SampleIdent,907A-9-3/25,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 9-aug-1993 18:06,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 92, 96, 90, 117, 114, 102, 96, 102 117, 92, 94, 106, 83, 110, 92, 106 98, 77, 94, 100, 98, 90, 94, 114 86, 121, 90, 94, 110, 88, 86, 102 110, 88, 100, 104, 92, 121, 92, 94 108, 112, 104, 100, 110, 108, 102, 106 125, 117, 112, 114, 128, 94, 104, 112 112, 125, 119, 114, 119, 114, 121, 135 106, 123, 110, 102, 125, 106, 125, 119 104, 125, 106, 130, 110, 121, 92, 96 123, 106, 119, 119, 119, 117, 130, 132 132, 121, 135, 151, 130, 137, 117, 130 125, 123, 117, 117, 139, 135, 125, 121 121, 110, 121, 128, 135, 123, 102, 119 117, 130, 112, 132, 117, 90, 119, 123 121, 154, 94, 139, 117, 102, 125, 128 130, 119, 114, 102, 137, 132, 121, 114 123, 125, 144, 121, 112, 110, 104, 108 130, 130, 117, 117, 121, 108, 96, 121 125, 121, 94, 110, 123, 135, 117, 121 106, 123, 104, 114, 121, 106, 142, 123 112, 110, 135, 98, 108, 100, 98, 98 112, 117, 104, 106, 92, 125, 110, 102 123, 121, 106, 117, 112, 112, 117, 114 121, 102, 100, 106, 114, 104, 119, 112 88, 110, 90, 83, 98, 106, 96, 94 119, 104, 106, 100, 90, 108, 100, 98 100, 94, 96, 88, 106, 121, 79, 92 104, 98, 100, 83, 110, 117, 98, 106 114, 96, 85, 86, 100, 104, 88, 88 92, 94, 85, 94, 104, 100, 86, 94 94, 100, 85, 104, 98, 81, 86, 86 90, 90, 92, 79, 81, 96, 94, 96 96, 100, 92, 81, 100, 90, 104, 98 98, 100, 100, 94, 88, 96, 98, 88 100, 85, 92, 100, 90, 86, 86, 88 106, 100, 88, 98, 85, 102, 96, 98 90, 90, 100, 106, 86, 86, 108, 77 96, 81, 86, 90, 104, 79, 96, 92 72, 92, 77, 96, 83, 106, 104, 106 86, 110, 90, 79, 85, 92, 100, 92 92, 92, 110, 71, 86, 92, 96, 77 92, 85, 86, 64, 86, 86, 94, 94 90, 92, 106, 121, 100, 106, 92, 83 96, 94, 100, 92, 102, 106, 94, 94 96, 90, 100, 137, 94, 104, 114, 79 106, 90, 92, 96, 104, 108, 98, 96 98, 94, 74, 85, 88, 88, 85, 94 88, 71, 100, 81, 85, 90, 81, 76 90, 71, 83, 83, 94, 69, 81, 96 79, 83, 69, 67, 94, 72, 102, 83 79, 83, 77, 76, 85, 72, 85, 86 76, 90, 96, 90, 102, 79, 100, 86 96, 86, 102, 98, 96, 100, 74, 114 88, 86, 90, 86, 92, 98, 83, 85 83, 90, 85, 81, 67, 72, 88, 79 88, 77, 86, 71, 85, 98, 81, 90 85, 96, 77, 92, 76, 92, 92, 88 85, 76, 102, 90, 79, 76, 77, 85 77, 77, 86, 92, 67, 88, 77, 85 77, 79, 86, 100, 96, 74, 85, 71 72, 79, 85, 85, 90, 72, 77, 92 90, 90, 85, 85, 81, 77, 67, 88 83, 83, 94, 92, 88, 69, 77, 83 76, 76, 83, 76, 85, 79, 92, 88 86, 77, 79, 79, 72, 71, 74, 85 71, 102, 85, 102, 88, 76, 92, 79 79, 92, 85, 83, 77, 85, 90, 85 79, 62, 83, 