SampleIdent,907A-4-3/77,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 9-aug-1993 0:57,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 106, 94, 102, 102, 110, 114, 96, 100 92, 86, 88, 104, 108, 117, 104, 100 110, 108, 110, 121, 100, 106, 121, 104 96, 86, 117, 108, 108, 110, 98, 117 112, 96, 123, 110, 96, 108, 106, 121 117, 102, 96, 108, 121, 123, 112, 110 104, 128, 119, 110, 102, 146, 137, 137 132, 137, 117, 125, 135, 110, 132, 130 117, 149, 135, 112, 144, 139, 125, 139 119, 139, 137, 132, 128, 121, 119, 151 123, 108, 130, 137, 139, 135, 123, 121 144, 110, 137, 166, 121, 121, 106, 135 121, 139, 130, 156, 119, 154, 132, 151 151, 125, 128, 135, 119, 123, 137, 128 137, 154, 137, 144, 121, 121, 142, 135 125, 121, 130, 123, 125, 135, 130, 146 112, 130, 110, 132, 149, 117, 123, 142 125, 114, 135, 132, 100, 132, 137, 108 137, 130, 137, 121, 130, 137, 154, 123 119, 130, 128, 135, 151, 149, 144, 130 108, 117, 137, 125, 125, 121, 128, 146 137, 132, 119, 164, 144, 139, 149, 154 139, 119, 117, 146, 135, 149, 139, 185 146, 156, 177, 144, 154, 156, 177, 146 177, 159, 174, 151, 164, 146, 123, 114 132, 119, 100, 130, 96, 104, 119, 114 102, 106, 102, 114, 112, 104, 96, 112 102, 104, 98, 100, 92, 119, 108, 117 86, 106, 104, 86, 98, 92, 100, 102 110, 108, 110, 92, 98, 106, 110, 104 106, 114, 104, 100, 94, 96, 94, 94 98, 88, 100, 110, 102, 86, 106, 90 102, 96, 112, 98, 81, 108, 74, 98 114, 104, 85, 117, 119, 114, 144, 112 92, 121, 121, 128, 96, 85, 100, 110 88, 108, 90, 100, 98, 79, 100, 86 83, 86, 86, 94, 100, 112, 79, 86 96, 92, 96, 88, 112, 86, 88, 86 94, 102, 88, 83, 96, 100, 88, 92 98, 90, 88, 104, 81, 102, 94, 92 83, 102, 86, 92, 79, 98, 86, 86 83, 106, 83, 98, 90, 100, 102, 104 90, 98, 98, 98, 104, 85, 92, 98 100, 110, 98, 128, 112, 106, 112, 98 90, 119, 94, 106, 128, 132, 123, 114 119, 142, 121, 121, 142, 130, 135, 156 135, 146, 177, 164, 135, 151, 156, 169 135, 154, 135, 114, 123, 112, 94, 106 100, 96, 108, 96, 98, 85, 92, 79 123, 102, 88, 86, 90, 88, 88, 94 96, 86, 74, 79, 88, 100, 88, 85 88, 85, 86, 112, 96, 88, 86, 85 94, 86, 90, 86, 79, 92, 77, 81 92, 94, 104, 96, 88, 94, 98, 90 100, 85, 92, 106, 110, 110, 108, 98 96, 112, 102, 130, 94, 94, 88, 96 98, 96, 86, 72, 76, 94, 90, 83 104, 94, 106, 64, 85, 67, 90, 90 52, 98, 88, 74, 83, 85, 83, 67 86, 83, 83, 83, 76, 90, 77, 85 71, 79, 79, 94, 94, 88, 81, 92 86, 69, 88, 81, 90, 88, 86, 90 72, 76, 90, 88, 92, 98, 77, 92 98, 92, 76, 88, 79, 85, 90, 94 85, 85, 77, 72, 64, 92, 67, 69 69, 79, 76, 96, 55, 71, 85, 86 71, 66, 72, 86, 67, 72, 