SampleIdent,907A 6H-1 55-56 BULK,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,13-aug-1993 17:22,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 98, 90, 104, 92, 92, 96, 85, 85 77, 86, 79, 83, 79, 71, 79, 76 81, 76, 88, 90, 88, 94, 83, 94 85, 66, 85, 85, 88, 98, 77, 88 88, 76, 67, 83, 90, 98, 86, 86 76, 88, 96, 94, 100, 102, 83, 94 104, 88, 88, 86, 112, 81, 81, 76 121, 92, 86, 106, 121, 100, 83, 106 81, 102, 94, 86, 110, 96, 102, 114 110, 110, 79, 98, 110, 94, 83, 112 98, 121, 112, 110, 121, 100, 110, 90 104, 100, 108, 100, 102, 102, 119, 110 117, 86, 104, 110, 121, 98, 100, 123 104, 119, 96, 92, 92, 94, 114, 110 110, 108, 92, 102, 100, 104, 108, 96 98, 108, 85, 86, 117, 96, 100, 114 104, 112, 96, 108, 100, 110, 110, 102 108, 104, 102, 104, 104, 132, 110, 108 117, 106, 100, 88, 100, 114, 106, 100 100, 88, 100, 92, 88, 104, 94, 90 110, 98, 86, 110, 123, 94, 102, 102 96, 104, 110, 92, 128, 100, 112, 106 114, 102, 123, 106, 90, 110, 88, 110 86, 110, 112, 98, 123, 100, 112, 96 112, 79, 98, 88, 104, 117, 83, 86 112, 94, 102, 106, 108, 88, 96, 88 94, 90, 94, 112, 104, 94, 83, 100 104, 110, 86, 102, 90, 94, 88, 92 79, 71, 96, 96, 86, 106, 96, 86 104, 77, 98, 92, 108, 88, 86, 79 106, 106, 86, 92, 96, 96, 86, 96 86, 79, 104, 88, 100, 102, 94, 92 81, 79, 76, 86, 90, 90, 86, 108 74, 94, 86, 79, 86, 85, 94, 90 86, 71, 79, 79, 86, 94, 86, 79 88, 100, 74, 81, 88, 77, 83, 71 72, 90, 64, 85, 92, 77, 85, 92 76, 88, 85, 77, 86, 108, 86, 83 88, 88, 81, 88, 83, 77, 79, 88 72, 259, 77, 67, 77, 98, 74, 86 67, 83, 77, 79, 85, 86, 92, 104 79, 85, 74, 79, 90, 94, 79, 90 83, 102, 88, 83, 76, 86, 79, 100 92, 76, 67, 83, 72, 86, 104, 86 79, 92, 100, 83, 98, 90, 102, 77 81, 94, 86, 106, 96, 96, 96, 104 110, 112, 100, 86, 100, 114, 100, 94 100, 112, 96, 104, 110, 96, 81, 88 106, 86, 110, 88, 81, 77, 92, 88 76, 72, 98, 94, 74, 96, 71, 64 86, 83, 67, 76, 62, 61, 96, 69 81, 102, 72, 98, 77, 67, 72, 62 92, 71, 79, 92, 53, 79, 79, 88 96, 66, 81, 76, 76, 86, 92, 94 62, 85, 100, 74, 72, 76, 81, 77 72, 100, 76, 81, 85, 86, 85, 79 77, 64, 94, 62, 88, 76, 77, 83 77, 67, 67, 71, 76, 83, 88, 72 76, 83, 62, 81, 66, 72, 74, 83 83, 61, 72, 50, 62, 77, 79, 76 86, 74, 66, 66, 88, 72, 66, 66 79, 76, 76, 76, 69, 58, 67, 77 67, 77, 76, 69, 77, 83, 83, 67 66, 81, 79, 77, 67, 58, 52, 88 76, 76, 76, 74, 66, 64, 55, 66 76, 58, 72, 58, 64, 66, 72, 72 62, 72, 72, 48, 85, 62, 66, 62 79, 77, 69, 66, 86, 357, 71, 72 94, 71, 48, 