SampleIdent,907A-12-3/27,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 9-aug-1993 20:53,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 90, 102, 92, 88, 102, 76, 83, 76 90, 108, 100, 94, 98, 104, 94, 98 92, 106, 102, 96, 106, 102, 94, 106 86, 104, 100, 104, 100, 119, 90, 98 117, 96, 104, 102, 92, 110, 108, 106 100, 98, 92, 114, 108, 86, 104, 114 108, 114, 110, 83, 114, 100, 102, 114 123, 130, 108, 108, 121, 106, 121, 125 137, 114, 130, 135, 125, 139, 114, 102 108, 114, 132, 128, 123, 130, 128, 119 114, 102, 119, 114, 139, 154, 123, 132 106, 139, 154, 137, 130, 121, 137, 128 102, 135, 108, 132, 119, 128, 121, 130 121, 92, 125, 130, 121, 114, 114, 128 117, 119, 130, 130, 121, 146, 119, 132 130, 130, 159, 137, 130, 142, 121, 121 137, 139, 137, 117, 137, 123, 117, 119 130, 137, 128, 121, 135, 137, 123, 117 112, 106, 121, 114, 100, 114, 121, 132 128, 114, 110, 114, 137, 110, 117, 135 137, 135, 128, 110, 117, 117, 121, 114 128, 130, 132, 114, 108, 119, 119, 119 108, 135, 114, 112, 130, 102, 114, 106 123, 135, 121, 123, 121, 139, 121, 125 142, 128, 130, 130, 110, 123, 128, 114 104, 98, 88, 114, 102, 90, 100, 112 102, 108, 98, 96, 96, 96, 110, 86 123, 100, 112, 104, 102, 106, 85, 94 94, 100, 83, 108, 92, 102, 96, 94 102, 85, 125, 100, 106, 90, 85, 83 98, 102, 96, 77, 90, 94, 106, 110 85, 104, 100, 94, 96, 85, 72, 108 98, 96, 94, 110, 77, 102, 104, 104 85, 79, 106, 86, 110, 106, 106, 117 92, 79, 81, 92, 98, 112, 102, 77 104, 90, 83, 77, 85, 96, 77, 110 110, 96, 86, 90, 88, 104, 94, 72 85, 85, 96, 96, 96, 119, 96, 83 100, 79, 90, 85, 85, 94, 85, 88 106, 100, 98, 90, 106, 79, 106, 77 100, 108, 85, 96, 96, 79, 83, 90 96, 100, 98, 102, 88, 100, 90, 96 110, 106, 88, 96, 106, 92, 112, 92 90, 100, 94, 76, 83, 90, 92, 92 96, 98, 119, 94, 94, 98, 88, 104 112, 108, 114, 100, 110, 102, 119, 100 110, 104, 102, 106, 121, 130, 92, 132 117, 128, 130, 130, 119, 123, 110, 98 86, 98, 86, 94, 86, 94, 108, 76 77, 72, 88, 88, 85, 83, 72, 76 94, 100, 90, 72, 85, 77, 94, 85 77, 90, 83, 86, 83, 88, 79, 85 96, 86, 90, 90, 100, 76, 76, 90 85, 77, 79, 90, 86, 98, 88, 81 98, 72, 83, 96, 77, 76, 90, 86 86, 83, 86, 88, 92, 94, 77, 85 67, 98, 85, 77, 85, 92, 85, 81 66, 81, 86, 83, 67, 88, 74, 76 67, 88, 85, 88, 98, 88, 77, 90 72, 77, 92, 79, 72, 71, 62, 85 289, 83, 79, 79, 81, 83, 94, 96 90, 88, 83, 86, 81, 85, 79, 100 88, 83, 85, 74, 79, 67, 92, 86 83, 85, 83, 85, 77, 94, 83, 86 79, 85, 96, 90, 85, 62, 92, 79 72, 79, 67, 72, 74, 86, 88, 92 76, 94, 77, 77, 83, 81, 88, 98 92, 86, 92, 86, 76, 94, 96, 81 92, 83, 90, 74, 77, 85, 81, 92 