64, 85 79, 72, 85, 83, 79, 85, 83, 77 79, 100, 71, 83, 67, 64, 88, 66 85, 67, 85, 72, 94, 77, 76, 86 72, 58, 76, 64, 55, 79, 83, 74 88, 77, 77, 86, 79, 76, 62, 81 71, 71, 71, 85, 81, 76, 88, 85 81, 72, 100, 67, 83, 53, 72, 62 86, 66, 72, 81, 92, 79, 74, 77 85, 69, 86, 85, 71, 94, 83, 74 92, 76, 74, 88, 85, 100, 90, 72 69, 88, 85, 92, 92, 72, 100, 77 98, 102, 67, 88, 98, 88, 83, 100 112, 85, 96, 106, 104, 106, 110, 114 117, 96, 100, 92, 85, 102, 90, 83 94, 79, 76, 90, 86, 71, 64, 72 81, 77, 83, 86, 94, 83, 83, 85 72, 88, 90, 76, 86, 72, 83, 79 76, 74, 81, 92, 86, 86, 71, 90 94, 96, 92, 94, 90, 98, 408, 96 110, 112, 112, 110, 114, 100, 92, 98 114, 108, 90, 98, 92, 94, 98, 100 108, 85, 114, 94, 110, 102, 94, 106 98, 130, 102, 96, 135, 110, 104, 114 114, 114, 144, 125, 130, 154, 159, 182 164, 174, 169, 202, 188, 246, 228, 216 234, 246, 240, 246, 237, 231, 259, 228 216, 196, 210, 182, 199, 185, 199, 180 166, 169, 177, 182, 154, 149, 159, 159 177, 130, 142, 146, 146, 149, 142, 137 144, 132, 159, 154, 130, 137, 137, 137 139, 144, 177, 151, 193, 159, 219, 228 269, 303, 328, 357, 408, 488, 524, 493 571, 520, 548, 462, 412, 299, 213, 196 188, 161, 128, 149, 112, 137, 142, 108 142, 125, 123, 108, 125, 132, 104, 117 130, 114, 144, 144, 108, 125, 108, 123 132, 108, 110, 114, 104, 117, 130, 130 88, 106, 90, 117, 106, 400, 117, 130 130, 114, 135, 149, 146, 169, 151, 174 164, 177, 202, 204, 182, 202, 185, 180 137, 130, 132, 119, 102, 123, 125, 117 110, 108, 112, 125, 102, 123, 130, 108 110, 104, 110, 128, 137, 112, 108, 112 117, 121, 114, 106, 114, 119, 114, 114 117, 123, 128, 137, 144, 132, 125, 130 112, 125, 135, 123, 139, 151, 128, 112 117, 125, 149, 119, 123, 114, 123, 117 102, 100, 102, 125, 121, 346, 119, 135 139, 182, 156, 177, 151, 166, 177, 185 188, 213, 202, 177, 172, 182, 154, 161 146, 130, 164, 144, 139, 144, 144, 166 121, 164, 137, 142, 151, 142, 132, 151 159, 156, 161, 190, 213, 207, 256, 253 250, 231, 256, 246, 246, 246, 204, 199 196, 161, 123, 154, 154, 123, 142, 119 106, 110, 154, 154, 104, 119, 125, 137 130, 142, 159, 139, 132, 149, 137, 130 142, 142, 172, 156, 144, 156, 161, 156 154, 169, 166, 166, 207, 193, 234, 193 216, 207, 231, 219, 207, 190, 188, 202 174, 207, 182, 182, 182, 202, 196, 199 185, 213, 188, 240, 228, 266, 286, 272 279, 216, 210, 213, 182, 159, 159, 156 144, 149, 154, 128, 125, 142, 139, 149 139, 132, 151, 149, 135, 149, 164, 164 149, 164, 190, 185, 161, 180, 188, 207 207, 231, 259, 279, 313, 428, 480, 640 724, 961, 1043, 1211, 1391, 1640, 2172, 2570 2862, 3260, 3600, 