SampleIdent,907A 6H-3 9-10 CLAY,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,14-aug-1993 12:12,/ DataAngleRange, 2.0000, 39.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 85, 71, 77, 90, 74, 66, 71, 83 96, 77, 79, 74, 77, 88, 76, 88 69, 79, 67, 71, 85, 83, 85, 77 85, 94, 72, 76, 67, 67, 71, 74 62, 66, 81, 77, 88, 67, 83, 67 64, 62, 71, 67, 85, 71, 67, 55 59, 76, 72, 67, 66, 62, 74, 81 56, 62, 66, 72, 77, 72, 269, 77 66, 67, 66, 61, 56, 67, 62, 62 55, 86, 79, 67, 76, 62, 86, 83 76, 72, 53, 72, 56, 79, 72, 79 67, 79, 69, 86, 79, 79, 72, 85 77, 90, 79, 79, 88, 77, 92, 74 79, 86, 98, 67, 100, 85, 86, 86 100, 77, 88, 104, 106, 88, 90, 106 81, 90, 106, 102, 102, 110, 81, 100 92, 94, 100, 88, 100, 94, 108, 81 85, 94, 90, 119, 119, 108, 240, 88 108, 114, 102, 94, 100, 106, 104, 85 121, 102, 110, 106, 98, 88, 100, 100 104, 121, 110, 112, 130, 108, 112, 102 90, 98, 94, 90, 119, 106, 102, 104 121, 104, 110, 128, 125, 102, 117, 106 104, 121, 132, 106, 117, 96, 108, 119 102, 98, 106, 114, 132, 117, 128, 92 125, 132, 119, 108, 128, 119, 121, 112 119, 121, 106, 130, 94, 104, 159, 119 119, 110, 119, 121, 106, 121, 125, 128 119, 110, 350, 123, 135, 135, 110, 121 123, 137, 139, 130, 128, 142, 128, 132 139, 139, 128, 139, 119, 139, 146, 137 151, 137, 110, 130, 149, 130, 169, 128 137, 132, 135, 135, 139, 146, 139, 137 154, 156, 146, 144, 154, 164, 144, 142 132, 132, 172, 154, 128, 121, 159, 144 154, 142, 139, 144, 142, 149, 166, 156 159, 164, 154, 139, 180, 146, 174, 144 159, 132, 180, 130, 130, 164, 149, 169 156, 172, 154, 161, 169, 159, 154, 149 154, 166, 166, 169, 177, 161, 166, 161 159, 159, 193, 161, 146, 161, 180, 190 188, 166, 164, 166, 185, 159, 174, 164 177, 196, 172, 169, 180, 188, 151, 190 177, 151, 188, 199, 207, 166, 177, 188 174, 174, 196, 177, 193, 188, 182, 164 199, 182, 188, 180, 177, 185, 169, 193 228, 174, 193, 199, 199, 202, 185, 222 202, 202, 196, 196, 210, 196, 199, 213 193, 196, 188, 216, 190, 199, 193, 231 216, 185, 210, 210, 216, 216, 219, 219 243, 228, 256, 240, 231, 246, 282, 222 262, 240, 256, 256, 250, 243, 272, 253 286, 303, 259, 276, 272, 259, 253, 259 259, 253, 246, 266, 243, 246, 259, 243 237, 240, 243, 256, 240, 276, 246, 246 253, 286, 234, 259, 231, 250, 253, 246 250, 243, 240, 243, 246, 246, 262, 276 256, 231, 272, 276, 266, 237, 262, 243 246, 259, 234, 262, 243, 256, 256, 286 259, 237, 246, 266, 259, 279, 269, 256 269, 237, 289, 272, 256, 276, 259, 256 272, 269, 276, 276, 279, 266, 272, 303 272, 306, 253, 279, 286, 262, 292, 282 272, 250, 272, 262, 259, 303, 289, 262 266, 292, 282, 292, 282, 289, 246, 296 296, 286, 276, 292, 303, 266, 286, 282 269, 289, 286, 303, 306, 246, 303, 350 292, 279, 289, 262, 296, 306, 299, 299 286, 289, 313, 272, 276, 