SampleIdent,907A-16-3/22,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,10-aug-1993 0:36,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 81, 98, 98, 90, 114, 81, 85, 86 92, 92, 98, 98, 94, 114, 79, 86 88, 98, 94, 77, 85, 83, 88, 86 96, 92, 86, 94, 96, 108, 76, 108 92, 98, 102, 92, 88, 110, 90, 100 102, 79, 92, 94, 119, 102, 98, 117 119, 96, 114, 119, 114, 121, 108, 125 110, 96, 117, 117, 112, 108, 117, 121 102, 94, 119, 102, 112, 106, 106, 106 119, 128, 119, 110, 110, 117, 108, 110 125, 119, 104, 119, 132, 112, 121, 108 132, 100, 117, 132, 106, 98, 110, 108 128, 123, 130, 128, 114, 121, 119, 104 123, 121, 110, 130, 108, 117, 125, 121 128, 114, 125, 119, 130, 135, 123, 112 144, 130, 123, 102, 125, 119, 104, 117 125, 108, 123, 123, 119, 90, 119, 119 123, 110, 100, 110, 196, 112, 102, 114 100, 102, 96, 114, 117, 112, 96, 121 114, 117, 117, 94, 102, 119, 123, 117 121, 100, 110, 112, 112, 110, 114, 106 112, 94, 94, 106, 98, 110, 110, 88 92, 108, 108, 117, 114, 121, 125, 123 102, 117, 119, 114, 125, 114, 117, 121 142, 104, 117, 128, 119, 104, 108, 98 100, 119, 108, 90, 106, 119, 112, 94 121, 108, 117, 98, 100, 96, 110, 98 121, 98, 94, 86, 94, 90, 117, 96 90, 112, 94, 83, 114, 90, 88, 108 96, 94, 96, 117, 90, 90, 96, 108 88, 83, 92, 102, 90, 106, 85, 90 79, 102, 76, 90, 114, 98, 90, 104 117, 85, 108, 71, 90, 106, 110, 106 94, 85, 79, 83, 92, 83, 119, 110 94, 79, 90, 121, 112, 83, 83, 94 90, 106, 94, 94, 86, 94, 81, 102 94, 90, 79, 92, 98, 324, 106, 86 104, 76, 98, 98, 104, 90, 77, 85 85, 108, 98, 90, 83, 77, 98, 112 92, 104, 85, 96, 92, 106, 104, 102 86, 88, 96, 92, 94, 92, 90, 98 123, 100, 83, 77, 100, 83, 96, 98 86, 88, 102, 90, 88, 90, 100, 98 72, 92, 90, 83, 98, 92, 104, 96 98, 92, 83, 94, 94, 112, 102, 86 108, 98, 90, 94, 110, 100, 79, 94 92, 112, 119, 102, 106, 106, 112, 110 100, 94, 108, 94, 96, 90, 104, 104 110, 86, 71, 83, 88, 94, 96, 76 92, 90, 77, 86, 81, 85, 76, 85 100, 85, 86, 88, 72, 90, 94, 96 98, 85, 81, 83, 96, 92, 85, 69 86, 92, 81, 86, 90, 90, 83, 85 100, 66, 77, 102, 98, 164, 237, 185 142, 128, 102, 85, 86, 96, 104, 90 83, 108, 81, 102, 77, 110, 79, 79 79, 90, 83, 96, 98, 79, 94, 102 76, 96, 86, 92, 98, 88, 100, 81 85, 90, 77, 83, 85, 90, 77, 96 92, 92, 85, 88, 98, 81, 79, 90 76, 102, 88, 96, 98, 92, 96, 90 76, 98, 90, 79, 96, 90, 76, 100 83, 83, 85, 83, 92, 90, 79, 88 76, 98, 92, 72, 74, 94, 96, 100 100, 94, 100, 108, 85, 85, 86, 77 100, 79, 72, 92, 92, 96, 106, 77 85, 86, 88, 98, 96, 96, 102, 94 83, 104, 96, 81, 92, 90, 98, 90 90, 92, 106, 90, 83, 88, 96, 86 94, 110, 81, 92, 81, 79, 98, 85 90, 