3564, 3080, 2391, 1980, 1444 942, 595, 471, 412, 372, 369, 313, 253 262, 234, 216, 234, 199, 237, 243, 222 207, 204, 216, 185, 202, 228, 246, 207 216, 193, 222, 222, 222, 237, 234, 292 279, 346, 380, 376, 357, 353, 342, 324 313, 310, 324, 350, 350, 328, 449, 420 471, 480, 458, 480, 449, 458, 502, 543 655, 745, 829, 778, 784, 650, 620, 524 404, 313, 276, 250, 231, 243, 222, 207 185, 213, 193, 177, 172, 154, 185, 169 149, 146, 132, 123, 159, 174, 174, 146 166, 164, 154, 121, 154, 125, 114, 125 108, 108, 117, 102, 125, 106, 125, 139 102, 112, 110, 114, 121, 128, 123, 123 128, 106, 114, 128, 114, 119, 114, 104 108, 100, 108, 108, 119, 98, 130, 117 98, 102, 121, 119, 114, 110, 121, 121 119, 144, 117, 119, 123, 121, 121, 146 123, 123, 135, 128, 142, 149, 159, 151 199, 207, 202, 193, 164, 161, 169, 166 144, 174, 139, 154, 161, 159, 177, 172 180, 193, 185, 172, 190, 169, 159, 169 151, 144, 159, 139, 169, 182, 196, 234 279, 225, 250, 188, 172, 166, 169, 130 156, 108, 112, 142, 125, 128, 137, 132 130, 137, 130, 146, 121, 132, 114, 98 137, 104, 125, 128, 121, 121, 114, 117 121, 121, 110, 146, 125, 149, 149, 146 151, 135, 135, 144, 128, 130, 108, 106 119, 106, 130, 114, 121, 123, 144, 149 166, 149, 164, 180, 180, 207, 204, 222 222, 180, 177, 185, 149, 132, 104, 128 117, 98, 102, 92, 130, 108, 102, 119 104, 94, 108, 106, 104, 108, 110, 90 94, 83, 106, 85, 69, 98, 94, 104 92, 81, 92, 88, 102, 102, 86, 83 90, 96, 83, 90, 79, 83, 77, 71 69, 79, 86, 72, 77, 76, 98, 74 85, 86, 77, 77, 86, 90, 83, 86 83, 92, 96, 100, 102, 98, 96, 85 90, 61, 92, 88, 77, 88, 98, 77 94, 106, 88, 88, 76, 83, 94, 96 92, 106, 71, 96, 81, 86, 100, 77 88, 106, 71, 96, 96, 98, 100, 94 125, 98, 114, 94, 112, 114, 104, 114 149, 139, 119, 117, 98, 102, 130, 112 114, 128, 128, 117, 117, 139, 135, 169 132, 154, 172, 172, 180, 172, 196, 193 210, 180, 219, 196, 213, 225, 234, 225 228, 216, 210, 234, 219, 266, 219, 234 259, 234, 234, 272, 292, 292, 246, 331 328, 269, 296, 317, 272, 317, 286, 299 296, 279, 272, 256, 250, 246, 228, 210 185, 222, 219, 190, 180, 169, 164, 164 174, 182, 169, 151, 156, 159, 139, 137 146, 135, 130, 149, 156, 149, 142, 144 135, 142, 161, 146, 144, 146, 154, 144 161, 144, 151, 121, 149, 146, 146, 146 137, 137, 114, 144, 137, 125, 128, 137 146, 146, 156, 146, 130, 154, 177, 210 228, 243, 237, 237, 310, 328, 428, 671 918, 980, 870, 610, 576, 655, 581, 493 313, 231, 210, 196, 182, 177, 166, 174 151, 149, 164, 169, 172, 174, 156, 177 199, 174, 161, 202, 164, 159, 177, 142 149, 149, 169, 146, 161, 172, 149, 169 166, 