SampleIdent,907A 4H-1 25 BULK,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 6-aug-1993 15:52,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 79, 79, 79, 100, 86, 98, 83, 88 86, 74, 90, 90, 86, 98, 96, 88 104, 100, 88, 92, 92, 77, 74, 96 85, 77, 98, 76, 76, 85, 77, 88 92, 72, 86, 90, 94, 100, 92, 92 88, 88, 92, 88, 92, 100, 85, 85 108, 108, 106, 96, 88, 94, 90, 102 110, 130, 100, 100, 106, 104, 104, 112 110, 102, 100, 114, 90, 96, 100, 110 130, 92, 92, 102, 110, 104, 102, 119 110, 128, 112, 121, 132, 119, 96, 102 110, 112, 106, 100, 121, 112, 123, 125 123, 123, 125, 96, 112, 104, 121, 125 112, 108, 104, 106, 119, 117, 108, 112 102, 108, 110, 130, 110, 117, 104, 106 104, 112, 104, 106, 106, 112, 104, 110 121, 104, 106, 85, 128, 108, 110, 96 90, 112, 121, 86, 100, 125, 100, 112 123, 130, 104, 106, 110, 125, 114, 102 98, 112, 102, 108, 106, 119, 98, 106 106, 121, 117, 112, 100, 121, 104, 100 108, 108, 108, 119, 102, 114, 96, 104 106, 117, 108, 114, 104, 121, 121, 104 106, 128, 104, 123, 139, 117, 114, 114 125, 104, 100, 132, 96, 114, 117, 114 121, 98, 85, 81, 102, 100, 77, 100 88, 96, 94, 100, 88, 88, 108, 92 108, 110, 88, 92, 96, 100, 94, 106 98, 85, 76, 86, 81, 102, 86, 108 108, 90, 94, 96, 90, 106, 64, 86 100, 85, 85, 88, 88, 96, 94, 98 92, 81, 112, 77, 86, 90, 110, 86 83, 94, 85, 86, 86, 86, 98, 92 86, 98, 86, 79, 86, 79, 92, 86 98, 96, 92, 79, 86, 98, 74, 346 100, 83, 106, 100, 92, 117, 85, 90 96, 94, 110, 106, 96, 90, 102, 90 104, 106, 72, 100, 88, 85, 86, 90 83, 104, 85, 86, 79, 92, 90, 104 90, 98, 83, 86, 69, 88, 94, 94 96, 77, 94, 71, 83, 85, 74, 74 83, 106, 106, 76, 83, 81, 72, 85 94, 83, 90, 72, 79, 90, 62, 94 90, 83, 92, 86, 98, 92, 77, 86 90, 79, 94, 90, 85, 86, 90, 86 94, 90, 94, 108, 106, 110, 110, 90 98, 114, 112, 119, 110, 121, 128, 125 102, 110, 104, 114, 100, 119, 102, 85 104, 85, 71, 92, 76, 86, 90, 88 79, 86, 88, 96, 86, 86, 83, 81 77, 86, 72, 72, 81, 79, 77, 86 85, 76, 100, 83, 86, 79, 79, 74 90, 74, 85, 92, 83, 76, 85, 74 85, 90, 76, 83, 79, 74, 96, 86 90, 81, 86, 76, 96, 100, 100, 92 92, 77, 79, 81, 94, 92, 96, 92 83, 77, 92, 72, 86, 83, 76, 71 79, 79, 74, 86, 62, 86, 71, 71 76, 77, 81, 85, 66, 79, 86, 83 72, 76, 83, 76, 83, 83, 88, 92 90, 88, 74, 71, 74, 86, 71, 86 74, 67, 72, 100, 64, 90, 85, 88 59, 83, 88, 72, 71, 85, 69, 62 85, 92, 67, 86, 71, 86, 58, 77 74, 72, 71, 67, 55, 96, 88, 76 69, 88, 62, 67, 69, 69, 76, 88 66, 76, 86, 83, 69, 92, 72, 71 71, 66, 86, 88, 88, 94, 77, 72 72, 85, 81, 72, 76, 90, 77, 83 66, 83, 69, 69, 72, 77, 74, 69 76, 76, 67, 100, 79, 71, 71, 