SampleIdent,907A-14-3/26,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 9-aug-1993 22:45,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 83, 79, 81, 104, 92, 100, 90, 86 90, 92, 86, 98, 102, 79, 67, 90 98, 96, 85, 85, 77, 102, 85, 83 94, 83, 102, 96, 76, 71, 85, 90 90, 85, 88, 77, 90, 79, 88, 96 81, 90, 90, 85, 92, 106, 76, 94 119, 106, 96, 102, 79, 102, 117, 106 98, 100, 98, 104, 94, 86, 77, 85 94, 104, 94, 98, 114, 100, 119, 98 96, 100, 119, 108, 125, 121, 114, 104 100, 94, 108, 104, 94, 121, 100, 128 112, 117, 104, 92, 106, 117, 106, 110 114, 110, 114, 121, 108, 100, 119, 92 114, 108, 119, 121, 90, 94, 130, 98 119, 365, 108, 100, 112, 108, 117, 108 100, 102, 121, 102, 119, 102, 114, 102 108, 114, 100, 110, 123, 125, 121, 114 92, 106, 123, 104, 114, 112, 92, 123 117, 104, 123, 108, 119, 121, 85, 119 119, 121, 102, 112, 108, 98, 88, 98 104, 96, 110, 100, 112, 108, 102, 94 106, 110, 98, 121, 92, 94, 100, 114 102, 86, 102, 83, 86, 106, 98, 94 104, 104, 108, 117, 117, 98, 106, 117 110, 104, 102, 106, 98, 110, 104, 121 86, 102, 102, 92, 104, 83, 106, 96 96, 100, 114, 88, 96, 112, 86, 114 102, 90, 92, 83, 106, 79, 114, 88 90, 96, 76, 90, 86, 104, 100, 94 86, 106, 100, 100, 85, 102, 83, 85 83, 100, 86, 94, 88, 88, 112, 81 85, 108, 114, 94, 86, 85, 88, 96 94, 94, 108, 79, 88, 114, 69, 117 96, 92, 88, 85, 86, 72, 88, 100 79, 83, 83, 100, 112, 69, 86, 86 86, 85, 85, 81, 106, 86, 100, 100 76, 71, 77, 86, 90, 85, 83, 94 81, 94, 94, 85, 90, 98, 72, 79 85, 88, 90, 66, 94, 90, 100, 88 83, 104, 83, 79, 83, 79, 88, 76 77, 424, 76, 108, 83, 104, 88, 85 92, 98, 102, 86, 102, 79, 76, 88 72, 85, 104, 102, 79, 88, 98, 83 98, 86, 86, 71, 81, 90, 85, 92 102, 71, 94, 77, 88, 117, 77, 90 86, 102, 94, 94, 96, 102, 85, 83 85, 94, 74, 88, 100, 108, 85, 104 90, 90, 96, 88, 79, 81, 79, 81 104, 108, 77, 67, 79, 79, 67, 106 79, 102, 74, 92, 92, 79, 67, 100 90, 102, 92, 77, 88, 88, 81, 72 72, 90, 102, 77, 83, 71, 94, 94 76, 86, 77, 90, 102, 85, 86, 85 79, 96, 76, 74, 85, 100, 94, 83 90, 76, 77, 96, 72, 92, 67, 88 98, 72, 76, 85, 86, 79, 79, 98 79, 86, 74, 72, 85, 77, 83, 85 85, 64, 71, 76, 92, 88, 88, 79 77, 86, 83, 83, 67, 88, 72, 92 98, 92, 77, 86, 76, 94, 61, 79 96, 86, 83, 90, 76, 86, 86, 79 72, 83, 83, 83, 83, 85, 83, 86 81, 96, 94, 77, 85, 77, 72, 77 85, 69, 92, 86, 86, 72, 94, 76 106, 77, 77, 81, 72, 83, 72, 76 81, 83, 67, 72, 77, 71, 88, 79 92, 86, 76, 72, 77, 62, 72, 83 88, 83, 88, 56, 74, 69, 83, 83 69, 90, 67, 104, 100, 77, 76, 81 64, 76, 77, 66, 77, 79, 72, 92 77, 67, 67, 71, 67, 83, 76, 66 