SampleIdent,907A-10-3/24,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 9-aug-1993 19:02,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 94, 98, 96, 100, 96, 96, 92, 86 104, 102, 94, 96, 102, 76, 100, 100 79, 106, 85, 85, 110, 96, 94, 88 102, 88, 100, 98, 85, 98, 94, 92 79, 92, 100, 108, 106, 94, 108, 83 117, 119, 92, 98, 104, 88, 102, 106 100, 96, 96, 112, 102, 100, 90, 98 98, 102, 112, 98, 102, 128, 102, 104 106, 110, 112, 88, 110, 96, 123, 108 119, 98, 98, 100, 88, 86, 110, 121 112, 121, 130, 114, 112, 108, 110, 121 112, 121, 106, 100, 108, 108, 139, 144 110, 108, 137, 119, 119, 117, 135, 125 132, 142, 117, 110, 112, 117, 112, 119 90, 110, 110, 112, 108, 104, 119, 108 104, 117, 102, 123, 106, 108, 119, 104 104, 119, 102, 104, 121, 114, 119, 102 100, 114, 117, 112, 125, 117, 88, 121 106, 102, 106, 108, 110, 108, 114, 96 130, 112, 102, 90, 96, 132, 106, 112 128, 98, 121, 114, 110, 119, 100, 90 119, 121, 104, 106, 106, 125, 114, 119 90, 117, 128, 125, 108, 114, 104, 102 114, 121, 135, 121, 106, 123, 110, 108 106, 110, 114, 112, 98, 117, 94, 117 88, 104, 102, 106, 88, 92, 96, 106 81, 79, 100, 106, 92, 94, 85, 86 88, 85, 86, 86, 92, 85, 100, 104 108, 104, 112, 92, 71, 102, 85, 77 121, 100, 85, 100, 86, 90, 98, 96 102, 117, 94, 94, 94, 81, 90, 83 94, 86, 86, 86, 114, 94, 98, 94 71, 92, 88, 92, 83, 74, 104, 92 92, 108, 81, 92, 94, 96, 79, 100 96, 96, 86, 83, 106, 79, 90, 92 86, 96, 92, 92, 102, 88, 88, 92 79, 94, 77, 108, 108, 74, 108, 86 100, 90, 79, 96, 106, 96, 92, 98 90, 85, 92, 94, 94, 83, 88, 96 86, 92, 86, 98, 81, 94, 85, 90 100, 86, 90, 85, 102, 76, 98, 96 81, 98, 102, 92, 96, 98, 100, 106 83, 114, 102, 98, 110, 104, 85, 98 67, 83, 92, 81, 96, 72, 72, 83 92, 92, 110, 90, 94, 98, 90, 90 108, 96, 119, 100, 83, 98, 110, 94 121, 114, 119, 100, 86, 102, 90, 112 112, 108, 92, 77, 114, 90, 98, 83 96, 90, 85, 88, 90, 79, 85, 86 88, 96, 81, 79, 85, 100, 92, 94 100, 76, 79, 108, 86, 79, 85, 86 81, 64, 96, 81, 76, 67, 83, 92 85, 85, 76, 81, 90, 90, 71, 86 88, 96, 92, 83, 92, 86, 85, 98 79, 77, 90, 94, 102, 77, 94, 92 86, 85, 77, 83, 85, 96, 90, 69 79, 79, 77, 71, 83, 66, 86, 76 67, 50, 100, 72, 94, 76, 83, 79 79, 72, 88, 72, 67, 94, 83, 71 79, 71, 83, 86, 71, 74, 79, 76 81, 100, 102, 94, 74, 72, 88, 85 64, 83, 74, 72, 71, 79, 92, 85 85, 71, 90, 77, 98, 90, 74, 72 85, 85, 76, 79, 94, 76, 62, 86 69, 83, 69, 85, 76, 86, 77, 85 86, 72, 83, 86, 90, 79, 85, 90 69, 83, 83, 88, 85, 76, 81, 85 76, 77, 86, 79, 88, 64, 72, 90 86, 85, 83, 71, 76, 96, 67, 86 77, 