SampleIdent,907A-7-2/23,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 9-aug-1993 16:15,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 106, 92, 96, 88, 85, 104, 100, 96 83, 96, 102, 96, 85, 104, 104, 123 106, 100, 110, 79, 85, 100, 94, 83 94, 88, 108, 96, 92, 94, 94, 98 85, 86, 104, 98, 98, 121, 108, 94 92, 100, 106, 104, 92, 98, 108, 114 96, 108, 108, 114, 121, 94, 112, 106 104, 106, 112, 108, 114, 119, 130, 128 100, 117, 102, 121, 117, 125, 106, 108 104, 114, 114, 112, 125, 98, 130, 123 114, 125, 96, 104, 110, 117, 112, 108 114, 106, 123, 123, 108, 121, 119, 125 106, 117, 125, 114, 112, 123, 104, 114 125, 106, 121, 114, 104, 110, 137, 125 110, 123, 100, 104, 128, 128, 104, 156 108, 121, 125, 100, 106, 112, 106, 98 132, 98, 94, 108, 104, 106, 96, 106 121, 98, 96, 102, 119, 125, 108, 94 104, 88, 114, 96, 96, 100, 88, 132 100, 104, 121, 100, 88, 119, 100, 135 86, 112, 114, 106, 108, 110, 98, 106 106, 94, 110, 121, 112, 110, 112, 110 92, 110, 112, 104, 108, 117, 94, 102 110, 117, 104, 96, 135, 98, 112, 100 112, 110, 110, 114, 94, 92, 100, 114 76, 108, 92, 96, 106, 110, 125, 90 106, 86, 86, 90, 104, 106, 72, 79 72, 98, 88, 90, 100, 94, 90, 92 96, 112, 110, 88, 94, 83, 96, 110 94, 92, 100, 98, 90, 96, 92, 92 100, 86, 94, 94, 96, 92, 90, 88 98, 96, 110, 94, 106, 98, 83, 96 94, 92, 76, 100, 94, 79, 108, 86 85, 92, 106, 102, 92, 94, 92, 81 96, 86, 94, 94, 92, 92, 88, 119 94, 94, 88, 88, 112, 94, 94, 94 90, 77, 94, 94, 94, 94, 94, 106 85, 92, 92, 90, 98, 86, 86, 94 85, 96, 72, 96, 98, 90, 92, 92 83, 100, 94, 98, 94, 92, 92, 81 90, 79, 76, 88, 90, 94, 86, 92 92, 92, 83, 90, 100, 86, 85, 94 88, 90, 94, 79, 100, 71, 92, 81 72, 100, 88, 94, 83, 79, 90, 96 98, 96, 102, 110, 102, 96, 98, 88 76, 102, 102, 96, 98, 104, 114, 114 112, 94, 110, 102, 102, 104, 94, 130 104, 112, 112, 94, 90, 83, 100, 94 92, 88, 88, 92, 96, 81, 56, 86 92, 76, 77, 88, 86, 90, 86, 86 81, 76, 83, 83, 100, 77, 83, 56 94, 85, 74, 98, 83, 79, 96, 66 85, 102, 94, 74, 72, 90, 79, 81 90, 79, 86, 72, 88, 83, 77, 90 85, 94, 90, 76, 77, 83, 72, 79 83, 74, 74, 96, 77, 83, 77, 90 79, 79, 94, 86, 85, 79, 62, 79 71, 86, 76, 72, 96, 88, 81, 72 76, 85, 71, 77, 77, 67, 83, 79 90, 86, 76, 71, 71, 86, 67, 77 85, 72, 77, 56, 67, 76, 98, 76 86, 76, 98, 69, 76, 83, 100, 72 76, 100, 76, 62, 59, 74, 62, 79 79, 79, 67, 86, 72, 71, 72, 67 83, 88, 72, 62, 79, 62, 76, 74 72, 71, 83, 83, 90, 81, 83, 76 69, 90, 71, 76, 76, 72, 76, 79 79, 71, 77, 83, 85, 81, 72, 114 85, 76, 62, 85, 79, 86, 90, 81 79, 85, 77, 66, 