SampleIdent,907A-11-3/22,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 9-aug-1993 19:58,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 119, 104, 102, 85, 106, 104, 110, 104 117, 108, 112, 121, 83, 104, 125, 100 102, 102, 102, 106, 112, 130, 130, 102 117, 117, 123, 100, 94, 121, 132, 96 102, 104, 119, 108, 121, 128, 110, 98 121, 119, 132, 102, 117, 112, 104, 117 110, 123, 125, 135, 130, 114, 108, 123 130, 132, 119, 125, 123, 130, 117, 128 128, 149, 121, 121, 117, 110, 121, 130 137, 130, 125, 128, 132, 130, 137, 110 117, 137, 149, 139, 142, 154, 132, 125 130, 117, 135, 142, 125, 137, 102, 159 128, 144, 121, 137, 156, 137, 130, 125 137, 123, 125, 137, 123, 169, 156, 128 108, 117, 123, 123, 161, 142, 121, 144 139, 119, 135, 121, 139, 135, 146, 139 144, 125, 135, 123, 130, 128, 130, 121 144, 146, 144, 119, 117, 137, 146, 132 132, 121, 149, 112, 108, 123, 121, 108 121, 119, 149, 139, 130, 110, 137, 121 132, 128, 108, 114, 130, 128, 130, 119 114, 142, 139, 128, 123, 119, 112, 128 121, 137, 139, 128, 130, 128, 142, 130 139, 137, 128, 146, 154, 132, 146, 125 137, 114, 119, 128, 110, 119, 110, 110 108, 117, 121, 110, 119, 88, 64, 110 114, 108, 100, 96, 100, 128, 92, 98 110, 106, 88, 110, 100, 112, 114, 90 96, 88, 100, 110, 112, 88, 108, 112 110, 90, 110, 100, 88, 102, 104, 102 117, 92, 96, 102, 94, 100, 92, 104 94, 100, 88, 114, 100, 83, 104, 102 98, 100, 90, 102, 104, 104, 79, 96 85, 125, 90, 90, 102, 108, 86, 92 104, 90, 98, 92, 88, 79, 117, 94 94, 90, 86, 88, 85, 98, 90, 98 102, 102, 88, 102, 90, 100, 79, 100 100, 86, 88, 112, 79, 94, 90, 108 94, 96, 104, 88, 90, 88, 92, 102 92, 94, 85, 92, 79, 108, 92, 85 90, 90, 79, 98, 100, 92, 98, 96 88, 106, 104, 98, 85, 90, 102, 117 94, 100, 88, 104, 86, 90, 90, 106 86, 106, 83, 96, 102, 98, 108, 119 119, 94, 108, 114, 106, 130, 104, 108 98, 117, 92, 86, 108, 130, 100, 117 104, 114, 144, 121, 102, 130, 104, 108 112, 98, 96, 112, 92, 83, 106, 102 79, 88, 88, 88, 100, 79, 90, 77 85, 92, 79, 96, 98, 94, 108, 86 86, 81, 72, 85, 90, 83, 83, 86 114, 102, 83, 83, 104, 90, 85, 85 88, 94, 81, 90, 102, 96, 88, 77 94, 88, 108, 100, 100, 94, 100, 92 86, 90, 77, 92, 86, 106, 108, 94 83, 96, 102, 428, 83, 102, 88, 86 86, 86, 92, 76, 90, 77, 108, 92 100, 77, 72, 74, 74, 92, 79, 88 79, 86, 74, 88, 86, 67, 79, 81 98, 88, 71, 100, 85, 88, 76, 100 86, 76, 88, 72, 96, 102, 76, 72 85, 92, 92, 72, 104, 90, 92, 94 77, 92, 94, 85, 83, 90, 94, 76 71, 77, 83, 79, 74, 86, 85, 77 92, 110, 77, 88, 92, 83, 77, 86 86, 102, 77, 62, 96, 88, 83, 79 100, 92, 90, 77, 66, 71, 90, 77 74, 86, 81, 86, 