77, 88, 67, 72, 88, 88, 88, 83 64, 79, 94, 74, 79, 72, 76, 76 71, 77, 81, 98, 77, 85, 98, 83 72, 94, 83, 72, 85, 92, 79, 79 83, 88, 86, 86, 88, 79, 77, 100 77, 72, 83, 85, 77, 85, 85, 85 67, 83, 83, 83, 77, 81, 67, 76 100, 85, 90, 88, 96, 96, 92, 74 83, 88, 81, 90, 81, 83, 88, 404 76, 96, 83, 88, 94, 328, 106, 83 88, 94, 85, 92, 98, 77, 92, 94 108, 86, 102, 102, 106, 100, 90, 81 96, 77, 96, 96, 81, 98, 88, 106 92, 98, 83, 96, 123, 77, 85, 112 100, 92, 112, 86, 106, 98, 106, 94 86, 83, 98, 88, 102, 114, 92, 96 121, 112, 83, 83, 119, 102, 110, 94 98, 117, 86, 96, 98, 119, 102, 110 121, 98, 117, 112, 112, 121, 125, 119 128, 114, 114, 137, 135, 121, 117, 130 144, 166, 137, 174, 149, 154, 177, 166 172, 180, 164, 188, 174, 196, 202, 199 174, 188, 216, 188, 185, 149, 169, 185 185, 154, 182, 154, 174, 149, 144, 164 185, 169, 156, 161, 149, 144, 172, 151 159, 166, 137, 164, 149, 174, 130, 154 177, 174, 154, 146, 166, 164, 164, 177 137, 166, 161, 156, 185, 180, 161, 202 169, 193, 202, 213, 228, 204, 193, 196 193, 188, 144, 182, 154, 182, 151, 174 154, 154, 137, 130, 169, 139, 149, 144 149, 119, 130, 144, 164, 139, 149, 123 149, 146, 123, 137, 164, 139, 139, 130 137, 137, 159, 137, 149, 132, 146, 137 137, 135, 132, 139, 151, 132, 132, 132 151, 139, 159, 177, 154, 174, 164, 159 174, 151, 202, 177, 166, 161, 159, 151 144, 144, 130, 139, 132, 135, 144, 132 132, 128, 169, 125, 149, 132, 135, 130 164, 146, 149, 146, 169, 125, 144, 146 144, 130, 154, 154, 166, 156, 161, 149 164, 146, 132, 151, 144, 119, 130, 144 154, 166, 166, 149, 135, 137, 130, 159 139, 135, 135, 159, 149, 130, 154, 139 144, 151, 139, 151, 119, 149, 166, 144 149, 159, 172, 139, 154, 159, 180, 185 174, 182, 188, 169, 164, 149, 149, 146 139, 172, 182, 159, 156, 132, 130, 137 146, 169, 139, 149, 154, 177, 149, 154 146, 161, 193, 177, 161, 142, 169, 151 146, 144, 177, 174, 164, 149, 161, 132 144, 149, 154, 161, 166, 174, 169, 149 164, 156, 174, 164, 142, 142, 144, 166 139, 164, 166, 164, 164, 123, 159, 161 166, 151, 151, 166, 151, 169, 146, 156 169, 137, 169, 149, 177, 154, 174, 154 161, 180, 130, 164, 166, 185, 177, 177 164, 172, 177, 166, 161, 174, 164, 154 185, 182, 159, 154, 169, 159, 174, 144 151, 166, 174, 151, 177, 146, 149, 154 159, 166, 177, 144, 166, 164, 151, 151 161, 182, 180, 182, 149, 164, 144, 159 166, 182, 149, 146, 182, 182, 177, 193 169, 199, 196, 207, 219, 240, 310, 339 365, 357, 388, 404, 424, 445, 437, 416 424, 441, 445, 437, 441, 365, 372, 306 289, 237, 243, 216, 219, 199, 196, 207 182, 182, 196, 174, 159, 169, 190, 