96, 102, 88, 83, 90, 88, 106 98, 83, 100, 85, 72, 100, 92, 85 83, 88, 86, 81, 94, 98, 85, 85 88, 104, 96, 94, 102, 92, 76, 96 98, 86, 85, 90, 100, 88, 85, 104 96, 98, 76, 98, 106, 112, 79, 98 94, 96, 92, 90, 90, 88, 106, 90 114, 88, 72, 94, 100, 100, 100, 119 106, 94, 114, 112, 92, 100, 90, 106 86, 94, 94, 110, 117, 100, 125, 92 106, 104, 110, 117, 106, 90, 98, 108 92, 102, 121, 96, 96, 110, 94, 83 117, 88, 100, 98, 110, 90, 96, 110 88, 112, 100, 104, 88, 117, 98, 102 76, 121, 104, 121, 104, 119, 108, 100 114, 83, 96, 114, 108, 98, 117, 96 119, 112, 110, 121, 114, 117, 128, 108 128, 106, 119, 102, 94, 125, 137, 100 117, 121, 132, 123, 135, 137, 128, 123 119, 135, 128, 139, 144, 156, 149, 135 130, 144, 130, 169, 156, 161, 177, 172 180, 174, 185, 169, 185, 180, 180, 185 210, 164, 204, 202, 204, 199, 177, 182 199, 182, 199, 185, 188, 180, 199, 159 174, 164, 161, 164, 161, 185, 154, 156 144, 174, 169, 190, 177, 159, 193, 132 159, 146, 172, 149, 154, 180, 135, 164 174, 166, 172, 154, 159, 180, 172, 193 202, 154, 177, 177, 210, 231, 240, 246 250, 228, 237, 237, 196, 210, 188, 193 169, 185, 174, 149, 174, 166, 161, 177 164, 135, 166, 154, 144, 156, 159, 156 149, 139, 164, 306, 185, 154, 144, 164 159, 169, 154, 135, 154, 169, 159, 174 159, 130, 169, 159, 169, 159, 177, 174 130, 177, 151, 151, 193, 169, 188, 172 180, 185, 169, 182, 164, 199, 149, 161 174, 190, 154, 132, 159, 154, 159, 154 151, 137, 174, 182, 154, 154, 144, 156 135, 151, 142, 159, 151, 164, 159, 174 159, 151, 180, 180, 182, 161, 156, 172 172, 188, 164, 161, 164, 169, 172, 169 180, 164, 161, 185, 161, 166, 169, 164 164, 164, 164, 159, 172, 156, 180, 172 144, 174, 156, 161, 161, 159, 169, 149 169, 159, 193, 172, 169, 188, 180, 156 177, 188, 188, 193, 182, 222, 210, 169 182, 174, 182, 185, 174, 204, 149, 169 172, 166, 185, 166, 174, 156, 190, 164 164, 164, 169, 182, 185, 177, 161, 185 146, 164, 159, 188, 190, 185, 193, 188 164, 164, 202, 188, 202, 182, 196, 174 188, 174, 169, 174, 180, 149, 166, 172 182, 188, 174, 182, 177, 174, 154, 180 185, 177, 210, 177, 177, 177, 193, 193 174, 193, 185, 174, 185, 182, 174, 177 202, 172, 180, 182, 182, 172, 182, 188 196, 169, 182, 177, 185, 177, 210, 182 182, 196, 174, 240, 204, 190, 196, 188 154, 182, 188, 207, 174, 193, 177, 188 159, 172, 177, 177, 177, 180, 174, 174 172, 180, 177, 169, 180, 299, 180, 177 180, 177, 177, 196, 193, 144, 196, 182 174, 190, 180, 185, 196, 207, 182, 225 228, 276, 320, 339, 310, 400, 420, 493 557, 630, 671, 724, 702, 660, 671, 571 506, 392, 339, 292, 219, 234, 240, 237 219, 177, 210, 216, 177, 190, 