SampleIdent,907A-5-3/27,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 9-aug-1993 1:52,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 96, 85, 112, 90, 102, 100, 90, 112 96, 123, 117, 108, 108, 102, 110, 106 100, 96, 83, 96, 100, 96, 98, 108 79, 102, 96, 117, 106, 106, 117, 98 108, 104, 121, 104, 100, 104, 110, 117 117, 104, 123, 121, 104, 100, 108, 110 114, 108, 106, 102, 121, 123, 110, 125 128, 135, 119, 123, 130, 132, 130, 117 123, 125, 130, 137, 119, 121, 123, 110 137, 128, 139, 117, 125, 121, 121, 121 130, 128, 137, 137, 130, 125, 96, 123 144, 139, 130, 123, 139, 142, 130, 144 108, 123, 135, 142, 117, 137, 164, 128 144, 110, 110, 130, 128, 119, 125, 458 104, 117, 130, 123, 139, 121, 137, 146 125, 114, 121, 130, 119, 123, 123, 130 121, 123, 130, 117, 117, 123, 125, 108 125, 135, 137, 119, 106, 137, 130, 125 125, 130, 102, 117, 156, 130, 119, 156 119, 114, 130, 85, 121, 130, 114, 119 135, 100, 106, 154, 146, 132, 114, 125 137, 137, 108, 132, 110, 130, 130, 123 117, 125, 121, 119, 137, 137, 132, 172 154, 161, 142, 164, 154, 151, 132, 151 135, 108, 100, 121, 104, 98, 102, 106 110, 96, 119, 104, 90, 108, 88, 98 88, 106, 96, 100, 121, 112, 94, 114 90, 90, 100, 104, 94, 98, 94, 92 106, 108, 92, 92, 108, 98, 106, 88 119, 98, 74, 85, 108, 100, 94, 90 108, 117, 94, 88, 108, 86, 72, 108 96, 104, 83, 85, 94, 83, 98, 102 117, 88, 100, 100, 94, 98, 102, 92 92, 92, 98, 100, 79, 98, 92, 92 85, 83, 81, 100, 110, 92, 94, 94 94, 94, 98, 79, 85, 86, 100, 88 96, 94, 100, 98, 85, 100, 94, 96 104, 96, 77, 100, 85, 98, 88, 74 77, 98, 94, 100, 96, 88, 106, 96 102, 108, 79, 94, 100, 94, 79, 76 76, 96, 94, 85, 102, 100, 98, 81 98, 90, 88, 92, 83, 132, 108, 90 85, 106, 88, 88, 94, 92, 112, 86 90, 96, 102, 100, 98, 79, 112, 104 106, 110, 119, 114, 114, 98, 112, 114 110, 106, 106, 144, 156, 142, 149, 146 164, 154, 142, 144, 130, 130, 123, 132 132, 130, 125, 108, 117, 83, 96, 88 72, 100, 86, 86, 106, 106, 83, 98 92, 86, 79, 102, 81, 77, 88, 86 79, 77, 86, 88, 76, 86, 98, 98 67, 98, 59, 85, 67, 71, 86, 88 88, 98, 67, 94, 98, 88, 94, 88 98, 79, 96, 96, 86, 92, 85, 88 94, 88, 102, 92, 104, 125, 98, 90 106, 79, 104, 106, 104, 79, 85, 90 79, 88, 94, 98, 96, 88, 104, 79 92, 86, 85, 85, 76, 85, 79, 83 102, 96, 79, 79, 76, 74, 67, 77 56, 90, 83, 92, 64, 77, 76, 83 81, 83, 74, 81, 72, 69, 85, 83 83, 86, 74, 79, 83, 85, 77, 83 94, 85, 79, 100, 96, 77, 81, 76 86, 76, 79, 86, 90, 102, 72, 77 66, 88, 71, 72, 88, 88, 61, 59 77, 79, 83, 88, 76, 92, 72, 88 85, 88, 74, 85, 76, 94, 83, 62 85, 