169, 172, 172, 169, 193, 172, 174 185, 172, 169, 169, 174, 188, 164, 210 207, 196, 180, 193, 177, 182, 169, 174 177, 154, 169, 149, 130, 130, 119, 112 96, 96, 100, 104, 132, 117, 121, 110 94, 104, 108, 114, 110, 117, 121, 108 100, 114, 123, 112, 114, 110, 112, 121 123, 130, 125, 132, 135, 125, 102, 102 102, 112, 104, 104, 90, 128, 117, 112 98, 102, 121, 102, 112, 104, 119, 102 104, 94, 102, 112, 94, 94, 90, 100 104, 108, 102, 96, 108, 119, 106, 114 130, 130, 144, 169, 180, 188, 228, 256 250, 292, 310, 299, 276, 262, 240, 193 193, 193, 159, 182, 110, 123, 123, 108 119, 117, 117, 98, 96, 119, 125, 112 121, 128, 108, 112, 100, 114, 110, 130 137, 139, 166, 156, 130, 137, 180, 185 172, 210, 225, 259, 299, 246, 240, 216 202, 190, 161, 159, 139, 102, 92, 104 104, 110, 94, 100, 94, 100, 100, 110 112, 104, 92, 98, 119, 110, 117, 100 106, 112, 123, 110, 94, 123, 119, 106 96, 100, 112, 110, 112, 94, 102, 110 102, 112, 110, 112, 130, 137, 117, 130 119, 112, 110, 106, 128, 130, 121, 98 112, 117, 119, 108, 117, 128, 117, 135 128, 142, 117, 125, 146, 139, 144, 164 137, 121, 130, 144, 135, 137, 130, 130 125, 121, 130, 137, 144, 139, 139, 156 174, 161, 164, 149, 166, 154, 161, 177 222, 199, 190, 234, 240, 234, 279, 313 320, 310, 266, 240, 240, 237, 213, 213 207, 154, 149, 125, 117, 137, 139, 130 114, 110, 110, 123, 130, 104, 119, 100 92, 121, 125, 85, 104, 108, 64, 98 85, 85, 106, 96, 90, 76, 102, 96 86, 79, 102, 83, 94, 94, 85, 90 100, 102, 92, 94, 102, 108, 114, 92 85, 88, 92, 94, 85, 119, 79, 96 100, 83, 317, 94, 104, 94, 85, 88 92, 110, 98, 85, 117, 110, 106, 102 121, 108, 135, 88, 119, 119, 102, 117 96, 85, 96, 88, 98, 88, 100, 71 79, 96, 94, 100, 114, 128, 112, 108 123, 123, 130, 159, 164, 169, 137, 146 137, 149, 130, 125, 128, 123, 123, 102 123, 117, 130, 117, 114, 135, 132, 121 135, 121, 117, 119, 117, 154, 139, 144 112, 144, 144, 154, 146, 172, 199, 193 216, 202, 237, 237, 256, 234, 282, 234 193, 193, 216, 196, 193, 216, 193, 199 219, 196, 204, 207, 231, 243, 272, 289 246, 243, 228, 182, 193, 185, 174, 151 151, 128, 125, 119, 117, 108, 106, 96 102, 94, 96, 85, 92, 100, 96, 72 90, 92, 114, 86, 88, 88, 92, 100 77, 83, 72, 77, 77, 67, 88, 85 90, 79, 88, 96, 94, 83, 79, 71 66, 94, 67, 96, 76, 71, 94, 85 77, 62, 71, 92, 112, 79, 92, 96 100, 83, 76, 86, 90, 66, 72, 77 90, 62, 69, 72, 81, 85, 76, 72 76, 77, 79, 79, 79, 79, 77, 66 64, 90, 86, 79, 92, 85, 79, 59 67, 81, 85, 79, 79, 83, 85, 119 88, 104, 90, 100, 96, 92, 104, 98 90, 92, 104, 100, 94, 123, 100, 110 100, 88, 90, 117, 96, 102, 117, 96 83, 