SampleIdent,907A 6H-1 75-76 BULK,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,13-aug-1993 18:17,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 81, 106, 98, 88, 92, 96, 90, 102 71, 98, 66, 90, 104, 79, 88, 98 104, 83, 92, 100, 106, 92, 88, 72 85, 86, 96, 108, 88, 92, 79, 104 92, 86, 96, 79, 92, 106, 106, 98 86, 83, 102, 92, 76, 85, 83, 96 98, 112, 94, 96, 92, 102, 110, 96 100, 86, 114, 112, 104, 110, 102, 94 102, 94, 104, 114, 90, 108, 90, 121 92, 114, 108, 121, 110, 112, 104, 92 108, 100, 104, 106, 108, 102, 106, 102 100, 114, 102, 94, 106, 98, 100, 100 83, 100, 117, 102, 112, 96, 104, 98 114, 106, 100, 110, 110, 119, 104, 106 106, 121, 112, 114, 110, 110, 104, 92 96, 108, 94, 106, 114, 119, 104, 106 108, 112, 86, 96, 121, 106, 104, 110 112, 110, 100, 94, 94, 121, 100, 106 112, 104, 108, 90, 92, 85, 98, 106 114, 98, 114, 106, 104, 106, 104, 100 90, 102, 98, 106, 106, 102, 104, 92 117, 100, 104, 117, 110, 86, 110, 92 106, 92, 123, 90, 121, 123, 121, 108 108, 119, 112, 121, 106, 119, 108, 114 96, 100, 135, 100, 114, 104, 137, 98 123, 98, 102, 90, 83, 104, 102, 94 90, 121, 94, 112, 94, 92, 106, 81 66, 100, 94, 96, 83, 88, 96, 81 98, 98, 98, 90, 94, 86, 100, 90 92, 86, 110, 85, 85, 94, 96, 106 85, 98, 83, 72, 92, 100, 92, 92 98, 76, 76, 85, 81, 83, 90, 112 94, 96, 88, 79, 96, 81, 72, 83 85, 85, 88, 98, 86, 98, 85, 86 100, 104, 59, 86, 86, 96, 94, 74 90, 69, 92, 85, 77, 90, 96, 85 100, 83, 83, 77, 79, 85, 106, 85 86, 85, 85, 79, 76, 96, 90, 66 88, 92, 98, 79, 83, 81, 71, 83 79, 90, 88, 94, 85, 85, 98, 72 94, 96, 79, 88, 92, 76, 85, 85 77, 86, 77, 85, 94, 81, 79, 98 88, 86, 77, 76, 90, 98, 83, 86 100, 90, 96, 58, 92, 104, 94, 79 98, 85, 81, 88, 86, 102, 117, 92 100, 90, 110, 98, 85, 110, 119, 114 119, 108, 88, 102, 104, 108, 110, 110 117, 96, 96, 121, 108, 98, 106, 94 92, 114, 88, 69, 79, 86, 83, 74 81, 86, 77, 85, 67, 96, 85, 81 92, 94, 79, 92, 79, 72, 71, 92 92, 90, 69, 76, 88, 85, 88, 90 81, 71, 77, 96, 71, 72, 71, 69 85, 96, 106, 62, 77, 86, 72, 88 94, 81, 79, 96, 86, 83, 90, 79 92, 114, 76, 83, 90, 71, 86, 90 79, 72, 86, 85, 67, 79, 66, 77 90, 72, 85, 83, 81, 85, 79, 86 79, 85, 66, 72, 69, 85, 81, 72 79, 83, 72, 71, 72, 67, 96, 90 85, 79, 72, 72, 66, 79, 85, 83 94, 72, 81, 83, 81, 71, 79, 66 74, 98, 53, 77, 76, 77, 83, 79 79, 77, 71, 79, 86, 77, 66, 76 76, 62, 94, 71, 72, 74, 83, 86 66, 71, 92, 76, 69, 88, 71, 67 72, 74, 72, 71, 71, 83, 69, 90 79, 81, 72, 77, 59, 66, 85, 77 85, 79, 72, 98, 74, 67, 76, 76 61, 77, 83, 66, 69, 83, 