67 64, 76, 77, 83, 83, 67, 90, 76 90, 72, 61, 88, 79, 79, 92, 85 67, 71, 76, 79, 77, 72, 72, 58 56, 79, 66, 64, 90, 72, 69, 61 66, 79, 81, 76, 61, 62, 72, 59 90, 88, 67, 72, 76, 66, 71, 66 86, 66, 66, 77, 85, 71, 76, 71 72, 83, 79, 90, 77, 72, 86, 100 100, 83, 79, 86, 96, 88, 94, 102 90, 85, 85, 77, 92, 76, 79, 98 76, 83, 72, 98, 74, 71, 69, 72 79, 83, 71, 72, 83, 67, 85, 67 72, 79, 77, 69, 76, 81, 83, 83 72, 77, 92, 83, 66, 66, 85, 71 88, 81, 74, 77, 98, 85, 66, 76 79, 88, 98, 106, 100, 100, 96, 259 90, 85, 88, 90, 96, 59, 86, 58 79, 77, 85, 79, 88, 88, 96, 83 88, 106, 98, 102, 76, 96, 102, 98 102, 119, 108, 117, 110, 108, 106, 117 139, 112, 121, 142, 151, 154, 135, 166 159, 149, 139, 151, 146, 174, 156, 182 161, 174, 139, 159, 149, 159, 154, 156 139, 123, 144, 121, 130, 121, 123, 130 104, 132, 112, 123, 117, 119, 112, 139 110, 112, 110, 142, 121, 108, 130, 123 110, 114, 117, 123, 102, 137, 137, 117 125, 132, 139, 130, 151, 177, 222, 228 250, 250, 256, 289, 243, 262, 328, 372 296, 276, 246, 185, 142, 106, 159, 135 117, 137, 119, 117, 123, 100, 117, 119 135, 117, 106, 112, 128, 121, 104, 100 121, 125, 112, 108, 102, 114, 81, 112 110, 112, 121, 106, 117, 110, 104, 96 132, 114, 121, 128, 119, 121, 119, 137 132, 154, 156, 159, 207, 185, 164, 159 156, 149, 137, 146, 121, 114, 119, 119 98, 100, 98, 92, 94, 100, 102, 86 110, 102, 104, 94, 100, 119, 94, 100 108, 92, 112, 98, 108, 106, 106, 121 108, 104, 110, 121, 128, 128, 102, 130 106, 132, 117, 123, 121, 112, 121, 117 132, 108, 108, 108, 119, 125, 108, 106 108, 94, 102, 104, 130, 98, 119, 102 114, 123, 119, 139, 146, 139, 144, 144 174, 144, 177, 193, 193, 188, 190, 177 174, 154, 164, 135, 146, 156, 159, 142 154, 142, 117, 137, 121, 123, 117, 119 121, 125, 123, 119, 110, 142, 146, 135 146, 149, 172, 185, 177, 169, 142, 182 161, 164, 177, 159, 149, 119, 132, 119 137, 121, 121, 123, 130, 132, 110, 117 125, 110, 117, 130, 135, 112, 121, 121 125, 139, 128, 139, 135, 114, 128, 146 128, 117, 151, 139, 139, 149, 161, 159 144, 169, 144, 180, 159, 190, 190, 164 128, 159, 172, 177, 166, 154, 151, 177 174, 161, 180, 180, 177, 174, 149, 149 159, 159, 151, 154, 172, 144, 137, 144 130, 144, 185, 151, 135, 132, 164, 149 139, 135, 130, 139, 114, 130, 123, 106 142, 139, 130, 142, 121, 149, 144, 154 135, 137, 151, 161, 172, 164, 188, 169 225, 234, 272, 289, 342, 424, 493, 645 734, 853, 912, 1018, 999, 1190, 1376, 1429 1318, 1197, 1063, 841, 615, 484, 353, 279 234, 234, 225, 207, 188, 222, 182, 144 166, 174, 154, 144, 166, 169, 169, 146 166, 174, 164, 169, 177, 188, 207, 193 213, 