266, 286, 303 303, 292, 289, 276, 269, 310, 259, 243 303, 324, 286, 306, 306, 303, 286, 289 310, 292, 303, 279, 303, 292, 296, 282 286, 289, 256, 299, 299, 292, 272, 276 303, 306, 289, 292, 296, 276, 335, 313 303, 328, 339, 320, 306, 296, 339, 282 320, 357, 306, 320, 303, 320, 320, 339 317, 310, 299, 313, 328, 342, 299, 313 331, 331, 328, 282, 342, 342, 342, 342 361, 335, 331, 350, 339, 317, 346, 361 317, 353, 369, 369, 380, 361, 357, 388 380, 369, 412, 365, 380, 400, 369, 376 416, 404, 424, 424, 412, 424, 408, 454 454, 445, 424, 437, 433, 454, 471, 488 497, 488, 515, 548, 511, 548, 581, 620 571, 581, 630, 557, 595, 581, 571, 557 566, 520, 548, 511, 515, 462, 458, 437 412, 400, 365, 346, 353, 339, 320, 350 282, 303, 299, 262, 292, 250, 250, 286 269, 262, 276, 253, 243, 234, 225, 210 207, 234, 202, 213, 199, 219, 196, 216 199, 190, 199, 180, 196, 180, 182, 213 193, 182, 182, 193, 172, 188, 193, 177 174, 164, 159, 182, 174, 146, 182, 159 177, 156, 161, 149, 156, 164, 166, 169 180, 164, 177, 159, 149, 169, 159, 142 149, 137, 169, 144, 149, 161, 144, 151 149, 161, 159, 154, 149, 172, 132, 135 135, 139, 161, 139, 154, 128, 182, 144 135, 139, 139, 144, 166, 132, 137, 142 144, 144, 132, 137, 117, 125, 156, 135 144, 144, 128, 119, 154, 125, 154, 125 128, 156, 135, 139, 125, 135, 125, 135 125, 135, 137, 130, 121, 159, 149, 137 128, 128, 135, 130, 121, 128, 117, 132 125, 135, 125, 121, 137, 130, 114, 135 123, 135, 132, 121, 110, 94, 117, 114 130, 112, 114, 132, 159, 144, 128, 110 137, 121, 132, 121, 121, 125, 128, 128 121, 114, 114, 132, 112, 106, 123, 130 121, 125, 102, 130, 125, 112, 132, 137 125, 121, 125, 128, 137, 125, 128, 135 121, 130, 142, 132, 121, 130, 137, 119 125, 149, 123, 137, 112, 110, 125, 144 121, 142, 139, 123, 130, 139, 102, 128 117, 144, 108, 119, 121, 121, 130, 117 144, 114, 121, 142, 144, 108, 106, 121 117, 119, 130, 135, 137, 137, 132, 135 121, 132, 121, 128, 130, 117, 121, 228 149, 130, 137, 169, 117, 139, 139, 110 130, 132, 108, 117, 128, 125, 135, 154 139, 137, 169, 125, 130, 144, 110, 154 161, 135, 149, 137, 154, 159, 144, 144 139, 174, 161, 151, 166, 154, 142, 137 146, 154, 156, 149, 174, 174, 144, 161 164, 174, 169, 202, 169, 172, 210, 182 185, 202, 199, 219, 228, 225, 228, 210 222, 216, 237, 250, 234, 256, 246, 276 262, 256, 289, 299, 339, 339, 353, 380 342, 384, 353, 400, 376, 420, 437, 424 449, 458, 475, 497, 484, 543, 538, 506 506, 538, 502, 538, 552, 511, 524, 484 497, 458, 454, 433, 392, 400, 339, 346 313, 324, 296, 262, 250, 237, 231, 222 216, 213, 193, 185, 193, 169, 182, 144 199, 169, 154, 154, 154, 149, 164, 156 154, 137, 144, 128, 130, 149, 144, 135 137, 130, 128, 130, 132, 146, 144, 135 144, 125, 128, 130, 130, 117, 114, 128 114, 108, 121, 130, 