96, 102, 77, 94, 85, 77, 96 85, 81, 90, 92, 83, 90, 90, 77 81, 92, 71, 90, 88, 102, 76, 83 79, 94, 86, 98, 76, 96, 96, 85 92, 88, 88, 88, 98, 106, 110, 90 110, 102, 92, 76, 112, 110, 106, 110 98, 108, 102, 94, 104, 123, 125, 119 117, 104, 110, 121, 125, 114, 121, 117 119, 132, 125, 119, 142, 151, 164, 144 169, 149, 146, 149, 164, 196, 231, 246 310, 350, 445, 557, 610, 630, 702, 812 858, 876, 790, 692, 562, 515, 502, 471 376, 317, 237, 202, 154, 139, 119, 100 125, 121, 123, 125, 128, 144, 132, 164 159, 151, 193, 166, 182, 182, 174, 174 164, 142, 130, 125, 128, 104, 121, 106 90, 88, 100, 100, 102, 90, 79, 114 108, 121, 100, 114, 125, 123, 104, 110 96, 110, 123, 108, 102, 121, 102, 110 110, 110, 92, 108, 114, 100, 92, 125 94, 88, 102, 76, 96, 79, 86, 85 69, 79, 64, 67, 71, 67, 55, 71 67, 76, 67, 79, 76, 77, 59, 66 94, 76, 86, 83, 90, 85, 98, 81 90, 83, 100, 102, 94, 72, 96, 90 86, 106, 77, 92, 86, 100, 90, 83 67, 100, 88, 98, 83, 100, 76, 92 85, 76, 77, 92, 94, 79, 96, 94 96, 90, 96, 121, 102, 85, 102, 83 96, 104, 96, 94, 98, 90, 108, 128 128, 104, 106, 123, 104, 119, 94, 92 104, 117, 100, 98, 104, 102, 90, 102 94, 104, 110, 114, 112, 108, 100, 119 92, 86, 102, 110, 90, 108, 108, 135 130, 128, 114, 106, 121, 106, 135, 130 114, 112, 117, 132, 128, 108, 139, 123 144, 119, 128, 125, 132, 130, 130, 119 128, 121, 132, 125, 149, 125, 128, 128 135, 139, 144, 135, 139, 121, 146, 137 151, 123, 151, 144, 159, 182, 204, 202 237, 234, 292, 317, 317, 324, 299, 299 272, 276, 282, 269, 234, 234, 246, 219 199, 177, 172, 159, 177, 154, 169, 180 164, 190, 188, 199, 204, 166, 182, 190 172, 174, 180, 188, 177, 166, 146, 130 137, 144, 123, 146, 130, 149, 139, 139 142, 142, 132, 159, 149, 132, 144, 137 121, 135, 130, 146, 123, 117, 137, 121 112, 130, 130, 117, 132, 114, 139, 102 110, 125, 130, 128, 110, 114, 132, 123 119, 112, 121, 123, 144, 159, 112, 151 130, 151, 130, 125, 121, 110, 130, 130 110, 104, 119, 96, 117, 121, 108, 123 110, 104, 100, 104, 100, 121, 79, 104 108, 110, 90, 125, 98, 106, 119, 112 112, 121, 108, 98, 106, 130, 100, 112 121, 139, 106, 114, 123, 100, 108, 88 106, 104, 100, 94, 106, 79, 86, 96 94, 102, 92, 96, 106, 106, 94, 86 114, 85, 100, 96, 121, 86, 98, 94 90, 92, 100, 112, 108, 102, 94, 86 94, 92, 100, 110, 74, 94, 98, 123 104, 98, 102, 119, 106, 102, 130, 96 112, 114, 110, 106, 121, 102, 123, 139 142, 146, 142, 121, 149, 139, 117, 139 130, 132, 125, 121, 119, 117, 117, 108 119, 106, 114, 123, 100, 104, 88, 108 121, 108, 121, 92, 119, 130, 121, 106 121, 112, 119, 119, 104, 117, 121, 