62, 77, 88, 76, 76 76, 61, 71, 66, 81, 83, 56, 76 76, 66, 66, 66, 69, 71, 76, 85 62, 66, 62, 66, 74, 66, 61, 59 62, 64, 72, 74, 62, 76, 59, 72 61, 67, 61, 64, 56, 50, 71, 62 77, 62, 72, 66, 77, 50, 62, 67 56, 86, 77, 71, 77, 83, 56, 67 66, 71, 53, 50, 58, 67, 79, 64 81, 69, 71, 79, 79, 71, 67, 66 71, 56, 85, 71, 79, 77, 67, 79 86, 94, 83, 98, 71, 76, 74, 85 90, 67, 77, 83, 85, 86, 81, 96 79, 92, 92, 90, 86, 86, 85, 69 76, 72, 67, 79, 66, 76, 71, 74 71, 74, 76, 77, 94, 85, 61, 79 74, 61, 79, 74, 59, 66, 76, 67 71, 72, 76, 67, 81, 90, 71, 94 94, 98, 76, 83, 76, 85, 76, 77 86, 94, 81, 77, 71, 79, 83, 66 85, 79, 71, 59, 90, 74, 71, 77 76, 92, 96, 96, 100, 88, 94, 96 94, 121, 90, 98, 102, 92, 77, 104 106, 92, 117, 110, 117, 104, 146, 137 114, 151, 137, 144, 159, 156, 384, 144 159, 132, 151, 142, 166, 185, 159, 137 144, 128, 110, 119, 125, 135, 125, 121 121, 114, 108, 108, 104, 123, 108, 96 112, 94, 117, 130, 100, 98, 106, 121 90, 117, 119, 117, 102, 117, 146, 128 121, 161, 159, 159, 159, 151, 161, 174 188, 174, 182, 207, 202, 225, 216, 225 250, 225, 210, 190, 172, 174, 151, 149 108, 110, 106, 108, 77, 117, 77, 92 98, 96, 85, 90, 114, 94, 100, 98 72, 79, 106, 96, 77, 81, 92, 94 83, 96, 96, 79, 90, 90, 88, 102 100, 92, 79, 102, 88, 110, 121, 121 110, 110, 110, 86, 117, 121, 119, 121 117, 106, 106, 100, 121, 125, 128, 108 117, 104, 96, 85, 98, 94, 85, 88 94, 96, 86, 92, 96, 92, 88, 106 90, 90, 71, 85, 86, 114, 102, 96 98, 71, 77, 102, 71, 96, 86, 86 110, 96, 98, 114, 90, 114, 100, 114 104, 90, 106, 123, 88, 94, 102, 92 85, 83, 102, 92, 102, 88, 106, 102 102, 112, 112, 104, 112, 98, 106, 102 92, 106, 117, 114, 154, 146, 151, 144 137, 121, 130, 151, 161, 125, 137, 128 125, 108, 132, 125, 123, 100, 117, 121 128, 125, 125, 146, 125, 164, 159, 154 161, 174, 188, 172, 151, 177, 172, 174 188, 185, 177, 193, 166, 164, 182, 174 154, 132, 144, 123, 154, 114, 102, 121 117, 102, 110, 100, 108, 125, 117, 108 102, 110, 119, 98, 121, 114, 112, 114 108, 130, 130, 130, 123, 121, 144, 159 114, 128, 146, 123, 146, 154, 132, 159 177, 169, 137, 149, 149, 156, 151, 139 154, 174, 166, 172, 154, 174, 139, 149 144, 139, 149, 132, 114, 146, 130, 112 123, 117, 119, 130, 110, 106, 121, 112 112, 104, 130, 108, 121, 94, 88, 112 121, 104, 119, 106, 119, 112, 125, 114 135, 128, 130, 149, 146, 182, 207, 193 240, 289, 335, 365, 462, 538, 543, 630 630, 713, 751, 790, 853, 980, 1122, 1232 1340, 1332, 1429, 1452, 1459, 1267, 