SampleIdent,907A 6H-3 79-80 BULK,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,15-aug-1993 3:52,/ DataAngleRange, 2.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 71, 98, 90, 77, 81, 71, 76, 71 72, 67, 77, 67, 86, 98, 79, 66 59, 71, 59, 62, 71, 77, 76, 62 56, 72, 59, 83, 50, 72, 61, 357 59, 64, 59, 77, 64, 62, 62, 59 59, 66, 67, 59, 62, 76, 77, 67 61, 62, 69, 90, 72, 77, 62, 71 72, 90, 62, 76, 83, 59, 79, 67 71, 74, 204, 72, 69, 71, 66, 74 79, 76, 71, 66, 59, 83, 50, 71 61, 64, 62, 59, 71, 76, 69, 71 66, 67, 62, 85, 55, 66, 79, 79 86, 71, 76, 83, 77, 72, 74, 71 83, 67, 72, 56, 76, 74, 83, 88 76, 72, 85, 74, 76, 76, 71, 100 81, 85, 77, 96, 77, 85, 74, 76 86, 76, 64, 96, 72, 94, 92, 76 79, 79, 85, 100, 85, 79, 74, 72 108, 74, 85, 86, 86, 77, 88, 86 96, 96, 76, 86, 353, 71, 94, 86 77, 94, 85, 79, 92, 243, 88, 92 96, 100, 92, 98, 88, 83, 85, 100 92, 88, 86, 88, 108, 94, 90, 130 94, 104, 123, 106, 100, 98, 85, 88 106, 100, 121, 86, 104, 100, 98, 117 121, 96, 102, 104, 98, 130, 102, 117 106, 94, 121, 100, 96, 112, 123, 96 98, 102, 88, 108, 104, 121, 119, 110 121, 98, 114, 106, 106, 104, 106, 108 121, 123, 125, 104, 123, 128, 108, 108 106, 112, 102, 132, 114, 117, 108, 98 128, 110, 119, 104, 100, 100, 100, 90 121, 119, 117, 114, 106, 106, 114, 125 110, 88, 112, 123, 104, 114, 94, 88 108, 114, 121, 110, 112, 104, 114, 135 104, 86, 132, 110, 121, 104, 112, 114 112, 119, 94, 121, 110, 117, 121, 106 110, 117, 119, 128, 117, 106, 92, 112 108, 104, 96, 117, 135, 125, 119, 100 125, 112, 110, 121, 117, 121, 114, 117 139, 132, 139, 102, 108, 106, 108, 117 123, 135, 121, 108, 119, 114, 123, 132 123, 121, 98, 121, 123, 102, 112, 106 121, 121, 125, 128, 117, 106, 119, 106 106, 88, 94, 104, 123, 114, 102, 119 92, 106, 94, 108, 102, 110, 112, 104 108, 108, 86, 108, 100, 106, 98, 94 90, 88, 86, 90, 98, 112, 117, 108 100, 119, 104, 112, 77, 100, 83, 94 119, 104, 98, 92, 121, 88, 88, 96 85, 110, 86, 90, 86, 102, 67, 92 88, 94, 92, 108, 81, 98, 94, 98 106, 86, 77, 98, 96, 92, 79, 79 72, 110, 88, 86, 85, 86, 85, 98 100, 96, 94, 83, 100, 102, 86, 85 94, 94, 104, 90, 94, 104, 106, 90 90, 81, 100, 86, 92, 86, 85, 83 77, 83, 76, 86, 100, 85, 102, 92 92, 98, 76, 83, 123, 104, 100, 81 92, 83, 102, 90, 92, 83, 102, 85 94, 88, 88, 85, 77, 108, 92, 104 98, 86, 110, 92, 94, 96, 98, 96 106, 100, 94, 112, 94, 108, 96, 92 96, 108, 121, 119, 106, 112, 130, 123 119, 117, 125, 130, 132, 123, 144, 149 125, 112, 139, 139, 137, 114, 130, 114 128, 121, 98, 139, 117, 98, 77, 92 83, 108, 74, 85, 88, 98, 92, 77 77, 79, 71, 98, 77, 88, 85, 79 92, 86, 88, 88, 64, 83, 83, 96 90, 72, 94, 76, 