85, 88, 77, 74, 81, 59, 77 72, 72, 79, 67, 83, 59, 71, 64 69, 66, 81, 77, 72, 66, 72, 72 83, 79, 69, 67, 79, 66, 76, 77 83, 72, 79, 88, 71, 88, 50, 76 72, 77, 81, 71, 76, 67, 85, 77 86, 90, 72, 90, 67, 77, 77, 77 76, 69, 67, 81, 61, 74, 83, 88 62, 72, 81, 79, 90, 66, 85, 72 72, 67, 77, 83, 77, 61, 77, 77 69, 69, 86, 79, 86, 94, 74, 94 85, 85, 102, 106, 86, 83, 110, 104 106, 88, 83, 90, 86, 102, 79, 94 104, 85, 100, 90, 76, 85, 76, 96 77, 90, 79, 77, 90, 74, 71, 90 79, 86, 102, 74, 74, 81, 69, 85 77, 71, 92, 83, 88, 66, 79, 71 90, 76, 90, 76, 71, 92, 85, 85 79, 90, 94, 96, 88, 96, 112, 102 88, 85, 90, 88, 81, 108, 92, 77 92, 85, 100, 88, 88, 88, 108, 92 108, 77, 98, 104, 98, 90, 104, 123 98, 90, 110, 112, 128, 104, 106, 146 135, 135, 137, 137, 142, 156, 154, 135 210, 182, 185, 193, 207, 196, 161, 243 210, 210, 193, 228, 213, 202, 207, 169 185, 199, 172, 185, 193, 166, 144, 151 135, 156, 164, 146, 128, 139, 149, 144 117, 164, 149, 149, 130, 130, 125, 142 137, 144, 117, 132, 130, 137, 144, 137 137, 164, 159, 169, 193, 225, 259, 253 299, 299, 320, 324, 342, 357, 384, 396 416, 361, 342, 324, 240, 246, 188, 182 156, 139, 142, 130, 139, 121, 108, 130 112, 128, 119, 114, 125, 119, 119, 117 119, 123, 117, 119, 108, 112, 100, 98 108, 117, 121, 102, 92, 110, 137, 86 128, 112, 119, 119, 110, 119, 117, 112 121, 144, 139, 156, 130, 169, 182, 172 154, 174, 180, 159, 188, 154, 132, 142 121, 102, 128, 90, 94, 100, 110, 108 96, 123, 110, 102, 90, 102, 121, 112 98, 112, 102, 104, 106, 112, 77, 88 130, 112, 112, 110, 121, 121, 121, 130 121, 123, 112, 142, 104, 137, 114, 137 130, 132, 151, 151, 137, 137, 125, 139 151, 117, 112, 132, 110, 94, 90, 130 144, 125, 137, 142, 149, 174, 154, 130 169, 177, 137, 161, 199, 161, 180, 193 199, 166, 172, 169, 177, 139, 139, 144 135, 135, 125, 123, 117, 137, 121, 119 135, 104, 125, 142, 130, 119, 174, 174 151, 151, 161, 156, 164, 172, 161, 182 180, 149, 159, 185, 166, 172, 154, 130 149, 159, 130, 144, 142, 117, 123, 117 110, 121, 130, 132, 121, 121, 119, 106 121, 146, 139, 123, 142, 159, 137, 121 437, 137, 144, 149, 164, 149, 146, 169 159, 154, 174, 159, 144, 199, 177, 185 161, 180, 164, 172, 182, 174, 166, 169 182, 185, 185, 202, 177, 190, 199, 213 199, 174, 177, 159, 164, 166, 169, 164 149, 137, 161, 149, 156, 125, 137, 132 144, 112, 104, 98, 112, 128, 108, 117 121, 132, 128, 123, 142, 128, 146, 137 156, 146, 177, 174, 193, 196, 202, 234 219, 253, 313, 320, 369, 497, 534, 686 756, 942, 1163, 1310, 1459, 1529, 1624, 1806 1823, 1910, 1756, 1616, 