SampleIdent,907A 6H-1 45-46 BULK,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,13-aug-1993 16:26,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 77, 96, 92, 86, 72, 79, 86, 92 88, 94, 92, 69, 81, 94, 79, 104 79, 96, 90, 92, 94, 106, 88, 86 98, 96, 79, 104, 100, 85, 92, 88 104, 100, 96, 108, 104, 98, 92, 100 100, 119, 112, 106, 114, 98, 102, 121 106, 92, 102, 121, 104, 108, 94, 130 117, 108, 130, 110, 125, 112, 117, 83 121, 128, 112, 106, 114, 110, 128, 108 123, 130, 128, 104, 123, 121, 119, 121 130, 130, 104, 94, 130, 125, 110, 112 135, 123, 128, 110, 135, 117, 114, 108 117, 114, 112, 130, 130, 128, 137, 121 130, 128, 114, 121, 96, 130, 119, 117 108, 117, 130, 132, 142, 117, 139, 128 135, 137, 135, 128, 123, 119, 135, 121 119, 128, 130, 128, 128, 135, 132, 114 123, 144, 142, 123, 121, 130, 144, 139 142, 130, 121, 142, 117, 132, 119, 132 106, 142, 123, 154, 125, 128, 132, 139 121, 130, 767, 123, 132, 146, 130, 128 130, 132, 159, 156, 128, 149, 154, 151 156, 142, 164, 149, 172, 146, 174, 177 161, 149, 159, 188, 169, 180, 174, 164 161, 188, 159, 159, 159, 132, 149, 117 132, 119, 117, 117, 114, 119, 90, 114 121, 117, 119, 104, 108, 110, 106, 123 106, 106, 108, 92, 88, 102, 90, 90 98, 121, 114, 108, 100, 110, 106, 98 90, 108, 112, 106, 98, 130, 110, 117 110, 106, 108, 112, 117, 110, 112, 92 112, 92, 94, 100, 88, 98, 100, 98 96, 74, 98, 92, 88, 90, 88, 96 98, 83, 77, 88, 98, 86, 92, 102 96, 108, 83, 85, 83, 104, 94, 92 114, 85, 90, 88, 94, 72, 96, 88 90, 86, 94, 85, 92, 88, 88, 92 100, 96, 100, 106, 92, 104, 96, 100 85, 98, 79, 119, 90, 79, 98, 376 92, 106, 98, 86, 92, 96, 86, 94 77, 100, 83, 92, 94, 102, 557, 88 67, 98, 88, 90, 100, 94, 94, 83 79, 104, 77, 92, 94, 85, 86, 102 102, 79, 94, 90, 94, 88, 90, 102 119, 114, 104, 128, 98, 104, 130, 121 125, 142, 149, 139, 128, 135, 151, 151 139, 159, 156, 151, 144, 151, 169, 149 164, 137, 159, 164, 139, 108, 104, 108 108, 110, 92, 108, 94, 88, 92, 92 102, 81, 79, 92, 92, 90, 86, 69 94, 77, 92, 88, 86, 83, 88, 86 98, 85, 94, 94, 72, 77, 83, 81 85, 90, 67, 69, 85, 77, 92, 88 85, 88, 108, 90, 76, 77, 77, 81 83, 85, 83, 90, 90, 108, 102, 81 102, 100, 98, 83, 106, 94, 90, 92 76, 90, 77, 69, 96, 85, 83, 81 67, 72, 71, 90, 86, 77, 85, 81 77, 76, 86, 94, 71, 72, 86, 76 77, 88, 85, 92, 72, 77, 86, 77 90, 81, 71, 88, 77, 66, 64, 67 79, 79, 83, 56, 79, 77, 72, 74 86, 92, 81, 67, 79, 79, 92, 81 79, 76, 77, 77, 88, 74, 85, 86 77, 76, 72, 81, 59, 83, 71, 71 94, 76, 79, 88, 72, 77, 83, 86 83, 85, 77, 85, 76, 64, 79, 76 72, 