SampleIdent,907a 6h-3 33-34bulk,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,18-aug-1993 9:02,/ DataAngleRange, 2.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 86, 90, 71, 92, 94, 83, 67, 76 79, 92, 66, 62, 85, 79, 71, 79 58, 62, 66, 66, 66, 85, 71, 61 69, 67, 71, 71, 66, 56, 53, 59 69, 77, 74, 59, 79, 71, 71, 69 72, 71, 81, 72, 62, 79, 61, 52 53, 61, 74, 85, 67, 62, 56, 76 56, 69, 62, 62, 77, 67, 62, 62 59, 79, 76, 77, 72, 56, 62, 69 50, 77, 72, 85, 85, 79, 62, 90 67, 67, 72, 62, 77, 72, 69, 71 86, 79, 66, 85, 77, 77, 83, 88 83, 62, 67, 66, 71, 83, 71, 69 76, 83, 72, 71, 83, 98, 79, 77 72, 72, 72, 79, 79, 71, 85, 88 96, 86, 88, 77, 72, 76, 77, 85 72, 71, 76, 83, 72, 86, 98, 88 81, 83, 86, 77, 79, 86, 90, 90 96, 96, 98, 88, 79, 96, 108, 96 79, 96, 96, 98, 86, 90, 76, 114 83, 98, 76, 88, 98, 98, 114, 100 102, 112, 104, 100, 102, 83, 102, 100 92, 88, 110, 81, 85, 88, 96, 112 98, 106, 125, 121, 104, 106, 94, 123 81, 121, 112, 117, 102, 119, 104, 106 135, 94, 110, 112, 106, 123, 123, 119 110, 102, 130, 139, 125, 106, 86, 121 100, 151, 106, 94, 119, 123, 117, 128 112, 119, 365, 108, 100, 130, 135, 125 114, 114, 125, 112, 142, 119, 132, 121 135, 114, 121, 121, 114, 137, 135, 137 154, 123, 132, 123, 117, 128, 117, 108 108, 102, 114, 123, 117, 137, 112, 137 119, 114, 104, 114, 125, 121, 125, 104 144, 144, 104, 130, 119, 121, 130, 110 106, 110, 112, 106, 104, 128, 121, 119 114, 125, 96, 114, 117, 88, 117, 132 119, 108, 110, 108, 110, 102, 123, 123 125, 135, 125, 98, 130, 112, 117, 121 121, 104, 96, 110, 117, 104, 110, 106 102, 108, 121, 104, 106, 128, 114, 121 102, 137, 106, 102, 123, 142, 132, 117 117, 132, 114, 128, 100, 119, 108, 106 123, 102, 121, 94, 102, 121, 106, 83 117, 98, 96, 110, 112, 102, 108, 92 106, 98, 112, 83, 94, 110, 98, 92 98, 88, 74, 112, 108, 94, 104, 102 108, 88, 90, 104, 125, 92, 104, 98 94, 104, 86, 98, 86, 85, 108, 94 94, 96, 81, 83, 88, 96, 94, 106 92, 94, 88, 100, 104, 100, 86, 90 94, 102, 83, 90, 94, 88, 112, 96 79, 90, 100, 88, 96, 98, 88, 104 102, 100, 81, 86, 98, 100, 86, 100 96, 79, 92, 79, 88, 104, 98, 90 94, 102, 100, 96, 86, 69, 81, 86 104, 100, 83, 102, 83, 96, 98, 108 94, 96, 85, 76, 79, 100, 85, 114 92, 74, 104, 85, 86, 98, 92, 77 85, 98, 71, 96, 96, 88, 92, 90 102, 92, 106, 94, 85, 102, 96, 98 85, 104, 88, 88, 90, 86, 90, 110 86, 92, 90, 94, 86, 85, 112, 110 108, 86, 110, 85, 90, 96, 110, 96 121, 112, 106, 121, 108, 114, 106, 137 132, 110, 110, 125, 114, 112, 123, 106 106, 90, 77, 96, 104, 96, 102, 83 88, 85, 86, 94, 98, 86, 79, 88 72, 83, 71, 90, 90, 77, 81, 83 88, 88, 90, 86, 88, 79, 85, 88 77, 88, 77, 94, 71, 77, 85, 94 79, 83, 88, 81, 90, 79, 85, 86 79, 79, 77, 76, 104, 119, 104, 88 92, 94, 