SampleIdent,907a 17h-1 49-50bulk,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,18-aug-1993 10:58,/ DataAngleRange, 2.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 110, 88, 100, 100, 94, 94, 85, 83 92, 90, 86, 102, 81, 83, 94, 94 92, 88, 77, 77, 88, 108, 74, 88 81, 59, 79, 72, 77, 76, 79, 69 85, 92, 77, 85, 88, 69, 79, 90 92, 83, 76, 83, 86, 92, 74, 77 83, 83, 90, 86, 83, 77, 77, 85 71, 72, 100, 92, 76, 86, 79, 79 85, 76, 83, 96, 100, 98, 77, 112 94, 90, 92, 71, 67, 88, 98, 94 86, 90, 110, 92, 98, 83, 104, 100 104, 86, 102, 85, 81, 92, 92, 104 86, 100, 90, 117, 100, 92, 112, 94 90, 102, 108, 108, 114, 98, 92, 96 88, 96, 104, 92, 108, 90, 98, 100 112, 98, 119, 112, 106, 112, 104, 94 119, 102, 112, 98, 100, 108, 104, 112 88, 94, 117, 110, 110, 121, 114, 117 106, 92, 112, 121, 121, 94, 114, 88 117, 112, 119, 112, 108, 102, 112, 104 108, 110, 121, 112, 121, 121, 130, 106 132, 106, 110, 119, 110, 102, 130, 119 98, 137, 125, 110, 114, 104, 135, 137 125, 146, 130, 130, 137, 128, 123, 106 128, 128, 121, 128, 149, 123, 146, 144 137, 151, 135, 144, 130, 137, 144, 125 159, 123, 149, 135, 130, 132, 139, 135 142, 169, 149, 151, 161, 149, 137, 144 164, 149, 142, 159, 164, 137, 144, 132 142, 161, 137, 125, 142, 128, 135, 146 139, 154, 144, 137, 164, 159, 142, 169 174, 149, 159, 142, 149, 125, 130, 130 156, 159, 130, 139, 154, 135, 130, 161 132, 149, 139, 154, 149, 142, 128, 154 154, 146, 159, 128, 137, 142, 130, 130 144, 132, 135, 112, 130, 135, 135, 144 137, 135, 123, 108, 117, 121, 144, 110 144, 130, 144, 130, 123, 121, 123, 130 128, 137, 144, 117, 114, 149, 123, 119 130, 128, 132, 135, 128, 123, 119, 149 132, 121, 123, 108, 119, 130, 125, 139 128, 123, 135, 135, 146, 128, 130, 130 117, 130, 137, 125, 117, 108, 135, 104 110, 112, 104, 110, 114, 102, 117, 121 117, 121, 117, 106, 108, 112, 108, 121 110, 102, 102, 110, 112, 98, 90, 112 106, 117, 119, 130, 96, 108, 108, 100 98, 125, 112, 90, 102, 106, 119, 102 108, 108, 79, 98, 86, 119, 108, 121 98, 98, 102, 110, 100, 104, 117, 121 102, 100, 110, 90, 90, 100, 92, 117 112, 83, 98, 100, 96, 96, 94, 100 96, 100, 88, 98, 164, 92, 100, 92 94, 100, 112, 100, 106, 112, 112, 112 112, 114, 108, 90, 104, 110, 117, 86 88, 92, 83, 86, 104, 100, 106, 88 110, 98, 104, 96, 100, 92, 98, 102 92, 96, 90, 110, 110, 102, 119, 114 96, 88, 86, 112, 112, 100, 121, 100 98, 104, 106, 130, 92, 100, 98, 106 98, 104, 114, 108, 112, 102, 112, 94 102, 121, 108, 106, 110, 88, 106, 102 102, 108, 100, 110, 102, 98, 112, 104 94, 112, 128, 112, 85, 130, 130, 106 102, 128, 98, 137, 144, 125, 121, 132 104, 94, 90, 98, 94, 108, 96, 100 106, 96, 104, 98, 100, 98, 112, 102 102, 96, 100, 90, 98, 