262, 256, 286, 310, 331, 299, 313 272, 279, 259, 262, 243, 272, 256, 279 296, 331, 313, 350, 361, 408, 396, 424 471, 428, 467, 502, 502, 475, 511, 475 445, 424, 384, 369, 342, 292, 289, 243 253, 234, 237, 216, 219, 213, 202, 182 166, 177, 177, 174, 151, 169, 142, 151 142, 132, 110, 135, 135, 121, 154, 106 132, 130, 106, 128, 128, 114, 119, 110 112, 121, 119, 110, 123, 119, 130, 121 121, 121, 106, 119, 130, 135, 110, 130 117, 104, 112, 100, 106, 106, 119, 104 96, 114, 112, 108, 114, 110, 123, 137 117, 121, 128, 123, 128, 132, 117, 144 123, 130, 142, 149, 142, 154, 149, 166 154, 210, 174, 169, 169, 190, 182, 182 172, 174, 193, 174, 172, 169, 182, 146 169, 177, 169, 177, 185, 199, 172, 182 196, 216, 253, 365, 428, 412, 392, 353 357, 279, 272, 188, 207, 169, 146, 166 144, 137, 151, 128, 137, 130, 132, 139 121, 144, 164, 149, 146, 128, 154, 169 182, 172, 149, 132, 174, 154, 142, 114 110, 117, 121, 142, 125, 142, 128, 146 132, 132, 149, 137, 149, 139, 137, 139 132, 139, 144, 151, 149, 151, 144, 196 169, 174, 199, 202, 199, 193, 231, 237 250, 225, 219, 243, 219, 210, 193, 169 188, 154, 164, 182, 123, 128, 144, 130 121, 123, 137, 128, 130, 108, 130, 108 94, 119, 121, 102, 104, 108, 90, 117 102, 104, 102, 114, 96, 123, 106, 112 86, 108, 104, 119, 108, 114, 114, 104 106, 106, 110, 100, 108, 106, 102, 98 106, 114, 110, 100, 96, 96, 104, 92 106, 104, 98, 79, 94, 102, 135, 110 102, 96, 90, 119, 102, 102, 106, 121 102, 139, 125, 123, 114, 112, 114, 100 128, 128, 106, 117, 117, 104, 117, 90 112, 114, 110, 123, 106, 108, 114, 104 119, 98, 117, 121, 117, 137, 106, 96 114, 112, 125, 96, 123, 128, 117, 135 128, 139, 139, 128, 125, 128, 137, 117 149, 125, 110, 154, 154, 144, 144, 146 177, 164, 156, 182, 196, 193, 193, 182 188, 196, 199, 196, 231, 204, 216, 202 196, 204, 213, 182, 207, 216, 219, 222 256, 228, 225, 243, 250, 231, 243, 231 276, 225, 286, 240, 286, 256, 246, 228 234, 202, 228, 243, 216, 219, 219, 216 193, 202, 204, 199, 204, 190, 180, 177 169, 210, 169, 185, 185, 193, 185, 193 182, 154, 177, 166, 169, 159, 174, 164 144, 146, 144, 142, 172, 149, 156, 151 151, 137, 146, 137, 137, 177, 161, 149 154, 137, 114, 151, 142, 119, 123, 135 125, 130, 137, 180, 128, 164, 196, 174 193, 177, 234, 246, 246, 276, 296, 296 289, 266, 202, 207, 231, 204, 199, 139 151, 180, 159, 156, 154, 130, 159, 174 154, 164, 137, 146, 135, 144, 161, 139 149, 137, 142, 154, 125, 135, 156, 146 149, 149, 174, 156, 156, 169, 169, 180 144, 142, 177, 159, 161, 159, 164, 149 164, 156, 174, 166, 172, 185, 156, 166 166, 164, 172, 166, 169, 154, 146, 