, 85, 72, 98, 71, 85, 90, 59 72, 79, 76, 67, 83, 94, 79, 86 86, 85, 74, 83, 72, 88, 76, 86 81, 79, 90, 59, 83, 69, 83, 74 66, 76, 83, 92, 74, 81, 66, 79 86, 76, 90, 86, 81, 79, 64, 67 69, 72, 72, 79, 88, 85, 85, 66 74, 86, 83, 83, 71, 81, 86, 79 96, 76, 76, 86, 90, 86, 69, 66 67, 64, 74, 71, 76, 59, 64, 50 86, 85, 94, 76, 79, 86, 81, 71 76, 81, 59, 77, 62, 59, 79, 79 56, 71, 77, 88, 74, 64, 77, 76 71, 76, 76, 81, 67, 59, 81, 88 76, 76, 67, 67, 85, 92, 76, 86 67, 79, 86, 72, 106, 59, 85, 76 72, 74, 72, 72, 62, 72, 77, 76 81, 86, 88, 85, 94, 62, 77, 72 71, 56, 81, 81, 69, 86, 79, 85 90, 85, 76, 102, 88, 94, 88, 94 92, 85, 96, 98, 100, 86, 79, 96 104, 100, 88, 79, 98, 79, 86, 85 74, 72, 96, 88, 66, 86, 81, 83 85, 85, 79, 66, 104, 92, 71, 83 79, 85, 81, 92, 90, 81, 85, 86 94, 92, 86, 90, 85, 98, 79, 83 83, 83, 85, 102, 86, 104, 106, 104 94, 104, 83, 106, 102, 90, 96, 90 112, 88, 104, 92, 86, 83, 98, 69 77, 79, 85, 71, 71, 96, 106, 85 85, 86, 90, 100, 121, 102, 108, 98 108, 125, 132, 135, 119, 123, 121, 144 144, 154, 161, 149, 177, 159, 164, 161 164, 174, 166, 193, 172, 161, 154, 174 161, 174, 169, 174, 151, 166, 149, 142 144, 142, 130, 159, 149, 144, 144, 144 142, 135, 135, 144, 125, 114, 135, 114 119, 119, 121, 110, 119, 130, 135, 132 121, 119, 156, 174, 146, 146, 177, 151 177, 185, 185, 240, 243, 225, 262, 246 243, 256, 246, 266, 207, 213, 207, 213 199, 193, 193, 151, 161, 119, 112, 125 119, 123, 121, 102, 102, 96, 94, 94 117, 98, 100, 108, 132, 117, 125, 123 100, 94, 92, 98, 112, 112, 110, 117 96, 100, 110, 108, 119, 108, 102, 123 128, 114, 139, 123, 123, 123, 123, 132 128, 132, 142, 130, 130, 146, 137, 130 213, 231, 185, 172, 151, 130, 102, 114 108, 119, 108, 114, 94, 108, 106, 96 114, 104, 94, 92, 94, 90, 117, 100 110, 110, 86, 92, 110, 85, 100, 106 106, 104, 104, 102, 114, 123, 119, 94 123, 112, 114, 125, 112, 125, 114, 117 110, 119, 121, 110, 119, 96, 112, 128 137, 104, 100, 98, 114, 130, 125, 128 144, 112, 164, 130, 149, 166, 154, 166 156, 161, 159, 146, 159, 156, 137, 151 142, 149, 132, 151, 144, 132, 132, 142 137, 132, 104, 130, 128, 139, 117, 130 144, 128, 146, 149, 121, 172, 154, 142 156, 125, 161, 146, 190, 159, 151, 139 149, 169, 177, 139, 151, 139, 121, 130 135, 117, 135, 139, 132, 130, 135, 125 110, 128, 149, 139, 130, 159, 154, 130 159, 125, 182, 151, 137, 149, 151, 164 177, 188, 156, 185, 164, 193, 182, 185 190, 193, 199, 207, 164, 177, 180, 177 177, 216, 169, 180, 182, 174, 172, 188 161, 156, 154, 172, 161, 169, 146, 174 149, 137, 137, 161, 132, 161, 151, 149 128, 151, 159, 130, 125, 128, 121, 137 125, 