SampleIdent,907A-13-3/84,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 9-aug-1993 21:49,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 114, 123, 121, 102, 128, 128, 121, 108 102, 121, 119, 121, 108, 114, 139, 117 114, 119, 119, 94, 123, 114, 119, 117 130, 117, 119, 117, 123, 119, 139, 119 123, 112, 104, 137, 121, 119, 119, 135 121, 139, 121, 119, 146, 130, 125, 137 128, 128, 137, 137, 149, 151, 137, 139 151, 135, 156, 139, 139, 146, 166, 139 130, 151, 154, 142, 128, 135, 154, 161 149, 142, 135, 164, 161, 159, 132, 166 164, 161, 154, 135, 130, 144, 154, 151 149, 180, 164, 149, 154, 144, 106, 137 142, 151, 156, 146, 156, 149, 172, 137 166, 161, 146, 172, 164, 144, 144, 128 137, 139, 135, 128, 144, 144, 142, 154 130, 135, 151, 144, 169, 144, 142, 144 132, 137, 139, 137, 159, 114, 144, 121 132, 125, 139, 144, 146, 121, 139, 144 137, 137, 149, 130, 146, 125, 130, 151 135, 121, 137, 123, 139, 130, 128, 137 128, 130, 144, 154, 144, 137, 112, 119 119, 123, 130, 144, 149, 121, 114, 125 125, 125, 123, 130, 161, 112, 144, 119 142, 130, 144, 146, 123, 161, 161, 132 139, 135, 121, 119, 130, 121, 114, 125 110, 112, 108, 123, 106, 112, 106, 106 110, 132, 96, 106, 130, 108, 114, 123 106, 100, 94, 102, 108, 108, 123, 114 96, 98, 114, 104, 92, 83, 98, 121 112, 100, 100, 100, 110, 106, 104, 92 94, 104, 114, 106, 94, 125, 86, 92 110, 92, 98, 106, 114, 104, 100, 96 98, 86, 85, 96, 90, 88, 88, 100 114, 90, 88, 98, 108, 98, 92, 86 98, 98, 106, 112, 119, 90, 86, 104 102, 128, 102, 121, 96, 96, 100, 102 88, 104, 100, 102, 94, 102, 98, 90 102, 96, 104, 102, 88, 100, 92, 90 110, 86, 108, 92, 102, 114, 104, 108 119, 85, 100, 79, 86, 98, 88, 98 102, 119, 96, 104, 96, 104, 110, 86 96, 104, 92, 92, 92, 117, 96, 100 94, 102, 79, 94, 85, 96, 100, 96 90, 104, 110, 104, 100, 110, 98, 110 104, 128, 90, 125, 128, 96, 108, 114 108, 119, 119, 121, 104, 121, 117, 125 123, 119, 132, 108, 137, 114, 121, 94 92, 92, 98, 98, 117, 106, 90, 72 90, 102, 81, 96, 94, 85, 92, 76 77, 88, 88, 94, 92, 86, 102, 86 108, 108, 102, 92, 67, 102, 94, 90 96, 102, 114, 90, 92, 94, 102, 83 86, 100, 79, 88, 100, 86, 104, 96 98, 96, 94, 90, 85, 92, 100, 92 96, 100, 96, 98, 104, 98, 102, 88 114, 106, 76, 94, 100, 86, 88, 108 90, 83, 79, 102, 86, 88, 96, 69 92, 85, 102, 104, 90, 77, 104, 71 92, 100, 74, 77, 94, 98, 90, 123 112, 96, 96, 79, 83, 128, 90, 88 106, 88, 86, 90, 90, 106, 83, 86 88, 77, 92, 85, 92, 90, 98, 104 88, 100, 88, 86, 92, 96, 92, 96 71, 83, 100, 71, 88, 102, 90, 83 110, 79, 94, 98, 94, 96, 90, 102 92, 77, 74, 102, 94, 71, 100, 102 88, 102, 85, 86, 86, 88, 102, 112 