72, 69 66, 69, 83, 58, 69, 79, 72, 69 81, 72, 67, 62, 66, 85, 67, 104 71, 64, 74, 56, 76, 71, 72, 64 86, 86, 88, 86, 71, 72, 72, 86 71, 71, 74, 79, 77, 77, 71, 72 61, 74, 79, 66, 72, 72, 67, 69 72, 66, 64, 77, 74, 83, 92, 66 66, 62, 79, 83, 69, 79, 79, 79 76, 85, 85, 86, 71, 96, 74, 94 94, 90, 59, 67, 96, 83, 92, 104 112, 85, 96, 81, 83, 71, 92, 85 72, 90, 94, 76, 71, 71, 69, 64 77, 72, 62, 74, 71, 66, 66, 79 79, 67, 85, 72, 90, 71, 77, 76 64, 76, 90, 85, 77, 90, 74, 74 77, 77, 77, 58, 94, 96, 85, 85 86, 90, 92, 86, 86, 94, 88, 76 96, 104, 88, 98, 88, 92, 90, 86 79, 86, 102, 96, 110, 90, 108, 98 110, 92, 98, 114, 98, 102, 98, 104 117, 123, 110, 112, 112, 132, 132, 110 104, 132, 117, 119, 137, 135, 169, 151 174, 125, 188, 166, 174, 177, 161, 172 177, 182, 219, 154, 202, 172, 177, 161 149, 154, 161, 166, 161, 154, 123, 142 130, 142, 144, 132, 159, 128, 123, 121 117, 117, 121, 112, 123, 112, 121, 130 132, 142, 139, 112, 114, 128, 149, 159 154, 185, 199, 199, 204, 199, 193, 219 180, 219, 225, 243, 320, 292, 292, 246 237, 231, 219, 185, 164, 149, 149, 117 130, 121, 112, 110, 108, 119, 102, 117 130, 112, 98, 119, 104, 117, 132, 92 114, 119, 106, 108, 106, 106, 110, 110 106, 121, 110, 108, 117, 125, 104, 112 104, 114, 119, 128, 104, 110, 123, 139 144, 130, 123, 146, 132, 151, 156, 161 172, 159, 137, 149, 139, 144, 121, 117 96, 119, 98, 112, 90, 104, 121, 106 104, 100, 102, 104, 112, 114, 100, 117 100, 114, 119, 100, 100, 106, 88, 114 102, 106, 117, 114, 110, 106, 123, 110 112, 123, 117, 106, 108, 121, 110, 114 121, 112, 108, 130, 104, 106, 121, 114 94, 110, 108, 94, 104, 112, 110, 92 130, 149, 128, 132, 130, 135, 125, 108 125, 128, 146, 132, 161, 149, 132, 149 130, 149, 156, 139, 130, 149, 137, 149 125, 130, 123, 123, 132, 125, 117, 112 125, 96, 114, 125, 114, 125, 146, 137 139, 156, 135, 166, 132, 142, 132, 132 125, 149, 159, 151, 144, 125, 146, 135 123, 130, 130, 144, 139, 119, 119, 117 121, 106, 123, 104, 96, 112, 142, 125 151, 117, 117, 104, 110, 137, 123, 144 117, 156, 135, 117, 132, 142, 154, 149 154, 164, 144, 149, 151, 137, 149, 130 174, 146, 164, 154, 185, 177, 159, 159 164, 159, 149, 159, 142, 169, 164, 159 154, 146, 130, 151, 130, 135, 146, 130 123, 142, 110, 135, 142, 123, 117, 100 121, 146, 121, 144, 123, 137, 144, 121 132, 139, 135, 139, 146, 146, 146, 151 149, 144, 164, 161, 174, 199, 188, 231 286, 339, 404, 529, 590, 625, 734, 676 724, 784, 824, 912, 986, 918, 1005, 992 924, 980, 912, 778, 773, 635, 520, 420 317, 282, 243, 231, 213, 