77, 67, 59, 83, 67 83, 88, 72, 79, 79, 90, 76, 77 88, 98, 96, 96, 67, 71, 71, 69 79, 85, 72, 72, 77, 72, 86, 86 85, 85, 85, 90, 77, 69, 72, 86 77, 88, 74, 72, 94, 79, 86, 76 86, 81, 85, 81, 69, 90, 90, 83 74, 67, 83, 92, 85, 71, 86, 81 90, 62, 83, 86, 71, 90, 72, 77 88, 83, 71, 79, 90, 83, 102, 86 90, 83, 83, 85, 74, 88, 88, 79 104, 81, 92, 85, 85, 102, 85, 90 74, 72, 98, 100, 81, 77, 100, 85 71, 83, 90, 94, 71, 72, 108, 90 92, 83, 85, 104, 83, 77, 92, 83 79, 92, 71, 88, 92, 83, 88, 86 83, 77, 74, 81, 92, 104, 92, 100 90, 83, 79, 72, 69, 86, 79, 86 102, 100, 83, 92, 102, 98, 92, 92 88, 106, 86, 86, 94, 72, 96, 106 102, 94, 117, 108, 114, 121, 81, 96 110, 114, 110, 132, 100, 123, 135, 132 132, 137, 132, 137, 161, 159, 154, 146 149, 164, 193, 164, 182, 177, 182, 193 196, 182, 180, 182, 149, 159, 159, 161 151, 202, 174, 151, 164, 169, 139, 156 146, 139, 137, 121, 161, 128, 151, 132 132, 151, 104, 139, 135, 144, 121, 121 106, 121, 139, 125, 144, 149, 146, 154 161, 135, 123, 144, 174, 164, 177, 190 207, 196, 169, 188, 177, 207, 193, 213 185, 202, 199, 190, 210, 190, 188, 166 128, 139, 128, 130, 128, 130, 128, 117 130, 123, 132, 110, 114, 117, 106, 128 102, 121, 94, 130, 139, 114, 135, 130 114, 130, 130, 98, 121, 121, 144, 135 128, 156, 130, 151, 123, 135, 159, 137 154, 144, 161, 164, 177, 169, 188, 185 182, 172, 185, 154, 177, 146, 146, 144 149, 130, 132, 112, 102, 106, 102, 106 125, 112, 114, 121, 112, 128, 108, 117 117, 100, 121, 125, 117, 135, 108, 121 137, 137, 137, 144, 121, 130, 132, 125 132, 130, 130, 135, 117, 135, 125, 139 130, 123, 123, 125, 110, 123, 112, 117 112, 108, 117, 121, 114, 121, 117, 119 130, 121, 149, 112, 149, 142, 125, 137 123, 151, 149, 151, 146, 169, 180, 199 188, 190, 172, 156, 154, 185, 185, 156 149, 164, 166, 130, 137, 135, 135, 135 137, 130, 146, 132, 139, 149, 135, 144 164, 154, 139, 182, 164, 159, 159, 159 149, 164, 146, 139, 149, 164, 166, 142 159, 146, 123, 144, 149, 144, 151, 144 137, 137, 135, 139, 125, 123, 106, 110 104, 117, 135, 119, 144, 119, 123, 137 112, 123, 108, 125, 123, 121, 135, 132 137, 135, 125, 123, 128, 146, 123, 130 139, 123, 132, 135, 135, 123, 146, 151 149, 149, 137, 144, 139, 128, 130, 169 156, 146, 144, 137, 161, 139, 156, 161 130, 149, 139, 144, 139, 130, 117, 146 149, 164, 144, 154, 144, 130, 125, 128 130, 137, 146, 144, 135, 154, 119, 125 139, 172, 142, 161, 151, 130, 135, 174 174, 166, 204, 199, 219, 289, 276, 339 372, 458, 488, 566, 620, 630, 734, 718 718, 630, 595, 620, 605, 502, 400, 365 306, 256, 