72, 83, 77, 77, 85, 102, 85, 86 110, 76, 72, 72, 83, 92, 94, 92 83, 77, 69, 66, 77, 85, 96, 90 100, 77, 67, 90, 94, 71, 88, 96 86, 79, 79, 88, 96, 86, 85, 98 92, 67, 83, 85, 102, 94, 86, 83 79, 76, 98, 90, 104, 110, 79, 100 79, 59, 76, 88, 92, 90, 74, 96 79, 90, 94, 72, 102, 66, 76, 74 94, 77, 90, 102, 90, 76, 83, 92 90, 66, 90, 102, 96, 106, 104, 106 98, 125, 102, 92, 90, 102, 81, 83 94, 94, 96, 104, 86, 92, 102, 77 71, 92, 86, 108, 94, 76, 86, 88 81, 85, 85, 88, 86, 90, 90, 79 102, 83, 83, 92, 85, 83, 79, 90 83, 92, 88, 102, 86, 102, 102, 100 77, 94, 83, 110, 110, 112, 96, 92 90, 100, 90, 110, 106, 90, 106, 112 90, 92, 114, 110, 112, 121, 130, 121 117, 121, 128, 123, 110, 125, 154, 144 130, 149, 172, 137, 154, 164, 188, 188 177, 202, 199, 237, 231, 213, 243, 231 243, 279, 256, 253, 303, 292, 328, 310 272, 286, 269, 259, 262, 240, 250, 213 216, 222, 240, 210, 228, 190, 196, 202 202, 202, 216, 207, 196, 202, 204, 210 213, 185, 202, 190, 210, 180, 193, 182 196, 164, 196, 202, 182, 190, 193, 193 210, 204, 237, 219, 228, 231, 289, 279 320, 320, 350, 357, 339, 296, 246, 243 243, 169, 166, 161, 180, 149, 159, 169 156, 161, 161, 159, 174, 156, 137, 146 151, 172, 164, 154, 156, 164, 154, 151 164, 166, 139, 174, 144, 137, 149, 121 154, 142, 164, 161, 146, 154, 142, 139 159, 137, 159, 159, 156, 156, 169, 164 190, 185, 210, 202, 193, 204, 185, 188 177, 185, 169, 146, 159, 154, 156, 149 142, 149, 156, 121, 132, 149, 130, 128 139, 132, 159, 125, 177, 119, 164, 144 128, 121, 154, 132, 154, 128, 154, 159 161, 161, 154, 159, 159, 154, 154, 169 166, 164, 130, 156, 164, 137, 154, 154 144, 132, 161, 144, 146, 149, 146, 161 144, 146, 154, 164, 151, 137, 112, 164 123, 159, 146, 149, 137, 172, 161, 180 188, 190, 177, 199, 188, 159, 180, 166 169, 182, 161, 169, 169, 172, 156, 177 180, 156, 146, 137, 146, 151, 177, 154 154, 151, 182, 169, 149, 159, 174, 172 182, 161, 193, 188, 196, 193, 196, 196 204, 199, 188, 154, 159, 161, 185, 149 154, 146, 144, 139, 125, 164, 149, 161 164, 156, 149, 182, 182, 146, 169, 169 180, 190, 188, 159, 185, 161, 177, 174 190, 182, 172, 199, 188, 188, 169, 202 193, 202, 207, 202, 193, 225, 219, 216 210, 204, 190, 180, 185, 169, 159, 216 207, 213, 207, 177, 177, 207, 204, 185 188, 177, 177, 204, 169, 144, 199, 169 156, 151, 172, 154, 193, 177, 154, 166 156, 174, 144, 151, 149, 174, 159, 166 174, 164, 182, 172, 144, 144, 151, 164 161, 177, 172, 196, 225, 196, 237, 219 262, 289, 339, 380, 524, 571, 645, 734 912, 1102, 1282, 1475, 1608, 1529, 1253, 1024 807, 615, 511, 376, 317, 279, 272, 262 266, 256, 216, 