76, 92, 76, 77 85, 85, 85, 77, 74, 90, 72, 92 88, 67, 85, 67, 90, 90, 76, 86 76, 92, 79, 92, 79, 81, 69, 81 74, 72, 86, 74, 86, 79, 72, 77 83, 81, 83, 69, 90, 85, 76, 83 94, 81, 85, 88, 96, 71, 79, 77 90, 69, 86, 76, 69, 77, 94, 81 90, 74, 102, 76, 72, 98, 86, 96 72, 77, 83, 77, 90, 66, 77, 83 77, 76, 72, 79, 79, 100, 79, 85 83, 88, 88, 98, 102, 79, 92, 102 106, 86, 76, 92, 100, 90, 108, 104 110, 83, 88, 88, 100, 104, 90, 96 94, 85, 90, 85, 98, 96, 79, 86 102, 104, 86, 100, 85, 94, 94, 90 96, 86, 76, 85, 83, 83, 88, 86 79, 88, 83, 86, 86, 85, 85, 92 92, 86, 96, 104, 86, 98, 100, 96 88, 100, 119, 100, 94, 106, 94, 102 79, 100, 86, 100, 96, 98, 86, 121 123, 102, 112, 117, 117, 114, 117, 137 125, 132, 149, 119, 154, 128, 130, 130 121, 137, 142, 149, 161, 159, 182, 180 204, 213, 204, 202, 207, 216, 228, 246 259, 276, 276, 243, 234, 234, 234, 272 234, 231, 240, 190, 213, 222, 196, 177 190, 213, 185, 185, 169, 193, 188, 174 182, 177, 188, 182, 164, 180, 164, 185 193, 164, 190, 185, 185, 185, 180, 199 166, 172, 185, 174, 169, 190, 185, 213 202, 225, 259, 286, 259, 262, 282, 292 272, 256, 219, 243, 219, 180, 213, 166 164, 119, 144, 149, 144, 177, 146, 169 166, 144, 164, 172, 164, 149, 164, 174 161, 144, 135, 142, 161, 156, 128, 174 166, 154, 151, 164, 154, 166, 159, 159 149, 151, 164, 164, 135, 164, 169, 169 154, 164, 180, 174, 202, 174, 204, 202 190, 222, 177, 182, 166, 156, 151, 154 154, 132, 144, 149, 139, 114, 137, 130 125, 117, 144, 135, 125, 110, 117, 125 123, 144, 128, 123, 112, 130, 130, 125 128, 144, 125, 146, 139, 123, 135, 128 159, 159, 161, 146, 149, 154, 174, 154 130, 161, 144, 144, 137, 130, 144, 146 139, 125, 135, 135, 121, 137, 112, 144 164, 151, 114, 132, 128, 139, 154, 146 123, 164, 182, 159, 177, 177, 182, 210 228, 199, 225, 210, 180, 213, 174, 185 161, 182, 174, 154, 169, 166, 169, 159 146, 166, 142, 142, 166, 159, 174, 225 228, 185, 222, 185, 174, 166, 146, 166 188, 159, 185, 210, 199, 202, 202, 172 182, 174, 137, 156, 159, 166, 142, 142 164, 161, 146, 139, 149, 154, 156, 135 146, 149, 149, 149, 156, 139, 174, 164 154, 154, 164, 166, 174, 185, 161, 149 174, 154, 169, 172, 180, 182, 169, 151 169, 174, 196, 174, 190, 185, 159, 164 188, 180, 177, 185, 180, 182, 164, 164 172, 188, 149, 182, 142, 174, 151, 144 169, 164, 169, 172, 151, 149, 161, 185 144, 149, 146, 164, 144, 137, 137, 164 193, 154, 130, 142, 154, 130, 130, 169 159, 154, 177, 146, 169, 169, 174, 199 172, 185, 199, 199, 222, 259, 276, 328 372, 475, 640, 1024, 1089, 999, 1011, 1149 1163, 1018, 973, 930, 795, 650, 506, 420 335, 331, 253, 