83, 74, 71, 66, 90, 81, 83 85, 86, 83, 72, 77, 92, 76, 79 85, 66, 74, 67, 77, 77, 86, 67 79, 76, 79, 67, 79, 83, 69, 76 74, 67, 79, 61, 102, 74, 67, 81 92, 66, 90, 79, 66, 100, 85, 69 79, 71, 71, 85, 62, 88, 74, 62 77, 77, 96, 76, 104, 79, 66, 72 88, 98, 77, 81, 66, 85, 85, 102 83, 85, 83, 71, 88, 88, 77, 104 79, 96, 85, 86, 102, 77, 62, 90 90, 77, 76, 85, 104, 98, 90, 86 83, 79, 71, 86, 83, 86, 94, 83 94, 72, 88, 79, 76, 90, 94, 72 71, 98, 83, 88, 88, 88, 72, 83 79, 79, 71, 88, 86, 85, 88, 85 81, 92, 92, 94, 81, 88, 98, 85 100, 100, 92, 100, 86, 77, 96, 108 85, 85, 90, 90, 102, 94, 104, 94 102, 85, 130, 104, 94, 104, 96, 112 83, 114, 106, 108, 100, 112, 149, 130 128, 142, 159, 149, 139, 159, 164, 185 193, 156, 199, 185, 199, 174, 169, 210 199, 216, 204, 202, 207, 207, 196, 161 196, 172, 164, 169, 172, 172, 196, 156 164, 156, 174, 146, 144, 169, 142, 154 149, 161, 164, 154, 159, 132, 159, 161 128, 144, 139, 142, 137, 161, 154, 154 144, 159, 149, 172, 174, 188, 199, 213 196, 199, 193, 207, 196, 190, 216, 207 222, 216, 196, 182, 177, 185, 185, 161 180, 144, 137, 132, 137, 149, 144, 121 114, 119, 144, 142, 119, 125, 144, 121 139, 144, 125, 119, 121, 128, 128, 128 106, 128, 130, 137, 135, 137, 128, 135 132, 151, 123, 128, 137, 128, 137, 164 144, 151, 149, 169, 166, 154, 159, 164 149, 154, 172, 154, 142, 128, 128, 142 125, 119, 117, 102, 92, 130, 114, 119 123, 130, 132, 121, 117, 108, 121, 144 114, 108, 108, 130, 104, 104, 130, 121 114, 128, 102, 130, 132, 125, 112, 128 142, 146, 130, 146, 132, 123, 130, 123 125, 114, 142, 137, 125, 125, 137, 132 132, 121, 139, 119, 121, 90, 128, 117 121, 137, 110, 121, 128, 154, 146, 149 128, 132, 146, 144, 139, 142, 188, 149 169, 169, 174, 174, 144, 166, 161, 169 159, 144, 144, 137, 123, 130, 151, 130 130, 128, 137, 132, 125, 149, 154, 121 154, 144, 144, 154, 146, 142, 177, 149 144, 144, 164, 137, 149, 142, 159, 137 151, 146, 130, 169, 132, 130, 130, 108 149, 151, 121, 130, 123, 144, 108, 154 137, 123, 144, 137, 119, 139, 146, 130 149, 117, 306, 128, 149, 146, 125, 123 149, 142, 146, 128, 144, 137, 132, 142 149, 137, 164, 146, 151, 149, 174, 144 169, 172, 166, 144, 156, 154, 156, 139 135, 164, 164, 149, 128, 159, 154, 139 137, 146, 156, 161, 151, 144, 117, 151 164, 159, 137, 108, 128, 121, 121, 151 121, 130, 137, 128, 137, 144, 130, 110 135, 144, 154, 154, 161, 172, 149, 185 169, 225, 210, 259, 303, 372, 365, 416 471, 493, 548, 610, 595, 615, 650, 713 708, 681, 666, 713, 581, 529, 416, 357 303, 250, 231, 202, 204, 207, 169, 