1608, 1414, 1116, 906 697, 566, 408, 335, 276, 256, 276, 237 237, 222, 253, 210, 216, 210, 202, 177 174, 202, 213, 174, 164, 172, 164, 177 193, 161, 166, 185, 213, 188, 202, 213 231, 234, 259, 272, 225, 240, 272, 246 289, 303, 303, 342, 299, 357, 380, 353 384, 548, 380, 412, 428, 424, 424, 424 471, 445, 433, 412, 400, 369, 369, 445 605, 734, 681, 590, 458, 484, 408, 286 219, 207, 207, 204, 188, 193, 166, 164 185, 154, 156, 137, 156, 123, 106, 110 121, 130, 125, 123, 121, 132, 128, 98 139, 112, 132, 114, 114, 123, 106, 108 106, 96, 104, 117, 92, 106, 123, 135 119, 121, 130, 121, 121, 106, 110, 112 114, 98, 92, 121, 112, 117, 96, 102 100, 114, 117, 100, 106, 108, 98, 119 112, 108, 112, 119, 114, 108, 130, 130 144, 151, 149, 142, 180, 132, 166, 193 156, 159, 185, 154, 166, 172, 172, 161 164, 174, 172, 169, 174, 166, 151, 151 137, 128, 135, 130, 149, 142, 156, 128 139, 180, 243, 253, 188, 196, 204, 202 169, 151, 130, 166, 135, 146, 137, 135 132, 128, 125, 142, 151, 185, 174, 199 161, 144, 137, 146, 132, 108, 104, 119 121, 108, 117, 104, 112, 112, 117, 106 125, 112, 125, 121, 142, 164, 149, 139 130, 142, 130, 130, 125, 139, 110, 114 123, 119, 108, 123, 108, 119, 117, 125 151, 149, 128, 177, 159, 174, 151, 156 169, 164, 146, 156, 125, 146, 121, 117 128, 117, 110, 96, 114, 121, 104, 106 90, 76, 108, 119, 94, 94, 110, 94 98, 72, 85, 98, 94, 90, 100, 92 90, 85, 92, 83, 77, 88, 90, 79 81, 88, 85, 64, 67, 85, 76, 62 62, 79, 79, 59, 88, 74, 76, 94 92, 96, 77, 83, 88, 106, 83, 72 96, 90, 81, 74, 100, 94, 85, 88 77, 106, 88, 94, 88, 79, 98, 104 94, 92, 85, 77, 81, 346, 83, 96 76, 77, 96, 77, 94, 94, 88, 86 137, 135, 161, 144, 121, 112, 151, 125 132, 119, 117, 144, 119, 98, 125, 139 128, 112, 104, 114, 106, 121, 125, 110 130, 130, 149, 123, 139, 135, 154, 156 149, 159, 149, 132, 182, 196, 188, 202 207, 207, 213, 225, 213, 216, 234, 225 228, 246, 237, 231, 231, 246, 276, 246 262, 282, 299, 306, 279, 282, 335, 299 320, 292, 328, 266, 256, 286, 303, 266 286, 256, 225, 204, 210, 199, 196, 182 177, 185, 151, 172, 154, 174, 154, 164 146, 164, 164, 139, 154, 146, 144, 139 135, 125, 156, 125, 164, 144, 151, 188 169, 144, 139, 156, 151, 151, 144, 130 149, 156, 144, 128, 128, 146, 128, 135 137, 125, 137, 117, 139, 125, 159, 130 151, 142, 132, 135, 172, 169, 185, 190 207, 237, 262, 272, 292, 299, 313, 350 372, 515, 475, 420, 376, 331, 372, 299 243, 222, 207, 185, 169, 166, 149, 161 135, 166, 169, 182, 149, 139, 154, 177 159, 149, 156, 135, 144, 164, 169, 172 146, 128, 132, 137, 146, 169, 