132 146, 114, 132, 130, 106, 104, 121, 121 135, 128, 121, 119, 112, 121, 114, 119 132, 128, 137, 130, 139, 144, 132, 121 123, 144, 128, 142, 130, 137, 123, 106 112, 117, 98, 110, 128, 121, 121, 132 121, 121, 112, 102, 108, 114, 114, 125 117, 119, 117, 108, 102, 112, 121, 94 108, 128, 110, 128, 94, 114, 98, 110 100, 121, 106, 137, 112, 123, 144, 146 144, 144, 172, 154, 174, 154, 169, 213 202, 182, 213, 144, 164, 154, 161, 139 144, 156, 102, 110, 108, 132, 114, 135 121, 119, 106, 119, 106, 123, 117, 125 112, 112, 100, 130, 117, 135, 128, 106 128, 123, 123, 121, 132, 130, 169, 146 159, 151, 144, 154, 135, 125, 132, 125 135, 112, 112, 123, 112, 94, 100, 128 125, 121, 104, 121, 96, 114, 104, 123 98, 100, 110, 117, 106, 96, 123, 106 108, 424, 117, 125, 102, 110, 114, 108 117, 102, 121, 110, 132, 114, 125, 119 108, 117, 121, 102, 102, 110, 121, 112 119, 106, 106, 110, 98, 110, 121, 110 90, 112, 121, 132, 123, 112, 132, 137 112, 137, 132, 135, 142, 125, 128, 106 125, 130, 128, 112, 159, 144, 125, 125 123, 130, 123, 149, 144, 132, 119, 117 130, 159, 156, 164, 164, 177, 154, 193 180, 199, 253, 328, 416, 538, 511, 449 353, 292, 361, 331, 303, 234, 185, 172 156, 144, 128, 144, 137, 142, 146, 135 110, 128, 114, 117, 139, 114, 132, 121 135, 110, 106, 114, 128, 125, 119, 110 108, 106, 96, 106, 106, 119, 92, 123 94, 100, 110, 123, 96, 119, 96, 108 92, 100, 114, 98, 121, 114, 104, 98 110, 94, 106, 117, 123, 121, 121, 128 130, 130, 132, 151, 121, 128, 144, 137 144, 125, 149, 161, 121, 151, 123, 149 135, 130, 139, 112, 125, 104, 100, 102 114, 110, 106, 106, 128, 139, 110, 144 164, 188, 164, 169, 210, 193, 180, 166 169, 174, 159, 146, 151, 137, 130, 112 117, 137, 125, 108, 123, 108, 128, 123 125, 142, 144, 135, 130, 144, 166, 151 154, 149, 169, 154, 164, 151, 174, 144 169, 196, 199, 222, 213, 213, 216, 222 213, 213, 231, 228, 219, 196, 156, 182 172, 159, 149, 177, 149, 193, 144, 154 159, 164, 174, 185, 154, 164, 193, 149 144, 154, 137, 144, 139, 135, 132, 119 114, 104, 94, 125, 90, 98, 102, 100 100, 96, 90, 130, 100, 90, 94, 92 98, 102, 108, 96, 100, 92, 98, 108 104, 79, 88, 85, 98, 90, 77, 81 108, 98, 90, 98, 86, 86, 86, 90 94, 102, 90, 88, 74, 83, 96, 77 92, 92, 79, 100, 112, 102, 104, 100 88, 96, 100, 94, 83, 92, 90, 85 86, 79, 92, 83, 104, 100, 90, 88 86, 92, 81, 71, 67, 81, 77, 86 71, 108, 102, 98, 90, 85, 96, 92 79, 90, 85, 98, 100, 102, 90, 108 106, 137, 121, 112, 104, 108, 112, 100 90, 139, 121, 104, 123, 108, 110, 108 102, 112, 108, 102, 123, 112, 96, 102 114, 104, 106, 83, 71, 83, 114, 88 96, 88, 85, 88, 96, 67, 83, 