256, 219, 234, 219, 188 193, 207, 199, 204, 199, 193, 190, 159 164, 190, 174, 196, 166, 190, 161, 202 166, 210, 225, 210, 219, 256, 228, 269 276, 243, 282, 286, 269, 272, 266, 237 299, 282, 292, 310, 299, 328, 346, 412 408, 376, 404, 400, 400, 392, 357, 353 328, 328, 310, 299, 276, 299, 269, 240 246, 240, 213, 213, 177, 182, 164, 144 169, 177, 159, 166, 185, 154, 196, 182 182, 156, 193, 166, 177, 142, 177, 144 139, 149, 128, 137, 132, 132, 132, 144 108, 144, 149, 117, 146, 142, 144, 119 114, 128, 121, 128, 128, 121, 121, 121 119, 144, 144, 135, 135, 142, 137, 135 128, 130, 139, 121, 144, 137, 128, 149 108, 130, 125, 139, 149, 154, 144, 185 156, 142, 156, 137, 132, 135, 144, 180 146, 151, 172, 166, 199, 196, 188, 237 188, 202, 172, 185, 159, 159, 164, 177 149, 151, 144, 156, 161, 135, 149, 144 164, 154, 154, 164, 154, 135, 159, 156 164, 164, 169, 166, 185, 169, 146, 159 142, 149, 128, 151, 146, 144, 128, 144 132, 137, 166, 154, 159, 144, 137, 151 149, 130, 146, 139, 144, 132, 125, 121 132, 121, 125, 119, 125, 125, 137, 139 135, 149, 142, 130, 161, 154, 149, 130 137, 142, 139, 169, 137, 154, 142, 151 156, 137, 159, 144, 174, 180, 216, 243 256, 303, 339, 392, 339, 380, 412, 420 384, 339, 289, 225, 222, 190, 164, 135 151, 114, 130, 137, 132, 119, 135, 128 104, 114, 106, 102, 121, 108, 106, 123 125, 110, 98, 119, 90, 92, 98, 112 112, 104, 110, 98, 128, 94, 85, 119 104, 102, 104, 106, 112, 100, 102, 88 106, 96, 92, 108, 102, 102, 94, 96 117, 104, 81, 100, 104, 108, 104, 96 121, 128, 128, 121, 102, 100, 110, 121 106, 112, 108, 108, 96, 125, 88, 102 98, 90, 104, 108, 104, 110, 96, 102 100, 100, 112, 106, 119, 112, 98, 108 106, 110, 121, 119, 112, 119, 135, 123 125, 92, 121, 135, 119, 100, 110, 128 102, 98, 125, 125, 112, 130, 144, 132 114, 112, 121, 132, 132, 144, 137, 128 149, 174, 169, 180, 159, 202, 180, 190 202, 210, 185, 219, 222, 213, 219, 246 237, 228, 250, 222, 231, 262, 266, 256 246, 259, 286, 289, 279, 320, 303, 296 299, 310, 331, 276, 310, 286, 282, 269 262, 246, 231, 279, 240, 228, 213, 237 243, 237, 231, 246, 222, 250, 204, 246 222, 237, 240, 190, 219, 199, 202, 240 228, 228, 225, 231, 219, 250, 250, 213 219, 237, 213, 199, 180, 193, 193, 188 172, 174, 185, 169, 159, 169, 182, 169 154, 169, 149, 151, 149, 149, 154, 182 142, 137, 161, 161, 161, 202, 172, 193 177, 196, 202, 216, 228, 216, 204, 256 253, 234, 228, 234, 207, 207, 190, 207 188, 202, 164, 190, 174, 166, 146, 172 169, 182, 177, 139, 142, 149, 188, 182 156, 182, 156, 177, 180, 174, 174, 156 164, 164, 159, 156, 151, 151, 177, 144 154, 161, 161, 182, 