188 156, 199, 185, 156, 196, 185, 190, 169 188, 196, 216, 185, 188, 196, 199, 202 185, 210, 213, 225, 204, 225, 213, 222 225, 216, 222, 246, 259, 213, 269, 286 289, 246, 299, 286, 286, 256, 256, 246 246, 246, 188, 216, 219, 207, 207, 199 225, 216, 193, 202, 188, 204, 164, 172 169, 154, 169, 182, 174, 172, 180, 177 177, 177, 161, 180, 177, 154, 161, 172 174, 177, 164, 149, 161, 156, 154, 142 154, 156, 144, 166, 137, 149, 151, 128 137, 144, 151, 164, 159, 161, 142, 149 156, 137, 151, 144, 137, 144, 128, 146 146, 137, 130, 125, 149, 156, 137, 130 154, 151, 144, 135, 159, 166, 182, 149 177, 159, 154, 174, 164, 164, 146, 146 177, 188, 174, 182, 174, 154, 172, 182 174, 204, 174, 151, 177, 169, 146, 142 149, 142, 159, 156, 135, 151, 149, 144 135, 164, 159, 144, 151, 161, 166, 146 137, 169, 164, 164, 172, 166, 146, 172 182, 144, 135, 144, 164, 156, 142, 159 164, 166, 174, 142, 125, 159, 154, 146 132, 142, 174, 156, 137, 154, 146, 125 125, 123, 135, 130, 132, 142, 159, 125 149, 130, 128, 137, 132, 135, 135, 144 123, 137, 142, 130, 130, 130, 169, 144 161, 174, 188, 210, 250, 237, 276, 320 335, 310, 353, 331, 331, 331, 353, 346 353, 328, 299, 292, 243, 216, 231, 174 182, 151, 132, 130, 130, 146, 161, 125 112, 137, 102, 117, 110, 108, 114, 114 108, 114, 94, 112, 125, 114, 96, 108 102, 121, 110, 102, 100, 117, 121, 102 117, 85, 86, 121, 104, 102, 106, 92 121, 121, 128, 100, 119, 130, 128, 94 123, 130, 159, 159, 156, 144, 169, 144 128, 156, 146, 151, 132, 146, 130, 154 137, 130, 125, 144, 112, 106, 110, 108 117, 106, 117, 94, 106, 88, 132, 112 96, 108, 114, 121, 119, 119, 114, 100 130, 100, 106, 94, 112, 149, 112, 132 117, 132, 125, 112, 112, 121, 146, 142 119, 130, 125, 117, 125, 125, 154, 123 144, 139, 132, 139, 156, 144, 164, 137 154, 172, 164, 169, 172, 164, 174, 180 188, 188, 190, 185, 182, 199, 213, 210 225, 210, 222, 202, 207, 196, 202, 222 213, 234, 256, 228, 243, 253, 204, 259 222, 266, 207, 246, 228, 225, 231, 188 216, 204, 219, 196, 190, 207, 196, 207 216, 180, 188, 188, 193, 174, 204, 196 185, 207, 174, 190, 190, 164, 185, 207 193, 193, 180, 174, 188, 190, 204, 361 213, 188, 193, 146, 174, 196, 202, 135 180, 188, 154, 139, 174, 172, 142, 146 149, 154, 154, 137, 137, 164, 161, 135 139, 166, 146, 154, 149, 156, 164, 164 154, 149, 149, 177, 182, 177, 161, 190 174, 202, 144, 190, 182, 156, 190, 164 169, 190, 169, 164, 156, 154, 149, 149 164, 172, 164, 166, 146, 185, 177, 188 185, 174, 199, 185, 182, 182, 159, 174 137, 166, 151, 149, 156, 154, 137, 137 146, 130, 174, 142, 144, 144, 142, 137 