83, 76, 76, 76 88, 71, 72, 81, 92, 94, 86, 98 86, 94, 92, 79, 72, 77, 86, 90 86, 106, 96, 85, 94, 98, 96, 104 114, 88, 79, 102, 79, 90, 76, 83 66, 77, 85, 79, 88, 94, 90, 77 72, 81, 77, 88, 88, 98, 77, 69 83, 72, 72, 77, 98, 79, 77, 81 90, 72, 72, 76, 85, 83, 77, 85 66, 71, 72, 79, 71, 76, 86, 72 71, 77, 64, 72, 79, 79, 85, 69 88, 77, 76, 85, 77, 85, 85, 90 74, 79, 88, 83, 69, 77, 74, 77 79, 67, 77, 88, 79, 71, 92, 77 66, 72, 90, 62, 92, 90, 90, 66 64, 85, 77, 67, 83, 83, 86, 83 62, 90, 77, 79, 74, 83, 71, 67 90, 79, 71, 83, 71, 83, 76, 79 71, 76, 81, 76, 67, 76, 79, 77 85, 106, 76, 92, 79, 69, 81, 90 71, 71, 83, 67, 71, 58, 85, 62 100, 71, 74, 81, 71, 64, 76, 74 67, 66, 77, 66, 71, 74, 72, 83 67, 72, 74, 79, 94, 77, 81, 86 83, 74, 83, 77, 71, 59, 85, 71 90, 77, 69, 72, 92, 86, 76, 86 74, 77, 79, 88, 81, 81, 77, 90 92, 102, 100, 88, 92, 88, 96, 100 106, 119, 121, 94, 104, 98, 92, 94 94, 90, 83, 92, 88, 92, 77, 88 77, 72, 88, 71, 102, 79, 81, 83 108, 76, 72, 76, 98, 86, 77, 71 83, 74, 59, 79, 94, 83, 86, 83 90, 88, 98, 96, 79, 69, 81, 92 85, 86, 104, 98, 102, 83, 104, 110 85, 94, 92, 96, 92, 98, 92, 76 90, 86, 85, 76, 72, 92, 74, 83 79, 85, 86, 83, 88, 98, 85, 90 85, 110, 98, 392, 98, 90, 86, 102 121, 104, 112, 117, 106, 106, 121, 112 142, 123, 114, 112, 121, 128, 144, 121 132, 130, 132, 149, 128, 130, 130, 146 128, 123, 108, 114, 114, 112, 117, 117 117, 117, 104, 96, 100, 100, 85, 102 104, 102, 106, 102, 121, 104, 110, 112 112, 144, 104, 112, 123, 123, 121, 117 123, 110, 130, 149, 164, 182, 190, 253 259, 292, 313, 286, 266, 246, 289, 286 324, 266, 282, 282, 225, 193, 188, 137 128, 130, 100, 114, 106, 110, 119, 106 98, 79, 88, 92, 98, 81, 102, 86 88, 72, 106, 108, 88, 92, 110, 98 110, 96, 85, 90, 104, 88, 81, 357 100, 106, 94, 121, 96, 98, 112, 119 130, 114, 139, 121, 142, 135, 130, 130 108, 123, 130, 135, 130, 146, 146, 139 193, 225, 216, 182, 159, 151, 137, 128 94, 106, 98, 98, 98, 104, 114, 88 88, 94, 102, 96, 88, 94, 94, 102 102, 102, 121, 98, 110, 104, 104, 110 106, 104, 114, 135, 108, 112, 119, 108 128, 108, 123, 102, 130, 121, 98, 98 92, 102, 106, 96, 98, 98, 86, 102 108, 117, 108, 112, 106, 121, 121, 137 119, 125, 123, 156, 132, 177, 146, 169 172, 149, 142, 132, 121, 119, 128, 112 106, 119, 100, 98, 112, 100, 114, 96 104, 98, 125, 117, 106, 92, 104, 137 102, 135, 161, 144, 132, 154, 125, 161 156, 135, 132, 154, 135, 137, 144, 144 104, 123, 132, 142, 130, 121, 142, 125 125, 132, 121, 130, 137, 149, 139, 149 164, 137, 154, 177, 166, 166, 210, 166 182, 188, 177, 174, 196, 204, 182, 207 196, 199, 188, 164, 199, 193, 188, 185 213, 190, 202, 207, 188, 