193, 210 196, 188, 190, 207, 199, 188, 177, 177 207, 182, 202, 216, 225, 193, 188, 213 246, 222, 210, 234, 231, 207, 225, 202 219, 202, 250, 237, 231, 250, 259, 256 276, 286, 269, 306, 289, 313, 286, 269 306, 266, 253, 269, 269, 296, 259, 256 253, 210, 219, 213, 204, 207, 182, 193 177, 196, 196, 188, 177, 182, 196, 185 169, 199, 174, 204, 166, 182, 216, 188 172, 196, 185, 169, 190, 182, 182, 161 161, 164, 159, 169, 151, 172, 146, 159 188, 161, 174, 169, 156, 169, 161, 139 177, 144, 159, 169, 154, 164, 164, 156 151, 151, 172, 174, 156, 149, 161, 149 146, 159, 161, 177, 146, 166, 169, 161 166, 190, 164, 166, 164, 166, 156, 180 196, 213, 219, 207, 196, 234, 193, 216 219, 243, 262, 231, 231, 207, 207, 196 188, 164, 159, 172, 142, 324, 156, 169 166, 159, 169, 149, 149, 188, 182, 161 169, 190, 213, 177, 190, 210, 253, 216 190, 196, 185, 190, 190, 177, 177, 199 164, 154, 144, 154, 177, 164, 156, 172 159, 142, 164, 169, 154, 132, 149, 172 156, 159, 154, 144, 135, 154, 139, 144 149, 142, 137, 149, 146, 169, 149, 149 164, 135, 144, 137, 164, 144, 142, 142 151, 164, 151, 169, 185, 190, 182, 231 259, 276, 331, 342, 412, 384, 449, 488 467, 484, 480, 428, 392, 339, 262, 262 196, 180, 182, 188, 137, 144, 156, 144 142, 154, 149, 139, 114, 121, 112, 119 112, 128, 149, 130, 117, 117, 137, 139 121, 123, 98, 128, 102, 123, 110, 119 119, 135, 112, 110, 119, 117, 125, 114 117, 114, 132, 132, 125, 123, 112, 117 119, 132, 128, 154, 125, 172, 154, 164 156, 151, 161, 188, 174, 146, 142, 161 154, 128, 142, 144, 128, 142, 123, 137 135, 130, 128, 114, 130, 142, 130, 137 110, 106, 110, 102, 106, 117, 128, 112 130, 128, 119, 142, 104, 142, 125, 123 142, 151, 117, 132, 119, 114, 132, 121 114, 130, 108, 100, 125, 128, 142, 139 121, 110, 144, 137, 164, 132, 137, 149 142, 146, 169, 156, 164, 135, 159, 146 177, 172, 188, 177, 185, 193, 202, 199 202, 204, 193, 196, 231, 216, 204, 202 210, 204, 210, 213, 199, 216, 210, 246 202, 222, 199, 231, 222, 243, 231, 216 213, 219, 196, 190, 188, 196, 202, 202 216, 180, 190, 196, 182, 169, 188, 202 177, 177, 188, 188, 185, 190, 204, 196 196, 193, 199, 216, 202, 210, 216, 210 180, 188, 156, 196, 177, 182, 164, 174 177, 156, 172, 161, 156, 154, 154, 125 144, 164, 137, 121, 149, 149, 144, 164 130, 135, 154, 144, 125, 151, 154, 144 149, 144, 139, 172, 174, 188, 185, 169 172, 202, 182, 204, 207, 182, 193, 188 177, 182, 169, 154, 144, 132, 130, 149 159, 130, 119, 164, 149, 144, 169, 169 182, 180, 164, 188, 169, 172, 161, 159 164, 188, 144, 164, 154, 156, 130, 139 137, 142, 149, 123, 156, 139, 151, 144 142, 142, 142, 137, 