74, 72, 81, 79 77, 62, 88, 83, 62, 69, 74, 66 62, 83, 85, 67, 71, 74, 79, 72 88, 100, 79, 86, 90, 90, 72, 85 79, 83, 72, 94, 76, 66, 81, 62 86, 72, 86, 71, 90, 98, 76, 85 76, 76, 81, 85, 86, 83, 79, 86 79, 76, 79, 71, 64, 79, 66, 90 81, 81, 76, 81, 88, 72, 66, 81 79, 66, 77, 71, 88, 79, 85, 88 90, 71, 98, 77, 88, 106, 108, 92 86, 98, 102, 79, 67, 90, 85, 83 77, 76, 86, 90, 83, 90, 71, 85 90, 67, 67, 92, 76, 76, 69, 94 71, 100, 85, 86, 90, 88, 86, 76 86, 79, 71, 76, 69, 76, 76, 77 83, 67, 88, 98, 83, 79, 98, 102 86, 90, 88, 90, 98, 86, 86, 96 90, 90, 85, 86, 88, 92, 72, 94 85, 88, 85, 100, 90, 100, 104, 346 102, 102, 96, 112, 114, 121, 123, 96 98, 121, 125, 121, 132, 130, 139, 130 146, 125, 156, 125, 151, 156, 182, 161 151, 151, 193, 177, 193, 190, 151, 169 188, 172, 159, 159, 156, 161, 139, 144 146, 144, 169, 146, 149, 172, 159, 149 128, 161, 137, 137, 119, 121, 130, 132 114, 121, 137, 128, 132, 130, 128, 128 137, 135, 123, 135, 144, 130, 139, 151 174, 182, 166, 169, 207, 243, 228, 210 213, 225, 207, 210, 231, 222, 240, 188 154, 169, 177, 142, 130, 121, 139, 125 128, 108, 135, 112, 108, 108, 135, 139 125, 108, 106, 104, 128, 121, 110, 106 121, 137, 110, 137, 100, 110, 108, 110 139, 104, 123, 132, 110, 119, 123, 106 121, 128, 117, 130, 121, 146, 144, 121 132, 144, 144, 128, 174, 156, 135, 139 142, 121, 137, 128, 142, 130, 108, 112 104, 106, 114, 102, 100, 112, 125, 114 121, 112, 98, 98, 137, 121, 119, 117 108, 117, 94, 94, 112, 119, 108, 98 117, 119, 130, 117, 119, 117, 130, 130 114, 128, 123, 121, 130, 130, 106, 139 92, 121, 121, 106, 119, 96, 128, 119 114, 135, 100, 106, 112, 112, 106, 121 119, 123, 108, 137, 121, 132, 139, 137 164, 177, 146, 151, 146, 164, 149, 146 139, 156, 130, 130, 130, 135, 146, 159 110, 144, 132, 128, 146, 114, 135, 144 130, 119, 137, 125, 144, 151, 130, 151 137, 149, 142, 156, 137, 144, 139, 132 135, 139, 146, 149, 132, 146, 137, 130 151, 132, 137, 146, 132, 142, 114, 119 121, 135, 149, 108, 130, 121, 125, 119 112, 119, 121, 137, 132, 149, 139, 137 132, 149, 137, 130, 128, 149, 114, 174 139, 130, 135, 146, 166, 146, 159, 151 149, 151, 139, 125, 144, 128, 159, 146 164, 154, 151, 169, 139, 144, 149, 137 128, 144, 154, 166, 219, 196, 172, 159 161, 154, 149, 114, 128, 139, 151, 151 151, 149, 132, 135, 130, 135, 128, 144 137, 130, 146, 137, 139, 117, 137, 144 149, 161, 180, 177, 216, 243, 266, 240 282, 335, 376, 384, 441, 424, 538, 543 635, 681, 745, 888, 767, 824, 1063, 1096 1063, 894, 729, 625, 471, 289, 276, 237 204, 216, 193, 177, 188, 