193, 169, 177 188, 159, 182, 161, 177, 156, 161, 166 174, 154, 182, 174, 154, 159, 159, 142 161, 149, 154, 161, 137, 117, 117, 144 156, 119, 142, 123, 137, 132, 146, 130 139, 154, 117, 137, 154, 137, 156, 139 166, 139, 154, 177, 180, 190, 180, 216 228, 243, 259, 339, 437, 625, 807, 961 973, 1156, 1253, 1267, 1340, 1303, 1475, 1552 1616, 1772, 1714, 1616, 1444, 1267, 1063, 949 756, 625, 502, 388, 365, 313, 286, 282 246, 276, 222, 256, 246, 262, 216, 199 190, 213, 225, 210, 172, 182, 204, 196 174, 193, 199, 210, 213, 228, 237, 231 213, 225, 222, 243, 253, 219, 225, 279 222, 256, 262, 269, 243, 240, 276, 266 328, 339, 467, 511, 548, 557, 557, 562 520, 454, 365, 342, 331, 303, 269, 259 246, 213, 199, 219, 188, 185, 177, 156 149, 196, 202, 193, 182, 177, 169, 166 174, 169, 139, 139, 146, 137, 135, 123 137, 110, 114, 137, 121, 123, 123, 121 135, 125, 119, 130, 106, 117, 123, 123 128, 125, 110, 119, 121, 123, 112, 123 114, 106, 119, 119, 132, 151, 102, 110 137, 112, 98, 135, 114, 142, 106, 100 137, 117, 110, 123, 119, 121, 123, 125 137, 123, 128, 137, 117, 149, 142, 151 128, 132, 139, 161, 137, 146, 130, 159 169, 166, 161, 159, 166, 161, 159, 130 159, 142, 123, 144, 139, 144, 112, 154 135, 135, 130, 119, 119, 132, 146, 100 128, 159, 142, 142, 149, 142, 159, 151 174, 159, 169, 144, 128, 144, 146, 125 110, 130, 121, 106, 125, 130, 123, 121 108, 117, 117, 98, 121, 112, 125, 108 110, 117, 104, 85, 121, 110, 102, 94 114, 128, 114, 119, 137, 114, 128, 132 132, 144, 137, 149, 137, 144, 142, 125 142, 151, 144, 135, 161, 151, 137, 166 164, 149, 132, 169, 144, 128, 144, 121 132, 121, 96, 106, 102, 112, 96, 125 112, 96, 102, 123, 92, 121, 110, 123 79, 102, 102, 104, 104, 110, 96, 85 104, 98, 102, 79, 81, 98, 90, 88 83, 90, 81, 88, 92, 100, 102, 77 79, 96, 77, 90, 94, 90, 64, 94 88, 86, 85, 94, 88, 77, 83, 81 86, 88, 79, 96, 72, 90, 85, 94 69, 69, 86, 76, 77, 88, 98, 79 79, 96, 69, 66, 61, 71, 81, 76 64, 88, 86, 72, 62, 90, 86, 88 85, 81, 86, 85, 77, 94, 96, 108 98, 76, 96, 88, 98, 79, 100, 100 104, 79, 83, 83, 94, 96, 90, 90 96, 102, 92, 76, 94, 86, 96, 83 88, 96, 117, 96, 112, 117, 114, 119 112, 135, 130, 137, 130, 137, 130, 135 135, 151, 119, 137, 144, 156, 142, 123 144, 128, 154, 172, 164, 139, 166, 151 164, 185, 188, 177, 142, 149, 188, 190 182, 193, 177, 188, 190, 177, 185, 172 174, 166, 154, 146, 172, 139, 154, 128 144, 137, 121, 98, 139, 130, 128, 137 104, 130, 130, 125, 139, 142, 135, 121 119, 130, 125, 130, 112, 121, 119, 117 135, 121, 106, 132, 130, 142, 123, 125 130, 135, 114, 119, 132, 130, 112, 125 114, 137, 108, 96, 94, 125, 121, 119 112, 128, 132, 142, 137, 