100, 79, 100, 90, 76, 96 106, 90, 94, 92, 88, 94, 86, 79 86, 90, 85, 77, 79, 85, 77, 88 72, 79, 94, 90, 79, 79, 59, 96 79, 72, 77, 83, 67, 77, 62, 69 88, 96, 182, 83, 98, 76, 86, 77 96, 79, 83, 86, 94, 90, 88, 81 81, 117, 94, 74, 85, 86, 79, 77 96, 106, 71, 79, 90, 83, 72, 92 77, 67, 79, 79, 85, 85, 81, 88 81, 90, 71, 85, 77, 88, 77, 86 98, 72, 83, 72, 94, 79, 85, 88 83, 90, 79, 83, 67, 112, 92, 94 77, 88, 81, 83, 96, 88, 77, 92 86, 66, 79, 77, 88, 81, 86, 74 76, 83, 86, 67, 77, 83, 77, 90 77, 79, 88, 62, 74, 83, 86, 88 106, 90, 67, 76, 74, 100, 85, 92 102, 76, 83, 90, 90, 72, 94, 88 72, 86, 85, 76, 90, 88, 79, 86 85, 86, 72, 85, 79, 72, 83, 85 85, 72, 90, 106, 90, 67, 100, 85 96, 72, 71, 81, 85, 104, 79, 96 88, 83, 90, 86, 102, 98, 79, 79 92, 90, 96, 88, 104, 98, 98, 104 88, 102, 86, 92, 90, 102, 110, 102 98, 85, 90, 94, 77, 86, 86, 88 104, 81, 106, 90, 100, 85, 98, 88 90, 86, 94, 86, 90, 81, 96, 104 106, 96, 90, 83, 102, 79, 77, 86 90, 94, 98, 90, 79, 114, 108, 96 106, 98, 86, 98, 104, 117, 108, 102 106, 86, 92, 86, 117, 104, 85, 100 98, 96, 96, 77, 110, 98, 88, 102 94, 112, 128, 114, 98, 130, 108, 104 102, 125, 100, 106, 123, 102, 139, 123 142, 130, 149, 128, 159, 159, 149, 159 159, 161, 159, 154, 204, 169, 166, 154 177, 177, 185, 185, 182, 169, 177, 174 151, 172, 172, 135, 159, 169, 125, 139 151, 154, 128, 128, 164, 130, 125, 137 110, 139, 149, 130, 142, 151, 135, 142 137, 142, 169, 151, 146, 164, 166, 139 149, 149, 159, 177, 156, 174, 182, 216 210, 222, 237, 225, 237, 240, 250, 282 266, 222, 202, 210, 174, 156, 144, 149 144, 135, 121, 128, 128, 132, 123, 146 128, 123, 128, 114, 154, 130, 117, 123 123, 146, 117, 142, 137, 128, 135, 128 123, 135, 117, 130, 117, 130, 132, 137 132, 112, 137, 132, 132, 137, 151, 135 154, 169, 164, 164, 164, 196, 207, 207 174, 196, 199, 174, 185, 174, 174, 130 128, 123, 128, 156, 142, 130, 125, 135 144, 132, 121, 130, 142, 121, 123, 132 132, 130, 114, 114, 142, 128, 102, 121 114, 156, 132, 119, 123, 164, 151, 149 144, 144, 146, 151, 137, 146, 146, 156 149, 110, 146, 142, 130, 144, 137, 128 130, 137, 125, 154, 128, 117, 137, 139 151, 119, 149, 137, 151, 139, 164, 161 137, 149, 164, 169, 154, 180, 174, 169 190, 182, 185, 180, 169, 164, 156, 139 164, 135, 151, 149, 149, 149, 154, 137 123, 174, 146, 139, 164, 151, 144, 159 142, 180, 159, 154, 172, 169, 177, 177 202, 213, 188, 222, 188, 177, 169, 199 161, 166, 154, 174, 151, 154, 169, 130 159, 135, 144, 151, 156, 146, 151, 142 151, 159, 142, 159, 164, 154, 142, 159 164, 149, 172, 164, 164, 154, 188, 174 174, 164, 156, 156, 188, 177, 199, 182 172, 169, 196, 154, 172, 169, 177, 182 193, 182, 174, 182, 188, 172, 174, 174 172, 154, 193, 174, 166, 149, 169, 156 180, 