185, 172, 164, 182 146, 180, 188, 159, 174, 188, 174, 159 193, 190, 196, 169, 174, 180, 174, 174 172, 156, 164, 156, 149, 166, 159, 149 121, 149, 135, 128, 135, 146, 137, 137 142, 139, 137, 123, 159, 125, 142, 135 159, 151, 159, 132, 151, 161, 144, 149 154, 149, 177, 146, 137, 149, 130, 146 114, 123, 121, 108, 132, 119, 125, 132 135, 106, 125, 142, 125, 135, 121, 112 114, 114, 88, 119, 108, 117, 130, 108 144, 121, 142, 119, 123, 112, 146, 125 139, 142, 149, 177, 169, 172, 174, 159 199, 216, 202, 182, 182, 169, 142, 144 159, 154, 137, 132, 132, 130, 108, 123 104, 106, 108, 114, 130, 117, 130, 137 98, 110, 144, 151, 108, 142, 117, 144 144, 139, 130, 130, 144, 123, 146, 151 151, 159, 169, 174, 177, 166, 130, 149 151, 146, 123, 142, 119, 139, 112, 130 132, 125, 137, 130, 130, 121, 132, 119 121, 119, 119, 123, 139, 128, 132, 114 130, 146, 117, 114, 135, 123, 132, 123 119, 128, 151, 135, 108, 137, 106, 100 121, 108, 130, 123, 119, 139, 98, 119 128, 117, 108, 112, 114, 110, 110, 130 123, 144, 104, 110, 106, 128, 123, 132 125, 119, 112, 106, 128, 135, 166, 112 128, 156, 135, 114, 142, 169, 137, 117 130, 142, 130, 121, 156, 135, 154, 142 166, 149, 177, 177, 156, 164, 166, 177 180, 180, 172, 182, 202, 177, 219, 185 225, 193, 156, 159, 149, 172, 156, 146 117, 130, 123, 130, 117, 114, 104, 130 112, 104, 121, 112, 130, 117, 130, 125 420, 117, 104, 114, 132, 114, 123, 110 114, 106, 90, 108, 100, 98, 96, 110 96, 119, 96, 92, 112, 94, 102, 104 119, 100, 106, 98, 100, 104, 114, 117 102, 100, 96, 100, 98, 104, 114, 90 114, 106, 108, 106, 88, 106, 130, 137 135, 139, 135, 121, 137, 130, 142, 132 137, 137, 144, 130, 102, 121, 90, 130 114, 121, 83, 119, 96, 117, 130, 119 130, 110, 132, 130, 121, 139, 149, 156 169, 185, 185, 196, 185, 174, 174, 172 172, 161, 132, 154, 151, 144, 104, 149 125, 128, 123, 125, 125, 112, 128, 146 137, 123, 139, 119, 130, 139, 149, 123 144, 154, 166, 174, 156, 222, 240, 237 240, 317, 317, 317, 350, 346, 372, 335 282, 286, 237, 276, 204, 207, 196, 177 174, 166, 188, 156, 177, 185, 154, 166 169, 154, 159, 144, 132, 144, 130, 104 110, 112, 123, 114, 117, 123, 117, 104 96, 104, 86, 104, 98, 96, 106, 96 96, 98, 96, 81, 108, 94, 92, 98 98, 104, 94, 94, 102, 92, 94, 114 85, 100, 90, 76, 100, 94, 85, 96 94, 94, 90, 94, 94, 85, 108, 96 104, 90, 94, 86, 88, 88, 106, 81 104, 96, 102, 94, 90, 90, 100, 92 102, 90, 83, 83, 88, 96, 90, 98 94, 96, 88, 94, 92, 94, 76, 71 86, 88, 85, 83, 86, 94, 77, 76 104, 90, 85, 90, 94, 74, 102, 96 100, 79, 104, 98, 112, 94, 96, 94 112, 88, 104, 98, 94, 104, 104, 104 102, 112, 100, 92, 