161, 185, 161, 130, 144, 149, 121, 161 161, 149, 164, 144, 166, 139, 137, 137 149, 154, 117, 130, 125, 137, 125, 132 104, 130, 132, 142, 123, 164, 139, 114 149, 117, 149, 106, 112, 137, 156, 142 128, 108, 110, 128, 108, 130, 130, 110 130, 119, 108, 114, 110, 104, 108, 121 121, 110, 119, 112, 110, 121, 135, 119 119, 96, 110, 117, 123, 117, 117, 108 121, 94, 137, 100, 100, 110, 112, 110 117, 123, 114, 121, 108, 130, 125, 117 135, 144, 128, 142, 132, 139, 146, 146 139, 159, 137, 149, 130, 130, 130, 123 121, 135, 121, 132, 114, 130, 110, 112 139, 112, 125, 119, 117, 130, 117, 125 132, 130, 106, 123, 123, 119, 128, 121 149, 132, 139, 139, 114, 135, 135, 132 128, 130, 135, 121, 132, 142, 144, 135 144, 123, 128, 121, 114, 123, 121, 123 144, 146, 146, 149, 128, 144, 137, 137 144, 164, 137, 135, 125, 164, 164, 151 142, 117, 121, 125, 146, 114, 123, 117 154, 121, 117, 114, 104, 132, 117, 104 110, 117, 96, 132, 123, 121, 121, 123 137, 108, 100, 104, 114, 144, 112, 121 121, 114, 128, 130, 121, 112, 123, 132 119, 104, 117, 125, 137, 130, 112, 114 112, 125, 114, 125, 110, 104, 149, 142 139, 135, 128, 137, 135, 142, 132, 123 154, 132, 151, 137, 135, 154, 142, 144 166, 169, 174, 149, 185, 156, 156, 144 164, 161, 159, 156, 137, 142, 156, 128 151, 121, 137, 130, 125, 123, 94, 125 125, 112, 137, 112, 119, 117, 119, 108 121, 114, 112, 102, 119, 112, 114, 110 98, 121, 110, 106, 135, 123, 117, 112 117, 104, 98, 123, 96, 94, 114, 121 102, 98, 117, 96, 110, 106, 106, 85 104, 108, 114, 135, 117, 125, 123, 110 114, 144, 123, 108, 110, 146, 149, 135 135, 114, 130, 121, 139, 114, 123, 104 119, 117, 125, 121, 104, 104, 117, 114 112, 142, 128, 121, 142, 151, 154, 132 169, 177, 142, 166, 180, 174, 156, 164 144, 137, 144, 146, 132, 125, 96, 121 98, 117, 108, 114, 90, 112, 98, 108 121, 114, 100, 108, 128, 125, 128, 108 142, 142, 137, 114, 146, 135, 137, 159 159, 180, 199, 204, 256, 231, 272, 292 296, 303, 299, 320, 292, 317, 303, 303 279, 259, 279, 222, 202, 188, 204, 172 172, 177, 154, 132, 146, 139, 164, 123 142, 137, 128, 128, 117, 114, 135, 128 121, 132, 88, 106, 98, 110, 92, 100 123, 112, 98, 94, 96, 104, 98, 100 102, 104, 102, 104, 88, 88, 112, 94 102, 96, 100, 72, 86, 83, 79, 90 114, 92, 110, 104, 90, 104, 98, 102 110, 96, 100, 98, 92, 90, 112, 94 85, 108, 100, 85, 83, 92, 106, 106 96, 104, 83, 90, 112, 94, 112, 102 96, 125, 106, 110, 123, 135, 125, 119 137, 121, 114, 114, 102, 108, 114, 100 81, 106, 102, 96, 106, 98, 90, 102 86, 83, 88, 110, 76, 92, 100, 83 83, 106, 98, 85, 77, 98, 83, 94 83, 96, 102, 86, 92, 