161, 154, 156, 137, 161, 154, 174 156, 159, 161, 154, 146, 159, 154, 166 144, 151, 164, 166, 159, 154, 144, 149 169, 159, 159, 188, 149, 180, 185, 193 202, 202, 213, 250, 279, 276, 339, 392 475, 548, 635, 724, 841, 986, 1076, 1089 1102, 1037, 980, 900, 751, 557, 454, 412 313, 272, 250, 250, 243, 231, 202, 193 199, 199, 182, 202, 174, 199, 180, 174 177, 188, 172, 196, 193, 182, 185, 169 177, 216, 213, 216, 219, 231, 240, 231 237, 256, 228, 253, 276, 213, 272, 502 225, 269, 262, 276, 279, 256, 289, 320 331, 313, 369, 342, 412, 392, 392, 458 458, 408, 388, 342, 335, 342, 353, 365 380, 296, 246, 256, 225, 207, 169, 185 210, 169, 174, 196, 177, 182, 202, 161 161, 161, 169, 164, 149, 149, 166, 154 130, 149, 137, 161, 154, 151, 144, 172 149, 146, 144, 151, 132, 144, 137, 144 159, 137, 137, 154, 154, 149, 137, 144 149, 149, 166, 164, 154, 144, 169, 159 144, 156, 144, 146, 144, 149, 142, 137 156, 159, 146, 185, 156, 142, 151, 156 156, 161, 185, 161, 166, 166, 193, 188 193, 190, 190, 219, 193, 196, 182, 202 182, 190, 196, 185, 166, 177, 159, 166 180, 172, 177, 188, 154, 172, 166, 182 151, 188, 151, 182, 161, 180, 180, 188 177, 204, 204, 188, 182, 193, 159, 174 174, 190, 174, 177, 188, 174, 169, 182 151, 154, 161, 149, 177, 169, 172, 146 159, 185, 161, 142, 144, 137, 154, 142 159, 137, 149, 144, 151, 146, 149, 125 164, 130, 159, 151, 159, 144, 156, 151 144, 169, 137, 159, 144, 128, 149, 159 151, 188, 164, 177, 199, 225, 246, 276 276, 276, 320, 303, 320, 339, 324, 320 292, 296, 237, 204, 207, 169, 154, 156 139, 144, 400, 154, 125, 123, 142, 144 121, 121, 144, 130, 144, 132, 151, 137 137, 123, 135, 146, 114, 144, 135, 139 123, 123, 137, 121, 132, 123, 135, 139 114, 128, 114, 139, 130, 130, 117, 135 119, 123, 128, 110, 125, 112, 125, 121 123, 130, 128, 135, 137, 135, 135, 149 110, 114, 128, 135, 132, 112, 104, 110 132, 128, 123, 135, 137, 130, 121, 135 132, 137, 121, 132, 137, 135, 121, 137 139, 119, 119, 146, 146, 128, 114, 149 139, 149, 108, 125, 144, 128, 106, 144 135, 125, 149, 130, 112, 149, 159, 117 137, 130, 144, 130, 132, 154, 132, 144 132, 125, 144, 159, 146, 164, 146, 156 154, 164, 164, 164, 182, 169, 196, 169 185, 169, 177, 169, 199, 199, 182, 204 174, 225, 177, 225, 185, 193, 199, 231 225, 228, 213, 216, 250, 262, 246, 266 253, 234, 237, 213, 256, 222, 234, 204 246, 225, 216, 190, 185, 185, 185, 182 172, 196, 188, 180, 202, 185, 177, 172 169, 193, 159, 166, 185, 180, 185, 180 172, 174, 182, 161, 182, 202, 156, 161 177, 146, 159, 172, 144, 169, 159, 146 185, 142, 144, 180, 154, 144, 135, 139 137, 139, 159, 135, 169, 125, 137, 151 125, 123, 146, 139, 159, 149, 156, 149 196, 169, 182, 193, 190, 231, 193, 210 234, 246, 231, 222, 237, 193, 188, 188 