108, 104, 117, 121 119, 119, 106, 117, 128, 98, 106, 123 117, 110, 117, 117, 100, 112, 121, 108 110, 108, 106, 121, 121, 110, 119, 114 121, 121, 102, 110, 119, 98, 123, 106 106, 100, 104, 104, 110, 94, 100, 94 94, 102, 110, 98, 104, 96, 104, 106 94, 86, 114, 102, 94, 98, 108, 112 112, 117, 110, 104, 108, 108, 106, 110 92, 104, 317, 117, 112, 117, 112, 96 88, 114, 121, 110, 88, 98, 112, 98 104, 106, 100, 114, 102, 86, 86, 114 104, 117, 104, 117, 110, 100, 121, 112 98, 96, 106, 114, 94, 119, 256, 117 106, 121, 92, 100, 106, 102, 88, 110 104, 94, 94, 106, 114, 121, 108, 98 104, 117, 112, 112, 121, 110, 114, 114 125, 117, 123, 125, 117, 121, 83, 86 110, 90, 123, 108, 98, 85, 125, 88 85, 90, 112, 92, 98, 92, 110, 102 102, 123, 100, 117, 106, 128, 106, 110 100, 110, 94, 110, 108, 88, 102, 106 110, 106, 110, 110, 92, 94, 104, 110 100, 123, 104, 123, 119, 92, 121, 125 112, 119, 123, 121, 102, 96, 86, 117 110, 86, 94, 77, 119, 149, 149 151, 161, 121, 144, 146, 139, 137, 154 144, 137, 146, 149, 164, 166, 159, 149 135, 161, 135, 154, 139, 146, 137, 172 137, 142, 142, 159, 125, 139, 144, 159 156, 151, 154, 149, 159, 144, 154, 154 159, 139, 142, 146, 128, 156, 121, 137 156, 151, 139, 137, 159, 151, 135, 149 154, 144, 144, 149, 135, 144, 128, 164 154, 146, 146, 121, 119, 130, 149, 154 123, 159, 142, 149, 142, 137, 144, 139 144, 139, 151, 146, 139, 128, 154, 142 132, 130, 135, 135, 149, 146, 154, 164 149, 144, 159, 135, 156, 135, 169, 130 135, 144, 139, 159, 144, 161, 164, 174 180, 166, 159, 174, 159, 164, 174, 177 188, 164, 164, 159, 180, 188, 159, 166 177, 151, 174, 185, 156, 172, 164, 161 144, 159, 149, 144, 128, 161, 174, 151 142, 146, 166, 166, 149, 159, 144, 169 169, 144, 142, 137, 166, 137, 137, 164 164, 169, 159, 159, 174, 144, 156, 161 159, 185, 135, 164, 164, 149, 146, 159 159, 159, 159, 156, 177, 146, 149, 146 166, 142, 151, 161, 132, 137, 169, 132 159, 161, 174, 149, 135, 169, 159, 154 156, 182, 156, 156, 166, 164, 149, 149 151, 164, 154, 146, 164, 169, 159, 146 172, 166, 164, 151, 174, 146, 166, 164 169, 164, 159, 164, 144, 185, 172, 159 142, 144, 193, 159, 159, 172, 166, 161 174, 177, 164, 154, 169, 146, 169, 149 188, 169, 182, 185, 166, 172, 204, 174 180, 190, 202, 156, 156, 172, 174, 159 166, 185, 159, 177, 190, 174, 172, 142 185, 172, 169, 182, 177, 177, 174, 166 159, 177, 164, 172, 180, 185, 161, 164 159, 169, 169, 164, 169, 180, 161, 164 164, 185, 164, 164, 174, 174, 166, 154 166, 169, 180, 174, 188, 202, 174, 196 149, 185, 193, 164, 169, 172, 174, 185 199, 164, 185, 188, 188, 182, 182, 180 154, 190, 144, 156, 169, 188, 174, 185 164, 169, 193, 213, 196, 174, 164, 169 174, 182, 182, 182, 151, 182, 204, 199 185, 182, 166, 210, 164, 188, 376, 182 185, 185, 177, 193, 207, 169, 