132, 169, 166 193, 207, 256, 199, 272, 256, 225, 262 310, 328, 335, 286, 240, 243, 225, 210 169, 177, 146, 121, 144, 135, 119, 130 102, 121, 121, 94, 100, 132, 110, 132 121, 128, 110, 112, 119, 121, 104, 104 132, 132, 117, 146, 128, 119, 119, 121 121, 130, 128, 121, 144, 135, 144, 137 125, 139, 149, 128, 117, 112, 159, 146 166, 149, 151, 174, 149, 149, 159, 164 132, 96, 121, 146, 130, 112, 112, 100 100, 121, 114, 96, 108, 114, 125, 114 123, 104, 119, 125, 108, 137, 114, 125 121, 121, 100, 112, 110, 121, 121, 106 98, 100, 88, 102, 110, 100, 114, 102 94, 86, 106, 96, 94, 88, 114, 106 96, 94, 190, 121, 104, 108, 77, 86 92, 85, 83, 79, 88, 96, 90, 98 88, 81, 108, 104, 100, 96, 96, 132 128, 137, 154, 130, 177, 166, 188, 219 219, 193, 234, 213, 222, 196, 210, 172 180, 151, 149, 137, 121, 119, 102, 106 90, 110, 79, 100, 102, 90, 106, 98 88, 121, 92, 81, 79, 106, 108, 104 88, 420, 128, 121, 137, 125, 128, 142 159, 180, 144, 151, 207, 169, 169, 144 142, 151, 110, 112, 108, 104, 106, 104 106, 90, 104, 88, 72, 94, 85, 90 96, 92, 90, 88, 94, 76, 112, 96 88, 102, 88, 85, 90, 83, 106, 85 92, 77, 106, 94, 90, 88, 98, 117 108, 106, 117, 94, 119, 102, 98, 88 85, 121, 90, 96, 96, 98, 94, 96 92, 108, 114, 96, 119, 106, 108, 135 121, 108, 132, 110, 98, 121, 119, 96 104, 112, 98, 96, 108, 102, 86, 106 100, 110, 90, 110, 112, 128, 123, 110 110, 117, 125, 117, 132, 159, 188, 172 213, 228, 237, 266, 237, 219, 202, 262 256, 253, 262, 246, 216, 199, 182, 169 142, 137, 139, 128, 110, 106, 123, 125 104, 102, 112, 106, 108, 90, 100, 102 119, 88, 102, 85, 104, 132, 104, 106 90, 102, 96, 83, 106, 83, 100, 110 98, 90, 98, 86, 104, 100, 83, 102 119, 94, 100, 114, 88, 77, 106, 104 384, 94, 106, 100, 81, 121, 110, 86 112, 94, 108, 102, 123, 123, 119, 104 106, 106, 79, 85, 100, 88, 108, 92 92, 94, 104, 104, 90, 100, 100, 88 102, 102, 100, 104, 119, 114, 106, 123 110, 123, 132, 169, 154, 164, 146, 149 169, 154, 146, 130, 135, 135, 125, 106 130, 350, 96, 112, 110, 117, 117, 104 130, 123, 123, 114, 110, 121, 130, 144 130, 135, 125, 137, 144, 125, 137, 169 185, 188, 164, 182, 185, 188, 177, 207 193, 166, 177, 243, 188, 196, 210, 213 190, 196, 174, 169, 185, 196, 210, 185 190, 207, 199, 225, 196, 213, 253, 256 243, 237, 243, 199, 188, 172, 159, 142 144, 130, 149, 125, 106, 98, 135, 102 104, 112, 98, 102, 98, 96, 96, 85 92, 76, 88, 102, 112, 94, 98, 77 100, 79, 88, 71, 112, 98, 79, 83 88, 90, 92, 86, 88, 85, 90, 83 85, 96, 92, 83, 88, 92, 85, 79 94, 92, 94, 100, 92, 86, 79, 90 79, 79, 104, 79, 71, 92, 66, 77 86, 66, 77, 72, 81, 94, 71, 71 90, 71, 72, 88, 92, 79, 85, 76 85, 88, 85, 76, 85, 90, 