202, 188, 188 161, 169, 164, 177, 172, 144, 154, 151 164, 182, 161, 196, 164, 164, 182, 204 182, 210, 207, 210, 193, 231, 210, 222 222, 225, 231, 234, 237, 225, 237, 266 225, 228, 253, 262, 262, 296, 313, 310 328, 335, 365, 350, 369, 396, 376, 388 342, 372, 350, 313, 279, 256, 262, 240 216, 210, 177, 193, 164, 185, 159, 164 144, 142, 130, 142, 128, 164, 139, 112 144, 139, 119, 130, 137, 132, 114, 112 123, 92, 100, 125, 119, 106, 110, 102 96, 110, 110, 108, 92, 117, 110, 112 121, 110, 106, 92, 104, 121, 104, 94 96, 102, 110, 108, 114, 137, 139, 123 114, 137, 114, 104, 108, 104, 114, 102 106, 106, 79, 102, 125, 92, 142, 137 142, 146, 132, 172, 199, 313, 380, 292 269, 276, 256, 234, 196, 196, 169, 154 139, 142, 159, 146, 151, 172, 144, 128 110, 135, 137, 149, 146, 142, 144, 149 135, 144, 159, 146, 130, 172, 128, 130 135, 185, 169, 156, 144, 154, 154, 159 144, 139, 164, 132, 156, 121, 144, 128 121, 137, 106, 130, 119, 144, 121, 108 135, 114, 132, 117, 137, 102, 112, 121 110, 123, 117, 125, 123, 117, 135, 119 142, 125, 132, 132, 128, 137, 135, 123 128, 125, 139, 161, 164, 146, 154, 166 188, 188, 172, 199, 225, 216, 210, 246 222, 250, 246, 262, 262, 253, 282, 292 253, 262, 228, 196, 169, 177, 154, 114 100, 100, 112, 125, 104, 100, 110, 102 86, 117, 88, 98, 81, 98, 100, 110 83, 104, 90, 100, 96, 90, 79, 72 90, 77, 85, 98, 90, 86, 83, 83 81, 83, 86, 81, 77, 83, 85, 86 92, 102, 104, 85, 81, 98, 69, 104 106, 72, 100, 102, 108, 92, 94, 90 100, 108, 96, 100, 96, 92, 88, 94 106, 86, 98, 94, 100, 88, 100, 102 88, 86, 92, 100, 106, 98, 117, 102 92, 98, 96, 108, 94, 92, 106, 100 108, 100, 100, 90, 112, 128, 130, 104 96, 96, 121, 110, 117, 123, 135, 121 112, 149, 119, 112, 123, 121, 112, 123 132, 121, 135, 154, 135, 161, 142, 182 154, 144, 151, 172, 193, 188, 210, 193 210, 185, 180, 231, 237, 225, 266, 222 237, 222, 246, 222, 253, 231, 250, 266 259, 269, 269, 266, 296, 262, 262, 266 269, 282, 276, 243, 259, 272, 262, 240 228, 225, 234, 228, 204, 199, 216, 188 188, 196, 169, 169, 161, 182, 164, 172 161, 149, 156, 166, 151, 164, 149, 137 172, 137, 172, 151, 142, 177, 164, 164 149, 169, 154, 139, 149, 137, 149, 123 146, 144, 125, 132, 142, 146, 132, 142 137, 128, 156, 154, 144, 144, 142, 135 142, 161, 164, 166, 177, 182, 188, 204 222, 222, 246, 259, 213, 225, 246, 253 237, 234, 240, 219, 204, 225, 210, 182 154, 193, 159, 159, 156, 177, 166, 166 146, 137, 159, 161, 144, 164, 149, 169 139, 161, 154, 154, 146, 177, 142, 151 151, 149, 185, 166, 164, 146, 172, 130 159, 