188, 185, 193, 174, 166, 166 137, 149, 161, 169, 156, 172, 142, 146 159, 146, 142, 172, 169, 164, 166, 199 156, 151, 177, 196, 213, 231, 256, 262 250, 266, 306, 361, 324, 328, 376, 365 365, 353, 392, 441, 515, 475, 493, 511 484, 475, 515, 454, 493, 586, 718, 595 562, 520, 484, 488, 380, 342, 331, 328 282, 266, 225, 193, 234, 169, 207, 207 144, 169, 188, 188, 185, 174, 182, 207 159, 154, 164, 169, 161, 169, 139, 139 132, 142, 146, 149, 132, 121, 114, 121 119, 121, 114, 117, 144, 94, 119, 137 121, 132, 130, 135, 130, 137, 130, 132 123, 142, 132, 104, 114, 123, 108, 125 132, 125, 114, 121, 142, 125, 117, 132 137, 130, 125, 135, 139, 142, 149, 177 169, 151, 188, 188, 243, 219, 225, 262 292, 286, 256, 259, 269, 256, 276, 286 276, 282, 310, 282, 299, 282, 231, 213 202, 159, 166, 151, 161, 159, 154, 164 166, 149, 169, 182, 177, 190, 207, 188 243, 185, 185, 177, 193, 193, 188, 180 174, 182, 166, 182, 161, 188, 185, 139 188, 182, 166, 149, 154, 154, 149, 159 164, 121, 146, 154, 146, 139, 128, 117 121, 108, 108, 94, 110, 92, 114, 114 119, 112, 137, 110, 108, 121, 121, 121 128, 132, 132, 121, 130, 144, 128, 144 144, 156, 154, 169, 193, 266, 299, 296 317, 313, 310, 328, 303, 282, 279, 256 250, 237, 219, 204, 199, 151, 159, 137 128, 114, 112, 130, 119, 119, 110, 96 92, 102, 110, 108, 98, 71, 112, 94 102, 85, 100, 86, 67, 96, 94, 79 100, 79, 98, 98, 88, 100, 104, 96 102, 94, 94, 69, 83, 88, 102, 94 88, 92, 98, 85, 117, 85, 104, 92 98, 85, 112, 98, 102, 112, 112, 112 106, 108, 104, 110, 110, 119, 114, 110 94, 100, 72, 86, 81, 98, 94, 86 96, 90, 90, 83, 92, 96, 92, 88 81, 85, 90, 102, 106, 104, 128, 98 121, 100, 90, 114, 100, 96, 88, 125 100, 102, 90, 104, 104, 86, 112, 119 104, 114, 104, 106, 108, 117, 119, 102 114, 114, 125, 128, 123, 121, 119, 142 130, 137, 132, 146, 144, 177, 154, 144 166, 174, 164, 151, 174, 172, 151, 156 182, 174, 180, 182, 210, 188, 204, 188 228, 222, 222, 246, 228, 259, 282, 253 279, 279, 250, 225, 228, 219, 225, 228 231, 193, 193, 225, 246, 216, 216, 216 240, 250, 210, 253, 234, 222, 210, 228 202, 199, 216, 219, 199, 228, 222, 231 219, 475, 243, 222, 237, 204, 222, 204 199, 190, 199, 193, 196, 185, 185, 156 169, 159, 137, 156, 185, 144, 146, 135 156, 135, 114, 161, 114, 121, 130, 128 110, 119, 137, 125, 139, 125, 123, 132 135, 146, 156, 166, 177, 166, 188, 185 185, 182, 240, 231, 196, 202, 199, 180 146, 177, 151, 119, 144, 128, 112, 137 132, 112, 114, 130, 161, 149, 130, 161 180, 121, 159, 123, 154, 154, 174, 154 149, 142, 151, 132, 149, 137, 123, 