85, 81 85, 76, 102, 108, 76, 96, 90, 117 92, 77, 88, 77, 119, 96, 110, 114 110, 98, 104, 98, 102, 112, 81, 98 79, 85, 79, 108, 96, 90, 88, 85 104, 76, 79, 86, 94, 67, 85, 90 98, 88, 77, 86, 72, 98, 85, 85 72, 81, 85, 85, 72, 67, 85, 96 67, 83, 94, 86, 86, 94, 62, 85 92, 81, 76, 79, 85, 92, 102, 79 74, 72, 86, 92, 106, 85, 79, 88 100, 92, 79, 77, 90, 98, 76, 92 83, 92, 100, 86, 98, 100, 102, 104 92, 102, 94, 108, 90, 98, 102, 112 114, 137, 114, 151, 154, 188, 188, 219 237, 303, 296, 331, 372, 376, 484, 520 524, 497, 497, 416, 433, 372, 353, 342 269, 253, 190, 159, 161, 137, 119, 119 112, 92, 114, 119, 123, 94, 112, 110 108, 108, 119, 108, 128, 102, 125, 114 98, 117, 104, 110, 92, 108, 88, 110 98, 86, 81, 100, 92, 117, 106, 102 102, 117, 108, 90, 114, 123, 121, 85 108, 77, 86, 96, 92, 90, 90, 86 96, 106, 85, 88, 79, 86, 83, 69 81, 96, 92, 83, 77, 86, 79, 67 71, 94, 86, 76, 77, 77, 67, 77 62, 74, 76, 90, 71, 85, 76, 86 81, 71, 81, 98, 92, 86, 67, 81 83, 92, 72, 76, 98, 79, 72, 76 94, 104, 88, 77, 77, 83, 104, 96 100, 98, 96, 79, 92, 81, 86, 96 114, 90, 90, 100, 83, 90, 102, 88 90, 88, 79, 96, 112, 94, 98, 106 81, 94, 86, 108, 94, 108, 104, 119 106, 121, 106, 104, 117, 117, 112, 98 92, 96, 114, 117, 104, 98, 98, 102 102, 112, 104, 102, 106, 121, 108, 114 117, 108, 98, 119, 92, 98, 128, 106 106, 96, 96, 117, 90, 102, 110, 137 128, 104, 123, 98, 88, 102, 106, 112 119, 110, 123, 123, 88, 121, 125, 108 130, 125, 106, 123, 92, 123, 130, 121 110, 128, 119, 128, 121, 112, 114, 119 123, 137, 154, 154, 188, 169, 172, 207 188, 193, 210, 228, 237, 243, 237, 243 237, 237, 210, 207, 234, 196, 207, 193 185, 159, 169, 169, 151, 182, 188, 185 228, 202, 210, 207, 210, 196, 207, 180 182, 174, 161, 182, 144, 142, 144, 142 137, 154, 135, 132, 130, 132, 130, 154 130, 151, 142, 149, 110, 123, 137, 132 137, 139, 142, 114, 125, 142, 114, 137 123, 121, 149, 106, 128, 121, 110, 108 112, 130, 125, 119, 121, 121, 125, 117 114, 130, 128, 106, 137, 130, 121, 108 100, 117, 104, 110, 100, 121, 119, 94 123, 119, 121, 94, 100, 102, 96, 108 110, 128, 130, 100, 86, 104, 117, 106 119, 100, 102, 106, 102, 117, 110, 117 121, 104, 104, 106, 110, 92, 117, 108 112, 125, 106, 119, 100, 117, 108, 102 94, 104, 119, 112, 100, 92, 121, 121 94, 114, 102, 114, 114, 85, 117, 104 100, 104, 98, 128, 90, 104, 106, 123 92, 114, 112, 90, 117, 77, 104, 102 106, 102, 108, 85, 92, 108, 98, 106 117, 100, 114, 114, 117, 102, 104, 114 119, 104, 108, 119, 121, 121, 119, 108 110, 121, 130, 130, 128, 121, 110, 125 128, 114, 121, 128, 117, 137, 106, 96 110, 100, 102, 123, 98, 104, 117, 125 121, 110, 123, 104, 98, 106, 