172, 177, 149 169, 169, 154, 166, 161, 161, 182, 159 174, 172, 207, 185, 196, 193, 228, 213 222, 219, 240, 207, 243, 237, 207, 219 250, 228, 225, 228, 213, 246, 246, 240 246, 269, 282, 306, 296, 324, 296, 335 279, 299, 292, 256, 292, 282, 303, 289 292, 276, 256, 228, 225, 243, 196, 177 174, 188, 174, 164, 182, 164, 146, 166 149, 196, 154, 154, 144, 169, 149, 121 130, 146, 119, 132, 130, 130, 125, 128 114, 119, 114, 121, 132, 106, 128, 114 123, 130, 142, 123, 114, 128, 130, 112 135, 135, 110, 137, 149, 125, 135, 128 135, 149, 102, 139, 110, 137, 110, 112 117, 125, 123, 139, 114, 123, 142, 142 144, 137, 156, 132, 146, 149, 132, 146 149, 146, 144, 161, 151, 174, 172, 190 151, 169, 174, 202, 199, 188, 182, 188 151, 174, 169, 164, 130, 149, 132, 144 172, 137, 159, 149, 146, 164, 151, 164 164, 156, 154, 193, 172, 196, 159, 172 185, 154, 151, 149, 149, 166, 144, 135 121, 128, 139, 121, 154, 130, 151, 144 166, 193, 282, 471, 870, 1024, 756, 515 610, 557, 441, 269, 164, 169, 144, 132 128, 121, 123, 128, 137, 117, 154, 102 112, 125, 132, 146, 112, 144, 119, 123 128, 142, 154, 146, 172, 169, 207, 216 259, 272, 279, 372, 372, 433, 524, 534 581, 650, 756, 795, 894, 812, 853, 718 600, 497, 396, 324, 243, 177, 142, 125 112, 139, 123, 121, 119, 98, 121, 98 110, 119, 112, 98, 106, 121, 106, 108 121, 112, 110, 123, 110, 272, 96, 94 117, 98, 100, 108, 92, 98, 98, 88 88, 90, 106, 76, 102, 98, 98, 94 94, 77, 98, 92, 108, 108, 104, 94 94, 98, 102, 98, 98, 121, 98, 102 117, 128, 132, 121, 125, 112, 114, 100 121, 96, 117, 90, 98, 90, 112, 112 106, 106, 117, 88, 79, 94, 94, 106 96, 98, 112, 104, 114, 94, 112, 104 121, 114, 121, 114, 112, 119, 104, 128 88, 125, 106, 119, 130, 121, 123, 128 151, 130, 144, 139, 142, 121, 149, 144 128, 161, 142, 174, 159, 161, 149, 137 166, 182, 161, 174, 193, 185, 159, 182 190, 182, 213, 185, 202, 231, 202, 213 234, 207, 216, 228, 253, 234, 246, 243 216, 246, 250, 269, 272, 259, 272, 262 266, 262, 246, 262, 222, 231, 243, 204 196, 213, 169, 185, 207, 228, 213, 193 185, 199, 185, 193, 188, 182, 182, 190 182, 177, 196, 237, 219, 207, 210, 204 216, 182, 166, 135, 180, 180, 144, 161 161, 154, 159, 149, 156, 149, 159, 166 123, 112, 144, 139, 130, 121, 130, 151 146, 142, 130, 137, 132, 164, 117, 142 139, 135, 185, 166, 182, 185, 180, 210 190, 196, 210, 193, 228, 246, 228, 213 207, 199, 180, 188, 180, 188, 149, 156 169, 154, 151, 154, 123, 151, 144, 154 156, 166, 144, 144, 146, 151, 149, 172 137, 137, 146, 130, 112, 144, 159, 159 142, 132, 144, 154, 132, 