216, 210, 202, 177, 213 210, 190, 185, 207, 188, 188, 204, 190 182, 164, 216, 182, 185, 185, 196, 210 207, 240, 228, 222, 266, 234, 213, 228 231, 234, 204, 222, 243, 253, 237, 243 259, 282, 259, 286, 369, 299, 299, 335 286, 320, 299, 317, 310, 299, 262, 272 250, 253, 219, 225, 210, 199, 199, 177 180, 193, 190, 169, 166, 177, 182, 190 177, 169, 185, 188, 188, 180, 169, 172 182, 188, 159, 164, 154, 159, 151, 164 139, 154, 139, 164, 149, 166, 149, 151 156, 159, 137, 172, 149, 135, 144, 151 135, 161, 137, 159, 154, 144, 128, 156 159, 144, 142, 159, 149, 110, 156, 137 130, 121, 121, 117, 146, 149, 151, 130 144, 149, 149, 156, 121, 146, 135, 146 151, 156, 137, 154, 164, 159, 159, 156 151, 199, 146, 182, 169, 154, 172, 164 172, 177, 164, 159, 159, 154, 154, 139 137, 139, 149, 146, 146, 142, 159, 149 144, 159, 154, 137, 180, 154, 151, 146 154, 144, 177, 159, 161, 172, 144, 139 135, 142, 132, 135, 135, 139, 144, 135 139, 132, 144, 144, 132, 132, 112, 125 102, 114, 110, 128, 119, 123, 135, 128 130, 139, 149, 137, 151, 159, 128, 159 154, 137, 139, 137, 123, 164, 146, 121 159, 130, 135, 159, 166, 154, 169, 169 188, 196, 225, 256, 313, 353, 384, 408 449, 480, 454, 392, 335, 279, 292, 202 164, 159, 142, 139, 123, 142, 128, 151 142, 146, 139, 110, 128, 112, 106, 121 125, 119, 123, 100, 102, 110, 102, 112 94, 130, 100, 92, 94, 100, 88, 104 112, 112, 96, 102, 112, 119, 98, 94 104, 96, 106, 110, 110, 96, 108, 117 100, 121, 100, 88, 114, 108, 112, 132 130, 130, 114, 135, 144, 132, 114, 144 112, 94, 117, 102, 114, 114, 108, 112 125, 102, 92, 112, 88, 114, 100, 117 108, 104, 86, 112, 117, 112, 106, 108 121, 104, 102, 128, 102, 123, 98, 108 112, 114, 125, 142, 108, 125, 121, 128 123, 100, 146, 128, 135, 117, 137, 149 132, 119, 132, 149, 154, 154, 161, 174 154, 190, 174, 213, 174, 182, 169, 174 196, 222, 219, 237, 210, 237, 279, 219 262, 246, 272, 286, 234, 269, 272, 243 276, 286, 269, 292, 310, 289, 331, 324 313, 328, 361, 303, 299, 320, 339, 306 299, 313, 313, 279, 243, 262, 237, 246 207, 266, 246, 234, 210, 225, 213, 210 196, 207, 196, 196, 204, 210, 188, 196 219, 188, 177, 196, 193, 193, 196, 193 174, 202, 174, 188, 164, 188, 188, 196 185, 169, 185, 185, 182, 196, 185, 180 188, 182, 169, 185, 339, 174, 188, 172 156, 177, 193, 182, 164, 174, 172, 172 166, 193, 182, 213, 199, 210, 216, 243 289, 269, 296, 276, 256, 272, 266, 253 210, 240, 225, 204, 253, 213, 196, 174 172, 199, 190, 182, 166, 185, 193, 185 185, 188, 202, 193, 213, 172, 193, 202 199, 172, 161, 166, 193, 144, 149, 372 159, 161, 169, 185, 174, 180, 193, 210 172, 