139, 142, 159, 142, 154, 164, 139 154, 123, 159, 177, 159, 159, 193, 190 228, 262, 272, 282, 324, 380, 428, 462 497, 552, 697, 773, 876, 876, 1005, 1063 1142, 1076, 1050, 1116, 1156, 1183, 1318, 1267 1376, 1482, 1239, 1063, 858, 708, 557, 392 324, 237, 256, 259, 240, 210, 225, 213 207, 199, 185, 210, 196, 185, 193, 182 193, 177, 210, 193, 202, 219, 210, 219 228, 262, 262, 237, 237, 262, 269, 266 299, 286, 289, 310, 303, 313, 279, 299 306, 320, 339, 365, 346, 357, 400, 408 396, 392, 437, 454, 484, 475, 437, 441 437, 576, 655, 666, 557, 493, 424, 384 253, 216, 188, 174, 174, 164, 169, 161 156, 128, 137, 144, 128, 154, 154, 135 128, 121, 139, 117, 117, 117, 114, 123 125, 114, 104, 104, 114, 104, 108, 121 92, 119, 108, 104, 123, 102, 100, 114 123, 117, 119, 114, 106, 100, 104, 96 102, 108, 130, 104, 108, 100, 104, 92 121, 121, 108, 130, 128, 128, 135, 121 110, 128, 130, 172, 156, 121, 135, 142 154, 123, 125, 144, 137, 144, 144, 135 154, 144, 144, 159, 154, 146, 132, 156 142, 154, 146, 169, 139, 169, 132, 154 154, 161, 139, 132, 132, 151, 135, 130 128, 125, 119, 146, 144, 137, 199, 216 188, 172, 149, 193, 180, 142, 125, 142 112, 132, 144, 130, 108, 142, 119, 144 137, 137, 137, 130, 154, 137, 128, 146 164, 154, 154, 128, 149, 146, 146, 135 149, 159, 149, 154, 185, 182, 151, 154 149, 166, 154, 128, 128, 128, 137, 156 137, 132, 142, 125, 154, 144, 149, 135 135, 172, 172, 169, 159, 182, 190, 149 177, 185, 169, 169, 182, 185, 185, 142 156, 149, 100, 102, 102, 110, 100, 98 112, 100, 85, 85, 94, 100, 100, 96 110, 112, 83, 86, 94, 81, 98, 104 114, 96, 96, 92, 104, 92, 92, 100 81, 85, 85, 74, 96, 62, 83, 88 71, 76, 83, 92, 88, 100, 81, 66 67, 100, 88, 85, 96, 90, 85, 90 92, 90, 94, 96, 100, 88, 100, 98 92, 92, 90, 269, 83, 83, 90, 92 88, 102, 96, 62, 86, 88, 96, 88 85, 100, 102, 104, 106, 104, 79, 102 100, 110, 106, 108, 102, 96, 85, 108 102, 96, 100, 98, 100, 117, 112, 110 102, 102, 108, 110, 108, 125, 114, 125 121, 123, 146, 139, 135, 139, 149, 139 135, 146, 154, 164, 154, 156, 169, 177 161, 166, 193, 193, 199, 219, 199, 210 199, 199, 228, 216, 219, 213, 234, 243 222, 243, 243, 222, 240, 259, 243, 246 262, 269, 256, 250, 282, 276, 246, 276 266, 231, 222, 234, 216, 234, 204, 231 216, 213, 185, 199, 190, 207, 196, 156 185, 164, 177, 174, 169, 169, 166, 156 166, 177, 156, 156, 166, 154, 174, 137 159, 139, 159, 149, 154, 164, 130, 130 144, 135, 130, 123, 128, 128, 132, 128 135, 130, 130, 121, 154, 119, 121, 142 123, 139, 146, 146, 154, 146, 159, 164 174, 156, 199, 161, 188, 207, 216, 213 231, 231, 222, 237, 250, 256, 219, 234 207, 222, 