174, 172, 149, 154, 169, 166, 137, 149 166, 142, 164, 180, 125, 139, 159, 154 149, 137, 156, 135, 144, 142, 149, 164 137, 139, 154, 130, 144, 146, 161, 137 142, 154, 151, 166, 169, 144, 169, 137 174, 139, 169, 169, 159, 174, 172, 121 196, 172, 154, 159, 151, 174, 146, 164 177, 154, 142, 142, 144, 128, 142, 128 108, 130, 146, 132, 130, 130, 128, 144 137, 121, 128, 161, 149, 166, 151, 144 132, 149, 137, 135, 132, 128, 130, 130 119, 121, 104, 146, 125, 128, 123, 104 123, 119, 110, 108, 123, 142, 110, 106 139, 112, 114, 125, 114, 121, 135, 130 104, 121, 100, 106, 114, 137, 123, 121 121, 119, 117, 121, 100, 117, 123, 137 130, 149, 130, 156, 164, 161, 177, 177 166, 164, 166, 188, 172, 169, 177, 130 130, 142, 146, 128, 112, 100, 117, 123 139, 123, 117, 139, 121, 125, 132, 110 142, 98, 130, 125, 142, 121, 132, 114 139, 130, 123, 128, 130, 144, 128, 149 151, 159, 128, 139, 161, 144, 161, 154 119, 149, 121, 121, 123, 123, 112, 121 117, 104, 137, 125, 125, 100, 123, 123 108, 121, 110, 119, 130, 142, 123, 130 146, 137, 139, 132, 137, 121, 112, 108 121, 130, 121, 139, 121, 114, 137, 137 114, 128, 117, 137, 125, 121, 123, 130 119, 119, 123, 123, 125, 114, 135, 121 137, 123, 146, 106, 123, 104, 114, 130 121, 110, 121, 135, 139, 142, 123, 114 125, 137, 121, 137, 130, 132, 135, 169 130, 135, 117, 139, 137, 137, 137, 146 144, 139, 151, 132, 139, 177, 190, 256 246, 219, 193, 190, 234, 259, 216, 199 196, 180, 188, 169, 164, 156, 142, 137 139, 142, 146, 125, 121, 123, 149, 114 139, 121, 125, 117, 114, 123, 117, 128 139, 146, 108, 100, 104, 121, 117, 110 110, 137, 121, 137, 117, 125, 123, 112 137, 132, 119, 110, 121, 130, 117, 125 137, 132, 125, 121, 125, 104, 132, 106 106, 98, 123, 104, 108, 119, 114, 117 123, 114, 123, 108, 132, 123, 132, 135 144, 128, 114, 137, 125, 123, 132, 128 132, 128, 121, 139, 114, 142, 112, 135 128, 106, 114, 121, 130, 119, 112, 144 151, 156, 166, 174, 164, 159, 180, 188 161, 166, 154, 156, 159, 137, 132, 125 144, 123, 125, 121, 139, 142, 149, 137 125, 130, 130, 104, 121, 137, 149, 135 149, 121, 144, 142, 132, 154, 137, 146 166, 180, 177, 177, 190, 213, 216, 231 222, 262, 262, 237, 246, 286, 253, 231 234, 237, 202, 188, 188, 190, 174, 161 144, 149, 149, 164, 172, 144, 149, 130 156, 166, 161, 137, 144, 132, 154, 146 114, 104, 117, 110, 119, 130, 137, 119 130, 125, 117, 106, 108, 114, 128, 125 110, 96, 112, 114, 119, 117, 110, 117 108, 110, 110, 106, 117, 112, 100, 121 102, 98, 104, 106, 110, 92, 94, 112 102, 102, 100, 104, 94, 114, 104, 102 108, 98, 106, 112, 125, 112, 86, 104 86, 114, 108, 112, 102, 108, 106, 106 102, 98, 102, 104, 90, 114, 108, 104 110, 92, 106, 104, 123, 96, 106, 123 112, 121, 100, 90, 90, 106, 94, 106 88, 100, 110, 