135 100, 123, 135, 128, 130, 125, 154, 161 169, 154, 137, 128, 142, 164, 180, 180 188, 210, 243, 234, 313, 328, 369, 488 529, 581, 600, 681, 615, 548, 520, 428 400, 400, 428, 388, 384, 320, 282, 234 177, 188, 161, 154, 128, 135, 128, 125 128, 114, 132, 159, 114, 123, 135, 121 123, 119, 139, 119, 123, 146, 130, 128 121, 104, 110, 108, 151, 119, 112, 144 144, 117, 130, 130, 144, 130, 125, 137 149, 130, 119, 139, 137, 169, 137, 156 169, 137, 172, 154, 146, 190, 172, 185 196, 190, 199, 234, 320, 380, 372, 376 289, 234, 237, 240, 276, 269, 303, 324 292, 253, 269, 234, 243, 210, 202, 219 228, 213, 213, 207, 202, 188, 213, 180 169, 199, 166, 204, 164, 172, 161, 159 166, 151, 159, 151, 177, 166, 144, 149 142, 144, 159, 123, 151, 128, 119, 137 142, 130, 114, 135, 110, 128, 108, 121 125, 137, 114, 100, 114, 108, 114, 100 108, 106, 112, 100, 104, 96, 92, 94 106, 106, 100, 86, 106, 112, 100, 96 100, 98, 90, 102, 98, 100, 121, 88 83, 96, 102, 123, 104, 94, 94, 96 110, 100, 110, 112, 114, 121, 123, 104 108, 121, 128, 112, 100, 92, 108, 119 139, 137, 149, 137, 128, 130, 142, 149 161, 137, 169, 204, 199, 210, 190, 172 174, 151, 177, 154, 142, 146, 130, 144 123, 121, 130, 112, 106, 88, 94, 90 85, 92, 104, 102, 83, 62, 106, 88 108, 96, 98, 90, 88, 100, 96, 98 98, 94, 106, 119, 110, 102, 106, 119 121, 151, 146, 114, 121, 142, 132, 137 130, 128, 139, 146, 132, 132, 139, 132 130, 119, 130, 123, 130, 125, 112, 100 121, 106, 117, 119, 135, 110, 112, 104 92, 114, 96, 104, 92, 100, 114, 125 100, 94, 114, 420, 123, 110, 104, 106 104, 130, 90, 96, 123, 110, 119, 125 112, 112, 114, 104, 123, 110, 110, 102 106, 142, 125, 119, 132, 135, 132, 130 114, 112, 130, 119, 100, 128, 110, 125 110, 114, 94, 98, 86, 96, 94, 106 96, 104, 98, 104, 96, 112, 114, 96 85, 102, 85, 110, 102, 100, 106, 94 104, 102, 102, 100, 106, 112, 121, 104 114, 125, 117, 128, 121, 110, 121, 117 114, 132, 119, 117, 125, 108, 125, 104 108, 108, 130, 117, 130, 110, 146, 139 174, 182, 225, 253, 324, 313, 353, 369 400, 400, 361, 317, 328, 292, 286, 292 317, 339, 306, 299, 303, 328, 310, 331 396, 462, 581, 630, 718, 676, 666, 571 475, 471, 449, 497, 576, 576, 506, 449 420, 404, 296, 250, 250, 240, 228, 204 204, 188, 164, 149, 125, 137, 125, 104 149, 112, 94, 123, 119, 117, 125, 106 117, 123, 104, 137, 128, 102, 98, 117 114, 108, 121, 110, 125, 119, 108, 121 112, 132, 110, 98, 130, 125, 112, 121 137, 125, 128, 132, 149, 139, 146, 128 146, 135, 114, 151, 137, 164, 151, 130 142, 128, 137, 125, 144, 125, 130, 137 159, 137, 149, 125, 130, 132, 123, 130 117,/