182, 188, 174, 207, 202, 188, 199 196, 180, 185, 180, 250, 219, 207, 199 196, 193, 199, 437, 177, 149, 156, 172 188, 180, 166, 159, 166, 172, 159, 156 164, 132, 146, 185, 172, 161, 159, 207 185, 185, 174, 193, 180, 164, 172, 149 161, 159, 149, 135, 164, 139, 144, 130 159, 135, 142, 137, 161, 135, 139, 139 137, 128, 137, 128, 121, 130, 137, 117 112, 137, 144, 125, 132, 121, 135, 142 144, 137, 142, 121, 144, 130, 139, 142 135, 144, 144, 146, 125, 146, 154, 154 159, 196, 207, 225, 253, 237, 272, 250 190, 188, 174, 174, 144, 156, 149, 119 139, 137, 137, 149, 139, 144, 128, 142 142, 123, 123, 132, 142, 139, 142, 139 135, 161, 139, 149, 121, 156, 149, 151 151, 149, 151, 169, 172, 388, 177, 180 185, 177, 156, 154, 149, 128, 144, 139 121, 135, 125, 125, 112, 154, 125, 135 112, 130, 169, 130, 139, 159, 164, 142 135, 139, 121, 161, 123, 149, 130, 146 130, 135, 142, 125, 130, 139, 123, 130 137, 144, 137, 144, 144, 137, 119, 130 117, 123, 130, 98, 123, 106, 121, 117 117, 108, 123, 144, 132, 132, 137, 130 137, 137, 144, 135, 132, 117, 121, 130 154, 144, 100, 135, 128, 159, 142, 139 142, 132, 121, 161, 132, 130, 102, 159 149, 156, 142, 135, 144, 117, 137, 149 130, 135, 149, 144, 159, 174, 185, 193 204, 199, 207, 219, 204, 174, 174, 185 166, 182, 169, 142, 144, 125, 121, 144 139, 117, 128, 112, 125, 130, 128, 128 128, 125, 130, 100, 139, 106, 119, 130 144, 121, 119, 119, 112, 135, 125, 90 117, 108, 114, 104, 114, 106, 130, 112 114, 112, 104, 110, 128, 110, 119, 114 117, 112, 146, 130, 114, 112, 125, 117 121, 102, 108, 108, 108, 114, 135, 128 132, 139, 132, 117, 144, 139, 151, 135 123, 128, 169, 121, 123, 137, 139, 121 114, 121, 106, 132, 119, 110, 104, 123 102, 106, 110, 130, 139, 146, 156, 174 144, 146, 166, 180, 180, 130, 154, 144 146, 144, 146, 110, 154, 144, 117, 130 112, 106, 130, 121, 108, 121, 117, 125 119, 130, 146, 123, 139, 137, 144, 137 146, 142, 146, 185, 161, 156, 159, 180 219, 228, 282, 313, 317, 365, 400, 428 433, 369, 380, 317, 328, 269, 266, 219 262, 190, 190, 164, 151, 166, 177, 172 182, 159, 166, 174, 174, 169, 154, 154 125, 128, 112, 114, 130, 112, 119, 137 119, 125, 114, 110, 104, 108, 100, 102 104, 121, 98, 121, 90, 108, 110, 98 112, 96, 110, 100, 94, 110, 110, 117 114, 104, 104, 90, 96, 110, 86, 92 96, 96, 86, 98, 96, 86, 92, 88 114, 92, 92, 104, 104, 96, 94, 112 110, 86, 94, 94, 98, 88, 96, 100 86, 81, 77, 106, 94, 106, 96, 96 81, 121, 102, 108, 98, 112, 100, 119 86, 79, 94, 102, 71, 83, 88, 88 90, 102, 88, 86, 110, 98, 102, 88 100, 110, 100, 98, 123, 108, 112, 98 117, 100, 92, 92, 106, 94, 96, 104 