177 202, 180, 174, 182, 142, 154, 146, 159 156, 149, 166, 172, 185, 185, 172, 196 204, 202, 207, 210, 246, 243, 250, 262 225, 276, 269, 272, 282, 240, 250, 228 259, 253, 237, 276, 279, 272, 292, 282 324, 353, 310, 313, 313, 310, 289, 292 502, 266, 256, 256, 256, 234, 222, 225 199, 196, 156, 172, 149, 164, 137, 149 154, 137, 137, 132, 132, 142, 142, 161 139, 159, 146, 161, 135, 139, 135, 139 137, 123, 132, 121, 121, 130, 117, 123 119, 121, 125, 108, 128, 117, 132, 119 123, 114, 135, 135, 119, 123, 112, 110 110, 117, 125, 132, 119, 121, 96, 119 128, 128, 108, 98, 100, 117, 100, 92 108, 132, 106, 135, 112, 130, 119, 114 132, 119, 144, 137, 139, 144, 132, 159 174, 161, 180, 166, 166, 202, 159, 188 174, 202, 164, 182, 169, 159, 161, 151 149, 139, 151, 154, 139, 149, 172, 144 172, 159, 137, 146, 149, 169, 161, 156 139, 164, 149, 146, 149, 119, 135, 159 132, 154, 154, 149, 144, 144, 144, 146 135, 132, 119, 123, 159, 135, 130, 137 128, 123, 135, 132, 121, 121, 114, 119 108, 121, 112, 114, 114, 135, 98, 106 108, 135, 135, 121, 130, 108, 123, 137 119, 137, 112, 154, 121, 149, 130, 164 159, 154, 193, 193, 222, 222, 202, 256 286, 282, 282, 320, 339, 357, 353, 339 310, 306, 279, 222, 190, 174, 169, 142 137, 117, 114, 121, 106, 96, 114, 102 117, 90, 94, 90, 104, 94, 88, 86 85, 88, 110, 102, 108, 94, 79, 110 83, 102, 102, 83, 81, 94, 92, 88 79, 76, 110, 98, 94, 86, 106, 102 102, 79, 85, 92, 96, 100, 94, 98 92, 77, 90, 96, 96, 102, 88, 102 117, 110, 106, 85, 119, 94, 100, 102 96, 98, 90, 79, 96, 86, 90, 71 104, 104, 79, 90, 90, 98, 90, 98 102, 106, 86, 102, 83, 121, 100, 108 98, 90, 114, 90, 114, 114, 119, 106 96, 104, 112, 104, 114, 112, 88, 132 137, 121, 98, 106, 119, 112, 125, 102 108, 139, 135, 119, 130, 128, 154, 144 154, 128, 177, 169, 164, 199, 188, 196 188, 193, 177, 222, 207, 213, 210, 222 219, 202, 204, 240, 237, 219, 262, 231 231, 289, 303, 262, 253, 279, 269, 289 279, 292, 269, 262, 276, 234, 259, 237 237, 225, 213, 240, 219, 246, 250, 246 234, 210, 225, 180, 204, 193, 222, 222 207, 182, 219, 237, 237, 234, 193, 204 182, 237, 207, 253, 222, 196, 188, 188 213, 210, 185, 166, 154, 174, 149, 154 139, 146, 159, 164, 146, 146, 132, 135 121, 139, 151, 139, 135, 142, 139, 159 135, 137, 137, 164, 149, 142, 156, 172 161, 190, 172, 190, 193, 213, 231, 219 231, 193, 190, 196, 196, 185, 193, 182 159, 166, 172, 159, 169, 137, 144, 121 144, 164, 130, 149, 154, 146, 154, 180 144, 139, 144, 149, 151, 156, 154, 135 142, 156, 137, 156, 151, 135, 161, 151 142, 146, 130, 161, 161, 