125, 121 110, 100, 125, 125, 110, 108, 110, 114 114, 104, 130, 110, 110, 125, 132, 121 112, 130, 114, 130, 130, 146, 139, 156 169, 182, 234, 246, 266, 296, 324, 357 376, 392, 424, 471, 441, 458, 416, 400 317, 313, 313, 303, 269, 272, 213, 222 199, 174, 137, 137, 144, 135, 135, 125 130, 110, 121, 125, 144, 146, 125, 128 135, 121, 96, 117, 137, 137, 117, 130 149, 139, 114, 135, 137, 114, 137, 125 144, 130, 132, 161, 123, 128, 144, 125 144, 132, 142, 112, 139, 144, 154, 159 130, 130, 146, 149, 149, 144, 146, 149 142, 144, 149, 146, 144, 139, 135, 174 137, 185, 130, 159, 154, 146, 156, 172 154, 159, 154, 169, 149, 169, 156, 159 144, 146, 174, 149, 132, 151, 135, 182 182, 182, 151, 169, 144, 123, 130, 121 151, 130, 125, 139, 149, 159, 110, 137 135, 130, 130, 119, 121, 123, 119, 114 110, 106, 125, 106, 125, 123, 119, 119 117, 112, 104, 121, 104, 119, 106, 119 121, 98, 121, 110, 79, 125, 130, 123 83, 106, 108, 108, 90, 94, 104, 102 90, 144, 128, 94, 114, 119, 110, 112 98, 102, 114, 117, 117, 121, 100, 110 102, 130, 104, 108, 112, 112, 108, 128 106, 117, 119, 114, 117, 121, 102, 100 125, 117, 121, 149, 108, 139, 135, 161 146, 164, 151, 166, 164, 164, 169, 156 169, 169, 151, 137, 151, 159, 146, 142 119, 146, 125, 128, 121, 130, 125, 123 102, 112, 102, 112, 110, 137, 117, 112 117, 110, 96, 121, 104, 121, 119, 104 123, 100, 130, 123, 114, 117, 123, 121 128, 125, 139, 128, 125, 137, 119, 144 114, 117, 137, 112, 125, 121, 125, 119 100, 121, 125, 123, 137, 117, 137, 123 117, 98, 130, 128, 119, 130, 112, 108 144, 130, 112, 142, 92, 130, 139, 108 106, 123, 125, 137, 128, 137, 135, 272 135, 128, 132, 117, 151, 137, 130, 117 130, 117, 132, 125, 137, 98, 106, 108 114, 104, 108, 139, 117, 119, 114, 114 110, 114, 104, 114, 121, 123, 130, 108 114, 108, 125, 98, 123, 104, 108, 102 110, 114, 96, 88, 102, 114, 108, 121 121, 117, 108, 108, 119, 130, 110, 125 137, 110, 112, 146, 121, 117, 125, 121 142, 135, 121, 149, 121, 125, 154, 128 137, 137, 139, 164, 117, 149, 123, 114 144, 121, 117, 137, 137, 144, 146, 166 188, 190, 234, 243, 231, 246, 246, 253 269, 350, 317, 328, 320, 310, 282, 246 219, 243, 253, 306, 276, 313, 317, 310 320, 346, 313, 335, 380, 437, 449, 462 480, 511, 441, 384, 437, 471, 449, 471 437, 437, 372, 303, 292, 243, 237, 262 237, 213, 213, 213, 154, 159, 139, 154 137, 135, 154, 135, 119, 130, 125, 114 117, 130, 106, 125, 114, 128, 128, 112 125, 135, 110, 123, 110, 130, 137, 130 137, 132, 117, 144, 130, 137, 154, 164 156, 166, 137, 154, 164, 166, 151, 172 149, 166, 169, 144, 149, 169, 135, 149 144, 144, 125, 142, 137, 125, 164, 146 130, 139, 135, 130, 146, 119, 139,/