92, 96, 110, 106, 104, 110, 85, 81 90, 88, 90, 92, 96, 94, 77, 96 90, 92, 86, 96, 90, 86, 76, 92 90, 92, 100, 90, 88, 102, 88, 88 86, 85, 102, 79, 90, 88, 92, 85 100, 86, 98, 86, 96, 79, 85, 86 108, 94, 102, 85, 100, 85, 92, 98 96, 96, 88, 98, 83, 100, 88, 88 92, 98, 88, 86, 77, 77, 88, 79 88, 94, 85, 98, 88, 96, 104, 114 94, 86, 92, 94, 104, 98, 100, 98 102, 104, 96, 100, 100, 98, 100, 98 112, 117, 114, 104, 102, 94, 108, 106 112, 114, 106, 92, 112, 110, 104, 104 110, 92, 92, 112, 110, 104, 98, 90 98, 90, 112, 104, 106, 83, 96, 100 104, 104, 96, 110, 106, 92, 108, 102 92, 100, 83, 83, 85, 100, 102, 108 123, 110, 112, 104, 96, 412, 88, 108 112, 98, 125, 104, 112, 106, 102, 106 96, 94, 121, 104, 114, 121, 108, 119 139, 130, 128, 114, 117, 121, 139, 151 161, 149, 146, 146, 137, 166, 169, 188 210, 174, 164, 182, 180, 169, 204, 207 237, 207, 225, 234, 222, 250, 253, 228 237, 246, 259, 240, 240, 228, 243, 222 202, 222, 199, 225, 207, 190, 199, 213 174, 188, 182, 154, 196, 172, 185, 182 182, 219, 199, 177, 193, 193, 188, 177 190, 182, 188, 159, 182, 180, 204, 190 202, 182, 182, 202, 207, 219, 188, 231 253, 231, 237, 262, 276, 292, 272, 259 259, 210, 213, 180, 180, 174, 185, 177 164, 151, 169, 169, 151, 180, 149, 169 169, 169, 185, 193, 190, 159, 151, 135 164, 166, 154, 149, 159, 182, 161, 137 174, 159, 174, 128, 151, 142, 159, 164 169, 174, 169, 166, 185, 169, 164, 182 174, 193, 219, 219, 210, 213, 204, 193 182, 190, 154, 159, 146, 164, 185, 135 166, 174, 146, 142, 125, 164, 177, 142 172, 159, 174, 164, 169, 154, 146, 199 164, 135, 161, 159, 166, 156, 164, 151 159, 164, 119, 156, 146, 180, 166, 182 159, 144, 159, 144, 154, 154, 151, 149 169, 166, 161, 149, 172, 151, 144, 154 180, 185, 154, 161, 177, 169, 159, 139 159, 154, 164, 166, 149, 196, 182, 188 146, 169, 174, 177, 213, 199, 182, 190 169, 182, 172, 185, 166, 159, 210, 164 161, 149, 169, 169, 174, 174, 151, 159 193, 151, 166, 172, 174, 156, 159, 149 149, 185, 164, 159, 185, 151, 172, 177 177, 188, 174, 185, 177, 182, 154, 182 166, 169, 161, 180, 182, 182, 210, 222 199, 199, 188, 196, 166, 177, 164, 174 182, 180, 169, 174, 174, 164, 154, 177 193, 190, 161, 177, 180, 182, 177, 161 193, 177, 174, 177, 177, 193, 193, 185 196, 199, 202, 188, 159, 196, 154, 174 185, 177, 182, 202, 180, 174, 185, 196 185, 169, 185, 172, 190, 172, 174, 166 161, 169, 172, 166, 149, 159, 180, 166 151, 169, 166, 182, 185, 190, 180, 185 180, 166, 156, 159, 164, 182, 169, 180 185, 159, 188, 172, 204, 166, 185, 180 210, 196, 213, 240, 289, 269, 299, 339 424, 529, 543, 660, 734, 751, 824, 773 740, 635, 524, 376, 365, 