130, 137, 164 156, 137, 159, 144, 156, 166, 164, 161 156, 154, 151, 144, 142, 154, 177, 161 146, 144, 151, 132, 139, 137, 135, 139 119, 169, 114, 125, 132, 130, 149, 112 106, 128, 110, 110, 132, 123, 144, 125 135, 137, 128, 144, 139, 132, 146, 102 123, 137, 119, 106, 112, 108, 125, 130 96, 125, 121, 112, 92, 110, 142, 98 112, 114, 114, 88, 92, 104, 98, 114 121, 102, 92, 114, 94, 104, 110, 114 104, 102, 104, 114, 112, 106, 121, 106 130, 117, 128, 128, 137, 123, 128, 132 172, 149, 149, 161, 151, 174, 177, 193 185, 161, 149, 142, 149, 137, 151, 144 121, 110, 119, 117, 108, 104, 128, 119 108, 128, 110, 112, 117, 112, 121, 121 139, 114, 130, 117, 110, 139, 104, 128 135, 119, 156, 137, 156, 151, 130, 177 142, 142, 114, 146, 139, 132, 110, 142 106, 132, 117, 123, 135, 130, 125, 110 119, 121, 98, 112, 123, 137, 110, 117 114, 119, 130, 117, 119, 114, 98, 92 104, 104, 114, 128, 112, 117, 125, 106 114, 104, 125, 123, 119, 108, 119, 114 117, 123, 146, 119, 106, 106, 130, 106 123, 114, 100, 117, 110, 121, 100, 139 123, 112, 123, 112, 119, 146, 132, 125 117, 130, 130, 137, 130, 121, 123, 130 121, 106, 121, 86, 135, 121, 142, 412 139, 128, 123, 130, 149, 121, 128, 159 164, 154, 132, 146, 172, 185, 169, 156 190, 182, 174, 180, 204, 193, 177, 159 159, 156, 144, 151, 123, 128, 137, 121 137, 128, 102, 108, 112, 114, 108, 121 121, 112, 114, 132, 110, 108, 112, 96 119, 106, 96, 98, 96, 121, 92, 119 106, 104, 98, 104, 106, 104, 110, 104 92, 121, 106, 110, 117, 96, 104, 88 114, 110, 110, 117, 108, 88, 94, 92 121, 108, 102, 83, 128, 92, 128, 110 123, 108, 132, 125, 135, 142, 117, 123 119, 119, 119, 121, 108, 130, 104, 104 106, 119, 92, 102, 121, 102, 110, 104 125, 88, 114, 123, 123, 149, 142, 156 196, 196, 161, 159, 180, 188, 151, 166 132, 130, 121, 130, 135, 98, 132, 121 106, 123, 106, 112, 104, 90, 102, 128 130, 117, 96, 132, 123, 130, 132, 128 110, 135, 156, 149, 154, 166, 190, 237 246, 276, 279, 299, 357, 346, 357, 372 428, 408, 458, 454, 412, 353, 357, 320 303, 286, 243, 222, 213, 161, 154, 161 137, 151, 144, 137, 154, 144, 159, 123 135, 121, 106, 135, 110, 121, 102, 128 90, 117, 86, 86, 98, 85, 88, 94 83, 96, 100, 100, 92, 96, 92, 90 96, 86, 110, 79, 88, 96, 85, 88 92, 85, 104, 92, 90, 110, 79, 85 90, 85, 110, 88, 72, 77, 94, 72 92, 112, 96, 72, 79, 90, 72, 85 85, 88, 76, 85, 88, 88, 74, 92 100, 77, 88, 94, 90, 79, 77, 83 71, 74, 86, 76, 88, 77, 74, 83 76, 71, 94, 69, 76, 79, 79, 79 85, 86, 81, 72, 76, 74, 125, 98 100, 74, 106, 104, 98, 96, 102, 102 106, 94, 92, 83, 100, 96, 