77, 77, 79, 76, 79, 77, 81 72, 76, 83, 74, 74, 85, 85, 62 85, 79, 77, 74, 83, 77, 76, 85 66, 72, 79, 83, 71, 77, 85, 81 64, 81, 76, 66, 77, 86, 72, 69 72, 90, 71, 88, 92, 72, 72, 71 85, 88, 77, 67, 71, 62, 79, 76 76, 79, 71, 85, 76, 72, 85, 77 72, 90, 72, 88, 72, 74, 86, 76 71, 72, 83, 62, 88, 98, 88, 72 77, 96, 74, 81, 67, 62, 83, 79 85, 106, 94, 100, 92, 92, 88, 94 110, 119, 100, 104, 114, 94, 100, 119 106, 104, 106, 112, 106, 128, 76, 86 96, 94, 96, 81, 74, 85, 96, 74 88, 88, 71, 94, 77, 71, 90, 77 76, 83, 77, 79, 86, 76, 83, 67 86, 94, 90, 79, 79, 77, 94, 86 88, 100, 100, 79, 77, 90, 92, 96 85, 88, 92, 102, 104, 100, 96, 94 117, 94, 88, 90, 77, 90, 90, 77 88, 100, 72, 76, 85, 98, 83, 85 90, 96, 94, 98, 90, 106, 112, 106 117, 88, 123, 123, 110, 114, 146, 139 128, 144, 149, 159, 149, 180, 185, 210 164, 180, 180, 188, 188, 193, 182, 182 193, 188, 185, 177, 196, 151, 154, 169 144, 137, 154, 137, 144, 144, 142, 137 146, 142, 128, 139, 132, 151, 119, 149 123, 108, 132, 144, 132, 106, 139, 128 130, 132, 130, 149, 125, 159, 139, 196 166, 219, 216, 228, 259, 292, 320, 339 458, 488, 471, 412, 400, 310, 266, 240 188, 193, 159, 159, 130, 128, 135, 135 130, 121, 112, 102, 119, 114, 117, 85 98, 100, 102, 114, 106, 102, 96, 102 98, 104, 112, 110, 88, 102, 100, 92 108, 106, 100, 100, 86, 114, 108, 114 108, 108, 110, 112, 128, 135, 112, 125 130, 130, 159, 149, 125, 151, 151, 139 135, 146, 119, 117, 106, 104, 114, 110 117, 104, 125, 114, 106, 121, 125, 128 121, 114, 110, 104, 117, 121, 98, 112 117, 132, 94, 94, 112, 96, 117, 110 130, 117, 119, 137, 132, 114, 121, 144 128, 117, 123, 104, 132, 123, 125, 117 112, 130, 102, 104, 114, 119, 123, 117 114, 123, 110, 112, 110, 117, 110, 112 119, 132, 123, 112, 154, 149, 142, 149 166, 164, 149, 169, 151, 142, 135, 135 151, 130, 135, 130, 130, 137, 128, 121 114, 106, 123, 135, 121, 128, 139, 137 135, 151, 144, 142, 182, 142, 174, 166 164, 169, 193, 210, 177, 196, 193, 199 199, 174, 151, 169, 146, 149, 139, 135 144, 112, 149, 121, 132, 142, 130, 119 121, 123, 139, 139, 117, 169, 172, 128 174, 146, 161, 159, 154, 188, 142, 164 169, 185, 188, 188, 177, 185, 196, 222 219, 210, 196, 204, 190, 196, 207, 193 188, 193, 207, 174, 199, 210, 219, 310 506, 586, 552, 408, 412, 342, 266, 174 182, 196, 207, 199, 190, 174, 169, 161 339, 154, 144, 128, 137, 139, 146, 144 151, 144, 130, 159, 149, 169, 142, 130 149, 144, 156, 166, 149, 161, 159, 196 190, 190, 190, 231, 250, 243, 317, 350 433, 484, 610, 824, 1170, 1332, 1584, 1665 1945, 1918, 1806, 1781, 