174, 188 177, 182, 185, 182, 196, 177, 188, 190 185, 207, 196, 182, 182, 190, 216, 196 216, 219, 219, 185, 202, 188, 185, 199 216, 199, 207, 193, 182, 202, 196, 204 202, 182, 193, 199, 196, 185, 207, 154 188, 202, 204, 182, 190, 190, 185, 202 193, 207, 188, 185, 213, 174, 174, 202 207, 188, 196, 190, 174, 213, 213, 213 213, 207, 216, 219, 202, 190, 193, 213 177, 196, 210, 262, 219, 219, 216, 240 196, 231, 202, 196, 202, 225, 259, 182 228, 219, 219, 246, 219, 210, 243, 199 213, 240, 210, 228, 219, 219, 228, 237 216, 262, 253, 240, 246, 246, 246, 240 216, 222, 222, 219, 246, 250, 234, 243 246, 240, 243, 269, 262, 269, 240, 256 225, 256, 259, 256, 269, 289, 296, 269 299, 292, 286, 299, 331, 306, 335, 317 310, 317, 342, 331, 339, 335, 365, 412 400, 388, 433, 424, 441, 433, 445, 480 437, 428, 437, 454, 462, 471, 515, 467 475, 449, 458, 515, 484, 515, 488, 534 497, 571, 543, 552, 502, 586, 571, 548 538, 571, 590, 586, 538, 600, 595, 625 566, 600, 562, 543, 524, 488, 480, 462 462, 416, 424, 445, 416, 396, 380, 380 365, 384, 380, 361, 357, 369, 313, 369 342, 317, 317, 346, 306, 320, 317, 331 328, 324, 328, 317, 299, 313, 292, 306 296, 331, 306, 299, 292, 303, 339, 296 324, 289, 296, 310, 331, 306, 313, 306 289, 286, 303, 299, 272, 313, 276, 310 331, 310, 313, 313, 320, 320, 296, 299 282, 296, 303, 303, 346, 282, 328, 303 303, 324, 361, 313, 339, 310, 299, 328 317, 346, 342, 353, 335, 331, 353, 306 331, 320, 324, 376, 376, 380, 350, 404 369, 350, 384, 404, 388, 396, 404, 420 404, 372, 384, 408, 416, 437, 437, 441 445, 437, 511, 445, 471, 520, 529, 543 630, 590, 610, 615, 625, 640, 671, 734 762, 784, 790, 751, 870, 829, 829, 835 894, 900, 942, 986, 961, 967, 955, 936 894, 912, 906, 870, 912, 912, 894, 876 864, 876, 882, 795, 841, 745, 740, 745 724, 718, 676, 635, 625, 645, 635, 620 562, 590, 524, 538, 534, 543, 515, 497 488, 484, 480, 462, 467, 471, 502, 445 462, 467, 420, 408, 441, 445, 437, 388 428, 437, 392, 408, 428, 437, 454, 424 433, 416, 388, 416, 392, 400, 416, 400 416, 404, 392, 388, 392, 376, 408, 424 388, 437, 388, 404, 392, 339, 369, 408 400, 353, 412, 346, 384, 369, 400, 357 365, 376, 335, 350, 350, 328, 384, 369 320, 365, 369, 350, 369, 353, 380, 376 365, 357, 392, 380, 369, 357, 346, 372 388, 372, 357, 376, 380, 350, 346, 353 357, 342, 365, 317, 396, 380, 353, 388 361, 339, 331, 331, 353, 286, 331, 306 335, 296, 317, 317, 342, 286, 272, 296 289, 292, 289, 286, 262, 296, 276, 292 272, 286, 282, 282, 269, 279, 266, 262 256, 310, 292, 269, 289, 246, 243, 259 231, 250, 266, 292, 286, 262, 253, 276 299, 240, 292, 246, 253, 256, 250, 272 276, 256, 276, 276, 259, 286, 266, 243 228, 246, 234, 279, 266, 250, 243, 250 243, 253, 243, 259, 259, 219, 240, 259 234, 282, 237, 262, 240, 