213, 188, 169, 190, 164, 174 166, 172, 139, 161, 146, 130, 154, 144 169, 135, 144, 132, 166, 156, 156, 144 164, 130, 156, 149, 149, 149, 149, 132 144, 151, 144, 166, 144, 159, 164, 159 159, 182, 166, 164, 185, 169, 182, 174 169, 144, 188, 149, 182, 169, 151, 156 172, 177, 166, 166, 144, 137, 144, 121 119, 125, 144, 117, 108, 121, 112, 104 119, 123, 106, 132, 119, 121, 130, 125 144, 137, 114, 112, 110, 112, 104, 114 119, 119, 123, 104, 132, 119, 114, 102 128, 96, 114, 110, 102, 102, 130, 76 94, 88, 86, 100, 94, 96, 100, 112 114, 110, 102, 112, 106, 106, 112, 110 98, 98, 108, 110, 102, 106, 92, 100 119, 128, 149, 161, 159, 139, 169, 144 164, 190, 204, 213, 193, 185, 228, 225 204, 196, 196, 164, 177, 149, 151, 151 149, 139, 92, 139, 112, 137, 106, 104 96, 98, 98, 104, 135, 108, 96, 104 123, 112, 139, 123, 139, 139, 146, 130 146, 149, 137, 142, 139, 154, 137, 154 151, 154, 112, 164, 135, 117, 117, 125 119, 123, 119, 117, 96, 110, 92, 98 108, 104, 94, 108, 130, 108, 92, 94 88, 108, 100, 117, 112, 104, 114, 123 106, 114, 121, 106, 108, 119, 119, 132 110, 114, 139, 132, 135, 128, 114, 132 119, 130, 139, 110, 102, 102, 108, 100 130, 117, 121, 121, 110, 135, 154, 121 121, 117, 128, 123, 110, 125, 117, 146 130, 128, 137, 139, 123, 117, 128, 119 121, 123, 114, 104, 125, 130, 132, 137 125, 104, 128, 142, 125, 144, 121, 161 156, 185, 185, 166, 210, 185, 207, 199 180, 202, 193, 193, 219, 240, 210, 234 225, 199, 193, 193, 156, 177, 188, 154 132, 132, 110, 106, 108, 112, 112, 98 104, 98, 100, 96, 130, 90, 90, 86 86, 92, 86, 88, 94, 94, 92, 102 104, 90, 92, 94, 90, 98, 86, 92 90, 100, 123, 102, 86, 104, 94, 96 92, 96, 79, 130, 108, 96, 112, 92 98, 106, 117, 90, 83, 102, 112, 98 96, 112, 123, 106, 121, 106, 117, 96 117, 94, 98, 98, 81, 94, 100, 90 79, 86, 117, 100, 106, 90, 77, 100 100, 110, 94, 98, 110, 112, 98, 130 110, 135, 130, 123, 114, 112, 121, 117 108, 106, 119, 132, 102, 106, 102, 119 125, 104, 119, 137, 100, 100, 128, 106 135, 137, 146, 117, 149, 139, 142, 137 156, 161, 159, 180, 185, 204, 177, 177 185, 196, 222, 199, 202, 207, 231, 193 213, 219, 219, 210, 246, 237, 225, 199 210, 188, 196, 193, 190, 177, 188, 172 177, 190, 361, 199, 177, 164, 149, 188 128, 139, 146, 123, 114, 146, 130, 100 130, 96, 104, 104, 96, 114, 90, 86 79, 92, 123, 104, 100, 106, 102, 88 98, 98, 96, 81, 100, 92, 98, 71 98, 94, 98, 81, 81, 85, 79, 104 85, 86, 77, 94, 71, 79, 90, 85 102, 92, 88, 85, 79, 72, 100, 83 90, 96, 76, 92, 90, 92, 88, 83 102, 74, 94, 85, 96, 85, 79, 72 86, 81, 92, 81, 62, 79, 76, 86 71, 83, 86, 85, 74, 74, 94, 59 71, 71, 85, 90, 90, 