77 85, 104, 108, 88, 88, 100, 81, 90 90, 100, 86, 85, 102, 114, 114, 102 106, 106, 106, 106, 104, 102, 102, 128 119, 85, 92, 121, 117, 100, 100, 119 119, 108, 112, 102, 121, 121, 112, 106 102, 123, 117, 135, 108, 98, 106, 100 130, 128, 132, 123, 135, 110, 146, 108 130, 144, 137, 137, 125, 185, 177, 207 213, 246, 240, 303, 310, 299, 269, 253 246, 240, 216, 188, 185, 182, 159, 142 130, 92, 114, 104, 104, 110, 102, 117 112, 110, 117, 117, 119, 114, 142, 98 132, 139, 130, 121, 121, 128, 121, 132 112, 100, 112, 112, 110, 96, 110, 104 110, 110, 117, 100, 112, 128, 144, 110 123, 121, 139, 130, 144, 123, 132, 102 98, 102, 128, 112, 121, 128, 130, 106 121, 117, 98, 102, 102, 110, 119, 104 94, 98, 85, 77, 90, 104, 94, 98 90, 92, 77, 85, 96, 96, 83, 83 100, 86, 96, 96, 114, 98, 108, 104 90, 100, 123, 104, 125, 110, 98, 114 98, 110, 100, 121, 125, 98, 96, 94 121, 98, 100, 98, 104, 86, 83, 98 121, 110, 98, 110, 92, 100, 94, 128 112, 100, 106, 94, 114, 106, 100, 106 104, 100, 121, 125, 130, 117, 102, 108 106, 135, 151, 137, 144, 164, 149, 159 119, 125, 121, 135, 130, 123, 135, 130 125, 125, 121, 123, 117, 130, 112, 108 102, 144, 114, 125, 117, 110, 125, 112 112, 117, 132, 128, 119, 137, 130, 137 130, 137, 135, 132, 110, 128, 121, 123 114, 123, 128, 137, 117, 144, 125, 137 137, 149, 121, 144, 123, 137, 128, 112 164, 117, 137, 121, 144, 123, 119, 123 139, 110, 130, 174, 130, 142, 132, 135 151, 149, 169, 161, 169, 159, 196, 185 240, 231, 204, 237, 204, 177, 172, 193 182, 188, 166, 169, 159, 128, 161, 177 166, 161, 154, 164, 172, 174, 132, 151 161, 156, 149, 156, 159, 132, 125, 135 151, 156, 142, 123, 137, 137, 146, 128 149, 132, 149, 125, 123, 130, 139, 139 144, 121, 137, 125, 130, 154, 135, 151 142, 132, 121, 117, 135, 142, 121, 108 128, 130, 123, 117, 121, 137, 132, 119 128, 149, 130, 149, 139, 169, 177, 159 149, 132, 146, 142, 169, 128, 151, 151 142, 137, 146, 132, 156, 128, 139, 137 123, 139, 137, 135, 144, 142, 123, 135 125, 114, 130, 121, 121, 128, 114, 117 121, 114, 149, 125, 119, 121, 112, 100 117, 114, 123, 121, 125, 106, 121, 119 128, 125, 119, 123, 121, 112, 119, 117 121, 102, 132, 112, 125, 135, 137, 121 121, 117, 132, 130, 117, 121, 117, 123 121, 121, 104, 123, 117, 125, 132, 114 121, 108, 102, 119, 114, 130, 135, 119 110, 102, 98, 110, 125, 130, 102, 121 117, 114, 128, 132, 119, 117, 104, 125 125, 92, 130, 137, 135, 112, 123, 135 137, 123, 156, 128, 156, 137, 130, 139 121, 110, 132, 100, 130, 117, 123, 137 114, 114, 132, 125, 135, 130, 117, 110 137, 121, 142, 130, 114, 135, 114, 139 125, 123, 132, 128, 128, 