253, 222, 231 234, 259, 243, 256, 216, 243, 243, 204 246, 222, 266, 222, 231, 240, 231, 243 225, 292, 237, 237, 228, 222, 262, 259 234, 246, 213, 222, 207, 237, 250, 216 246, 259, 234, 228, 246, 228, 262, 243 222, 234, 246, 231, 272, 225, 216, 250 231, 225, 246, 250, 234, 225, 234, 225 202, 225, 219, 240, 237, 207, 213, 250 199, 216, 213, 222, 234, 207, 228, 231 213, 240, 231, 237, 237, 210, 202, 253 237, 222, 237, 225, 240, 228, 228, 204 246, 225, 222, 231, 256, 219, 243, 219 222, 222, 243, 210, 237, 246, 237, 234 253, 246, 237, 216, 222, 213, 231, 225 225, 210, 202, 237, 216, 234, 216, 207 243, 234, 207, 234, 237, 228, 228, 225 210, 180, 234, 259, 204, 213, 204, 250 266, 225, 228, 237, 216, 228, 225, 228 213, 216, 219, 219, 246, 222, 234, 250 222, 240, 231, 222, 225, 204, 228, 213 234, 225, 216, 222, 234, 228, 219, 222 234, 222, 225, 222, 225, 216, 207, 246 231, 225, 225, 216, 199, 225, 210, 250 213, 222, 213, 225, 243, 234, 225, 202 243, 219, 219, 219, 231, 228, 231, 225 222, 202, 243, 246, 234, 246, 269, 222 246, 246, 207, 231, 228, 243, 240, 222 246, 216, 231, 213, 253, 262, 282, 253 256, 262, 234, 240, 243, 262, 269, 253 225, 250, 292, 225, 259, 246, 246, 246 276, 276, 310, 292, 303, 286, 313, 303 286, 286, 317, 357, 350, 416, 369, 357 412, 424, 428, 480, 529, 534, 576, 595 630, 734, 751, 847, 912, 973, 1056, 1142 1183, 1318, 1340, 1362, 1529, 1452, 1490, 1665 1656, 1697, 1600, 1689, 1697, 1673, 1592, 1568 1576, 1490, 1376, 1274, 1190, 1063, 992, 980 894, 745, 756, 692, 581, 543, 511, 462 420, 437, 392, 380, 324, 335, 372, 303 331, 289, 286, 272, 289, 276, 289, 234 262, 256, 246, 253, 250, 262, 262, 243 246, 225, 228, 219, 228, 228, 219, 216 207, 250, 228, 228, 213, 207, 240, 210 219, 240, 190, 213, 204, 193, 213, 213 193, 207, 207, 225, 185, 216, 193, 225 231, 207, 190, 202, 188, 210, 202, 177 219, 193, 182, 219, 202, 185, 199, 190 193, 202, 199, 190, 213, 180, 190, 210 207, 188, 185, 199, 159, 185, 202, 180 174, 182, 182, 188, 174, 172, 193, 174 154, 196, 202, 193, 174, 193, 210, 185 188, 196, 202, 210, 204, 193, 202, 196 193, 161, 193, 177, 174, 216, 199, 169 174, 177, 185, 193, 177, 199, 188, 177 156, 182, 185, 207, 182, 174, 177, 185 172, 164, 172, 190, 166, 182, 182, 177 204, 199, 190, 185, 190, 159, 174, 174 169, 193, 182, 188, 188, 169, 185, 177 188, 180, 185, 161, 185, 213, 180, 172 202, 174, 151, 190, 204, 182, 172, 174 144, 174, 166, 174, 174, 188, 174, 188 188, 164, 149, 154, 166, 188, 172, 174 193, 151, 174, 180, 182, 177, 156, 169 177, 161, 154, 180, 174, 169, 156, 202 154, 169, 154, 172, 156, 159, 190, 159 161, 156, 210, 190, 199, 172, 169, 169 174, 164, 164, 161, 161, 161, 174, 174 174, 159, 172, 174, 177, 182, 156, 174 190, 177, 154, 159, 185, 172, 159, 182 