79, 86, 85 88, 88, 85, 86, 94, 90, 106, 106 96, 96, 81, 86, 100, 85, 86, 94 72, 90, 86, 79, 86, 96, 76, 83 79, 86, 96, 79, 88, 86, 76, 98 77, 71, 86, 77, 83, 85, 86, 77 79, 81, 85, 61, 62, 85, 77, 72 79, 77, 83, 98, 77, 67, 83, 67 76, 79, 79, 81, 72, 98, 79, 86 66, 81, 94, 79, 85, 96, 76, 86 106, 98, 104, 94, 117, 79, 88, 85 92, 83, 88, 90, 90, 100, 88, 119 108, 119, 98, 104, 100, 110, 110, 106 108, 135, 135, 154, 149, 142, 156, 207 225, 279, 292, 299, 303, 262, 310, 303 303, 353, 335, 339, 328, 313, 279, 310 279, 243, 225, 193, 328, 142, 182, 164 137, 121, 117, 104, 110, 108, 106, 121 112, 123, 117, 102, 114, 114, 119, 104 128, 119, 130, 102, 104, 119, 114, 114 112, 90, 86, 92, 110, 106, 117, 106 88, 104, 92, 92, 114, 77, 102, 94 85, 110, 104, 100, 86, 108, 94, 90 79, 110, 83, 96, 90, 81, 67, 71 76, 66, 76, 77, 69, 76, 72, 64 79, 62, 66, 55, 74, 76, 76, 66 74, 79, 71, 66, 59, 71, 62, 94 79, 77, 85, 66, 77, 85, 79, 85 77, 98, 71, 96, 83, 77, 86, 86 94, 98, 100, 100, 98, 90, 85, 90 108, 96, 76, 92, 96, 98, 96, 106 83, 85, 108, 90, 88, 102, 92, 77 98, 83, 100, 90, 76, 100, 90, 121 94, 102, 98, 90, 96, 104, 92, 121 117, 102, 108, 117, 100, 102, 100, 102 104, 130, 94, 106, 104, 98, 108, 98 112, 100, 123, 100, 102, 128, 94, 117 106, 117, 112, 112, 108, 117, 119, 110 102, 112, 142, 125, 132, 132, 119, 135 137, 135, 108, 106, 125, 130, 121, 110 121, 112, 132, 119, 117, 132, 135, 117 108, 130, 132, 130, 149, 121, 123, 142 119, 123, 108, 121, 112, 125, 137, 149 137, 135, 139, 151, 161, 177, 151, 174 177, 207, 188, 204, 204, 169, 202, 190 246, 225, 225, 213, 231, 250, 237, 207 199, 188, 480, 213, 185, 166, 185, 188 159, 154, 166, 156, 180, 180, 169, 169 156, 156, 159, 151, 185, 139, 166, 151 151, 161, 159, 139, 154, 149, 137, 130 149, 144, 121, 154, 132, 146, 166, 132 135, 139, 154, 151, 114, 142, 121, 137 128, 125, 130, 130, 135, 112, 137, 114 125, 119, 114, 130, 142, 132, 110, 123 142, 130, 149, 151, 128, 146, 135, 154 144, 159, 151, 144, 149, 117, 130, 130 146, 142, 135, 125, 119, 121, 132, 114 125, 121, 123, 114, 108, 117, 94, 117 114, 119, 121, 110, 125, 110, 102, 94 88, 102, 112, 123, 104, 108, 123, 104 121, 108, 123, 106, 117, 342, 119, 119 94, 96, 92, 90, 108, 119, 90, 106 110, 100, 110, 114, 92, 100, 119, 110 102, 88, 96, 92, 102, 110, 90, 128 110, 102, 98, 98, 98, 119, 96, 108 108, 96, 117, 102, 102, 104, 88, 100 106, 102, 85, 100, 81, 96, 85, 86 81, 104, 110, 104, 98, 108, 117, 114 144, 108, 100, 92, 104, 108, 100, 117 121, 114, 121, 114, 112, 112, 114, 100 90, 96, 121, 106, 98, 112, 112, 94 119, 104, 110, 100, 104, 