1102, 936 762, 557, 416, 339, 286, 246, 276, 279 262, 259, 219, 240, 193, 166, 177, 177 185, 188, 188, 177, 144, 161, 144, 144 142, 132, 151, 144, 135, 169, 169, 172 182, 185, 188, 207, 204, 199, 207, 199 234, 240, 243, 240, 234, 225, 250, 253 266, 279, 279, 243, 250, 262, 272, 286 331, 276, 299, 256, 269, 237, 259, 188 222, 204, 199, 156, 139, 146, 128, 137 149, 132, 130, 137, 135, 130, 119, 123 117, 108, 121, 112, 110, 100, 110, 119 96, 92, 88, 90, 96, 88, 108, 88 94, 110, 96, 102, 86, 98, 104, 90 86, 90, 100, 92, 96, 100, 96, 94 94, 100, 108, 108, 92, 108, 85, 96 85, 98, 88, 85, 104, 85, 86, 94 86, 100, 86, 94, 106, 100, 96, 112 92, 114, 106, 102, 119, 112, 100, 119 121, 128, 142, 128, 119, 106, 135, 114 125, 132, 146, 144, 121, 125, 144, 119 132, 130, 121, 139, 142, 121, 125, 128 130, 117, 130, 108, 119, 119, 154, 161 144, 123, 121, 137, 154, 130, 102, 137 132, 110, 112, 125, 128, 128, 114, 123 137, 137, 123, 100, 114, 110, 139, 121 139, 154, 149, 149, 169, 146, 182, 199 199, 172, 228, 253, 250, 250, 296, 279 303, 335, 328, 335, 328, 350, 342, 357 369, 346, 361, 376, 346, 335, 346, 324 306, 296, 313, 259, 253, 250, 222, 228 210, 182, 207, 219, 213, 202, 177, 188 182, 188, 169, 174, 149, 121, 144, 130 123, 130, 112, 130, 114, 108, 121, 104 102, 98, 110, 117, 112, 98, 94, 90 106, 106, 94, 121, 108, 102, 108, 112 102, 110, 92, 74, 76, 86, 83, 62 79, 58, 79, 66, 79, 72, 71, 77 90, 67, 79, 61, 79, 76, 77, 77 86, 77, 79, 94, 71, 59, 74, 79 74, 83, 85, 79, 76, 79, 76, 79 77, 67, 71, 81, 79, 81, 59, 79 79, 69, 83, 71, 88, 86, 83, 86 71, 81, 102, 90, 72, 76, 83, 76 83, 85, 79, 88, 92, 67, 79, 90 85, 94, 90, 90, 90, 94, 90, 86 110, 94, 92, 92, 100, 117, 117, 102 106, 123, 123, 114, 106, 117, 92, 121 144, 142, 135, 169, 169, 144, 154, 139 169, 190, 169, 164, 159, 182, 166, 169 172, 190, 182, 196, 207, 213, 228, 196 219, 202, 204, 210, 225, 210, 207, 243 213, 216, 210, 219, 219, 213, 204, 207 169, 196, 193, 207, 180, 169, 164, 159 188, 154, 161, 166, 149, 156, 156, 142 142, 130, 117, 142, 128, 125, 125, 125 130, 119, 142, 146, 125, 130, 121, 117 128, 121, 130, 100, 112, 110, 100, 121 100, 119, 114, 117, 121, 100, 119, 96 132, 135, 112, 119, 108, 135, 130, 151 123, 119, 137, 114, 119, 137, 114, 159 177, 188, 199, 202, 207, 210, 250, 193 237, 210, 234, 219, 237, 182, 190, 199 193, 156, 174, 159, 144, 135, 128, 164 135, 139, 123, 132, 108, 137, 119, 123 125, 130, 108, 132, 146, 149, 119, 130 135, 