296, 253, 240 188, 216, 216, 225, 202, 196, 202, 210 169, 177, 177, 164, 188, 193, 180, 193 185, 196, 185, 193, 182, 213, 207, 180 180, 207, 202, 222, 199, 196, 225, 228 234, 246, 231, 222, 250, 207, 231, 222 222, 250, 250, 276, 320, 310, 320, 328 320, 317, 299, 320, 292, 313, 282, 493 296, 276, 266, 219, 240, 225, 156, 182 177, 177, 177, 207, 182, 164, 174, 174 199, 164, 174, 185, 164, 169, 180, 177 159, 174, 169, 188, 159, 164, 164, 172 135, 161, 144, 156, 137, 190, 144, 159 166, 159, 149, 166, 130, 154, 142, 166 159, 172, 146, 149, 164, 164, 156, 135 169, 174, 149, 156, 130, 164, 159, 144 156, 137, 149, 169, 166, 188, 135, 139 154, 151, 154, 149, 174, 180, 154, 164 169, 188, 177, 177, 174, 199, 219, 210 199, 204, 210, 177, 225, 182, 172, 199 177, 180, 188, 154, 142, 185, 137, 142 169, 146, 146, 130, 159, 151, 182, 169 149, 169, 146, 161, 177, 190, 174, 177 172, 169, 182, 185, 166, 146, 159, 164 185, 159, 177, 149, 169, 161, 172, 177 161, 154, 169, 164, 164, 137, 156, 149 159, 146, 125, 110, 146, 132, 130, 139 149, 123, 154, 151, 139, 139, 154, 146 161, 132, 135, 135, 144, 151, 164, 139 132, 139, 142, 144, 177, 149, 154, 169 172, 156, 190, 185, 216, 256, 331, 380 350, 428, 467, 511, 511, 445, 388, 372 320, 243, 213, 164, 146, 174, 154, 154 130, 154, 139, 149, 130, 135, 139, 125 130, 121, 130, 110, 114, 110, 100, 137 104, 121, 121, 110, 110, 125, 114, 128 110, 121, 128, 112, 121, 112, 106, 110 130, 110, 98, 121, 96, 110, 100, 108 119, 117, 117, 114, 119, 108, 125, 100 137, 114, 132, 149, 149, 154, 166, 151 149, 130, 123, 128, 125, 123, 100, 132 121, 114, 125, 123, 119, 125, 128, 104 121, 98, 132, 108, 108, 119, 110, 128 123, 112, 104, 121, 137, 114, 132, 125 137, 139, 135, 128, 112, 142, 117, 123 121, 130, 146, 137, 110, 119, 137, 146 132, 139, 139, 159, 146, 130, 154, 146 146, 149, 135, 154, 146, 174, 149, 164 177, 164, 193, 164, 193, 207, 210, 188 210, 207, 234, 204, 219, 210, 222, 199 210, 216, 237, 259, 219, 228, 231, 204 228, 266, 266, 266, 250, 272, 282, 253 246, 259, 292, 234, 256, 237, 256, 219 210, 231, 228, 213, 213, 210, 188, 185 180, 190, 164, 182, 199, 193, 166, 202 207, 222, 177, 174, 219, 204, 188, 199 190, 207, 182, 188, 202, 172, 193, 180 190, 196, 207, 185, 190, 159, 182, 204 169, 164, 169, 172, 182, 149, 161, 159 169, 164, 159, 159, 161, 135, 132, 180 135, 132, 135, 151, 154, 169, 166, 164 174, 199, 202, 210, 210, 204, 246, 193 240, 207, 196, 180, 174, 185, 169, 174 169, 144, 144, 139, 151, 156, 144, 154 172, 156, 137, 151, 159, 174, 172, 174 188, 199, 180, 185, 161, 144, 161, 154 149, 161, 151, 146, 161, 144, 