128, 112, 102 130, 130, 114, 106, 106, 108, 114, 142 110, 114, 123, 102, 106, 125, 108, 132 132, 121, 144, 121, 154, 146, 146, 154 174, 180, 185, 222, 240, 243, 306, 306 276, 303, 303, 299, 303, 306, 331, 369 388, 365, 376, 299, 286, 276, 246, 219 243, 210, 222, 202, 182, 166, 174, 151 139, 146, 149, 132, 119, 119, 125, 137 130, 96, 121, 125, 117, 119, 130, 130 121, 121, 130, 151, 119, 123, 142, 130 139, 149, 125, 139, 146, 137, 139, 154 154, 139, 139, 156, 139, 146, 166, 166 137, 174, 135, 166, 164, 177, 177, 174 174, 180, 177, 193, 185, 185, 169, 213 177, 190, 213, 199, 202, 216, 193, 234 207, 228, 204, 216, 219, 213, 219, 204 228, 202, 196, 228, 219, 190, 199, 193 188, 202, 185, 185, 154, 188, 185, 185 193, 172, 164, 172, 172, 159, 151, 166 154, 142, 161, 151, 137, 142, 159, 159 137, 151, 119, 151, 161, 146, 137, 125 137, 144, 110, 132, 125, 125, 128, 114 144, 123, 112, 112, 104, 106, 92, 104 110, 106, 102, 114, 106, 102, 94, 130 104, 110, 106, 110, 92, 110, 77, 114 98, 98, 100, 108, 119, 94, 114, 128 85, 110, 104, 114, 104, 110, 110, 121 123, 104, 121, 112, 121, 137, 114, 106 117, 130, 104, 135, 123, 142, 123, 123 117, 125, 128, 132, 137, 151, 142, 144 161, 149, 142, 146, 154, 156, 142, 128 130, 119, 123, 110, 117, 135, 110, 108 106, 121, 102, 112, 98, 114, 112, 104 98, 83, 104, 104, 110, 112, 100, 96 98, 83, 85, 117, 94, 94, 96, 108 114, 104, 119, 90, 104, 108, 108, 100 102, 86, 94, 128, 110, 112, 104, 114 112, 112, 100, 102, 98, 83, 114, 96 108, 123, 104, 110, 90, 102, 119, 94 88, 94, 114, 135, 100, 106, 108, 94 114, 100, 125, 98, 108, 135, 108, 106 121, 117, 110, 121, 121, 98, 100, 110 119, 125, 94, 108, 114, 108, 119, 112 102, 119, 108, 104, 102, 100, 130, 128 114, 125, 94, 102, 108, 104, 104, 90 100, 123, 96, 92, 86, 110, 92, 86 83, 81, 88, 71, 77, 81, 98, 98 108, 98, 94, 92, 102, 96, 88, 96 90, 96, 90, 110, 88, 92, 94, 102 100, 117, 102, 114, 96, 81, 135, 112 119, 96, 110, 77, 104, 117, 128, 88 121, 112, 100, 117, 137, 130, 139, 137 149, 188, 207, 177, 216, 225, 169, 210 266, 262, 272, 269, 253, 246, 234, 222 250, 246, 222, 222, 231, 228, 210, 269 225, 262, 259, 262, 240, 266, 289, 286 299, 306, 317, 384, 346, 380, 412, 388 376, 361, 328, 276, 253, 246, 253, 256 253, 219, 246, 172, 172, 174, 159, 139 137, 110, 112, 117, 123, 100, 125, 112 125, 110, 112, 114, 117, 117, 112, 104 121, 112, 114, 121, 125, 119, 114, 114 104, 106, 108, 117, 123, 130, 128, 130 112, 117, 137, 112, 110, 156, 130, 123 112, 130, 137, 142, 137, 123, 137, 112 110, 130, 123, 130, 128, 121, 104, 106 106, 130, 123, 110, 132, 123, 112, 108 117,/