119, 121, 123, 104, 117 114, 132, 102, 96, 121, 117, 110, 121 100, 100, 104, 110, 135, 125, 125, 112 100, 112, 142, 104, 125, 114, 130, 112 104, 110, 102, 128, 106, 121, 96, 112 121, 108, 88, 104, 88, 117, 92, 108 88, 130, 96, 100, 94, 100, 112, 119 96, 108, 104, 114, 104, 104, 102, 96 114, 119, 104, 110, 100, 114, 114, 100 94, 119, 117, 135, 94, 117, 102, 98 98, 106, 119, 119, 117, 110, 119, 130 104, 112, 119, 96, 114, 121, 135, 108 117, 125, 121, 132, 130, 123, 117, 112 130, 151, 130, 139, 130, 151, 172, 149 164, 182, 185, 202, 193, 234, 237, 231 253, 231, 228, 193, 182, 177, 174, 149 172, 130, 154, 106, 130, 119, 123, 106 112, 110, 114, 130, 114, 119, 130, 123 132, 125, 125, 123, 135, 137, 117, 114 121, 119, 137, 130, 112, 106, 102, 123 117, 112, 108, 106, 106, 106, 121, 125 106, 119, 108, 123, 119, 102, 110, 108 112, 100, 130, 123, 112, 121, 96, 106 112, 106, 110, 110, 121, 104, 119, 128 102, 117, 110, 123, 121, 117, 114, 112 106, 128, 108, 117, 123, 106, 108, 106 130, 117, 125, 114, 106, 110, 139, 117 108, 114, 94, 123, 108, 102, 135, 119 114, 142, 112, 100, 108, 130, 119, 121 102, 96, 100, 142, 104, 106, 123, 94 112, 117, 119, 98, 121, 119, 100, 106 104, 106, 114, 123, 114, 98, 96, 119 92, 108, 114, 110, 130, 121, 130, 121 112, 123, 139, 123, 114, 139, 130, 125 121, 121, 125, 123, 123, 123, 137, 106 121, 125, 132, 114, 119, 121, 139, 112 128, 121, 146, 123, 137, 137, 125, 117 128, 119, 132, 117, 132, 100, 139, 128 142, 106, 117, 130, 125, 159, 132, 121 144, 142, 121, 123, 128, 130, 123, 130 125, 121, 117, 123, 149, 130, 142, 144 154, 119, 154, 112, 130, 119, 121, 135 123, 137, 130, 142, 130, 135, 144, 117 137, 139, 156, 125, 135, 166, 151, 144 177, 169, 174, 177, 164, 202, 180, 180 172, 166, 164, 172, 159, 156, 154, 146 142, 137, 144, 174, 174, 156, 154, 169 159, 144, 159, 137, 149, 169, 142, 132 154, 154, 125, 151, 161, 144, 142, 137 130, 142, 137, 144, 144, 149, 125, 123 144, 132, 159, 149, 137, 137, 164, 142 149, 139, 142, 119, 144, 139, 144, 137 135, 135, 159, 130, 137, 149, 139, 130 110, 130, 142, 151, 159, 169, 149, 169 174, 174, 182, 154, 169, 196, 190, 154 185, 142, 135, 159, 159, 156, 169, 125 135, 159, 142, 135, 125, 137, 128, 125 142, 142, 117, 128, 137, 114, 137, 137 128, 135, 128, 161, 98, 137, 128, 128 135, 132, 121, 128, 130, 144, 119, 108 119, 112, 119, 112, 121, 112, 128, 114 125, 114, 137, 128, 117, 144, 142, 128 123, 117, 154, 139, 112, 121, 121, 142 121, 117, 128, 135, 128, 139, 130, 135 137, 139, 137, 128, 151, 149, 112, 123 142, 139, 128, 132, 123, 130, 144, 121 121, 135, 159, 142, 114, 130, 139, 112 125, 139, 130, 121, 130, 154, 139, 125 154, 135, 125, 121, 154, 137, 144, 128 154, 130, 128, 132, 130, 135, 139, 