SampleIdent,907a 6h-4 5-6 bulk,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,18-aug-1993 10:00,/ DataAngleRange, 2.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 96, 100, 90, 94, 88, 76, 86, 77 96, 83, 83, 85, 79, 88, 77, 88 85, 67, 88, 72, 71, 74, 79, 83 72, 64, 96, 61, 94, 66, 94, 72 79, 79, 106, 76, 76, 77, 72, 58 72, 66, 86, 61, 85, 77, 85, 96 76, 83, 85, 102, 94, 76, 392, 76 83, 72, 92, 92, 74, 96, 98, 71 90, 71, 88, 76, 86, 69, 90, 90 83, 83, 88, 94, 81, 79, 85, 85 86, 90, 83, 83, 86, 83, 83, 88 77, 83, 81, 79, 83, 92, 90, 86 100, 98, 66, 98, 104, 102, 79, 96 69, 90, 96, 81, 85, 85, 96, 94 102, 108, 94, 104, 106, 102, 108, 96 110, 83, 96, 86, 104, 90, 90, 112 86, 85, 100, 71, 112, 85, 110, 92 83, 88, 112, 92, 98, 92, 86, 92 98, 104, 88, 88, 108, 106, 108, 100 106, 96, 108, 94, 112, 102, 104, 114 106, 121, 102, 96, 110, 117, 106, 108 112, 106, 119, 117, 104, 114, 98, 108 132, 98, 108, 92, 137, 117, 128, 128 119, 100, 123, 114, 106, 121, 121, 123 130, 139, 114, 123, 132, 104, 117, 110 125, 119, 125, 121, 128, 119, 123, 132 139, 114, 135, 119, 114, 121, 112, 121 139, 132, 128, 130, 137, 137, 128, 132 125, 125, 142, 121, 128, 130, 123, 135 112, 144, 154, 104, 121, 125, 135, 142 130, 137, 119, 135, 139, 142, 121, 137 154, 132, 128, 123, 123, 137, 146, 128 132, 121, 132, 142, 139, 149, 139, 108 137, 123, 132, 396, 139, 130, 125, 142 135, 135, 146, 117, 114, 146, 137, 142 135, 121, 110, 114, 117, 119, 104, 125 128, 130, 119, 137, 121, 132, 144, 146 121, 114, 119, 110, 106, 108, 121, 128 123, 135, 106, 110, 121, 106, 128, 114 114, 114, 112, 121, 132, 132, 123, 137 123, 132, 128, 137, 125, 112, 144, 121 132, 149, 154, 135, 159, 154, 154, 135 132, 139, 96, 112, 121, 108, 119, 112 112, 114, 98, 117, 114, 100, 102, 112 125, 110, 102, 98, 106, 104, 121, 96 100, 112, 94, 88, 88, 114, 112, 85 96, 112, 102, 88, 96, 110, 114, 110 98, 104, 114, 92, 90, 112, 112, 112 114, 110, 106, 98, 98, 96, 100, 85 96, 94, 86, 102, 369, 90, 106, 121 92, 102, 117, 96, 96, 104, 85, 88 88, 92, 104, 102, 90, 104, 108, 110 104, 106, 102, 117, 90, 88, 104, 88 108, 112, 100, 102, 100, 98, 102, 104 96, 102, 108, 102, 100, 117, 98, 88 88, 96, 79, 90, 98, 92, 102, 90 85, 98, 108, 100, 114, 96, 100, 102 104, 108, 83, 96, 81, 79, 112, 83 88, 90, 86, 92, 117, 104, 112, 100 90, 88, 88, 83, 96, 88, 92, 100 94, 92, 98, 98, 94, 92, 88, 90 104, 121, 112, 96, 88, 90, 81, 112 98, 106, 102, 119, 114, 108, 110, 110 117, 119, 119, 119, 119, 142, 130, 144 159, 142, 125, 144, 159, 125, 123, 142 125, 119, 139, 102, 67, 125, 94, 92 102, 98, 104, 104, 86, 98, 102, 85 94, 96, 106, 98, 96, 85, 72, 83 85, 104, 88, 76, 90, 96, 92, 81 94, 76, 79, 92, 86, 96, 76, 79 83, 72, 77, 108, 86, 90, 92, 110 94, 112, 90, 90, 