146, 130, 169, 132, 156, 161, 166 166, 166, 188, 149, 177, 188, 185, 185 210, 199, 219, 196, 216, 207, 182, 169 185, 182, 210, 185, 161, 188, 180, 149 151, 139, 132, 128, 130, 112, 106, 114 121, 112, 100, 92, 106, 86, 104, 119 106, 106, 121, 110, 117, 102, 102, 90 110, 96, 106, 130, 104, 88, 86, 86 112, 106, 108, 88, 88, 92, 79, 102 90, 121, 74, 94, 94, 83, 94, 86 94, 81, 85, 81, 88, 81, 71, 86 83, 92, 85, 98, 83, 66, 79, 81 85, 94, 102, 104, 114, 106, 92, 110 114, 112, 123, 142, 125, 137, 144, 164 164, 146, 177, 177, 180, 376, 174, 193 146, 159, 135, 137, 125, 117, 90, 104 104, 81, 98, 100, 98, 104, 114, 92 96, 86, 104, 85, 108, 86, 121, 119 108, 125, 106, 119, 114, 110, 132, 130 121, 106, 132, 125, 159, 135, 156, 125 119, 139, 108, 117, 117, 88, 94, 90 90, 98, 88, 86, 62, 94, 76, 76 86, 74, 79, 83, 85, 94, 88, 106 104, 85, 104, 94, 108, 94, 106, 108 125, 96, 106, 110, 117, 128, 144, 128 139, 137, 135, 130, 142, 125, 146, 144 174, 180, 174, 156, 137, 172, 174, 169 169, 161, 142, 130, 142, 146, 132, 137 146, 125, 149, 123, 207, 231, 169, 159 117, 125, 164, 137, 128, 98, 100, 117 83, 106, 96, 108, 117, 114, 119, 114 119, 121, 139, 146, 130, 146, 137, 156 146, 166, 154, 172, 169, 199, 213, 216 185, 188, 213, 234, 199, 199, 151, 139 156, 139, 125, 114, 106, 86, 92, 86 100, 76, 96, 92, 86, 83, 83, 79 67, 90, 81, 88, 85, 85, 76, 79 72, 96, 98, 71, 96, 59, 83, 86 83, 81, 71, 79, 76, 83, 77, 85 98, 76, 72, 56, 83, 67, 83, 71 79, 79, 85, 79, 81, 85, 77, 100 88, 85, 86, 100, 108, 102, 106, 96 94, 96, 90, 92, 92, 88, 79, 92 85, 85, 86, 77, 72, 90, 88, 76 85, 74, 85, 72, 88, 92, 90, 104 117, 108, 119, 130, 154, 130, 144, 112 117, 144, 123, 117, 135, 112, 100, 94 98, 102, 98, 112, 108, 128, 130, 104 142, 117, 121, 139, 154, 144, 156, 149 146, 180, 154, 174, 180, 202, 190, 185 222, 196, 188, 219, 193, 225, 222, 188 234, 213, 216, 237, 216, 202, 213, 253 222, 234, 237, 243, 256, 250, 240, 219 204, 222, 188, 219, 207, 166, 190, 202 159, 164, 154, 142, 151, 119, 125, 149 112, 96, 85, 104, 100, 98, 102, 90 88, 85, 67, 74, 96, 66, 59, 79 90, 71, 71, 62, 71, 77, 86, 74 86, 62, 67, 94, 72, 77, 76, 61 59, 74, 81, 83, 71, 64, 66, 69 64, 85, 77, 83, 85, 71, 79, 79 85, 88, 90, 79, 67, 62, 77, 88 77, 71, 90, 83, 77, 88, 62, 72 67, 71, 66, 76, 79, 66, 69, 62 71, 59, 76, 67, 62, 67, 67, 69 55, 59, 62, 72, 74, 67, 76, 74 66, 74, 72, 66, 71, 88, 77, 90 81, 64, 66, 85, 79, 85, 96, 64 92, 81, 104, 90, 94, 92, 77, 