102, 106, 94 94, 100, 94, 96, 102, 92, 104, 94 94, 85, 74, 92, 106, 85, 86, 88 92, 90, 85, 96, 67, 98, 83, 72 92, 72, 108, 92, 88, 86, 72, 90 94, 96, 96, 96, 102, 92, 96, 86 86, 83, 85, 98, 88, 108, 86, 86 92, 86, 88, 94, 102, 106, 96, 117 96, 100, 94, 92, 117, 83, 92, 104 92, 100, 90, 100, 106, 86, 96, 85 104, 98, 96, 104, 100, 121, 106, 85 110, 94, 123, 123, 106, 123, 146, 128 154, 161, 142, 149, 156, 139, 169, 159 161, 169, 142, 151, 132, 159, 114, 96 119, 114, 102, 104, 86, 92, 94, 79 102, 92, 92, 92, 100, 90, 104, 94 86, 88, 98, 96, 94, 77, 96, 100 92, 96, 90, 88, 85, 94, 77, 104 92, 100, 77, 102, 86, 85, 92, 81 83, 88, 90, 88, 88, 92, 104, 96 110, 112, 86, 77, 106, 90, 94, 83 92, 92, 77, 106, 94, 86, 86, 100 96, 94, 77, 90, 90, 72, 94, 77 86, 74, 88, 83, 86, 83, 98, 100 86, 76, 72, 90, 86, 94, 86, 104 74, 90, 106, 123, 90, 92, 112, 112 98, 112, 100, 102, 90, 90, 128, 96 88, 100, 102, 94, 104, 98, 98, 94 100, 96, 86, 106, 100, 100, 104, 83 102, 85, 106, 100, 94, 114, 108, 92 106, 110, 90, 100, 100, 102, 104, 106 119, 110, 119, 125, 121, 108, 121, 130 121, 123, 128, 114, 98, 130, 130, 112 119, 104, 123, 112, 121, 119, 121, 121 119, 132, 128, 114, 132, 123, 128, 135 121, 121, 151, 135, 114, 137, 142, 149 130, 154, 253, 119, 121, 119, 164, 128 130, 139, 130, 114, 110, 117, 137, 139 137, 123, 117, 128, 128, 117, 130, 135 132, 135, 130, 130, 146, 135, 144, 130 114, 132, 117, 130, 142, 135, 130, 121 117, 119, 144, 121, 144, 154, 159, 125 121, 132, 149, 149, 159, 128, 142, 142 172, 132, 135, 137, 149, 130, 139, 132 376, 130, 159, 135, 144, 132, 139, 144 142, 135, 128, 144, 146, 121, 159, 123 128, 142, 128, 130, 146, 114, 114, 125 125, 132, 137, 144, 132, 132, 123, 161 123, 137, 135, 130, 137, 125, 112, 117 132, 137, 135, 130, 142, 137, 154, 185 161, 156, 177, 180, 182, 188, 199, 207 204, 228, 222, 246, 266, 240, 250, 246 204, 240, 213, 231, 219, 231, 204, 225 196, 166, 182, 159, 172, 149, 146, 159 306, 121, 144, 142, 164, 125, 130, 130 130, 137, 135, 128, 121, 100, 135, 100 123, 98, 102, 130, 100, 114, 119, 94 119, 119, 106, 104, 121, 119, 100, 106 86, 128, 117, 106, 104, 104, 92, 110 104, 96, 104, 100, 100, 108, 112, 123 100, 102, 96, 123, 88, 106, 102, 106 117, 104, 112, 92, 96, 94, 132, 104 98, 110, 110, 110, 117, 102, 110, 112 90, 106, 100, 117, 112, 110, 102, 128 123, 92, 104, 90, 121, 110, 117, 110 110, 112, 92, 123, 102, 104, 100, 106 100, 94, 108, 128, 102, 130, 114, 121 114, 114, 121, 119, 121, 128, 128, 125 98, 114, 108, 139, 108, 121, 125, 130 123, 102, 121, 112, 110, 121, 117, 