98, 92, 98, 81 100, 83, 106, 90, 98, 104, 92, 88 98, 86, 98, 94, 94, 96, 88, 72 96, 83, 100, 86, 88, 85, 79, 96 90, 83, 79, 79, 104, 98, 100, 76 83, 83, 108, 90, 96, 98, 83, 90 76, 90, 77, 96, 100, 92, 85, 79 114, 71, 94, 83, 94, 94, 83, 92 85, 85, 77, 85, 77, 85, 90, 106 96, 83, 94, 104, 86, 77, 119, 94 88, 76, 72, 86, 92, 88, 67, 86 92, 102, 108, 102, 79, 92, 85, 86 74, 100, 96, 85, 85, 90, 85, 96 88, 100, 86, 106, 92, 106, 92, 104 96, 77, 98, 102, 83, 96, 76, 90 94, 88, 100, 88, 79, 88, 96, 92 77, 92, 88, 83, 83, 76, 79, 96 90, 90, 92, 102, 90, 79, 69, 94 83, 92, 72, 79, 96, 100, 86, 98 86, 96, 112, 85, 85, 92, 74, 79 72, 102, 88, 98, 88, 90, 85, 94 86, 96, 76, 85, 90, 88, 88, 88 88, 106, 100, 106, 81, 98, 90, 110 90, 92, 98, 104, 94, 88, 104, 104 96, 96, 98, 85, 98, 92, 86, 96 121, 96, 110, 108, 108, 90, 108, 125 110, 119, 108, 128, 130, 114, 128, 135 132, 90, 96, 128, 96, 117, 106, 94 92, 92, 77, 92, 90, 94, 106, 88 104, 110, 100, 108, 106, 94, 94, 100 110, 102, 94, 94, 100, 102, 106, 112 119, 110, 79, 102, 83, 100, 114, 117 108, 106, 121, 117, 96, 123, 110, 102 123, 119, 119, 98, 114, 114, 110, 108 130, 110, 108, 112, 135, 125, 117, 114 123, 130, 137, 108, 117, 125, 130, 130 125, 117, 128, 114, 137, 137, 128, 132 123, 117, 142, 135, 123, 125, 119, 161 177, 161, 164, 172, 166, 199, 199, 169 207, 202, 207, 207, 185, 190, 193, 172 180, 166, 154, 149, 159, 156, 159, 137 180, 135, 169, 149, 154, 146, 149, 144 139, 149, 132, 128, 159, 154, 156, 174 161, 130, 146, 159, 151, 142, 166, 156 159, 144, 156, 154, 144, 169, 149, 182 210, 234, 256, 262, 276, 276, 272, 335 328, 286, 266, 272, 262, 213, 190, 169 164, 159, 154, 161, 142, 142, 177, 125 154, 139, 149, 146, 164, 139, 137, 132 149, 154, 154, 149, 159, 156, 172, 164 130, 149, 161, 164, 149, 159, 149, 149 159, 130, 144, 154, 154, 142, 123, 132 159, 156, 172, 161, 196, 193, 185, 172 193, 199, 199, 199, 213, 180, 210, 174 174, 177, 128, 146, 137, 154, 125, 130 156, 135, 154, 156, 149, 137, 144, 142 121, 132, 135, 144, 146, 149, 151, 130 144, 144, 156, 144, 154, 154, 154, 146 172, 144, 169, 149, 166, 169, 156, 172 172, 154, 182, 151, 172, 156, 174, 177 166, 146, 130, 159, 151, 172, 149, 154 169, 137, 142, 174, 149, 151, 180, 159 177, 172, 188, 185, 210, 199, 210, 180 188, 199, 213, 188, 182, 216, 174, 177 185, 180, 180, 185, 161, 177, 174, 166 182, 177, 172, 172, 174, 177, 172, 161 151, 188, 180, 196, 185, 188, 182, 225 222, 216, 246, 216, 199, 185, 185, 210 146, 174, 180, 164, 166, 159, 159, 182 156, 146, 161, 185, 182, 177, 156, 185 193, 207, 169, 177, 188, 196, 180, 169 185, 188, 207, 202, 196, 182, 188, 188 199, 225, 188, 190, 219, 225, 228, 266 219, 228, 237, 219, 199, 219, 210, 225 231, 213, 424, 237, 213, 202, 169, 213 