159, 161, 149, 182, 166, 169, 177 199, 182, 161, 177, 182, 151, 180, 185 376, 164, 161, 174, 159, 149, 137, 132 161, 139, 123, 117, 123, 135, 112, 132 96, 108, 110, 112, 106, 117, 114, 100 130, 114, 130, 104, 114, 102, 125, 114 79, 98, 119, 114, 102, 110, 110, 90 110, 104, 117, 98, 85, 104, 94, 110 94, 110, 104, 104, 98, 100, 130, 98 86, 96, 112, 112, 100, 100, 94, 108 102, 98, 98, 102, 108, 112, 121, 100 104, 121, 121, 94, 121, 164, 161, 166 180, 174, 161, 228, 269, 216, 210, 202 202, 210, 210, 196, 202, 204, 193, 159 142, 142, 132, 132, 132, 106, 130, 130 121, 114, 108, 112, 98, 112, 119, 100 104, 125, 144, 128, 104, 112, 114, 137 144, 144, 125, 146, 156, 139, 369, 159 144, 123, 174, 159, 161, 139, 144, 164 132, 132, 106, 104, 110, 130, 135, 100 128, 102, 108, 112, 123, 137, 119, 128 130, 121, 98, 144, 110, 108, 112, 117 123, 121, 137, 104, 119, 112, 100, 100 96, 114, 121, 104, 100, 108, 106, 98 100, 110, 119, 110, 123, 121, 108, 114 106, 104, 98, 96, 98, 102, 100, 90 98, 114, 100, 90, 106, 119, 98, 125 121, 130, 125, 119, 108, 114, 110, 100 119, 137, 142, 119, 123, 102, 119, 102 130, 119, 130, 121, 121, 149, 130, 130 144, 164, 164, 172, 188, 188, 210, 207 225, 216, 202, 213, 213, 225, 216, 222 234, 199, 154, 185, 164, 164, 151, 144 123, 128, 119, 121, 121, 119, 110, 106 114, 110, 104, 121, 102, 92, 102, 100 108, 85, 106, 104, 117, 106, 94, 79 92, 85, 112, 96, 88, 106, 98, 108 83, 90, 104, 79, 106, 94, 98, 98 104, 98, 77, 102, 102, 98, 88, 85 92, 102, 106, 88, 108, 100, 96, 104 104, 117, 108, 98, 88, 128, 106, 98 112, 98, 96, 86, 96, 100, 86, 104 98, 90, 98, 112, 83, 96, 92, 77 92, 92, 117, 90, 110, 117, 110, 121 112, 121, 146, 110, 121, 110, 88, 94 108, 114, 100, 98, 110, 108, 102, 100 92, 104, 85, 110, 119, 106, 108, 100 108, 144, 112, 123, 119, 142, 119, 135 149, 137, 154, 142, 166, 169, 169, 180 199, 202, 213, 231, 240, 237, 262, 250 276, 272, 296, 289, 276, 299, 306, 276 282, 259, 240, 222, 213, 210, 202, 225 154, 196, 156, 169, 174, 166, 174, 180 137, 142, 146, 128, 128, 125, 119, 114 112, 119, 92, 100, 100, 112, 92, 108 96, 106, 86, 86, 76, 77, 83, 100 88, 77, 83, 83, 79, 92, 79, 94 77, 90, 81, 90, 76, 92, 96, 85 98, 81, 86, 74, 81, 71, 74, 77 67, 96, 77, 83, 96, 72, 92, 74 85, 76, 77, 90, 98, 67, 72, 85 83, 92, 83, 90, 76, 88, 104, 90 74, 85, 94, 74, 79, 86, 85, 86 52, 67, 83, 83, 72, 72, 79, 72 67, 71, 69, 66, 76, 94, 77, 98 86, 69, 79, 86, 88, 72, 90, 86 92, 96, 88, 85, 90, 100, 85, 96 117, 100, 86, 110, 94, 86, 85, 90 98, 102, 