1815, 1521, 1444, 1362 1170, 967, 900, 713, 534, 445, 437, 320 310, 289, 253, 256, 256, 228, 246, 193 240, 207, 207, 210, 193, 213, 182, 177 199, 185, 188, 169, 169, 182, 193, 204 216, 219, 207, 246, 253, 269, 292, 299 306, 279, 299, 296, 339, 342, 342, 396 313, 335, 342, 365, 384, 433, 416, 396 428, 462, 416, 433, 511, 424, 471, 441 437, 404, 346, 317, 296, 246, 433, 204 210, 204, 210, 174, 161, 144, 172, 177 161, 169, 149, 154, 154, 161, 144, 132 154, 121, 135, 108, 121, 137, 110, 135 106, 119, 119, 119, 110, 98, 114, 119 102, 114, 121, 125, 123, 94, 110, 121 123, 119, 117, 100, 123, 96, 112, 132 88, 104, 121, 119, 128, 121, 112, 106 119, 117, 117, 110, 98, 108, 106, 121 110, 130, 108, 353, 98, 106, 114, 123 135, 128, 130, 137, 146, 149, 154, 169 169, 149, 161, 164, 144, 154, 144, 166 174, 172, 146, 161, 166, 177, 161, 164 151, 177, 156, 172, 156, 164, 169, 144 149, 161, 151, 142, 144, 130, 130, 156 156, 135, 135, 130, 130, 139, 119, 119 125, 144, 146, 130, 139, 117, 121, 137 123, 117, 137, 172, 199, 182, 169, 182 202, 185, 174, 172, 182, 159, 174, 193 185, 204, 202, 219, 246, 240, 210, 250 243, 282, 253, 272, 246, 289, 246, 269 253, 240, 202, 243, 222, 202, 188, 196 193, 196, 190, 202, 172, 199, 219, 182 188, 180, 180, 154, 164, 156, 146, 149 135, 146, 135, 102, 123, 125, 137, 119 121, 132, 102, 106, 102, 100, 112, 121 108, 106, 102, 102, 108, 102, 88, 90 96, 71, 92, 102, 92, 77, 88, 86 90, 85, 77, 88, 92, 71, 88, 83 71, 94, 83, 90, 79, 77, 76, 79 90, 86, 90, 96, 79, 83, 77, 88 71, 88, 98, 85, 88, 83, 86, 92 76, 98, 90, 67, 71, 69, 94, 81 83, 85, 72, 77, 72, 85, 86, 86 92, 90, 58, 74, 62, 85, 77, 98 94, 86, 96, 79, 85, 81, 79, 94 100, 96, 83, 76, 98, 90, 112, 102 108, 96, 108, 110, 85, 108, 119, 114 100, 106, 117, 117, 110, 123, 114, 130 121, 121, 117, 151, 135, 144, 146, 159 151, 180, 190, 161, 164, 154, 174, 196 196, 207, 182, 174, 207, 202, 199, 182 210, 196, 222, 202, 225, 216, 207, 225 269, 250, 253, 234, 231, 250, 250, 225 253, 228, 213, 240, 202, 204, 185, 166 202, 174, 164, 169, 182, 156, 177, 166 159, 154, 142, 166, 164, 177, 137, 149 139, 139, 164, 142, 154, 128, 137, 125 137, 156, 161, 137, 117, 125, 151, 137 132, 130, 135, 137, 128, 128, 137, 130 137, 135, 137, 139, 132, 144, 125, 159 104, 114, 121, 135, 123, 110, 130, 135 161, 156, 207, 199, 219, 246, 222, 231 266, 240, 292, 282, 317, 299, 272, 250 253, 219, 207, 199, 182, 190, 166, 139 180, 174, 146, 164, 144, 144, 137, 137 139, 159, 174, 151, 154, 137, 128, 132 169, 156, 146, 177, 130, 199, 