77 77, 86, 104, 94, 81, 76, 85, 86 88, 79, 64, 94, 77, 102, 121, 313 81, 71, 85, 71, 76, 83, 55, 66 85, 76, 69, 69, 64, 74, 59, 61 72, 85, 64, 76, 83, 66, 76, 86 81, 72, 77, 71, 83, 72, 74, 94 79, 100, 88, 79, 92, 72, 90, 102 86, 100, 92, 85, 77, 106, 92, 106 104, 100, 102, 106, 112, 112, 102, 121 114, 121, 110, 135, 125, 146, 130, 159 161, 166, 177, 253, 303, 320, 310, 292 269, 266, 292, 310, 331, 306, 317, 342 296, 282, 296, 286, 246, 228, 246, 188 182, 182, 164, 144, 137, 104, 108, 92 92, 88, 110, 90, 90, 102, 123, 96 117, 106, 100, 98, 106, 123, 110, 110 110, 117, 119, 130, 119, 125, 114, 123 108, 123, 137, 123, 146, 132, 154, 125 137, 154, 137, 159, 130, 123, 149, 156 144, 169, 149, 149, 154, 154, 159, 144 169, 159, 196, 151, 174, 497, 172, 188 172, 182, 172, 156, 146, 166, 137, 159 132, 164, 137, 146, 159, 154, 119, 137 135, 125, 121, 108, 121, 159, 108, 106 104, 96, 128, 96, 88, 96, 110, 121 104, 104, 88, 96, 86, 76, 86, 83 90, 94, 85, 79, 88, 92, 79, 90 92, 83, 76, 94, 83, 74, 96, 83 86, 85, 100, 79, 74, 96, 90, 92 85, 76, 88, 72, 98, 100, 86, 88 85, 88, 86, 88, 98, 83, 94, 94 90, 88, 86, 88, 108, 77, 90, 94 85, 104, 98, 282, 85, 76, 81, 79 86, 96, 77, 92, 86, 85, 88, 98 96, 94, 96, 90, 92, 106, 94, 102 112, 137, 83, 94, 119, 90, 102, 102 94, 114, 110, 123, 100, 88, 98, 106 96, 108, 86, 114, 94, 128, 123, 119 106, 114, 104, 112, 104, 114, 102, 96 98, 104, 85, 100, 108, 106, 98, 90 146, 102, 106, 130, 112, 177, 139, 135 151, 177, 161, 177, 196, 193, 185, 185 202, 174, 188, 182, 169, 166, 159, 169 128, 142, 142, 146, 142, 139, 142, 161 135, 144, 151, 156, 144, 146, 149, 177 137, 125, 125, 130, 117, 130, 121, 121 132, 128, 114, 146, 121, 108, 125, 112 117, 106, 121, 128, 123, 106, 130, 114 121, 104, 100, 137, 114, 77, 102, 117 96, 108, 123, 72, 96, 106, 121, 100 110, 117, 123, 110, 94, 121, 90, 104 102, 125, 123, 119, 110, 119, 110, 104 130, 130, 102, 110, 100, 119, 114, 92 98, 94, 88, 96, 90, 76, 76, 104 102, 102, 98, 90, 96, 85, 85, 81 90, 77, 83, 88, 81, 85, 94, 85 77, 104, 98, 94, 106, 90, 76, 100 88, 88, 100, 66, 102, 112, 88, 92 90, 90, 90, 76, 85, 83, 90, 86 88, 85, 76, 62, 86, 77, 88, 85 86, 90, 98, 66, 83, 88, 81, 76 67, 71, 77, 88, 83, 86, 88, 88 81, 86, 96, 92, 77, 81, 83, 86 85, 83, 77, 96, 98, 90, 86, 72 102, 96, 92, 100, 102, 108, 88, 90 96, 98, 102, 90, 92, 90, 100, 94 77, 94, 83, 88, 86, 85, 94, 100 100, 81, 88, 83, 94, 104, 96, 86 108, 112, 98, 108, 108, 132, 