112 128, 119, 121, 117, 130, 108, 104, 114 123, 114, 114, 117, 108, 121, 117, 128 102, 106, 117, 114, 125, 144, 110, 149 137, 135, 154, 154, 169, 149, 161, 169 182, 182, 174, 177, 164, 164, 174, 166 156, 161, 174, 151, 154, 139, 123, 156 149, 164, 135, 135, 114, 139, 137, 132 121, 130, 114, 117, 142, 132, 132, 108 156, 146, 144, 100, 132, 154, 123, 132 130, 142, 139, 130, 146, 144, 159, 169 151, 151, 188, 123, 161, 177, 169, 159 185, 151, 169, 177, 177, 185, 139, 185 172, 188, 166, 185, 177, 190, 188, 199 210, 182, 213, 207, 190, 196, 188, 177 202, 202, 202, 185, 207, 182, 185, 196 204, 185, 202, 180, 180, 185, 190, 166 193, 185, 177, 164, 174, 180, 185, 172 185, 174, 161, 166, 182, 146, 177, 161 149, 166, 142, 159, 151, 156, 161, 161 182, 135, 130, 135, 154, 159, 159, 154 161, 172, 135, 130, 121, 119, 132, 139 135, 137, 114, 106, 123, 117, 121, 128 128, 125, 110, 117, 114, 106, 130, 125 125, 102, 86, 108, 114, 114, 128, 114 102, 117, 104, 137, 114, 108, 117, 130 117, 123, 98, 96, 110, 108, 130, 108 106, 117, 94, 114, 90, 130, 119, 108 137, 110, 86, 104, 119, 110, 137, 117 119, 117, 110, 119, 108, 108, 106, 137 121, 123, 108, 128, 108, 123, 128, 130 119, 110, 149, 119, 135, 114, 128, 121 117, 121, 123, 123, 117, 114, 135, 137 128, 102, 100, 114, 117, 100, 114, 90 114, 128, 108, 117, 110, 100, 110, 117 121, 104, 86, 112, 100, 92, 86, 121 121, 90, 125, 102, 121, 102, 110, 112 94, 86, 102, 112, 110, 123, 106, 104 92, 110, 110, 108, 112, 100, 106, 98 92, 123, 102, 92, 94, 100, 94, 119 130, 110, 121, 104, 121, 119, 100, 102 125, 96, 128, 112, 98, 110, 125, 130 108, 139, 128, 135, 121, 128, 130, 106 121, 121, 114, 132, 135, 119, 132, 137 137, 132, 137, 121, 130, 125, 130, 146 121, 132, 119, 102, 117, 142, 121, 104 100, 112, 119, 92, 94, 114, 104, 106 98, 92, 96, 88, 110, 100, 94, 98 94, 90, 94, 98, 96, 110, 108, 96 117, 98, 112, 104, 100, 86, 110, 88 96, 94, 114, 108, 102, 106, 98, 92 100, 112, 117, 112, 100, 108, 112, 94 121, 94, 114, 106, 110, 128, 102, 128 117, 130, 137, 144, 151, 130, 142, 159 139, 121, 159, 149, 130, 151, 132, 159 149, 161, 445, 161, 142, 151, 161, 161 154, 154, 188, 169, 164, 199, 164, 154 123, 154, 169, 137, 159, 144, 146, 159 149, 146, 144, 128, 110, 112, 132, 104 130, 121, 114, 114, 121, 132, 106, 108 98, 125, 106, 98, 108, 104, 112, 104 92, 110, 104, 112, 117, 108, 96, 112 135, 98, 98, 128, 104, 121, 128, 100 112, 104, 102, 123, 128, 114, 128, 121 102, 121, 119, 117, 86, 123, 112, 114 130, 123, 128, 104, 119, 117, 86, 117 121, 112, 104, 96, 112, 108, 125, 125 98,/