100, 100, 94, 92, 100, 96, 102, 85 85, 88, 108, 85, 100, 98, 79, 90 86, 90, 79, 85, 77, 96, 88, 96 96, 92, 72, 81, 100, 79, 90, 88 77, 90, 137, 77, 98, 74, 90, 83 86, 85, 96, 88, 86, 83, 110, 88 96, 96, 92, 102, 100, 102, 96, 92 112, 98, 77, 96, 98, 90, 90, 81 98, 98, 96, 85, 96, 85, 102, 88 90, 88, 94, 104, 96, 94, 88, 76 110, 108, 106, 108, 86, 100, 106, 130 137, 130, 159, 154, 156, 196, 240, 237 279, 317, 313, 313, 292, 253, 199, 185 182, 174, 172, 142, 117, 100, 114, 98 88, 96, 86, 88, 79, 102, 108, 85 110, 117, 102, 104, 102, 110, 90, 88 102, 79, 98, 104, 100, 106, 86, 104 108, 102, 86, 83, 72, 85, 114, 77 79, 96, 100, 94, 86, 100, 114, 96 88, 106, 94, 94, 110, 114, 81, 92 90, 106, 92, 98, 112, 96, 92, 90 100, 79, 76, 81, 86, 79, 86, 79 79, 77, 85, 77, 74, 85, 83, 77 108, 79, 88, 88, 76, 74, 76, 90 81, 85, 86, 77, 90, 86, 86, 86 90, 98, 104, 85, 98, 94, 104, 106 71, 79, 96, 92, 85, 79, 92, 90 83, 98, 85, 85, 92, 90, 100, 94 98, 92, 94, 88, 98, 92, 104, 102 88, 86, 110, 104, 94, 110, 110, 98 94, 119, 114, 102, 114, 100, 100, 94 112, 119, 110, 117, 110, 123, 117, 110 125, 123, 128, 121, 123, 119, 128, 125 144, 112, 110, 144, 137, 102, 146, 121 151, 146, 149, 128, 128, 144, 137, 114 123, 154, 164, 154, 164, 149, 159, 177 161, 128, 151, 169, 144, 142, 114, 151 137, 137, 151, 128, 156, 144, 144, 164 154, 149, 159, 132, 151, 149, 151, 156 139, 135, 154, 144, 144, 146, 159, 149 149, 151, 149, 137, 144, 154, 117, 154 174, 188, 196, 210, 213, 243, 213, 228 216, 213, 210, 193, 185, 199, 182, 188 185, 180, 188, 185, 177, 164, 188, 182 193, 172, 164, 193, 185, 177, 188, 188 177, 188, 182, 174, 196, 174, 151, 154 154, 182, 159, 156, 159, 154, 174, 154 156, 180, 159, 144, 139, 151, 164, 164 169, 137, 144, 144, 161, 135, 174, 154 149, 137, 149, 182, 164, 151, 156, 177 159, 180, 174, 210, 177, 180, 196, 182 213, 196, 222, 193, 188, 234, 222, 225 213, 222, 185, 177, 188, 193, 166, 172 172, 159, 156, 146, 144, 128, 149, 121 130, 125, 130, 159, 144, 135, 130, 130 117, 137, 161, 117, 123, 130, 137, 123 119, 121, 110, 112, 110, 121, 119, 112 112, 121, 130, 106, 119, 123, 112, 125 108, 130, 117, 108, 108, 121, 117, 119 121, 117, 106, 110, 139, 121, 100, 121 108, 112, 102, 121, 121, 117, 119, 114 114, 135, 112, 110, 102, 114, 125, 119 94, 102, 114, 119, 98, 117, 100, 117 100, 102, 102, 102, 128, 100, 112, 114 104, 100, 100, 108, 106, 88, 119, 102 104, 102, 102, 137, 128, 114, 112, 100 121, 112, 130, 125, 128, 135, 100, 110 102, 114, 119, 121, 125, 121, 104, 125 142, 125, 125, 117, 121, 112, 106, 128 110, 119, 108, 117, 125, 