104, 117 137, 106, 112, 102, 112, 96, 114, 104 112, 117, 112, 125, 110, 125, 112, 121 130, 149, 121, 146, 144, 161, 182, 219 225, 240, 222, 250, 231, 250, 262, 286 328, 317, 320, 292, 320, 361, 289, 324 282, 269, 266, 210, 243, 222, 199, 196 177, 177, 172, 169, 166, 164, 180, 146 174, 149, 149, 161, 132, 125, 144, 132 151, 139, 142, 112, 130, 137, 108, 102 130, 110, 130, 128, 121, 112, 130, 112 128, 119, 125, 106, 137, 128, 125, 117 125, 112, 125, 132, 125, 135, 139, 135 144, 142, 156, 114, 154, 177, 156, 154 132, 164, 154, 137, 172, 161, 164, 177 185, 182, 185, 196, 216, 196, 174, 174 174, 180, 190, 199, 177, 159, 196, 185 185, 182, 172, 172, 180, 144, 188, 156 149, 135, 142, 149, 137, 164, 135, 151 132, 135, 135, 139, 139, 144, 128, 125 125, 144, 137, 128, 112, 119, 130, 112 114, 98, 110, 110, 106, 104, 86, 98 106, 96, 83, 100, 90, 94, 98, 98 92, 98, 104, 96, 94, 81, 96, 67 83, 85, 86, 62, 86, 92, 77, 67 100, 92, 94, 90, 86, 94, 98, 92 110, 100, 100, 94, 104, 100, 92, 100 104, 110, 117, 94, 92, 112, 119, 96 96, 119, 137, 98, 102, 112, 125, 121 137, 121, 125, 123, 117, 130, 128, 139 125, 137, 137, 166, 146, 139, 144, 169 137, 172, 144, 149, 149, 139, 135, 110 121, 106, 108, 102, 108, 114, 108, 104 108, 86, 86, 86, 86, 83, 94, 88 94, 102, 90, 85, 92, 79, 77, 90 96, 96, 90, 88, 96, 88, 88, 92 106, 92, 110, 79, 90, 94, 69, 123 96, 102, 121, 88, 112, 92, 110, 110 104, 106, 112, 94, 119, 98, 94, 123 106, 102, 106, 104, 108, 79, 114, 94 98, 94, 98, 96, 86, 100, 90, 92 119, 108, 112, 98, 96, 119, 100, 98 96, 102, 88, 102, 121, 102, 94, 98 98, 108, 88, 98, 86, 102, 104, 100 96, 98, 96, 81, 96, 112, 104, 104 90, 102, 98, 90, 77, 90, 92, 83 92, 98, 108, 83, 100, 79, 88, 94 72, 72, 79, 86, 94, 77, 86, 79 98, 86, 72, 76, 81, 100, 59, 83 104, 77, 90, 86, 92, 110, 92, 100 86, 92, 90, 85, 108, 86, 121, 108 96, 94, 104, 102, 104, 106, 125, 110 110, 123, 112, 123, 137, 144, 132, 169 164, 159, 199, 174, 202, 196, 250, 231 269, 286, 266, 240, 225, 243, 210, 228 237, 210, 246, 269, 250, 231, 231, 246 279, 310, 372, 353, 388, 339, 380, 350 324, 313, 286, 286, 310, 299, 299, 331 306, 296, 237, 210, 196, 177, 146, 164 149, 172, 154, 164, 117, 114, 100, 98 108, 96, 90, 77, 104, 104, 86, 83 83, 108, 79, 96, 92, 81, 96, 98 98, 96, 100, 106, 92, 112, 98, 112 94, 108, 106, 104, 98, 85, 98, 108 110, 114, 114, 128, 110, 130, 83, 108 100, 128, 102, 117, 146, 112, 108, 102 114, 117, 100, 106, 104, 110, 117, 102 88,/