130, 137 156, 161, 154, 156, 149, 164, 156, 159 159, 161, 172, 169, 190, 146, 159, 166 139, 193, 159, 180, 180, 164, 154, 161 169, 149, 156, 114, 123, 130, 123, 121 146, 142, 130, 137, 137, 121, 149, 144 135, 121, 149, 151, 135, 151, 149, 139 166, 279, 174, 169, 144, 146, 159, 151 151, 151, 144, 144, 125, 123, 130, 125 128, 100, 142, 117, 106, 110, 125, 117 142, 128, 130, 114, 121, 117, 112, 130 125, 137, 121, 154, 123, 125, 125, 86 106, 119, 121, 137, 130, 132, 121, 121 156, 144, 139, 151, 139, 164, 193, 159 196, 139, 139, 172, 164, 164, 137, 144 156, 132, 128, 123, 121, 110, 112, 112 144, 128, 125, 125, 121, 102, 125, 137 117, 117, 106, 149, 110, 121, 130, 119 132, 112, 137, 128, 144, 144, 128, 151 164, 135, 146, 139, 149, 154, 139, 119 125, 135, 128, 121, 112, 137, 128, 121 110, 117, 142, 142, 154, 121, 151, 130 161, 132, 135, 135, 135, 142, 144, 137 123, 144, 142, 123, 128, 154, 121, 142 112, 125, 149, 139, 110, 135, 128, 110 119, 114, 130, 106, 137, 110, 128, 112 130, 117, 92, 119, 112, 132, 117, 94 121, 112, 117, 114, 123, 100, 137, 121 128, 125, 144, 98, 114, 128, 121, 135 110, 121, 125, 121, 146, 102, 123, 139 137, 137, 164, 137, 135, 130, 149, 156 156, 159, 161, 177, 164, 154, 156, 161 180, 177, 182, 180, 182, 169, 161, 169 185, 166, 146, 161, 128, 139, 119, 123 121, 112, 100, 108, 121, 128, 123, 117 125, 110, 121, 100, 125, 106, 121, 114 121, 121, 125, 112, 104, 128, 104, 112 112, 117, 106, 144, 100, 106, 114, 117 106, 112, 112, 106, 117, 114, 114, 104 104, 114, 125, 128, 92, 119, 112, 110 108, 117, 108, 108, 102, 100, 102, 100 114, 108, 108, 106, 119, 119, 88, 132 128, 130, 132, 154, 121, 130, 130, 128 119, 110, 137, 108, 137, 137, 100, 125 108, 135, 128, 119, 125, 121, 128, 123 125, 119, 137, 121, 121, 132, 159, 172 174, 185, 202, 182, 182, 177, 161, 149 156, 144, 149, 142, 142, 144, 128, 142 117, 130, 125, 117, 130, 130, 137, 130 117, 121, 156, 121, 108, 159, 149, 144 154, 154, 204, 213, 213, 259, 299, 303 357, 335, 384, 346, 350, 350, 313, 282 269, 266, 222, 190, 180, 177, 161, 146 135, 159, 151, 149, 169, 123, 135, 128 146, 135, 142, 110, 125, 119, 125, 132 117, 128, 112, 112, 98, 88, 100, 90 98, 104, 100, 90, 106, 94, 102, 100 106, 106, 102, 110, 110, 112, 90, 96 98, 83, 85, 94, 102, 83, 100, 100 96, 108, 104, 96, 90, 121, 88, 98 110, 104, 85, 90, 90, 98, 119, 94 88, 104, 86, 100, 104, 76, 98, 100 92, 96, 108, 100, 94, 94, 119, 88 114, 88, 96, 112, 92, 106, 125, 106 90, 96, 90, 112, 92, 106, 85, 90 72, 94, 96, 90, 85, 94, 121, 94 90, 94, 104, 119, 112, 94, 94, 85 86, 108, 79, 100, 77, 83, 102, 94 96, 90, 88, 77, 98, 