132, 144, 154 130, 128, 123, 135, 151, 137, 144, 130 146, 156, 154, 128, 156, 149, 151, 174 180, 202, 231, 225, 279, 276, 262, 306 303, 269, 256, 269, 246, 256, 225, 219 219, 210, 199, 188, 177, 164, 142, 151 159, 139, 149, 130, 137, 154, 117, 112 135, 154, 154, 128, 142, 137, 139, 149 174, 137, 139, 144, 146, 154, 137, 182 156, 151, 135, 144, 166, 151, 164, 121 151, 174, 146, 149, 137, 159, 146, 149 169, 159, 169, 164, 182, 177, 161, 185 169, 159, 185, 180, 156, 169, 169, 154 164, 199, 169, 185, 164, 164, 174, 169 169, 196, 177, 169, 174, 216, 164, 164 169, 196, 185, 185, 166, 177, 159, 159 188, 202, 185, 174, 169, 169, 161, 172 180, 159, 144, 188, 169, 151, 169, 154 161, 166, 169, 172, 149, 172, 177, 130 169, 132, 161, 159, 172, 149, 149, 149 151, 130, 151, 137, 149, 142, 135, 137 146, 151, 146, 142, 132, 114, 144, 128 130, 144, 135, 132, 130, 112, 132, 130 117, 123, 125, 121, 130, 121, 110, 144 121, 137, 144, 114, 125, 121, 146, 130 112, 108, 142, 130, 125, 128, 125, 96 119, 139, 132, 130, 114, 121, 123, 137 144, 123, 142, 156, 149, 137, 128, 154 144, 174, 154, 128, 135, 154, 139, 172 151, 159, 149, 154, 149, 144, 137, 149 144, 164, 128, 144, 154, 139, 128, 142 110, 121, 117, 121, 142, 128, 94, 114 98, 125, 121, 117, 130, 119, 135, 112 102, 123, 121, 121, 108, 128, 117, 123 125, 117, 132, 112, 125, 159, 139, 182 137, 149, 142, 161, 135, 114, 117, 142 139, 137, 135, 139, 137, 128, 110, 106 130, 123, 121, 121, 125, 121, 119, 132 128, 112, 130, 125, 108, 125, 135, 121 119, 137, 149, 123, 137, 121, 132, 144 132, 142, 119, 139, 125, 139, 132, 110 139, 125, 125, 142, 149, 154, 130, 135 135, 130, 132, 123, 146, 117, 125, 108 112, 123, 135, 123, 130, 130, 130, 130 123, 112, 123, 119, 125, 121, 128, 119 102, 112, 94, 128, 125, 96, 110, 117 130, 90, 123, 108, 119, 112, 106, 121 108, 117, 104, 112, 121, 119, 119, 135 130, 128, 139, 130, 123, 130, 151, 114 110, 128, 142, 119, 137, 144, 121, 137 132, 139, 106, 123, 137, 135, 119, 132 112, 139, 130, 137, 166, 161, 151, 161 169, 166, 199, 177, 202, 210, 276, 219 213, 196, 177, 177, 193, 174, 199, 172 190, 144, 188, 202, 213, 193, 213, 237 228, 253, 222, 237, 253, 225, 231, 219 246, 262, 240, 204, 246, 228, 225, 164 188, 151, 177, 161, 156, 151, 144, 151 154, 139, 139, 151, 119, 114, 112, 119 121, 130, 108, 132, 144, 142, 128, 123 119, 135, 144, 146, 130, 112, 130, 144 130, 142, 128, 130, 159, 139, 125, 132 112, 144, 166, 128, 151, 144, 137, 156 149, 146, 139, 114, 139, 164, 169, 164 149, 128, 149, 119, 146, 142, 156, 146 149, 154, 139, 132, 130, 123, 123, 130 154,/