164, 149, 161 154, 156, 146, 161, 164, 156, 164, 166 196, 182, 164, 142, 174, 159, 151, 172 142, 177, 137, 146, 154, 137, 135, 142 102, 137, 125, 130, 121, 137, 123, 128 137, 119, 123, 123, 135, 132, 121, 137 130, 110, 123, 132, 137, 121, 121, 104 125, 104, 110, 121, 119, 108, 102, 108 110, 102, 132, 128, 104, 121, 108, 108 112, 94, 94, 100, 121, 119, 104, 102 128, 104, 121, 100, 121, 119, 137, 137 110, 114, 96, 114, 121, 132, 110, 137 130, 137, 144, 139, 144, 174, 142, 154 161, 154, 169, 144, 169, 154, 159, 149 112, 144, 112, 114, 108, 110, 102, 114 112, 96, 108, 119, 117, 110, 100, 98 123, 119, 112, 104, 112, 110, 128, 106 144, 144, 123, 123, 121, 128, 123, 139 130, 128, 139, 144, 144, 137, 128, 128 137, 123, 112, 106, 119, 114, 123, 132 121, 110, 132, 121, 106, 121, 135, 112 125, 98, 121, 110, 121, 125, 121, 102 128, 104, 110, 119, 104, 112, 112, 108 123, 96, 117, 123, 108, 104, 112, 117 92, 121, 130, 121, 108, 112, 119, 92 110, 123, 104, 110, 114, 121, 108, 114 100, 121, 92, 96, 110, 142, 112, 117 119, 114, 123, 114, 130, 102, 110, 100 125, 92, 121, 128, 128, 128, 117, 135 114, 106, 123, 144, 128, 146, 121, 117 135, 137, 128, 125, 139, 169, 135, 149 174, 182, 159, 177, 174, 177, 199, 149 159, 169, 174, 154, 154, 182, 142, 132 125, 137, 139, 146, 119, 117, 128, 130 128, 117, 104, 128, 130, 123, 130, 108 121, 114, 114, 106, 114, 106, 83, 123 104, 85, 112, 117, 123, 119, 90, 81 110, 98, 102, 83, 102, 98, 106, 92 74, 90, 96, 90, 88, 94, 88, 88 106, 86, 98, 85, 94, 104, 104, 96 100, 94, 112, 123, 119, 128, 100, 137 112, 110, 130, 125, 114, 132, 128, 123 106, 112, 96, 119, 121, 121, 96, 100 112, 123, 100, 102, 102, 117, 130, 98 121, 151, 149, 193, 166, 174, 193, 182 213, 188, 193, 188, 188, 182, 164, 159 154, 130, 132, 144, 112, 121, 119, 106 117, 100, 132, 137, 117, 112, 130, 125 121, 137, 137, 139, 149, 161, 159, 177 159, 193, 180, 204, 228, 246, 262, 272 276, 272, 276, 313, 324, 289, 320, 256 276, 262, 225, 225, 204, 185, 177, 151 174, 164, 132, 132, 159, 156, 139, 135 151, 154, 130, 130, 121, 108, 104, 104 98, 96, 117, 117, 106, 90, 106, 104 90, 112, 81, 90, 79, 90, 86, 90 79, 79, 104, 110, 86, 96, 83, 86 76, 88, 81, 100, 88, 102, 66, 83 96, 90, 104, 81, 79, 85, 90, 94 286, 85, 92, 88, 85, 98, 90, 79 92, 90, 104, 85, 83, 74, 86, 96 104, 90, 98, 102, 66, 76, 79, 110 92, 94, 83, 77, 72, 69, 86, 72 85, 86, 71, 85, 71, 79, 76, 77 72, 72, 66, 59, 77, 79, 77, 81 94, 72, 74, 94, 76, 90, 83, 110 79, 74, 85, 79, 83, 86, 106, 86 92, 96, 90, 90, 92, 94, 94, 106 