106, 90, 96 94, 77, 90, 92, 88, 117, 94, 79 94, 88, 112, 86, 90, 94, 88, 90 85, 96, 98, 94, 98, 104, 104, 90 94, 98, 94, 102, 86, 110, 94, 98 94, 100, 106, 86, 90, 90, 94, 86 90, 92, 88, 85, 94, 412, 94, 98 96, 79, 114, 100, 77, 98, 98, 72 77, 104, 94, 88, 102, 88, 79, 86 90, 110, 94, 94, 100, 100, 104, 102 88, 125, 96, 94, 92, 86, 94, 98 79, 88, 92, 85, 72, 86, 79, 92 88, 86, 96, 94, 104, 108, 108, 98 96, 88, 114, 90, 102, 110, 86, 100 86, 88, 90, 94, 121, 88, 88, 79 104, 90, 110, 102, 102, 104, 102, 114 92, 77, 88, 96, 100, 94, 119, 92 96, 71, 88, 83, 90, 104, 92, 86 90, 90, 94, 100, 96, 94, 108, 96 100, 108, 92, 86, 90, 98, 92, 106 112, 85, 90, 88, 83, 86, 74, 90 100, 92, 85, 110, 110, 92, 94, 90 104, 86, 96, 102, 88, 104, 108, 106 92, 86, 108, 94, 100, 96, 106, 96 85, 102, 110, 83, 110, 100, 92, 110 92, 92, 108, 90, 100, 90, 102, 94 98, 90, 102, 112, 112, 104, 102, 94 92, 102, 90, 121, 86, 102, 104, 108 88, 106, 98, 102, 88, 119, 108, 106 94, 94, 108, 128, 102, 98, 117, 104 102, 104, 121, 110, 121, 117, 121, 104 119, 106, 94, 100, 98, 125, 119, 102 121, 121, 108, 110, 104, 106, 121, 110 108, 112, 108, 94, 117, 121, 117, 132 117, 108, 100, 96, 110, 108, 144, 119 104, 102, 98, 108, 102, 128, 114, 110 104, 123, 106, 119, 110, 117, 106, 142 110, 112, 135, 117, 112, 119, 135, 112 154, 130, 96, 117, 135, 132, 119, 128 144, 142, 135, 121, 132, 125, 128, 132 144, 151, 139, 121, 144, 156, 164, 182 164, 159, 149, 172, 156, 149, 169, 164 169, 190, 177, 185, 185, 213, 210, 202 219, 228, 196, 207, 182, 196, 199, 213 210, 202, 199, 219, 185, 196, 207, 177 210, 190, 174, 159, 154, 193, 180, 180 174, 172, 174, 149, 177, 174, 174, 182 174, 174, 169, 169, 177, 185, 193, 207 164, 188, 169, 188, 222, 166, 193, 185 180, 193, 188, 225, 253, 276, 296, 310 292, 310, 292, 222, 222, 222, 193, 177 188, 185, 190, 185, 172, 159, 172, 159 188, 169, 166, 146, 177, 159, 164, 190 161, 169, 149, 166, 159, 164, 154, 188 156, 164, 156, 164, 180, 174, 166, 174 164, 166, 177, 154, 164, 180, 156, 172 180, 161, 219, 159, 188, 188, 169, 190 188, 182, 204, 177, 182, 185, 172, 166 182, 172, 182, 180, 193, 185, 169, 177 159, 156, 164, 161, 151, 174, 154, 182 180, 166, 159, 154, 132, 182, 149, 161 174, 182, 172, 177, 161, 156, 182, 188 188, 199, 174, 182, 174, 159, 185, 196 174, 188, 161, 177, 174, 169, 182, 180 174, 182, 174, 172, 193, 174, 182, 177 199, 177, 185, 177, 190, 196, 196, 185 185, 204, 193, 188, 174, 174, 188, 174 190, 219, 202, 207, 204, 185, 180, 180 199, 207, 190, 182, 210, 182, 207, 180 166, 185, 169, 172, 177, 182, 196, 188 177, 185, 177, 210, 207, 174, 174, 185 182, 185, 207, 202, 174, 207, 204, 207 207, 199, 174, 199, 177, 199, 