188, 204, 213, 196, 185, 202, 193, 193 202, 177, 222, 182, 174, 177, 169, 190 193, 149, 177, 166, 196, 188, 185, 174 174, 199, 182, 169, 172, 174, 188, 166 156, 190, 202, 185, 174, 182, 225, 196 199, 231, 216, 256, 213, 282, 272, 328 365, 480, 650, 818, 1037, 1142, 1347, 1369 1318, 1282, 1296, 1156, 1063, 912, 740, 534 462, 412, 388, 320, 296, 266, 262, 276 250, 240, 225, 231, 246, 222, 182, 216 213, 210, 222, 210, 202, 219, 199, 196 202, 188, 199, 240, 246, 256, 243, 253 272, 289, 250, 286, 282, 266, 253, 259 282, 259, 240, 266, 289, 296, 331, 306 292, 299, 320, 320, 292, 324, 313, 372 376, 346, 372, 384, 353, 350, 353, 306 256, 259, 237, 256, 237, 228, 228, 231 228, 228, 228, 210, 196, 196, 228, 202 216, 196, 185, 196, 199, 193, 193, 174 511, 169, 182, 146, 177, 161, 169, 154 166, 144, 166, 172, 169, 177, 172, 161 159, 161, 139, 161, 154, 149, 164, 154 169, 182, 154, 169, 146, 166, 164, 154 166, 177, 156, 149, 161, 149, 169, 156 151, 182, 174, 169, 164, 161, 151, 164 172, 174, 185, 159, 166, 180, 139, 164 177, 161, 202, 193, 199, 207, 213, 204 210, 193, 199, 202, 190, 166, 185, 202 159, 199, 193, 177, 207, 196, 196, 169 169, 199, 193, 188, 213, 174, 207, 193 180, 193, 182, 193, 177, 196, 190, 196 177, 193, 199, 144, 185, 190, 188, 180 199, 182, 174, 146, 156, 185, 174, 154 188, 180, 172, 174, 185, 137, 159, 164 166, 188, 159, 185, 130, 169, 142, 161 159, 182, 193, 169, 185, 185, 185, 188 169, 182, 164, 180, 174, 199, 188, 154 161, 164, 182, 188, 166, 159, 204, 196 188, 182, 193, 193, 193, 207, 240, 266 222, 234, 228, 213, 185, 188, 207, 190 177, 182, 520, 169, 154, 161, 164, 164 169, 161, 139, 156, 188, 164, 142, 137 146, 144, 151, 154, 149, 166, 164, 137 159, 130, 144, 164, 154, 142, 135, 128 137, 139, 137, 137, 137, 142, 125, 135 144, 121, 128, 130, 142, 137, 144, 128 142, 144, 137, 154, 169, 139, 169, 137 159, 144, 180, 151, 135, 146, 130, 142 137, 142, 137, 130, 130, 149, 156, 146 164, 137, 164, 123, 149, 128, 144, 130 139, 130, 137, 135, 151, 159, 130, 154 144, 161, 154, 156, 151, 144, 149, 146 144, 151, 159, 137, 135, 149, 149, 154 154, 151, 174, 151, 149, 154, 169, 161 149, 144, 164, 142, 177, 146, 172, 180 156, 172, 151, 161, 149, 169, 151, 188 225, 210, 185, 207, 196, 174, 196, 185 182, 180, 193, 188, 196, 182, 182, 196 207, 177, 174, 204, 210, 213, 231, 228 219, 225, 222, 216, 219, 182, 219, 202 222, 199, 234, 185, 190, 199, 204, 177 180, 174, 190, 164, 188, 169, 177, 174 159, 169, 159, 185, 177, 166, 169, 174 207, 180, 199, 182, 169, 159, 188, 161 169, 161, 169, 151, 151, 156, 164, 177 149, 180, 159, 161, 154, 139, 151, 135 156, 144, 149, 151, 159, 144, 132, 144 149, 177, 149, 139, 166, 182, 142, 161 159, 180, 199, 185, 164, 213, 225, 253 231, 231, 219, 