94, 123, 92, 102, 100, 106, 98, 83 88, 96, 74, 100, 85, 81, 88, 66 79, 86, 64, 90, 76, 76, 77, 88 85, 62, 66, 79, 86, 79, 92, 79 71, 71, 71, 72, 64, 77, 88, 71 100, 85, 83, 79, 79, 77, 96, 83 108, 92, 100, 92, 88, 90, 83, 77 90, 85, 98, 96, 90, 106, 83, 79 83, 88, 98, 90, 90, 104, 123, 104 112, 117, 114, 123, 121, 110, 92, 112 123, 117, 100, 130, 139, 154, 169, 180 185, 185, 202, 188, 151, 204, 204, 202 222, 213, 190, 174, 169, 169, 146, 125 142, 128, 123, 102, 112, 90, 81, 79 79, 90, 94, 104, 85, 88, 102, 102 102, 98, 98, 94, 96, 94, 112, 90 92, 130, 102, 92, 98, 86, 85, 90 98, 96, 85, 69, 98, 92, 83, 92 88, 114, 79, 85, 76, 88, 102, 98 92, 90, 76, 92, 90, 83, 85, 76 94, 90, 71, 81, 81, 92, 76, 85 88, 86, 62, 59, 86, 76, 59, 71 66, 85, 77, 64, 85, 74, 79, 76 77, 67, 67, 67, 92, 85, 67, 85 85, 83, 67, 85, 86, 90, 96, 98 94, 94, 104, 88, 98, 98, 92, 100 88, 106, 104, 85, 94, 90, 85, 92 94, 88, 88, 85, 77, 102, 96, 86 92, 92, 104, 104, 96, 94, 76, 88 90, 102, 88, 86, 117, 94, 100, 102 83, 98, 104, 96, 114, 108, 100, 117 112, 110, 108, 96, 117, 106, 98, 121 125, 119, 112, 137, 112, 121, 123, 128 110, 104, 114, 114, 132, 123, 108, 135 125, 102, 121, 123, 132, 114, 142, 135 142, 119, 130, 121, 132, 125, 128, 119 123, 137, 119, 121, 121, 130, 128, 121 121, 117, 119, 119, 121, 119, 121, 123 135, 146, 144, 137, 130, 135, 130, 123 119, 130, 135, 132, 132, 137, 110, 123 135, 144, 130, 125, 132, 117, 159, 172 169, 182, 166, 196, 169, 172, 166, 196 161, 154, 151, 177, 172, 146, 144, 166 159, 137, 132, 161, 142, 142, 149, 151 149, 164, 139, 149, 154, 137, 144, 154 154, 144, 135, 144, 146, 132, 156, 135 128, 142, 135, 142, 135, 125, 132, 151 135, 121, 123, 130, 132, 123, 146, 130 125, 132, 144, 119, 159, 112, 139, 142 142, 128, 132, 139, 125, 142, 142, 114 146, 144, 154, 174, 177, 188, 210, 185 207, 177, 199, 196, 213, 216, 202, 219 172, 185, 193, 151, 161, 185, 169, 154 132, 121, 137, 130, 121, 139, 128, 123 137, 114, 117, 106, 117, 130, 130, 119 117, 123, 102, 117, 125, 110, 110, 86 96, 112, 102, 121, 106, 102, 108, 110 110, 102, 96, 96, 100, 100, 121, 86 114, 110, 96, 67, 96, 121, 106, 102 96, 121, 104, 100, 94, 96, 92, 86 104, 88, 112, 96, 104, 110, 110, 119 108, 85, 100, 102, 86, 86, 119, 88 108, 90, 108, 98, 94, 100, 104, 98 96, 102, 106, 72, 81, 100, 106, 104 96, 92, 77, 92, 112, 98, 104, 92 106, 112, 106, 98, 104, 108, 96, 100 100, 98, 90, 88, 119, 106, 114, 125 104, 108, 123, 94, 88, 100, 108, 121 92, 90, 114, 121, 112, 86, 96, 112 102, 108, 114, 110, 119, 106, 