102, 110, 88 90, 100, 104, 79, 102, 90, 92, 88 69, 96, 90, 102, 85, 94, 86, 96 88, 69, 92, 71, 77, 102, 100, 88 79, 96, 98, 104, 83, 79, 92, 83 81, 85, 61, 86, 90, 110, 85, 98 79, 85, 125, 102, 88, 90, 85, 108 102, 96, 94, 102, 94, 104, 104, 110 98, 104, 98, 104, 88, 96, 88, 100 90, 92, 96, 90, 90, 98, 112, 106 112, 114, 119, 92, 108, 100, 96, 104 119, 90, 108, 130, 108, 137, 123, 159 156, 161, 190, 196, 202, 202, 210, 222 180, 142, 159, 156, 135, 123, 110, 135 83, 100, 79, 108, 106, 77, 76, 100 83, 88, 119, 110, 114, 108, 108, 119 94, 117, 110, 108, 108, 104, 102, 92 98, 98, 123, 106, 94, 94, 92, 98 104, 88, 96, 112, 100, 100, 108, 121 108, 102, 96, 110, 88, 119, 100, 96 88, 94, 92, 81, 86, 104, 96, 90 100, 90, 92, 106, 76, 85, 94, 100 79, 106, 86, 102, 96, 92, 76, 96 85, 83, 88, 86, 88, 77, 85, 106 81, 77, 86, 92, 100, 86, 94, 86 85, 112, 117, 98, 104, 106, 108, 106 110, 92, 92, 98, 100, 94, 90, 79 98, 108, 106, 94, 88, 98, 117, 104 79, 100, 88, 106, 112, 123, 106, 119 96, 106, 92, 108, 102, 110, 96, 123 130, 96, 92, 108, 106, 132, 106, 121 96, 125, 102, 86, 125, 112, 128, 106 123, 121, 121, 121, 137, 112, 125, 130 135, 130, 114, 119, 125, 110, 142, 117 102, 119, 117, 135, 121, 142, 125, 146 128, 132, 142, 154, 130, 146, 159, 154 146, 137, 156, 137, 130, 125, 121, 135 144, 137, 144, 161, 169, 121, 156, 137 119, 130, 128, 137, 117, 151, 149, 121 154, 151, 137, 156, 132, 151, 149, 139 128, 139, 156, 137, 149, 154, 121, 144 161, 149, 144, 144, 149, 159, 172, 213 193, 154, 149, 190, 164, 190, 159, 180 156, 166, 146, 130, 156, 142, 137, 172 146, 146, 146, 135, 149, 128, 159, 164 125, 161, 164, 159, 135, 149, 130, 159 151, 159, 137, 146, 161, 161, 142, 130 154, 151, 121, 142, 135, 130, 149, 142 172, 151, 142, 130, 137, 142, 137, 135 139, 146, 149, 156, 149, 156, 151, 146 156, 146, 149, 196, 185, 190, 199, 204 185, 193, 185, 190, 204, 228, 196, 228 225, 231, 202, 210, 231, 213, 202, 213 185, 202, 185, 185, 169, 174, 166, 142 125, 125, 139, 114, 130, 123, 125, 135 130, 112, 119, 132, 117, 106, 125, 130 130, 119, 128, 112, 112, 121, 108, 130 119, 130, 98, 114, 108, 108, 121, 132 117, 112, 100, 94, 130, 117, 106, 130 108, 110, 108, 102, 119, 119, 117, 104 106, 114, 102, 94, 112, 108, 130, 106 112, 94, 137, 114, 104, 121, 108, 114 121, 121, 112, 100, 106, 130, 123, 119 119, 100, 102, 102, 117, 83, 106, 114 108, 110, 98, 132, 104, 102, 128, 108 94, 123, 106, 112, 86, 117, 108, 128 100, 121, 121, 114, 130, 114, 110, 102 90, 128, 114, 100, 94, 121, 112, 123 104, 104, 130, 121, 104, 98, 121, 102 104, 130, 108, 125, 125, 137, 114, 130 90, 117, 119, 