139 128, 135, 119, 142, 159, 128, 128, 151 135, 135, 135, 112, 142, 144, 130, 135 132, 135, 137, 132, 121, 137, 132, 132 144, 144, 132, 151, 144, 132, 149, 132 169, 154, 146, 156, 159, 154, 149, 156 159, 169, 164, 159, 231, 188, 222, 240 262, 269, 282, 256, 279, 234, 222, 196 193, 196, 219, 188, 210, 159, 151, 164 156, 123, 149, 149, 166, 123, 132, 132 142, 146, 154, 130, 146, 142, 132, 144 135, 137, 156, 139, 174, 156, 149, 169 154, 146, 144, 149, 137, 154, 146, 159 154, 159, 144, 139, 154, 149, 164, 112 172, 159, 161, 159, 144, 169, 156, 166 164, 174, 159, 144, 182, 169, 182, 174 169, 199, 146, 177, 172, 166, 185, 159 161, 202, 156, 193, 202, 199, 190, 185 174, 159, 180, 190, 154, 202, 182, 169 193, 174, 164, 193, 172, 174, 169, 172 177, 174, 177, 159, 149, 177, 146, 172 146, 154, 199, 156, 156, 161, 149, 169 177, 159, 180, 164, 193, 177, 151, 161 166, 149, 166, 164, 117, 166, 142, 151 121, 169, 123, 161, 132, 144, 130, 156 142, 149, 172, 164, 144, 123, 142, 142 144, 154, 149, 130, 123, 164, 139, 117 139, 139, 130, 142, 135, 142, 137, 144 149, 132, 144, 117, 117, 125, 108, 130 166, 137, 125, 117, 128, 149, 130, 130 139, 142, 142, 139, 149, 128, 154, 137 121, 172, 144, 156, 151, 154, 135, 161 174, 182, 174, 164, 146, 154, 169, 166 164, 139, 144, 144, 149, 161, 128, 128 144, 146, 130, 156, 146, 164, 137, 144 117, 117, 139, 135, 128, 144, 139, 130 130, 132, 137, 123, 121, 174, 149, 125 135, 125, 169, 149, 132, 161, 125, 159 132, 144, 149, 139, 137, 135, 123, 128 159, 149, 159, 139, 137, 132, 137, 130 128, 132, 146, 139, 142, 132, 135, 154 142, 137, 139, 132, 130, 146, 144, 139 137, 142, 139, 123, 117, 149, 149, 142 149, 151, 144, 135, 142, 144, 156, 149 166, 154, 156, 144, 159, 139, 121, 161 154, 139, 151, 151, 169, 159, 177, 174 144, 164, 151, 144, 166, 151, 132, 151 123, 156, 132, 142, 151, 130, 119, 154 121, 123, 98, 132, 128, 121, 137, 149 125, 130, 114, 121, 132, 119, 149, 125 119, 142, 119, 137, 139, 130, 137, 142 139, 114, 130, 106, 144, 135, 130, 135 154, 137, 130, 142, 144, 154, 135, 137 154, 130, 139, 137, 135, 137, 132, 137 151, 132, 161, 151, 151, 149, 154, 154 159, 164, 185, 180, 219, 185, 216, 213 216, 199, 193, 169, 190, 177, 166, 185 149, 174, 156, 169, 161, 185, 185, 193 188, 185, 225, 225, 219, 243, 216, 222 190, 213, 240, 216, 219, 202, 210, 216 185, 225, 164, 161, 185, 159, 180, 144 174, 177, 144, 144, 172, 154, 154, 117 137, 108, 156, 164, 137, 135, 161, 130 144, 121, 121, 146, 159, 144, 123, 139 151, 132, 135, 135, 123, 139, 144, 154 161, 149, 130, 130, 130, 161, 132, 135 130, 159, 135, 137, 154, 149, 169, 139 154, 137, 139, 135, 135, 154, 137, 149 130, 164, 154, 144, 128, 117, 132, 154 117, 144, 130, 121, 139, 137, 125,/