219, 210, 196, 182, 213 177, 166, 172, 202, 149, 151, 169, 169 161, 144, 149, 142, 144, 149, 130, 159 128, 137, 135, 135, 142, 166, 139, 132 125, 135, 121, 169, 142, 146, 132, 139 159, 159, 149, 161, 144, 144, 132, 146 159, 151, 149, 146, 144, 177, 149, 174 151, 172, 169, 144, 144, 190, 151, 151 161, 149, 144, 137, 174, 144, 139, 114 149, 139, 149, 121, 132, 125, 130, 135 128, 130, 114, 123, 130, 130, 121, 130 117, 139, 121, 149, 149, 130, 149, 119 161, 130, 154, 135, 121, 151, 132, 123 104, 123, 130, 130, 137, 123, 102, 128 135, 139, 110, 137, 119, 121, 110, 132 137, 114, 117, 139, 137, 112, 139, 128 121, 130, 110, 137, 121, 119, 123, 119 125, 135, 142, 123, 154, 151, 190, 166 193, 199, 196, 164, 182, 196, 161, 151 161, 154, 135, 128, 125, 128, 117, 110 137, 123, 125, 130, 92, 132, 139, 125 130, 139, 121, 142, 130, 139, 112, 149 130, 112, 121, 149, 123, 130, 139, 149 156, 137, 161, 172, 156, 164, 185, 207 174, 154, 151, 149, 151, 114, 132, 139 125, 114, 142, 128, 102, 110, 94, 112 117, 112, 117, 132, 130, 146, 112, 112 130, 125, 144, 142, 137, 128, 123, 135 125, 144, 146, 121, 139, 106, 128, 139 149, 125, 151, 137, 130, 128, 130, 125 132, 112, 123, 132, 114, 112, 137, 137 123, 114, 119, 132, 139, 137, 123, 128 132, 125, 144, 121, 151, 177, 139, 144 149, 114, 130, 128, 135, 142, 125, 125 149, 142, 128, 144, 146, 135, 139, 135 128, 121, 125, 154, 125, 142, 146, 137 169, 169, 172, 174, 154, 169, 199, 188 216, 196, 182, 190, 166, 156, 169, 169 161, 142, 137, 125, 121, 130, 142, 121 139, 137, 139, 130, 130, 125, 144, 117 135, 151, 123, 137, 130, 121, 137, 137 128, 130, 128, 121, 135, 130, 123, 137 137, 151, 137, 130, 142, 135, 137, 121 142, 137, 132, 130, 132, 137, 159, 128 114, 121, 132, 117, 149, 130, 123, 121 117, 144, 121, 132, 119, 128, 121, 149 132, 128, 146, 142, 144, 125, 154, 128 154, 161, 135, 125, 139, 151, 132, 142 121, 130, 128, 121, 156, 144, 132, 144 149, 114, 144, 132, 137, 159, 146, 154 149, 164, 159, 172, 180, 202, 185, 182 199, 177, 169, 166, 172, 172, 154, 130 161, 128, 142, 142, 137, 161, 149, 137 137, 117, 142, 154, 125, 144, 154, 166 135, 177, 169, 174, 177, 174, 180, 193 182, 210, 222, 188, 216, 210, 240, 234 213, 199, 182, 213, 177, 180, 172, 146 154, 169, 166, 149, 172, 151, 177, 182 177, 174, 161, 174, 144, 149, 123, 156 161, 114, 137, 110, 117, 139, 114, 144 128, 137, 139, 125, 100, 144, 121, 112 123, 128, 110, 121, 121, 110, 117, 119 112, 112, 102, 119, 117, 114, 112, 108 98, 110, 121, 125, 125, 117, 108, 132 135, 123, 119, 108, 121, 110, 121, 119 123, 125, 104, 119, 98, 114, 125, 110 130, 123, 110, 112, 112, 119, 112, 125 121, 128, 86, 112, 114, 132, 98, 117 125, 112, 123, 110, 114, 114, 106, 112 110, 117, 123, 110, 125, 114, 112, 112 112, 135, 121, 