149, 174 151, 166, 177, 185, 159, 169, 177, 154 177, 193, 185, 193, 213, 172, 185, 228 190, 188, 188, 199, 174, 185, 185, 146 151, 159, 151, 149, 149, 125, 130, 104 112, 119, 114, 110, 108, 121, 96, 119 121, 98, 123, 104, 106, 121, 121, 112 137, 123, 130, 121, 135, 142, 108, 106 117, 117, 121, 114, 102, 123, 112, 110 98, 102, 121, 102, 110, 119, 110, 108 128, 117, 108, 98, 117, 121, 114, 117 98, 92, 98, 104, 102, 112, 98, 92 104, 100, 110, 106, 114, 100, 128, 130 132, 149, 154, 164, 182, 204, 193, 240 237, 276, 213, 256, 234, 240, 196, 196 190, 196, 151, 135, 128, 130, 114, 106 121, 106, 102, 100, 92, 117, 128, 117 128, 121, 110, 117, 106, 106, 110, 125 117, 128, 135, 128, 137, 161, 156, 164 159, 169, 174, 154, 174, 188, 180, 156 146, 161, 132, 130, 137, 110, 121, 110 96, 119, 112, 98, 104, 108, 94, 102 96, 117, 90, 92, 102, 108, 106, 114 102, 110, 100, 123, 100, 119, 104, 104 110, 96, 108, 108, 88, 123, 114, 114 137, 132, 114, 130, 112, 100, 104, 108 125, 102, 110, 98, 108, 119, 108, 104 88, 117, 110, 117, 123, 132, 100, 121 125, 92, 119, 130, 108, 119, 121, 137 104, 104, 135, 130, 128, 108, 121, 123 156, 117, 128, 114, 121, 128, 119, 137 125, 110, 149, 137, 156, 164, 180, 180 204, 240, 276, 346, 365, 346, 353, 310 313, 320, 279, 303, 246, 228, 193, 199 172, 169, 142, 149, 146, 121, 125, 114 125, 114, 100, 125, 104, 90, 98, 100 102, 98, 110, 123, 112, 114, 128, 106 110, 125, 121, 72, 79, 94, 96, 94 90, 96, 83, 85, 100, 83, 98, 104 79, 92, 85, 110, 86, 96, 100, 94 88, 117, 77, 88, 112, 102, 98, 92 106, 102, 98, 110, 98, 102, 72, 102 104, 85, 108, 119, 108, 106, 100, 121 114, 130, 104, 98, 100, 98, 90, 100 85, 106, 98, 94, 81, 96, 74, 98 98, 98, 96, 96, 100, 132, 121, 144 137, 149, 142, 139, 151, 149, 121, 117 108, 117, 123, 125, 92, 114, 102, 123 146, 100, 125, 130, 117, 114, 119, 137 130, 121, 112, 125, 132, 135, 130, 132 137, 154, 164, 149, 185, 159, 172, 174 159, 169, 180, 159, 216, 207, 202, 202 188, 185, 180, 154, 164, 174, 185, 177 164, 169, 159, 172, 213, 193, 237, 222 199, 199, 196, 164, 137, 149, 164, 159 137, 119, 128, 102, 117, 83, 94, 88 114, 104, 96, 79, 85, 96, 102, 83 94, 108, 106, 106, 98, 90, 85, 86 98, 92, 79, 96, 90, 100, 86, 92 79, 90, 74, 69, 76, 71, 85, 83 83, 88, 79, 62, 77, 88, 85, 96 67, 67, 94, 94, 100, 92, 92, 90 74, 88, 96, 88, 98, 85, 76, 90 72, 67, 79, 72, 71, 79, 72, 76 71, 83, 72, 72, 64, 62, 79, 58 62, 69, 83, 79, 62, 62, 71, 69 76, 62, 76, 90, 92, 76, 85, 77 94, 104, 96, 108, 110, 92, 100, 77 83, 92, 85, 104, 104, 121, 96, 92 104, 