106, 100, 114, 104, 121 139, 125, 108, 123, 119, 114, 121, 125 125, 130, 121, 154, 135, 154, 130, 151 137, 169, 169, 174, 182, 207, 222, 199 222, 193, 196, 225, 193, 169, 177, 185 182, 199, 190, 164, 151, 139, 149, 130 139, 151, 137, 139, 108, 154, 100, 125 135, 121, 117, 149, 128, 135, 128, 156 132, 130, 119, 132, 159, 135, 166, 137 144, 156, 123, 137, 154, 132, 149, 130 156, 156, 137, 154, 161, 156, 169, 177 180, 180, 164, 159, 166, 172, 185, 132 174, 169, 172, 174, 180, 202, 193, 196 174, 169, 169, 190, 199, 202, 207, 219 207, 199, 202, 210, 199, 199, 196, 207 207, 196, 202, 210, 225, 199, 196, 202 196, 169, 193, 185, 174, 193, 193, 174 164, 166, 180, 166, 151, 166, 196, 182 166, 180, 166, 182, 193, 156, 174, 174 169, 164, 169, 164, 154, 169, 164, 154 149, 154, 151, 137, 142, 137, 149, 149 144, 149, 125, 119, 139, 139, 137, 132 128, 130, 100, 117, 139, 135, 139, 130 125, 149, 98, 112, 135, 108, 121, 112 144, 114, 104, 137, 110, 114, 119, 123 137, 114, 130, 121, 121, 98, 121, 96 106, 106, 121, 114, 106, 128, 121, 121 100, 88, 121, 108, 123, 110, 114, 112 130, 130, 144, 114, 144, 121, 128, 130 125, 135, 125, 132, 128, 144, 149, 144 102, 139, 137, 110, 144, 112, 164, 130 125, 125, 135, 106, 114, 100, 114, 228 106, 96, 128, 96, 108, 112, 94, 125 96, 108, 94, 108, 100, 98, 102, 117 114, 98, 128, 88, 100, 106, 125, 114 139, 125, 110, 121, 110, 119, 132, 125 135, 149, 144, 112, 123, 110, 117, 114 114, 112, 130, 108, 114, 102, 110, 114 98, 123, 114, 98, 100, 108, 110, 125 121, 114, 119, 104, 106, 108, 125, 119 102, 114, 125, 132, 117, 92, 119, 137 119, 119, 135, 110, 108, 123, 117, 137 106, 112, 119, 123, 135, 106, 142, 164 164, 144, 174, 159, 154, 146, 149, 149 139, 130, 128, 135, 130, 121, 110, 128 110, 125, 108, 114, 86, 119, 104, 114 119, 117, 88, 100, 108, 114, 96, 106 94, 102, 128, 100, 106, 92, 110, 117 104, 114, 102, 106, 135, 100, 102, 119 92, 102, 117, 132, 96, 96, 121, 112 123, 123, 119, 100, 102, 110, 117, 108 130, 121, 86, 112, 108, 121, 123, 146 125, 146, 135, 164, 154, 174, 156, 164 169, 146, 128, 142, 128, 166, 128, 128 156, 149, 149, 172, 137, 169, 169, 213 207, 202, 225, 202, 196, 207, 193, 174 213, 196, 246, 213, 202, 199, 151, 156 135, 151, 188, 144, 146, 144, 135, 137 119, 121, 98, 130, 123, 121, 125, 130 125, 121, 108, 125, 102, 123, 128, 123 130, 128, 110, 121, 130, 94, 106, 117 121, 108, 108, 106, 119, 117, 119, 125 132, 121, 117, 106, 121, 112, 137, 108 117, 125, 119, 146, 121, 151, 117, 125 144, 114, 130, 117, 137, 121, 128, 108 130, 130, 130, 114, 104, 137, 117, 132 98, 125, 125, 128, 123, 128, 112, 123 135,/