100, 106, 100 96, 104, 137, 132, 104, 119, 106, 102 137, 112, 142, 128, 146, 154, 130, 125 146, 130, 142, 149, 161, 174, 166, 216 216, 231, 266, 279, 324, 310, 292, 253 231, 234, 234, 246, 228, 193, 228, 172 185, 159, 139, 146, 149, 144, 156, 166 146, 130, 130, 128, 156, 144, 128, 132 132, 130, 151, 154, 142, 139, 142, 144 128, 123, 137, 142, 169, 139, 139, 121 135, 164, 139, 164, 142, 169, 193, 166 172, 151, 161, 174, 164, 156, 164, 190 182, 182, 190, 188, 193, 199, 216, 213 182, 164, 204, 196, 193, 204, 202, 210 404, 216, 228, 234, 202, 237, 228, 243 266, 243, 256, 282, 256, 266, 272, 256 213, 243, 240, 243, 250, 228, 219, 222 219, 207, 240, 210, 207, 202, 207, 210 219, 199, 204, 225, 202, 202, 177, 188 193, 188, 196, 177, 185, 161, 169, 185 164, 151, 159, 151, 149, 161, 149, 125 156, 169, 144, 137, 137, 135, 137, 144 146, 144, 119, 110, 139, 121, 121, 110 112, 132, 123, 102, 117, 130, 108, 112 123, 114, 110, 142, 114, 100, 102, 104 110, 108, 121, 110, 123, 98, 110, 119 96, 108, 108, 119, 86, 96, 121, 112 130, 106, 104, 123, 100, 121, 123, 117 119, 123, 130, 108, 112, 119, 121, 104 132, 132, 130, 142, 137, 137, 123, 149 144, 156, 142, 156, 144, 135, 121, 114 130, 132, 132, 142, 110, 117, 121, 114 135, 119, 100, 106, 114, 108, 106, 110 88, 119, 119, 96, 112, 104, 106, 100 92, 104, 92, 96, 106, 98, 102, 98 114, 102, 123, 102, 117, 142, 110, 117 121, 106, 94, 121, 102, 102, 123, 96 130, 114, 119, 100, 117, 104, 121, 104 110, 121, 121, 96, 98, 112, 117, 119 94, 94, 123, 106, 112, 98, 112, 119 108, 114, 102, 112, 112, 106, 104, 125 108, 96, 123, 94, 110, 108, 130, 132 104, 125, 112, 117, 110, 123, 114, 128 108, 114, 151, 154, 151, 135, 142, 130 144, 142, 121, 125, 114, 125, 123, 114 125, 110, 110, 128, 94, 119, 94, 94 98, 88, 104, 104, 100, 108, 96, 96 86, 104, 114, 98, 88, 102, 102, 106 92, 102, 96, 92, 110, 102, 102, 98 98, 96, 110, 128, 110, 121, 98, 110 112, 98, 112, 98, 114, 100, 100, 128 106, 114, 112, 119, 130, 117, 104, 108 125, 119, 139, 156, 142, 169, 180, 182 190, 222, 216, 216, 177, 196, 169, 137 172, 182, 185, 185, 174, 174, 169, 161 164, 202, 199, 219, 243, 234, 250, 228 237, 231, 216, 204, 204, 237, 246, 250 213, 243, 219, 177, 180, 137, 174, 164 161, 151, 125, 144, 135, 117, 119, 135 100, 121, 106, 108, 117, 121, 123, 114 135, 121, 146, 137, 132, 121, 106, 132 90, 110, 121, 146, 149, 149, 202, 202 190, 154, 119, 135, 108, 125, 137, 137 164, 149, 166, 151, 149, 130, 117, 128 156, 121, 139, 119, 137, 128, 128, 137 130, 130, 135, 125, 123, 112, 128, 114 125, 114, 139, 125, 112, 110, 144, 106 114,/