94, 88, 83, 94, 76, 96 86, 88, 76, 85, 62, 86, 92, 71 72, 76, 66, 66, 83, 62, 85, 86 85, 76, 79, 66, 62, 71, 79, 86 67, 79, 77, 69, 76, 83, 71, 83 83, 90, 77, 102, 100, 106, 90, 100 86, 110, 112, 86, 104, 108, 96, 90 98, 90, 86, 71, 81, 81, 85, 86 98, 110, 98, 92, 98, 92, 104, 102 114, 114, 106, 119, 119, 114, 125, 128 159, 154, 169, 174, 207, 216, 210, 250 259, 216, 286, 256, 276, 317, 313, 286 276, 253, 246, 228, 207, 190, 164, 166 156, 144, 123, 121, 106, 114, 123, 94 104, 94, 108, 121, 106, 117, 119, 119 106, 121, 102, 130, 88, 102, 114, 92 92, 88, 76, 83, 100, 77, 100, 92 86, 86, 110, 96, 88, 85, 86, 106 96, 94, 98, 88, 96, 83, 92, 86 88, 96, 77, 88, 72, 88, 88, 79 85, 88, 77, 74, 79, 67, 81, 71 81, 66, 76, 79, 71, 94, 67, 72 83, 67, 77, 66, 71, 85, 74, 71 64, 71, 72, 96, 71, 76, 77, 76 83, 79, 76, 86, 92, 72, 94, 90 86, 86, 303, 102, 83, 100, 85, 90 83, 94, 96, 94, 102, 88, 83, 83 104, 83, 72, 94, 102, 77, 90, 81 92, 106, 96, 104, 100, 112, 106, 98 96, 117, 125, 100, 102, 98, 130, 106 117, 125, 100, 94, 108, 125, 121, 112 108, 112, 128, 98, 104, 117, 123, 104 132, 117, 102, 92, 108, 108, 117, 96 86, 104, 110, 104, 121, 110, 128, 128 114, 117, 117, 123, 110, 137, 100, 114 112, 125, 114, 130, 112, 135, 121, 114 108, 137, 121, 125, 123, 125, 125, 123 132, 114, 119, 119, 128, 123, 130, 130 104, 121, 130, 137, 112, 128, 110, 144 144, 139, 128, 125, 132, 149, 199, 161 196, 207, 213, 222, 412, 202, 156, 213 240, 246, 185, 207, 213, 207, 196, 193 193, 213, 193, 151, 180, 177, 174, 185 177, 164, 164, 149, 154, 174, 154, 159 164, 177, 154, 180, 159, 154, 135, 151 146, 166, 144, 132, 151, 142, 135, 151 137, 166, 137, 149, 130, 135, 137, 119 119, 123, 151, 154, 121, 139, 130, 139 125, 132, 166, 137, 142, 132, 135, 142 142, 328, 123, 135, 128, 177, 144, 156 174, 180, 166, 169, 177, 166, 164, 166 177, 159, 190, 196, 161, 161, 156, 164 177, 169, 151, 130, 159, 123, 121, 156 112, 104, 106, 144, 108, 123, 96, 108 123, 110, 100, 106, 106, 108, 114, 100 123, 90, 108, 110, 117, 125, 92, 106 110, 100, 94, 106, 96, 83, 119, 90 81, 90, 102, 88, 104, 125, 90, 108 74, 96, 112, 100, 83, 114, 96, 90 98, 110, 88, 100, 112, 106, 100, 96 90, 98, 98, 85, 108, 108, 100, 121 90, 90, 88, 86, 85, 104, 110, 90 92, 100, 104, 94, 96, 88, 106, 92 106, 90, 102, 90, 88, 104, 102, 110 94, 86, 104, 114, 108, 114, 94, 106 92, 79, 114, 110, 102, 102, 108, 117 108, 117, 104, 102, 114, 130, 114, 130 104, 102, 135, 94, 102, 123, 125, 104 108, 125, 117, 123, 112, 112, 132, 104 125, 132, 