159, 132, 174, 159 159, 177, 154, 142, 151, 139, 151, 149 159, 151, 144, 156, 117, 137, 146, 144 112, 114, 121, 121, 154, 125, 137, 130 117, 119, 121, 142, 132, 149, 137, 149 137, 139, 130, 121, 146, 121, 137, 110 121, 125, 114, 132, 125, 98, 112, 102 110, 132, 117, 110, 117, 135, 94, 112 104, 123, 117, 110, 106, 100, 121, 119 114, 98, 123, 104, 106, 114, 102, 112 102, 106, 117, 119, 135, 119, 121, 102 125, 128, 139, 114, 130, 108, 130, 166 164, 130, 164, 149, 174, 185, 159, 146 123, 166, 137, 130, 135, 125, 121, 132 142, 125, 130, 106, 125, 100, 130, 114 114, 100, 125, 121, 104, 108, 117, 110 128, 130, 110, 121, 128, 114, 117, 137 123, 114, 137, 121, 117, 132, 151, 128 121, 130, 132, 106, 100, 114, 137, 104 123, 106, 112, 139, 139, 357, 121, 156 149, 135, 139, 137, 144, 154, 169, 164 149, 166, 135, 139, 130, 125, 108, 114 112, 112, 123, 117, 98, 121, 117, 110 128, 128, 123, 123, 125, 110, 104, 125 121, 137, 112, 119, 123, 119, 110, 114 207, 108, 92, 144, 110, 119, 106, 108 100, 121, 128, 121, 102, 135, 112, 123 121, 106, 117, 119, 112, 119, 112, 114 114, 135, 132, 117, 146, 123, 106, 159 137, 135, 137, 117, 142, 159, 128, 135 149, 142, 154, 151, 164, 149, 151, 154 180, 177, 185, 177, 172, 146, 149, 144 137, 146, 132, 139, 128, 117, 110, 117 125, 130, 125, 121, 128, 108, 135, 121 114, 121, 137, 117, 128, 110, 106, 106 112, 123, 108, 121, 112, 130, 130, 121 108, 135, 119, 96, 83, 110, 86, 100 125, 114, 130, 112, 98, 98, 117, 100 119, 121, 112, 119, 114, 108, 114, 106 121, 110, 123, 114, 110, 96, 121, 117 100, 114, 94, 130, 121, 121, 106, 106 123, 132, 119, 112, 128, 130, 123, 102 119, 106, 100, 108, 112, 123, 119, 130 132, 149, 100, 123, 146, 130, 156, 146 142, 149, 137, 128, 114, 121, 112, 137 119, 125, 119, 108, 119, 106, 100, 117 110, 121, 121, 110, 96, 117, 128, 119 135, 119, 121, 130, 125, 114, 119, 128 125, 144, 137, 139, 174, 182, 188, 222 240, 253, 279, 331, 328, 392, 380, 404 416, 388, 339, 342, 342, 272, 237, 231 210, 193, 185, 154, 146, 125, 185, 154 130, 135, 96, 146, 128, 146, 108, 130 132, 100, 94, 121, 112, 98, 112, 110 92, 106, 114, 121, 104, 106, 102, 88 96, 108, 108, 76, 90, 112, 96, 96 106, 108, 100, 100, 98, 98, 106, 121 100, 102, 108, 79, 100, 90, 102, 94 77, 112, 104, 100, 117, 102, 102, 94 96, 110, 108, 90, 90, 110, 108, 94 102, 90, 100, 88, 92, 123, 100, 104 100, 106, 117, 110, 112, 128, 114, 110 123, 119, 100, 142, 119, 104, 96, 112 98, 117, 112, 104, 108, 86, 96, 110 77, 121, 98, 86, 88, 110, 86, 106 92, 86, 98, 96, 96, 104, 106, 83 100, 112, 98, 92, 98, 106, 92, 100 108, 85, 86, 112, 79, 110, 90, 