112, 96, 104, 90, 90, 83, 96 79, 88, 86, 92, 90, 77, 88, 76 67, 76, 77, 66, 72, 86, 72, 59 90, 71, 76, 83, 96, 71, 76, 72 71, 67, 92, 74, 88, 128, 161, 169 121, 98, 117, 112, 117, 135, 132, 98 98, 83, 100, 104, 88, 102, 100, 92 83, 71, 83, 85, 102, 77, 83, 100 81, 88, 100, 77, 104, 98, 94, 86 86, 106, 90, 112, 94, 130, 106, 123 119, 142, 130, 169, 154, 188, 228, 207 234, 286, 296, 346, 392, 462, 404, 467 497, 458, 437, 380, 353, 299, 296, 266 240, 216, 177, 151, 123, 117, 114, 104 110, 114, 117, 112, 104, 121, 117, 106 100, 121, 108, 146, 106, 121, 112, 104 110, 96, 121, 92, 79, 104, 102, 112 72, 102, 86, 94, 94, 94, 96, 88 88, 130, 117, 110, 104, 102, 100, 106 102, 106, 96, 92, 77, 76, 81, 85 77, 92, 67, 86, 71, 71, 62, 66 79, 69, 71, 58, 71, 72, 85, 69 66, 71, 76, 81, 72, 67, 66, 59 62, 72, 67, 56, 76, 62, 81, 74 83, 71, 76, 86, 72, 83, 108, 85 79, 90, 81, 77, 76, 85, 86, 85 88, 96, 90, 79, 85, 85, 83, 81 98, 85, 77, 72, 90, 88, 94, 81 85, 76, 92, 77, 83, 86, 88, 83 77, 81, 94, 92, 108, 100, 92, 100 90, 88, 104, 92, 83, 108, 117, 106 121, 112, 98, 130, 100, 98, 117, 132 108, 108, 104, 112, 102, 108, 96, 98 123, 117, 98, 102, 106, 100, 104, 86 104, 114, 106, 100, 110, 94, 117, 98 112, 117, 108, 112, 130, 110, 98, 130 119, 108, 128, 119, 121, 125, 114, 96 117, 114, 112, 125, 123, 112, 135, 108 119, 128, 110, 139, 119, 128, 146, 110 132, 121, 110, 100, 114, 123, 121, 121 130, 135, 156, 164, 172, 188, 174, 196 210, 259, 234, 256, 269, 228, 259, 250 213, 207, 237, 219, 216, 213, 188, 174 196, 180, 182, 174, 188, 166, 174, 210 202, 225, 225, 204, 216, 199, 207, 190 193, 180, 180, 159, 146, 169, 139, 149 132, 149, 119, 144, 142, 149, 164, 139 156, 146, 139, 135, 132, 128, 137, 139 130, 146, 135, 135, 130, 119, 123, 123 117, 130, 125, 121, 137, 156, 146, 169 151, 164, 108, 104, 121, 125, 144, 146 132, 114, 121, 144, 146, 135, 142, 132 94, 144, 142, 108, 130, 130, 123, 125 119, 114, 94, 108, 98, 100, 106, 106 119, 108, 96, 106, 110, 98, 102, 106 100, 110, 114, 119, 98, 104, 86, 88 85, 102, 85, 98, 110, 88, 83, 102 104, 110, 104, 98, 94, 102, 104, 98 98, 94, 92, 104, 106, 121, 119, 98 108, 112, 125, 135, 110, 110, 114, 106 90, 123, 128, 102, 92, 106, 92, 90 94, 94, 123, 77, 83, 112, 112, 112 85, 85, 96, 96, 92, 98, 79, 110 98, 102, 96, 104, 83, 112, 114, 76 98, 100, 125, 104, 110, 92, 121, 130 108, 77, 110, 112, 106, 117, 110, 110 117, 108, 90, 123, 102, 119, 94, 90 104, 110, 114, 112, 94, 104, 108, 96 123, 117, 132, 117, 108, 96, 108, 114 112, 104, 108, 128, 117, 353, 