161, 174, 174, 151, 164, 174, 169, 139 177, 164, 172, 180, 159, 135, 156, 159 151, 166, 180, 164, 151, 193, 164, 204 161, 182, 159, 164, 144, 172, 156, 185 174, 177, 164, 172, 174, 182, 164, 177 164, 169, 174, 174, 149, 169, 174, 172 174, 154, 144, 188, 174, 172, 190, 185 188, 190, 169, 164, 172, 182, 182, 159 161, 188, 159, 172, 169, 185, 149, 174 164, 137, 166, 151, 172, 156, 180, 193 149, 180, 164, 146, 166, 169, 164, 164 159, 164, 146, 151, 161, 172, 177, 182 164, 174, 182, 174, 159, 180, 159, 180 190, 174, 164, 164, 177, 177, 151, 169 174, 172, 190, 164, 182, 177, 159, 219 169, 193, 177, 190, 172, 180, 177, 161 190, 182, 180, 196, 182, 202, 185, 185 196, 188, 199, 199, 174, 202, 190, 185 166, 199, 185, 199, 182, 193, 204, 202 204, 180, 202, 199, 180, 196, 193, 202 190, 182, 169, 177, 193, 166, 182, 182 177, 180, 169, 149, 174, 159, 146, 174 166, 169, 172, 174, 177, 149, 154, 137 149, 154, 164, 156, 154, 154, 151, 135 156, 144, 146, 154, 154, 154, 128, 156 161, 182, 166, 137, 142, 135, 151, 156 142, 146, 166, 166, 151, 149, 188, 130 156, 142, 151, 137, 154, 139, 154, 166 154, 130, 149, 123, 142, 144, 164, 156 159, 135, 161, 142, 137, 164, 146, 144 151, 130, 149, 142, 135, 123, 137, 144 130, 144, 142, 110, 137, 142, 149, 125 128, 166, 151, 174, 166, 154, 144, 144 132, 132, 142, 149, 128, 117, 159, 121 139, 128, 135, 135, 137, 137, 130, 144 137, 154, 123, 146, 121, 137, 151, 149 149, 137, 132, 154, 125, 128, 149, 156 135, 142, 139, 146, 142, 154, 159, 130 149, 139, 135, 123, 142, 128, 144, 164 151, 144, 159, 161, 149, 159, 137, 130 164, 159, 151, 149, 159, 159, 164, 146 156, 164, 149, 149, 161, 137, 161, 156 135, 172, 177, 142, 169, 139, 137, 154 139, 144, 135, 159, 151, 139, 146, 137 139, 139, 114, 144, 135, 125, 144, 119 142, 146, 142, 137, 149, 137, 121, 123 142, 117, 144, 137, 135, 164, 154, 144 151, 137, 142, 156, 161, 137, 161, 169 169, 190, 144, 169, 156, 156, 188, 139 159, 151, 151, 156, 144, 125, 159, 128 137, 135, 149, 137, 156, 137, 137, 137 142, 125, 144, 139, 125, 137, 142, 125 161, 123, 123, 108, 128, 130, 132, 108 128, 130, 119, 128, 132, 121, 102, 139 119, 112, 108, 128, 121, 130, 119, 142 119, 106, 125, 139, 144, 132, 123, 123 110, 146, 130, 142, 130, 139, 117, 108 132, 121, 121, 123, 121, 130, 130, 110 137, 142, 144, 104, 119, 108, 137, 114 125, 137, 117, 125, 146, 121, 123, 135 137, 104, 132, 132, 142, 149, 110, 130 121, 139, 142, 121, 128, 154, 123, 130 139, 132, 144, 123, 149, 142, 119, 130 142, 130, 128, 130, 121, 149, 128, 146 137, 117, 137, 142, 135, 128, 139, 149 139, 135, 169, 135, 123, 125, 123, 130 114, 123, 135, 114, 130, 119, 135, 137 139, 114, 137, 117, 112, 149, 137, 137 128, 130, 139, 142, 128, 137, 135, 92 154, 119, 139, 130, 130, 121, 128,/