98, 98 369, 100, 90, 86, 96, 98, 85, 106 76, 110, 83, 86, 90, 110, 83, 94 88, 85, 98, 83, 86, 79, 81, 67 76, 90, 86, 86, 77, 77, 90, 86 81, 66, 81, 76, 85, 76, 71, 90 90, 83, 77, 98, 86, 62, 83, 85 86, 94, 106, 94, 83, 102, 96, 98 94, 92, 104, 79, 85, 79, 94, 92 104, 79, 79, 110, 110, 83, 66, 86 86, 112, 94, 100, 98, 86, 102, 108 90, 92, 114, 117, 117, 112, 110, 123 121, 125, 164, 182, 177, 188, 190, 190 219, 193, 190, 231, 204, 253, 199, 193 190, 188, 151, 151, 130, 106, 130, 106 112, 96, 102, 92, 98, 100, 114, 79 102, 92, 72, 92, 108, 86, 119, 114 121, 98, 114, 104, 92, 96, 100, 114 102, 98, 98, 94, 110, 98, 83, 108 96, 92, 100, 90, 119, 77, 88, 104 94, 92, 104, 104, 100, 88, 85, 94 86, 112, 104, 112, 81, 96, 83, 94 96, 86, 90, 88, 88, 76, 94, 62 72, 88, 77, 66, 71, 74, 77, 77 77, 66, 67, 83, 102, 79, 83, 79 90, 81, 83, 76, 86, 94, 88, 83 83, 102, 88, 88, 94, 86, 98, 71 94, 98, 76, 98, 100, 92, 88, 94 92, 96, 119, 94, 92, 86, 94, 85 85, 90, 100, 76, 90, 98, 94, 94 90, 112, 81, 86, 100, 90, 94, 92 102, 90, 102, 98, 121, 104, 123, 110 88, 102, 81, 96, 108, 112, 125, 117 112, 112, 117, 112, 106, 102, 92, 98 94, 125, 100, 96, 104, 104, 108, 106 108, 130, 112, 104, 108, 154, 117, 114 121, 121, 123, 119, 112, 132, 146, 130 149, 137, 114, 132, 121, 132, 119, 117 112, 121, 110, 121, 123, 119, 117, 123 125, 119, 125, 146, 121, 130, 119, 125 125, 92, 123, 114, 108, 130, 110, 117 130, 104, 137, 137, 135, 135, 142, 156 137, 144, 151, 151, 164, 166, 159, 196 182, 180, 190, 172, 161, 144, 154, 159 164, 169, 142, 139, 154, 139, 139, 156 146, 130, 137, 154, 137, 123, 161, 149 149, 144, 130, 142, 125, 149, 119, 139 108, 137, 135, 142, 128, 132, 137, 119 125, 106, 151, 110, 94, 128, 135, 132 137, 128, 121, 110, 121, 128, 98, 108 121, 117, 121, 132, 135, 132, 119, 121 123, 128, 130, 137, 135, 139, 139, 182 166, 210, 174, 161, 199, 199, 210, 222 262, 228, 246, 216, 193, 180, 174, 185 213, 188, 169, 154, 156, 139, 132, 112 121, 137, 92, 110, 132, 108, 108, 96 121, 106, 104, 108, 100, 110, 110, 110 94, 102, 100, 88, 100, 85, 108, 92 108, 106, 110, 92, 102, 117, 104, 90 117, 104, 106, 106, 96, 102, 98, 104 90, 102, 90, 98, 106, 110, 102, 106 100, 104, 110, 96, 96, 98, 104, 96 104, 77, 100, 106, 112, 83, 94, 110 102, 81, 98, 106, 96, 104, 98, 83 98, 102, 117, 96, 76, 94, 102, 108 104, 94, 96, 102, 96, 88, 102, 98 88, 86, 110, 117, 83, 112, 104, 121 106, 98, 108, 121, 106, 100, 104, 123 92, 88, 106, 86, 123, 98, 98, 92 117, 114, 94, 98, 112, 121, 104, 108 90, 121, 110, 110, 106, 