123, 137 110, 137, 102, 104, 139, 132, 128, 142 144, 125, 132, 123, 144, 151, 172, 180 185, 204, 269, 286, 296, 320, 350, 384 416, 404, 392, 458, 437, 412, 361, 384 320, 310, 286, 266, 292, 282, 231, 228 202, 164, 151, 151, 135, 154, 130, 130 130, 119, 132, 125, 123, 125, 132, 121 121, 123, 130, 125, 132, 132, 149, 123 117, 130, 128, 94, 144, 121, 121, 137 146, 154, 137, 132, 144, 123, 139, 139 142, 132, 154, 154, 146, 146, 146, 164 172, 149, 164, 172, 174, 164, 166, 169 188, 174, 225, 180, 190, 188, 225, 204 219, 225, 222, 193, 207, 243, 207, 259 240, 222, 237, 210, 210, 207, 216, 240 204, 210, 213, 202, 188, 174, 182, 172 177, 174, 196, 164, 169, 146, 151, 166 166, 144, 164, 142, 137, 151, 156, 151 130, 137, 159, 154, 114, 130, 125, 123 114, 121, 117, 108, 106, 90, 130, 98 117, 117, 125, 106, 98, 98, 110, 108 117, 98, 108, 106, 88, 86, 106, 94 81, 112, 104, 100, 112, 88, 92, 92 108, 86, 86, 85, 94, 94, 100, 88 96, 123, 98, 106, 96, 100, 117, 90 110, 104, 108, 108, 100, 117, 119, 110 100, 106, 117, 123, 125, 110, 130, 108 119, 114, 114, 135, 149, 139, 146, 154 123, 146, 139, 166, 144, 151, 174, 188 149, 149, 169, 146, 130, 137, 125, 132 108, 121, 117, 121, 96, 104, 102, 108 98, 119, 74, 94, 98, 100, 108, 76 96, 77, 76, 77, 108, 94, 92, 114 81, 96, 100, 114, 104, 92, 102, 100 94, 108, 123, 104, 106, 121, 102, 119 142, 125, 125, 135, 137, 112, 114, 128 110, 110, 121, 117, 130, 119, 104, 106 128, 121, 106, 106, 90, 114, 112, 110 79, 104, 104, 100, 117, 98, 94, 110 112, 135, 123, 132, 149, 130, 117, 114 119, 123, 121, 117, 119, 104, 108, 102 108, 137, 110, 104, 112, 92, 86, 104 108, 108, 119, 88, 100, 106, 121, 114 112, 106, 96, 119, 102, 108, 86, 108 96, 90, 90, 79, 90, 102, 98, 90 83, 96, 85, 86, 86, 96, 81, 83 88, 85, 76, 90, 74, 86, 85, 100 94, 90, 121, 100, 102, 102, 98, 92 94, 112, 125, 98, 128, 119, 108, 102 106, 128, 121, 119, 98, 100, 128, 114 123, 117, 117, 106, 137, 132, 137, 154 166, 196, 193, 228, 237, 299, 286, 279 310, 266, 262, 282, 237, 246, 282, 228 234, 240, 266, 228, 259, 253, 282, 276 292, 339, 376, 408, 420, 454, 449, 462 396, 400, 376, 384, 380, 376, 376, 365 339, 328, 282, 266, 210, 219, 199, 188 182, 146, 159, 149, 123, 128, 119, 110 102, 112, 104, 123, 98, 112, 92, 114 123, 114, 110, 92, 110, 110, 112, 102 132, 112, 100, 110, 112, 117, 106, 125 139, 108, 125, 139, 121, 144, 142, 114 119, 137, 146, 123, 146, 117, 110, 156 144, 144, 137, 130, 123, 125, 139, 159 121, 128, 135, 130, 139, 102, 123, 119 106, 108, 117, 98, 112, 108, 110, 102 128,/