86, 100, 85, 85 114, 100, 104, 98, 94, 83, 94, 90 98, 74, 71, 76, 96, 94, 79, 100 85, 76, 98, 86, 88, 102, 102, 96 69, 77, 71, 77, 81, 90, 92, 121 88, 72, 88, 106, 79, 88, 92, 88 92, 104, 114, 98, 86, 102, 110, 108 88, 110, 119, 102, 100, 100, 98, 128 114, 123, 102, 112, 117, 123, 108, 112 128, 106, 130, 110, 108, 137, 110, 135 98, 114, 92, 92, 132, 117, 130, 114 154, 166, 210, 231, 225, 222, 196, 262 256, 262, 246, 188, 159, 169, 169, 146 130, 139, 104, 104, 88, 85, 90, 98 83, 88, 94, 104, 79, 96, 119, 102 86, 90, 96, 104, 106, 128, 119, 117 112, 100, 108, 102, 88, 114, 83, 104 86, 96, 83, 92, 86, 114, 108, 88 108, 92, 85, 94, 96, 108, 102, 98 88, 117, 96, 81, 88, 90, 102, 90 79, 104, 96, 96, 110, 104, 96, 92 86, 81, 76, 86, 92, 94, 76, 77 69, 79, 79, 72, 88, 76, 74, 79 86, 83, 69, 67, 85, 67, 92, 76 98, 100, 92, 79, 92, 96, 98, 85 98, 104, 85, 104, 92, 96, 108, 86 102, 110, 98, 76, 94, 112, 94, 92 102, 96, 104, 92, 83, 81, 102, 104 104, 92, 98, 117, 88, 90, 106, 108 106, 114, 102, 119, 108, 100, 108, 100 79, 114, 110, 96, 117, 142, 114, 130 125, 125, 121, 110, 100, 132, 139, 117 121, 151, 130, 102, 104, 104, 137, 137 123, 142, 132, 123, 123, 137, 130, 130 144, 139, 137, 154, 123, 135, 137, 151 139, 130, 159, 135, 151, 156, 144, 166 151, 137, 139, 149, 149, 130, 128, 130 144, 130, 130, 128, 142, 139, 146, 156 164, 166, 125, 142, 132, 135, 132, 144 144, 151, 130, 137, 137, 139, 125, 177 137, 128, 154, 156, 146, 154, 172, 169 172, 174, 185, 196, 185, 190, 204, 188 177, 159, 210, 161, 156, 172, 159, 159 166, 156, 139, 135, 146, 159, 185, 164 159, 144, 172, 164, 164, 146, 159, 144 172, 169, 146, 166, 164, 154, 135, 154 132, 135, 149, 146, 137, 130, 154, 166 146, 144, 132, 123, 139, 137, 144, 149 146, 144, 130, 144, 159, 154, 161, 137 144, 137, 125, 146, 146, 142, 119, 164 161, 149, 159, 149, 193, 159, 188, 188 185, 199, 202, 210, 219, 210, 216, 216 207, 174, 172, 185, 188, 156, 156, 174 149, 144, 151, 159, 146, 128, 137, 130 121, 135, 128, 104, 135, 135, 130, 121 121, 125, 135, 125, 130, 117, 128, 104 132, 130, 121, 125, 137, 128, 139, 104 121, 104, 112, 137, 110, 102, 102, 104 121, 106, 108, 104, 121, 110, 90, 76 92, 117, 121, 112, 104, 108, 102, 114 112, 125, 112, 114, 90, 96, 104, 86 132, 94, 112, 98, 108, 128, 121, 112 100, 102, 102, 119, 100, 104, 98, 130 106, 119, 110, 112, 102, 102, 119, 94 102, 104, 108, 121, 108, 104, 106, 100 123, 112, 117, 128, 114, 100, 100, 117 114, 119, 110, 130, 102, 86, 102, 137 106, 117, 112, 114, 123, 114, 104, 123 123, 130, 100, 130, 128, 106, 121, 117 108, 112, 98, 132, 132, 