100, 106, 94 102, 128, 102, 100, 117, 123, 112, 100 121, 102, 102, 125, 110, 139, 125, 130 125, 114, 149, 159, 164, 154, 177, 174 210, 219, 219, 225, 213, 237, 243, 228 256, 237, 259, 219, 210, 196, 182, 185 185, 164, 180, 146, 132, 132, 151, 137 144, 121, 161, 125, 110, 119, 96, 149 149, 130, 125, 114, 121, 137, 130, 137 149, 110, 149, 121, 128, 130, 114, 161 128, 146, 130, 137, 142, 125, 125, 151 132, 146, 135, 159, 135, 169, 154, 159 154, 144, 154, 174, 182, 166, 169, 169 185, 169, 149, 199, 213, 172, 169, 180 190, 199, 196, 207, 213, 185, 204, 174 174, 190, 185, 204, 219, 202, 185, 196 207, 199, 193, 207, 210, 207, 196, 174 193, 199, 169, 174, 159, 169, 172, 142 169, 144, 161, 177, 144, 166, 142, 154 164, 139, 156, 159, 144, 144, 146, 130 137, 164, 130, 121, 144, 139, 139, 119 137, 121, 128, 128, 137, 123, 119, 100 110, 123, 114, 92, 121, 106, 121, 121 125, 117, 114, 117, 104, 119, 106, 106 94, 102, 123, 90, 117, 104, 100, 108 85, 96, 119, 102, 90, 114, 90, 114 92, 100, 117, 86, 123, 121, 92, 112 94, 106, 98, 104, 117, 119, 94, 106 110, 102, 102, 128, 102, 114, 132, 119 125, 130, 132, 137, 117, 117, 125, 123 149, 156, 121, 137, 106, 139, 108, 125 108, 123, 102, 112, 125, 125, 114, 108 112, 98, 102, 94, 96, 92, 112, 76 94, 112, 92, 104, 88, 108, 112, 98 77, 83, 83, 104, 106, 85, 108, 90 100, 128, 121, 108, 108, 100, 128, 90 106, 106, 112, 98, 104, 94, 100, 96 90, 86, 92, 100, 104, 96, 121, 106 102, 119, 85, 98, 108, 100, 96, 86 88, 108, 90, 106, 110, 92, 94, 114 98, 117, 104, 85, 108, 121, 114, 94 108, 104, 110, 130, 108, 114, 90, 98 94, 98, 110, 102, 123, 108, 110, 119 112, 135, 121, 132, 139, 151, 121, 169 193, 159, 182, 174, 156, 149, 130, 128 114, 128, 144, 135, 125, 123, 104, 114 100, 96, 102, 102, 94, 90, 81, 102 96, 96, 90, 90, 96, 110, 100, 106 106, 98, 74, 96, 94, 86, 102, 90 96, 86, 94, 102, 100, 83, 90, 102 92, 102, 130, 112, 114, 90, 90, 94 112, 106, 98, 110, 102, 98, 123, 110 119, 125, 130, 117, 154, 144, 144, 154 174, 182, 188, 182, 172, 188, 182, 185 174, 177, 159, 144, 151, 169, 154, 193 161, 185, 169, 199, 188, 188, 219, 222 228, 253, 253, 250, 234, 234, 237, 204 216, 196, 207, 190, 207, 169, 182, 166 144, 149, 130, 130, 96, 135, 119, 119 108, 128, 94, 98, 102, 114, 119, 108 106, 96, 102, 132, 100, 106, 112, 102 119, 102, 96, 104, 100, 100, 98, 106 106, 102, 98, 121, 92, 128, 96, 128 110, 139, 108, 117, 117, 121, 114, 130 130, 146, 106, 132, 119, 132, 117, 119 114, 92, 119, 121, 114, 121, 123, 123 117, 108, 114, 112, 130, 121, 96, 125 128,/