114, 132, 108, 119, 132 104, 128, 121, 108, 114, 117, 123, 132 137, 128, 119, 125, 123, 121, 112, 144 121, 121, 123, 130, 135, 110, 139, 110 112, 159, 135, 112, 121, 112, 137, 123 102, 117, 125, 135, 119, 117, 110, 119 125, 96, 114, 159, 117, 106, 98, 104 117, 146, 102, 106, 108, 96, 117, 144 132, 94, 119, 121, 121, 102, 135, 130 104, 100, 142, 132, 130, 106, 108, 114 108, 130, 121, 117, 125, 130, 132, 121 112, 121, 121, 106, 121, 132, 132, 135 137, 156, 121, 125, 142, 137, 130, 125 144, 132, 128, 142, 139, 132, 135, 151 137, 125, 172, 196, 207, 188, 185, 199 199, 219, 219, 222, 204, 202, 180, 169 146, 159, 146, 151, 151, 185, 196, 193 149, 130, 149, 166, 182, 180, 144, 146 149, 146, 144, 123, 156, 130, 135, 123 128, 137, 119, 128, 114, 125, 142, 117 121, 108, 106, 121, 121, 119, 100, 117 125, 132, 137, 123, 119, 132, 142, 108 108, 128, 123, 110, 112, 130, 123, 121 106, 139, 114, 112, 123, 108, 128, 121 102, 130, 114, 121, 121, 108, 123, 132 117, 106, 106, 121, 110, 104, 92, 125 102, 106, 119, 110, 119, 112, 114, 106 123, 110, 125, 125, 123, 102, 130, 135 119, 132, 125, 119, 149, 110, 121, 119 117, 112, 135, 121, 112, 139, 130, 128 117, 142, 137, 144, 117, 114, 132, 121 142, 104, 104, 139, 112, 117, 117, 128 144, 132, 117, 123, 125, 108, 125, 130 128, 121, 132, 130, 123, 132, 123, 121 125, 130, 135, 132, 144, 139, 130, 121 144, 135, 128, 146, 130, 123, 137, 144 117, 114, 132, 135, 119, 132, 121, 128 137, 128, 154, 132, 164, 149, 137, 146 154, 149, 139, 123, 149, 123, 151, 137 154, 149, 125, 137, 135, 132, 125, 123 137, 117, 146, 121, 144, 128, 119, 151 125, 144, 135, 139, 156, 142, 154, 130 164, 161, 154, 169, 130, 135, 149, 144 139, 125, 159, 130, 137, 132, 156, 144 159, 142, 166, 156, 169, 146, 188, 156 164, 172, 164, 159, 154, 174, 154, 142 154, 137, 128, 156, 161, 161, 154, 151 146, 144, 154, 154, 146, 156, 166, 159 149, 166, 146, 185, 149, 151, 149, 174 135, 142, 137, 142, 142, 146, 128, 132 146, 135, 159, 161, 164, 154, 154, 137 164, 151, 144, 166, 149, 132, 151, 154 172, 154, 125, 151, 135, 146, 146, 117 137, 137, 130, 151, 151, 164, 135, 142 144, 121, 142, 137, 144, 154, 146, 146 139, 149, 139, 156, 144, 144, 137, 151 151, 142, 149, 135, 149, 164, 130, 130 154, 128, 121, 119, 151, 142, 137, 142 146, 123, 119, 151, 125, 132, 146, 146 144, 137, 132, 121, 154, 137, 119, 137 144, 139, 144, 137, 144, 135, 125, 108 156, 121, 130, 125, 146, 128, 159, 151 125, 130, 142, 117, 130, 117, 130, 144 154, 130, 132, 130, 128, 139, 149, 137 117, 119, 132, 137, 125, 159, 130, 146 146, 135, 119, 132, 132, 117, 128, 130 128, 139, 142, 130, 146, 130, 137, 135 130, 125, 149, 142, 149, 144, 142, 135 123, 130, 146, 149, 132, 123, 149, 128 177, 149, 142, 154, 144, 139, 151, 154 132, 