123 331, 135, 139, 121, 130, 125, 156, 137 137, 106, 135, 151, 151, 149, 135, 139 161, 154, 151, 164, 166, 132, 144, 159 137, 130, 119, 119, 139, 125, 130, 108 114, 121, 117, 112, 125, 112, 94, 92 128, 100, 112, 102, 121, 112, 110, 121 121, 114, 123, 121, 142, 104, 100, 121 94, 94, 128, 114, 123, 100, 92, 112 96, 100, 98, 86, 102, 100, 104, 104 83, 108, 88, 110, 98, 102, 100, 100 96, 98, 108, 96, 117, 110, 108, 112 106, 98, 108, 100, 121, 112, 121, 92 121, 144, 144, 117, 139, 142, 132, 139 130, 137, 169, 149, 142, 144, 144, 114 128, 110, 137, 130, 117, 125, 121, 119 106, 108, 100, 100, 96, 108, 104, 98 92, 98, 100, 104, 85, 130, 96, 98 108, 104, 108, 108, 110, 100, 100, 108 119, 110, 104, 121, 108, 100, 108, 137 142, 121, 104, 123, 117, 139, 98, 117 108, 112, 108, 128, 142, 114, 106, 132 114, 119, 132, 125, 154, 125, 128, 139 112, 117, 130, 135, 125, 130, 121, 114 108, 98, 119, 100, 108, 112, 104, 119 114, 88, 94, 98, 100, 85, 114, 98 86, 88, 90, 117, 102, 92, 83, 98 104, 100, 104, 94, 117, 86, 90, 106 112, 132, 110, 108, 114, 132, 119, 114 119, 149, 130, 130, 114, 151, 135, 114 130, 132, 161, 130, 142, 164, 164, 174 182, 182, 196, 228, 219, 279, 303, 543 228, 216, 228, 222, 225, 210, 161, 190 172, 177, 182, 204, 182, 159, 166, 128 144, 144, 142, 139, 128, 161, 139, 169 130, 139, 125, 130, 128, 132, 114, 121 110, 114, 119, 117, 102, 106, 125, 114 94, 98, 102, 94, 104, 88, 94, 88 130, 88, 90, 76, 88, 88, 96, 74 85, 83, 85, 86, 77, 98, 77, 108 81, 90, 106, 88, 77, 96, 85, 88 77, 85, 117, 114, 96, 90, 94, 106 96, 117, 114, 384, 137, 123, 128, 106 117, 112, 106, 104, 114, 92, 94, 108 114, 121, 108, 104, 123, 114, 94, 128 119, 151, 154, 144, 137, 161, 151, 144 146, 144, 137, 108, 149, 121, 125, 121 137, 104, 108, 98, 76, 117, 104, 108 106, 117, 92, 100, 202, 96, 104, 100 112, 128, 114, 92, 117, 121, 102, 108 137, 132, 146, 154, 146, 156, 164, 190 185, 193, 210, 202, 225, 207, 202, 222 213, 213, 196, 185, 174, 177, 188, 172 154, 149, 151, 128, 144, 139, 135, 121 146, 137, 114, 128, 125, 117, 108, 114 100, 110, 106, 100, 88, 119, 85, 83 88, 86, 83, 88, 74, 85, 77, 85 72, 92, 92, 96, 83, 96, 77, 88 77, 85, 88, 90, 72, 92, 76, 83 83, 94, 90, 79, 92, 83, 79, 79 76, 90, 72, 83, 100, 74, 66, 71 88, 79, 92, 83, 88, 92, 81, 90 85, 88, 92, 106, 90, 90, 90, 90 96, 77, 92, 94, 85, 100, 92, 88 76, 102, 96, 98, 92, 92, 86, 85 90, 88, 59, 69, 77, 83, 59, 62 74, 67, 74, 85, 71, 74, 86, 74 72, 86, 77, 59, 85, 85, 86, 72 66, 79, 94, 77, 92, 104, 92, 90 94, 92, 83, 121, 102, 96, 102, 