259, 493 841, 912, 686, 400, 404, 576, 488, 353 256, 193, 207, 188, 199, 207, 204, 234 185, 202, 196, 185, 222, 193, 185, 193 185, 190, 174, 169, 144, 151, 139, 149 144, 119, 117, 106, 108, 114, 125, 130 106, 112, 121, 130, 128, 125, 151, 144 123, 132, 110, 128, 135, 117, 154, 110 106, 121, 121, 108, 121, 121, 121, 123 100, 108, 135, 100, 106, 110, 96, 106 106, 98, 96, 94, 88, 102, 90, 92 110, 102, 86, 110, 71, 90, 100, 72 81, 90, 104, 100, 102, 92, 110, 94 94, 104, 121, 121, 123, 144, 159, 185 202, 231, 256, 234, 289, 234, 256, 199 207, 243, 180, 172, 154, 142, 135, 125 108, 98, 119, 121, 110, 123, 100, 92 110, 121, 112, 104, 125, 119, 121, 102 123, 121, 130, 110, 104, 135, 128, 102 130, 149, 154, 149, 172, 182, 188, 151 177, 174, 169, 144, 139, 114, 119, 102 108, 98, 92, 96, 88, 110, 98, 100 98, 94, 104, 100, 90, 98, 90, 98 81, 90, 92, 102, 117, 123, 104, 96 85, 98, 112, 119, 100, 117, 102, 112 96, 121, 119, 128, 130, 144, 110, 117 137, 142, 156, 130, 137, 137, 123, 137 139, 137, 135, 121, 123, 137, 125, 125 112, 139, 130, 164, 142, 137, 123, 135 117, 137, 106, 119, 121, 121, 117, 117 117, 112, 102, 117, 128, 119, 119, 92 114, 117, 119, 102, 114, 104, 121, 119 146, 144, 144, 172, 210, 199, 222, 240 231, 237, 253, 225, 228, 199, 202, 188 190, 156, 154, 130, 123, 128, 142, 102 102, 114, 104, 100, 106, 94, 94, 100 108, 85, 102, 86, 77, 92, 77, 98 90, 64, 79, 83, 98, 86, 92, 88 92, 79, 77, 90, 90, 102, 79, 76 86, 86, 76, 90, 90, 88, 92, 94 96, 104, 104, 98, 92, 92, 96, 88 85, 86, 86, 100, 112, 76, 104, 121 90, 92, 102, 117, 110, 104, 88, 98 98, 94, 83, 110, 92, 102, 86, 67 79, 86, 94, 79, 71, 76, 85, 83 92, 96, 92, 110, 142, 106, 102, 137 125, 114, 144, 121, 108, 114, 104, 139 102, 112, 114, 119, 90, 112, 96, 94 119, 104, 130, 117, 117, 128, 132, 125 139, 135, 137, 139, 144, 146, 151, 149 144, 161, 156, 174, 177, 182, 180, 196 169, 207, 188, 204, 202, 199, 234, 240 222, 240, 246, 219, 243, 202, 228, 204 202, 216, 207, 213, 234, 207, 225, 210 185, 225, 188, 193, 188, 177, 204, 159 135, 128, 137, 130, 130, 125, 121, 106 108, 121, 102, 114, 117, 102, 98, 98 104, 100, 92, 98, 106, 94, 83, 86 77, 96, 100, 96, 83, 106, 77, 88 96, 86, 76, 98, 85, 72, 88, 86 79, 79, 76, 71, 81, 77, 85, 90 90, 88, 81, 66, 72, 86, 85, 66 86, 81, 106, 79, 92, 90, 76, 74 67, 77, 86, 71, 72, 64, 77, 66 83, 79, 62, 76, 86, 76, 71, 74 79, 64, 72, 79, 77, 83, 72, 79 77, 69, 79, 79, 77, 81, 96, 104 71, 72, 79, 90, 104, 98, 106, 83 79, 98, 106, 79, 94, 100, 92, 96 86, 85, 79, 104, 98, 77, 102, 98 