114 88, 86, 86, 90, 102, 98, 96, 96 100, 92, 90, 94, 92, 92, 90, 110 100, 98, 90, 110, 81, 108, 81, 90 90, 106, 104, 112, 104, 96, 85, 106 104, 92, 86, 90, 90, 106, 79, 92 108, 102, 112, 106, 104, 108, 96, 106 85, 125, 104, 104, 96, 94, 104, 81 98, 102, 83, 102, 83, 98, 92, 108 119, 114, 94, 92, 98, 112, 106, 110 121, 112, 108, 108, 106, 108, 98, 112 114, 106, 146, 146, 159, 177, 166, 146 182, 172, 177, 164, 154, 144, 259, 149 132, 117, 110, 114, 130, 102, 112, 96 110, 92, 114, 102, 88, 110, 108, 83 102, 88, 108, 100, 117, 102, 104, 117 94, 86, 104, 125, 92, 90, 94, 98 104, 77, 92, 90, 94, 90, 92, 98 88, 106, 100, 104, 98, 98, 88, 76 102, 77, 92, 96, 86, 85, 100, 121 77, 112, 96, 110, 98, 86, 85, 88 86, 102, 112, 104, 85, 100, 102, 98 90, 102, 92, 81, 88, 74, 96, 86 94, 94, 102, 98, 85, 94, 77, 98 88, 98, 100, 110, 104, 108, 106, 100 94, 108, 110, 100, 92, 108, 102, 108 102, 117, 104, 96, 106, 106, 90, 110 98, 119, 106, 104, 104, 102, 112, 108 119, 110, 94, 94, 104, 98, 96, 100 117, 86, 108, 90, 102, 112, 121, 102 96, 130, 92, 102, 100, 137, 121, 100 108, 117, 96, 132, 117, 112, 119, 104 123, 137, 142, 121, 98, 125, 128, 112 137, 125, 104, 123, 117, 137, 110, 123 132, 117, 119, 128, 132, 125, 125, 121 123, 139, 130, 144, 135, 130, 128, 130 137, 137, 135, 135, 132, 144, 121, 121 121, 119, 123, 114, 139, 128, 137, 128 121, 125, 117, 114, 125, 125, 137, 121 102, 142, 130, 135, 106, 117, 137, 110 110, 128, 130, 142, 130, 125, 121, 139 135, 121, 156, 159, 137, 151, 174, 146 193, 154, 142, 125, 137, 139, 164, 149 121, 144, 142, 144, 142, 137, 123, 142 130, 144, 132, 130, 121, 119, 144, 139 128, 125, 132, 137, 123, 128, 128, 128 132, 149, 130, 135, 108, 119, 125, 164 139, 125, 112, 149, 123, 151, 123, 132 132, 125, 130, 135, 125, 119, 135, 125 132, 149, 119, 159, 130, 159, 139, 177 185, 199, 216, 190, 199, 193, 213, 207 213, 207, 225, 231, 240, 228, 207, 240 219, 225, 188, 185, 213, 166, 177, 182 159, 180, 159, 161, 154, 128, 125, 123 130, 144, 132, 132, 146, 142, 130, 144 135, 128, 123, 112, 106, 112, 130, 119 110, 119, 130, 106, 123, 130, 125, 117 106, 104, 110, 104, 100, 110, 123, 110 114, 106, 104, 114, 96, 98, 119, 114 86, 106, 92, 130, 121, 114, 106, 114 121, 108, 110, 112, 98, 102, 102, 128 114, 110, 128, 90, 112, 125, 100, 108 110, 117, 98, 108, 104, 85, 110, 114 106, 100, 110, 100, 117, 102, 106, 92 108, 117, 96, 125, 102, 114, 102, 114 100, 112, 114, 119, 114, 110, 106, 125 121, 112, 121, 114, 114, 110, 125, 117 117, 102, 121, 117, 108, 135, 108, 128 128, 114, 125, 125, 119, 112, 121, 96 104, 110, 121, 114, 121, 112, 