94 106, 102, 108, 106, 98, 92, 98, 88 76, 92, 81, 92, 86, 85, 88, 71 77, 77, 77, 85, 77, 76, 88, 77 79, 83, 77, 76, 90, 67, 83, 74 86, 100, 98, 92, 96, 106, 110, 85 94, 85, 96, 94, 100, 94, 102, 121 98, 96, 100, 121, 132, 100, 132, 90 132, 110, 119, 130, 119, 102, 130, 125 114, 119, 102, 121, 114, 128, 104, 96 144, 123, 104, 104, 98, 117, 142, 144 164, 159, 146, 159, 169, 188, 182, 159 166, 172, 174, 169, 169, 161, 137, 123 144, 119, 98, 125, 102, 106, 90, 86 90, 112, 104, 100, 102, 104, 114, 98 110, 88, 106, 117, 125, 114, 92, 100 92, 102, 104, 104, 102, 104, 98, 88 92, 106, 76, 102, 92, 106, 90, 102 66, 76, 83, 98, 96, 100, 88, 100 79, 110, 108, 106, 104, 90, 106, 92 104, 90, 106, 77, 102, 100, 119, 104 83, 96, 100, 92, 98, 96, 96, 88 88, 81, 72, 83, 81, 77, 67, 90 90, 62, 85, 86, 98, 100, 96, 85 102, 121, 100, 119, 104, 100, 121, 114 119, 121, 110, 112, 117, 100, 114, 108 98, 96, 79, 119, 104, 100, 77, 94 86, 85, 96, 108, 98, 86, 90, 119 92, 79, 96, 85, 94, 83, 85, 98 100, 102, 83, 112, 106, 98, 119, 112 98, 94, 110, 121, 137, 121, 114, 137 98, 104, 125, 128, 130, 123, 112, 128 125, 88, 117, 106, 119, 121, 142, 90 104, 117, 90, 119, 112, 119, 121, 106 123, 130, 117, 112, 114, 100, 104, 102 121, 114, 112, 128, 108, 137, 123, 110 130, 102, 121, 114, 135, 117, 130, 130 108, 123, 112, 102, 119, 104, 98, 123 108, 112, 137, 106, 102, 128, 121, 104 110, 117, 110, 128, 104, 112, 121, 119 121, 144, 117, 108, 149, 139, 149, 132 135, 164, 156, 154, 164, 149, 137, 137 166, 154, 137, 125, 139, 139, 142, 119 125, 117, 142, 119, 125, 132, 121, 132 365, 114, 142, 108, 128, 128, 119, 121 130, 121, 130, 121, 125, 121, 132, 114 100, 110, 112, 100, 96, 88, 123, 98 106, 117, 100, 100, 94, 114, 112, 108 121, 117, 114, 130, 104, 135, 112, 159 135, 137, 139, 144, 159, 169, 154, 164 174, 174, 202, 166, 193, 199, 193, 182 188, 225, 190, 193, 182, 182, 190, 166 182, 172, 172, 174, 299, 161, 164, 123 146, 132, 132, 135, 144, 125, 110, 102 119, 119, 104, 125, 121, 114, 132, 119 110, 106, 100, 119, 110, 117, 104, 121 106, 96, 110, 114, 92, 112, 106, 106 106, 100, 114, 90, 121, 94, 123, 92 90, 96, 76, 94, 88, 106, 94, 104 92, 92, 92, 96, 94, 94, 83, 104 90, 98, 85, 71, 88, 100, 92, 92 92, 92, 74, 100, 100, 98, 88, 94 94, 110, 104, 92, 90, 114, 100, 98 81, 104, 100, 114, 104, 92, 81, 98 83, 102, 108, 81, 90, 96, 83, 112 86, 96, 100, 90, 96, 106, 100, 106 98, 83, 88, 90, 104, 90, 119, 110 96, 121, 117, 98, 106, 112, 106, 117 90, 96, 110, 98, 90, 102, 96, 102 117, 108, 104, 110, 119, 