88, 81, 79, 85, 72, 90, 85, 86 88, 62, 83, 62, 94, 76, 67, 66 74, 58, 76, 62, 76, 71, 69, 85 67, 61, 85, 77, 79, 85, 79, 88 72, 74, 76, 79, 92, 62, 96, 79 79, 83, 85, 106, 96, 86, 94, 94 98, 83, 90, 85, 90, 86, 92, 77 81, 92, 83, 98, 92, 121, 94, 96 85, 112, 102, 100, 96, 100, 137, 117 121, 144, 139, 166, 193, 256, 222, 174 180, 190, 246, 289, 339, 428, 384, 458 437, 428, 392, 428, 441, 412, 384, 331 303, 250, 213, 207, 161, 177, 161, 142 121, 117, 119, 106, 108, 110, 144, 130 139, 146, 112, 121, 117, 130, 112, 102 119, 146, 117, 123, 117, 112, 108, 94 119, 98, 121, 112, 112, 106, 119, 98 132, 117, 114, 121, 112, 125, 137, 149 119, 128, 144, 139, 146, 135, 117, 132 137, 144, 100, 139, 110, 128, 119, 128 123, 117, 114, 125, 119, 102, 121, 117 123, 119, 100, 102, 112, 104, 102, 102 114, 106, 92, 79, 102, 100, 86, 90 90, 85, 77, 100, 114, 121, 112, 92 90, 92, 92, 108, 106, 114, 130, 121 106, 88, 102, 83, 74, 83, 83, 81 79, 72, 81, 92, 79, 86, 83, 85 98, 79, 88, 83, 92, 88, 62, 86 83, 96, 96, 117, 100, 83, 92, 98 98, 100, 96, 90, 86, 102, 106, 104 86, 98, 100, 121, 104, 104, 110, 94 108, 114, 110, 104, 108, 106, 102, 81 92, 96, 108, 85, 108, 100, 108, 94 100, 102, 86, 104, 119, 110, 112, 112 100, 104, 114, 119, 114, 121, 110, 123 102, 121, 108, 102, 108, 121, 106, 114 117, 137, 94, 130, 130, 121, 117, 146 125, 130, 117, 135, 137, 123, 137, 128 144, 128, 104, 121, 132, 121, 121, 121 125, 137, 121, 117, 149, 146, 132, 161 188, 210, 207, 213, 219, 256, 222, 228 207, 240, 228, 231, 225, 188, 166, 185 172, 142, 139, 144, 164, 144, 154, 164 154, 159, 180, 177, 146, 185, 182, 169 172, 185, 172, 182, 154, 161, 164, 154 137, 154, 137, 130, 137, 125, 121, 144 144, 119, 142, 112, 137, 132, 142, 132 137, 125, 128, 146, 119, 144, 117, 121 100, 121, 121, 119, 125, 110, 123, 130 96, 137, 110, 132, 121, 108, 102, 112 112, 137, 123, 110, 128, 114, 114, 121 121, 104, 119, 128, 121, 114, 112, 108 102, 108, 96, 112, 117, 90, 92, 104 121, 92, 92, 108, 114, 106, 100, 98 106, 117, 125, 94, 104, 90, 102, 94 100, 108, 96, 106, 106, 88, 123, 121 86, 100, 83, 100, 94, 104, 98, 104 114, 83, 100, 92, 100, 98, 94, 96 88, 98, 94, 98, 102, 110, 110, 85 112, 85, 96, 90, 110, 94, 102, 88 119, 90, 96, 121, 104, 85, 77, 119 81, 88, 94, 86, 79, 85, 83, 90 108, 72, 88, 94, 100, 92, 61, 94 92, 86, 88, 106, 96, 94, 110, 83 92, 96, 92, 98, 106, 106, 106, 102 121, 108, 110, 125, 121, 121, 96, 98 98, 98, 102, 106, 85, 117, 123, 86 90, 92, 121, 117, 114, 108, 102, 100 135, 98, 117, 106, 119, 114, 112, 125 