110, 108 123, 108, 110, 123, 100, 135, 123, 130 123, 121, 137, 119, 132, 128, 151, 161 185, 180, 174, 172, 180, 193, 193, 207 225, 210, 222, 222, 213, 228, 204, 202 190, 182, 169, 174, 154, 159, 144, 151 161, 154, 123, 144, 142, 123, 142, 156 137, 114, 117, 112, 112, 132, 98, 121 102, 128, 98, 151, 108, 132, 108, 142 110, 121, 142, 151, 104, 154, 154, 149 166, 146, 128, 149, 135, 161, 172, 154 151, 172, 121, 164, 166, 161, 177, 185 174, 156, 182, 190, 207, 185, 185, 216 169, 185, 210, 190, 193, 193, 222, 199 213, 228, 219, 202, 199, 196, 204, 210 210, 346, 210, 202, 213, 219, 196, 190 243, 207, 185, 193, 196, 196, 202, 174 172, 202, 204, 174, 188, 196, 172, 172 202, 188, 180, 174, 166, 193, 180, 188 177, 174, 177, 159, 185, 137, 172, 149 142, 149, 130, 137, 137, 137, 135, 144 146, 121, 121, 151, 110, 130, 121, 142 119, 102, 112, 112, 121, 121, 123, 98 108, 121, 121, 102, 94, 119, 130, 90 119, 85, 96, 102, 104, 96, 102, 106 98, 88, 121, 121, 102, 102, 100, 77 92, 110, 98, 121, 104, 112, 108, 92 98, 92, 112, 92, 104, 100, 125, 108 112, 100, 96, 121, 125, 123, 130, 130 132, 128, 125, 130, 125, 132, 130, 98 125, 104, 121, 110, 108, 104, 114, 108 114, 106, 110, 108, 106, 104, 100, 85 102, 94, 104, 85, 86, 88, 92, 94 81, 88, 77, 92, 98, 90, 94, 90 98, 98, 98, 88, 92, 92, 108, 85 96, 125, 108, 112, 96, 106, 90, 86 121, 121, 112, 100, 85, 108, 104, 100 106, 114, 88, 100, 102, 117, 90, 98 114, 108, 94, 106, 100, 100, 104, 128 94, 102, 102, 137, 102, 98, 106, 88 108, 125, 112, 110, 123, 108, 102, 142 104, 117, 92, 119, 104, 106, 104, 112 92, 135, 121, 130, 102, 123, 119, 110 137, 135, 130, 119, 137, 128, 102, 119 100, 121, 119, 123, 110, 117, 114, 76 102, 100, 106, 83, 96, 121, 102, 74 94, 79, 86, 92, 85, 106, 108, 71 94, 94, 102, 108, 79, 88, 98, 94 102, 108, 125, 98, 85, 90, 104, 88 106, 96, 106, 88, 102, 104, 98, 102 114, 106, 102, 96, 106, 106, 106, 106 110, 123, 121, 110, 135, 104, 132, 149 149, 130, 169, 151, 169, 146, 154, 185 166, 182, 164, 161, 151, 149, 149, 169 164, 154, 174, 166, 166, 188, 177, 196 193, 216, 193, 177, 199, 216, 250, 185 213, 193, 199, 177, 199, 180, 204, 180 164, 177, 144, 125, 146, 130, 119, 130 135, 102, 130, 121, 114, 108, 100, 106 108, 114, 114, 88, 100, 130, 102, 108 112, 102, 106, 94, 96, 102, 106, 104 98, 110, 121, 104, 100, 137, 112, 121 117, 123, 104, 114, 110, 112, 128, 110 119, 125, 114, 121, 130, 117, 121, 112 135, 121, 121, 121, 100, 94, 110, 128 121, 137, 119, 100, 110, 96, 96, 100 106, 119, 106, 106, 132, 119, 96, 104 102,/