117, 110, 112 130, 106, 123, 123, 130, 144, 130, 128 125, 130, 137, 121, 132, 132, 149, 139 149, 151, 174, 188, 154, 207, 246, 222 234, 253, 243, 256, 231, 204, 213, 193 182, 182, 188, 216, 169, 159, 161, 156 137, 137, 144, 125, 146, 130, 125, 121 123, 151, 137, 123, 121, 154, 106, 123 121, 123, 130, 112, 128, 137, 151, 121 139, 149, 135, 132, 130, 149, 132, 151 156, 151, 159, 135, 151, 137, 144, 137 144, 174, 161, 161, 164, 159, 174, 161 174, 188, 193, 177, 166, 156, 164, 190 213, 174, 182, 225, 210, 222, 256, 196 213, 231, 199, 246, 216, 253, 237, 259 228, 250, 231, 243, 225, 237, 222, 216 256, 231, 193, 231, 222, 234, 196, 207 188, 222, 204, 188, 210, 213, 193, 188 210, 188, 193, 204, 213, 219, 207, 180 207, 190, 196, 199, 196, 180, 177, 144 164, 177, 149, 172, 196, 149, 161, 159 154, 164, 128, 137, 156, 139, 130, 128 139, 128, 142, 130, 130, 132, 119, 144 137, 121, 100, 104, 110, 114, 110, 110 108, 104, 119, 128, 117, 130, 128, 130 112, 128, 121, 98, 114, 114, 117, 121 117, 104, 106, 108, 121, 106, 96, 112 114, 108, 106, 121, 114, 139, 142, 125 123, 117, 108, 121, 112, 106, 142, 102 146, 130, 146, 154, 130, 123, 137, 132 144, 135, 130, 121, 125, 130, 114, 121 117, 121, 128, 110, 108, 121, 104, 108 106, 100, 90, 88, 102, 106, 114, 108 108, 100, 100, 100, 119, 128, 83, 130 96, 125, 112, 98, 96, 132, 117, 121 123, 119, 121, 98, 128, 125, 135, 128 121, 108, 112, 128, 123, 123, 128, 130 128, 132, 130, 123, 125, 110, 110, 135 114, 114, 114, 112, 94, 117, 114, 106 90, 130, 108, 114, 119, 135, 104, 123 114, 139, 117, 117, 104, 121, 130, 114 112, 130, 110, 112, 117, 98, 117, 135 114, 125, 121, 144, 125, 119, 117, 161 137, 144, 130, 159, 137, 135, 106, 139 117, 112, 146, 135, 139, 125, 100, 121 123, 106, 92, 88, 132, 90, 88, 102 106, 110, 77, 108, 90, 86, 88, 86 94, 92, 94, 100, 86, 90, 119, 92 83, 98, 96, 114, 117, 110, 112, 106 98, 96, 108, 108, 106, 110, 100, 102 98, 117, 114, 130, 130, 96, 125, 100 119, 121, 121, 117, 114, 130, 132, 130 144, 149, 139, 154, 159, 188, 180, 202 190, 199, 164, 156, 169, 166, 169, 156 159, 177, 159, 172, 190, 149, 177, 177 193, 222, 228, 225, 246, 250, 225, 237 228, 222, 231, 234, 216, 202, 228, 199 196, 196, 174, 172, 142, 169, 151, 159 137, 144, 130, 114, 130, 112, 98, 137 114, 114, 121, 96, 130, 121, 125, 104 104, 117, 114, 121, 119, 110, 130, 132 121, 117, 137, 117, 98, 142, 137, 106 86, 117, 104, 121, 130, 128, 110, 123 128, 121, 125, 139, 149, 132, 142, 135 125, 119, 130, 117, 130, 149, 123, 123 123, 135, 110, 130, 130, 121, 130, 121 98, 132, 114, 102, 130, 117, 128, 121 108,/