102, 110, 130, 117, 128, 137, 110, 114 114, 139, 130, 114, 108, 137, 121, 125 125, 151, 166, 169, 177, 190, 240, 243 259, 331, 282, 353, 324, 335, 372, 342 342, 365, 299, 286, 269, 246, 269, 234 253, 204, 185, 161, 172, 161, 164, 156 154, 123, 112, 130, 114, 128, 128, 128 117, 137, 139, 135, 112, 123, 125, 117 132, 144, 112, 142, 112, 156, 102, 146 137, 130, 121, 125, 132, 119, 106, 117 117, 139, 128, 125, 149, 137, 142, 154 149, 166, 156, 149, 174, 161, 151, 164 154, 159, 161, 174, 174, 169, 169, 172 210, 204, 177, 174, 182, 199, 182, 188 202, 204, 193, 213, 210, 177, 216, 188 207, 210, 204, 193, 161, 207, 196, 188 174, 185, 182, 164, 144, 154, 166, 156 202, 159, 149, 156, 154, 139, 144, 149 125, 172, 130, 123, 121, 119, 146, 142 106, 112, 128, 130, 139, 123, 123, 117 128, 117, 123, 92, 102, 135, 108, 100 108, 119, 104, 98, 100, 112, 106, 98 100, 92, 96, 98, 104, 108, 90, 86 100, 102, 94, 106, 110, 104, 106, 112 102, 104, 110, 90, 85, 102, 94, 112 117, 98, 114, 102, 100, 119, 92, 114 94, 102, 83, 100, 123, 117, 114, 125 104, 123, 117, 125, 112, 123, 125, 132 137, 135, 169, 159, 154, 156, 174, 159 151, 182, 174, 190, 166, 182, 159, 169 159, 139, 156, 130, 154, 114, 104, 110 98, 117, 102, 104, 102, 92, 98, 79 90, 90, 98, 83, 88, 104, 110, 88 104, 90, 92, 83, 104, 108, 102, 108 98, 114, 142, 117, 121, 104, 108, 114 123, 119, 104, 100, 125, 112, 112, 125 98, 100, 88, 112, 100, 121, 114, 104 102, 125, 104, 110, 117, 102, 104, 110 92, 106, 104, 94, 108, 108, 104, 98 121, 121, 96, 112, 123, 119, 110, 102 108, 119, 130, 117, 100, 117, 110, 90 102, 90, 125, 108, 110, 110, 110, 114 94, 110, 110, 98, 106, 123, 98, 108 139, 96, 98, 108, 102, 94, 100, 135 110, 110, 102, 85, 98, 108, 102, 94 100, 112, 79, 106, 67, 104, 94, 77 90, 110, 83, 108, 98, 79, 94, 90 112, 77, 96, 102, 114, 94, 92, 100 106, 114, 125, 117, 92, 110, 90, 110 92, 96, 112, 114, 108, 104, 104, 123 96, 125, 128, 130, 112, 123, 117, 128 144, 144, 180, 172, 182, 222, 259, 279 296, 306, 282, 289, 306, 317, 272, 292 292, 276, 269, 231, 289, 253, 266, 276 286, 286, 286, 313, 310, 289, 320, 331 313, 328, 353, 416, 342, 372, 380, 369 376, 400, 365, 361, 335, 259, 253, 222 231, 219, 219, 213, 202, 180, 159, 121 121, 142, 130, 98, 104, 114, 117, 123 90, 102, 112, 110, 114, 114, 106, 92 112, 121, 94, 90, 104, 102, 104, 106 119, 94, 117, 104, 128, 110, 100, 110 108, 119, 112, 121, 106, 121, 139, 125 135, 128, 146, 128, 117, 130, 135, 135 132, 125, 130, 154, 139, 132, 135, 104 100, 130, 119, 102, 117, 121, 112, 104 123,/