106, 96, 104 117, 100, 104, 88, 90, 104, 119, 69 128, 104, 117, 100, 135, 121, 117, 132 125, 132, 166, 135, 146, 177, 177, 166 182, 193, 188, 207, 180, 202, 193, 204 182, 164, 151, 139, 166, 177, 154, 132 121, 117, 123, 121, 128, 112, 119, 104 121, 125, 125, 108, 125, 121, 130, 96 117, 130, 117, 108, 104, 142, 135, 130 121, 110, 123, 130, 125, 130, 142, 119 139, 135, 137, 137, 142, 164, 137, 137 172, 156, 146, 149, 146, 164, 172, 177 164, 193, 151, 169, 196, 177, 159, 172 185, 199, 199, 193, 164, 188, 193, 193 202, 159, 188, 204, 202, 190, 164, 182 174, 180, 174, 196, 172, 188, 161, 161 174, 166, 159, 166, 177, 159, 190, 190 172, 182, 172, 166, 177, 188, 188, 149 166, 174, 159, 169, 144, 151, 144, 174 182, 149, 149, 142, 154, 149, 146, 156 139, 172, 149, 142, 125, 132, 142, 132 130, 154, 144, 137, 121, 125, 121, 130 130, 132, 112, 119, 114, 125, 121, 112 104, 121, 102, 106, 142, 110, 119, 100 92, 104, 100, 83, 117, 100, 106, 90 108, 110, 110, 119, 130, 88, 92, 90 98, 96, 96, 100, 94, 121, 114, 108 90, 104, 98, 112, 108, 102, 130, 100 108, 117, 114, 117, 119, 130, 114, 125 132, 202, 177, 188, 154, 130, 180, 123 135, 137, 156, 142, 128, 119, 117, 137 121, 117, 121, 94, 132, 112, 94, 117 92, 98, 86, 108, 86, 86, 94, 90 92, 76, 81, 79, 72, 94, 92, 100 86, 85, 94, 100, 96, 98, 85, 112 81, 96, 106, 100, 117, 98, 121, 86 110, 96, 112, 79, 112, 108, 98, 86 90, 110, 98, 130, 98, 100, 100, 96 92, 88, 94, 90, 104, 98, 123, 88 112, 98, 117, 125, 123, 92, 104, 96 121, 135, 108, 135, 108, 130, 132, 121 117, 144, 164, 146, 132, 130, 135, 139 164, 128, 154, 139, 144, 108, 132, 142 125, 130, 149, 128, 128, 135, 137, 128 128, 121, 137, 121, 125, 108, 128, 98 112, 106, 110, 106, 119, 106, 104, 108 79, 77, 96, 108, 96, 102, 90, 86 106, 104, 110, 90, 79, 83, 114, 77 86, 79, 123, 98, 102, 112, 112, 88 112, 108, 90, 106, 114, 106, 98, 106 121, 119, 135, 146, 193, 174, 149, 144 112, 104, 125, 121, 142, 125, 156, 154 123, 149, 149, 137, 156, 142, 154, 135 151, 154, 156, 144, 156, 149, 137, 137 146, 144, 142, 125, 137, 154, 161, 156 182, 161, 188, 161, 177, 174, 144, 172 190, 190, 166, 172, 159, 159, 174, 149 146, 159, 142, 117, 135, 130, 137, 139 104, 114, 119, 142, 121, 114, 108, 110 88, 106, 98, 85, 108, 100, 86, 104 108, 119, 94, 119, 119, 119, 108, 90 121, 104, 112, 112, 86, 121, 114, 92 100, 114, 117, 85, 106, 104, 102, 108 119, 117, 151, 130, 119, 130, 121, 149 135, 128, 125, 108, 108, 142, 108, 121 121, 121, 104, 98, 117, 119, 110, 125 114, 104, 108, 130, 100, 92, 94, 110 112,/