123, 106 117, 112, 130, 112, 123, 117, 121, 106 130, 108, 130, 125, 123, 104, 135, 130 123, 144, 146, 130, 139, 128, 151, 144 182, 174, 164, 188, 219, 210, 222, 185 196, 190, 177, 154, 154, 159, 335, 154 123, 142, 149, 154, 132, 125, 123, 121 128, 125, 132, 139, 121, 142, 112, 151 112, 117, 117, 125, 119, 128, 114, 137 130, 146, 146, 137, 121, 132, 144, 119 159, 166, 142, 123, 166, 180, 151, 164 149, 159, 172, 169, 174, 182, 169, 164 164, 159, 172, 193, 156, 154, 169, 169 204, 169, 174, 166, 213, 174, 182, 172 216, 164, 204, 213, 213, 207, 207, 169 196, 210, 204, 188, 177, 185, 182, 180 172, 185, 202, 169, 182, 174, 174, 169 146, 142, 156, 130, 169, 144, 151, 156 182, 137, 149, 154, 146, 137, 172, 174 132, 123, 159, 144, 137, 154, 146, 139 169, 151, 146, 123, 135, 135, 137, 137 123, 117, 128, 110, 154, 130, 119, 135 121, 135, 132, 119, 137, 123, 135, 137 104, 108, 119, 110, 106, 125, 125, 142 130, 104, 94, 106, 125, 119, 123, 94 110, 98, 104, 132, 114, 114, 104, 102 98, 125, 108, 96, 102, 104, 114, 106 110, 110, 110, 104, 110, 104, 106, 104 130, 114, 112, 104, 112, 114, 137, 132 119, 117, 125, 119, 135, 132, 132, 121 149, 125, 108, 128, 114, 137, 130, 125 139, 130, 110, 108, 119, 130, 123, 117 108, 146, 119, 123, 104, 112, 117, 102 110, 90, 96, 119, 100, 117, 123, 121 108, 110, 110, 117, 123, 102, 110, 110 125, 128, 130, 119, 108, 102, 121, 108 119, 112, 112, 114, 117, 119, 117, 110 102, 125, 104, 100, 119, 110, 112, 112 114, 114, 100, 104, 112, 100, 114, 108 94, 88, 112, 100, 125, 104, 112, 110 98, 98, 121, 125, 123, 125, 125, 123 121, 125, 130, 114, 146, 117, 132, 130 104, 135, 130, 146, 123, 139, 130, 164 164, 166, 135, 144, 166, 164, 146, 174 149, 139, 142, 125, 149, 119, 142, 121 121, 142, 125, 121, 104, 100, 96, 117 108, 119, 100, 108, 112, 100, 112, 106 79, 104, 94, 110, 96, 108, 114, 100 108, 100, 114, 123, 102, 110, 110, 110 100, 106, 108, 119, 125, 121, 110, 94 121, 90, 123, 110, 106, 139, 112, 114 117, 100, 121, 117, 112, 117, 146, 137 108, 121, 142, 119, 137, 142, 128, 159 161, 139, 139, 156, 142, 137, 130, 130 139, 128, 139, 149, 130, 156, 130, 156 149, 161, 166, 172, 169, 177, 174, 142 172, 199, 182, 169, 137, 144, 151, 166 159, 164, 139, 154, 144, 156, 139, 139 130, 119, 121, 125, 123, 117, 119, 102 110, 102, 112, 106, 108, 90, 96, 125 104, 104, 108, 106, 108, 130, 119, 102 92, 119, 117, 117, 128, 104, 121, 121 100, 112, 102, 117, 110, 114, 119, 154 125, 130, 130, 121, 142, 135, 169, 164 154, 144, 151, 130, 121, 130, 117, 125 123, 142, 149, 121, 102, 112, 135, 112 106, 94, 112, 96, 121, 102, 94, 102 110,/