144, 128, 112, 125, 114, 137 100, 135, 149, 125, 142, 123, 137, 151 154, 149, 151, 154, 196, 196, 210, 216 225, 219, 269, 246, 269, 266, 269, 266 331, 299, 299, 296, 282, 266, 246, 234 216, 225, 199, 207, 182, 164, 149, 151 132, 132, 142, 144, 125, 128, 123, 146 125, 114, 130, 130, 117, 106, 142, 135 130, 132, 135, 130, 135, 128, 135, 132 130, 135, 149, 142, 117, 137, 94, 144 128, 144, 172, 130, 144, 164, 146, 135 172, 151, 139, 154, 166, 166, 172, 164 188, 169, 317, 174, 161, 177, 182, 185 172, 204, 228, 185, 210, 188, 207, 193 185, 196, 202, 210, 213, 219, 219, 196 240, 231, 222, 222, 216, 219, 240, 199 202, 199, 204, 196, 202, 188, 177, 172 202, 159, 151, 161, 135, 149, 159, 172 146, 144, 164, 161, 156, 164, 159, 135 177, 159, 135, 144, 139, 135, 146, 149 121, 130, 117, 123, 110, 137, 137, 121 130, 112, 112, 125, 123, 112, 112, 108 106, 128, 94, 98, 100, 85, 108, 125 83, 92, 121, 83, 100, 96, 94, 92 112, 102, 98, 108, 104, 98, 94, 85 86, 121, 96, 104, 104, 102, 83, 102 132, 90, 114, 114, 92, 102, 98, 96 119, 112, 106, 100, 112, 121, 123, 125 106, 114, 121, 156, 112, 121, 146, 139 119, 135, 123, 154, 142, 164, 130, 146 139, 151, 117, 114, 108, 114, 135, 102 104, 114, 108, 112, 96, 90, 90, 110 88, 88, 98, 98, 88, 98, 83, 79 88, 94, 98, 104, 86, 108, 96, 106 96, 100, 106, 96, 112, 102, 100, 108 110, 100, 100, 104, 81, 117, 112, 119 110, 110, 112, 114, 114, 117, 96, 94 108, 110, 102, 90, 114, 110, 117, 112 121, 96, 104, 117, 104, 125, 125, 98 98, 121, 100, 100, 94, 104, 114, 102 112, 106, 117, 112, 128, 125, 98, 121 114, 106, 114, 114, 114, 106, 119, 125 132, 125, 130, 114, 151, 125, 112, 110 125, 121, 114, 130, 123, 114, 135, 121 137, 96, 106, 98, 130, 98, 114, 100 86, 90, 77, 83, 90, 79, 85, 100 86, 96, 94, 86, 100, 83, 90, 98 96, 104, 83, 86, 96, 114, 77, 96 102, 76, 94, 94, 110, 102, 108, 123 92, 96, 106, 132, 135, 400, 100, 96 121, 117, 106, 110, 112, 110, 114, 100 125, 117, 142, 121, 149, 144, 169, 159 188, 185, 180, 207, 213, 222, 216, 185 210, 237, 219, 199, 228, 213, 237, 199 240, 243, 266, 310, 346, 328, 320, 282 262, 262, 328, 303, 328, 342, 396, 339 292, 269, 269, 225, 243, 269, 256, 250 228, 196, 193, 188, 174, 139, 123, 139 151, 142, 135, 121, 106, 128, 106, 98 102, 102, 112, 130, 98, 98, 106, 100 98, 100, 112, 106, 98, 130, 92, 110 110, 104, 121, 121, 98, 102, 135, 100 132, 106, 117, 121, 125, 114, 130, 137 125, 112, 110, 130, 117, 130, 137, 130 125, 114, 117, 123, 121, 110, 104, 128 117, 108, 106, 110, 121, 110, 112, 112 110,/