130, 146, 149, 121, 151, 137, 119 128, 151, 151, 139, 146, 156, 137, 156 144, 159, 149, 154, 142, 166, 164, 154 154, 151, 135, 149, 135, 146, 139, 137 161, 161, 159, 156, 166, 159, 164, 159 142, 166, 164, 177, 166, 166, 193, 222 196, 216, 234, 213, 240, 262, 240, 204 219, 188, 204, 199, 193, 196, 185, 164 161, 169, 159, 154, 174, 151, 137, 180 159, 132, 135, 144, 154, 166, 154, 146 166, 146, 154, 130, 154, 139, 142, 151 159, 149, 137, 156, 139, 154, 169, 159 164, 146, 144, 161, 151, 156, 156, 149 156, 161, 161, 156, 182, 174, 166, 151 164, 154, 202, 169, 169, 172, 161, 174 161, 169, 164, 172, 180, 151, 182, 202 174, 169, 196, 164, 188, 169, 177, 185 207, 164, 193, 174, 202, 172, 174, 193 161, 177, 182, 172, 156, 164, 172, 174 177, 164, 180, 154, 149, 166, 177, 164 146, 159, 185, 146, 172, 196, 149, 149 159, 159, 164, 172, 154, 169, 169, 180 174, 169, 154, 180, 151, 142, 130, 149 172, 169, 161, 177, 174, 128, 161, 142 151, 151, 130, 144, 146, 137, 137, 144 151, 142, 135, 137, 161, 149, 125, 151 121, 114, 128, 137, 139, 123, 144, 142 169, 149, 142, 159, 159, 164, 137, 161 151, 132, 169, 151, 146, 149, 139, 137 154, 149, 144, 159, 149, 164, 137, 154 177, 151, 154, 177, 169, 161, 169, 154 149, 177, 146, 149, 177, 142, 161, 174 144, 159, 166, 151, 180, 159, 161, 151 144, 164, 149, 159, 188, 151, 132, 149 137, 146, 144, 130, 142, 121, 128, 130 154, 130, 146, 149, 135, 164, 154, 154 132, 149, 159, 132, 132, 151, 144, 130 142, 142, 154, 151, 149, 169, 144, 159 151, 174, 174, 169, 177, 164, 169, 151 149, 154, 144, 159, 174, 169, 146, 164 149, 159, 137, 161, 172, 137, 164, 151 161, 169, 169, 182, 151, 154, 125, 137 144, 132, 142, 161, 159, 156, 149, 142 154, 169, 135, 139, 166, 149, 144, 130 137, 142, 144, 149, 172, 154, 151, 146 151, 142, 128, 159, 144, 146, 164, 142 144, 182, 177, 151, 172, 202, 196, 219 202, 196, 182, 207, 196, 174, 166, 177 159, 185, 188, 166, 164, 182, 132, 139 154, 135, 130, 135, 159, 166, 132, 144 149, 146, 137, 137, 142, 149, 151, 144 130, 149, 151, 149, 135, 144, 149, 161 142, 159, 146, 142, 149, 142, 144, 132 156, 156, 144, 161, 159, 149, 159, 135 146, 137, 188, 172, 164, 185, 177, 193 193, 182, 219, 213, 196, 210, 188, 159 180, 207, 174, 159, 190, 169, 190, 177 185, 202, 188, 219, 193, 225, 234, 246 237, 276, 237, 202, 199, 225, 222, 216 225, 231, 202, 193, 161, 185, 154, 174 159, 159, 166, 144, 151, 130, 121, 132 128, 139, 125, 149, 142, 137, 135, 123 144, 146, 174, 149, 166, 139, 135, 144 164, 149, 139, 125, 151, 144, 156, 164 142, 144, 130, 130, 146, 156, 142, 151 142, 161, 177, 142, 137, 139, 166, 149 164, 185, 151, 137, 156, 151, 149, 146 149, 166, 144, 174, 144, 144, 149, 169 149, 149, 159, 149, 144, 144, 146, 149 156, 130, 166, 161, 146, 144, 135,/