190, 166 210, 196, 185, 180, 154, 177, 180, 193 207, 210, 193, 210, 180, 202, 180, 177 196, 210, 188, 207, 185, 185, 240, 202 190, 188, 182, 199, 222, 237, 202, 222 228, 213, 190, 174, 190, 228, 213, 199 196, 193, 213, 196, 199, 188, 237, 196 204, 213, 196, 204, 190, 213, 188, 188 207, 219, 169, 207, 207, 202, 174, 193 177, 196, 190, 196, 202, 188, 216, 202 180, 188, 207, 202, 202, 182, 213, 199 210, 188, 182, 193, 185, 196, 196, 180 193, 196, 196, 188, 243, 219, 237, 210 231, 262, 286, 313, 380, 437, 615, 660 762, 882, 882, 858, 740, 666, 557, 437 408, 299, 292, 262, 253, 253, 222, 237 210, 219, 210, 182, 202, 213, 199, 207 204, 199, 202, 196, 207, 204, 202, 174 190, 193, 202, 213, 246, 210, 225, 266 272, 228, 272, 310, 310, 313, 282, 286 259, 240, 272, 250, 240, 253, 246, 243 292, 228, 259, 250, 240, 262, 266, 276 259, 262, 266, 259, 243, 216, 228, 266 234, 228, 204, 216, 207, 193, 207, 193 193, 210, 202, 196, 207, 225, 213, 185 210, 185, 199, 190, 190, 190, 196, 216 207, 190, 185, 164, 174, 188, 166, 166 196, 182, 182, 182, 202, 185, 196, 202 188, 449, 188, 185, 172, 196, 182, 185 188, 185, 190, 196, 172, 204, 190, 149 199, 172, 169, 188, 174, 222, 174, 190 199, 213, 185, 180, 172, 190, 164, 159 188, 166, 193, 188, 180, 159, 193, 196 169, 188, 202, 196, 182, 188, 204, 216 199, 225, 213, 199, 199, 185, 177, 216 204, 174, 159, 193, 166, 188, 202, 180 174, 180, 166, 182, 182, 156, 166, 146 188, 182, 180, 180, 154, 196, 174, 182 164, 177, 204, 188, 169, 156, 199, 164 182, 151, 177, 185, 156, 154, 202, 159 188, 188, 164, 188, 185, 166, 199, 185 185, 202, 164, 164, 190, 172, 193, 182 166, 182, 177, 166, 177, 154, 159, 174 161, 185, 174, 169, 174, 159, 164, 149 177, 180, 149, 196, 199, 196, 202, 202 225, 228, 269, 299, 324, 380, 412, 388 380, 357, 335, 296, 234, 237, 219, 177 199, 185, 182, 159, 182, 174, 193, 151 169, 159, 169, 169, 180, 151, 177, 172 159, 159, 154, 164, 172, 161, 161, 154 130, 142, 177, 142, 164, 159, 156, 149 151, 149, 149, 159, 151, 139, 125, 159 154, 137, 139, 139, 169, 154, 169, 166 146, 149, 135, 161, 142, 177, 172, 169 159, 164, 169, 172, 169, 169, 182, 159 119, 139, 154, 149, 139, 144, 166, 144 159, 149, 142, 154, 161, 156, 151, 149 135, 161, 149, 151, 146, 135, 135, 119 146, 130, 174, 151, 159, 161, 156, 137 128, 149, 123, 164, 159, 161, 144, 144 154, 135, 159, 144, 146, 146, 161, 146 142, 169, 142, 149, 166, 159, 166, 159 166, 144, 164, 144, 161, 182, 177, 180 177, 190, 188, 169, 219, 216, 204, 174 207, 188, 207, 199, 188, 207, 185, 182 177, 231, 182, 219, 188, 234, 240, 202 204, 210, 210, 237, 222, 202, 207, 219 222, 210, 216, 202, 185, 199, 193, 180 174, 180, 185, 196, 196, 193, 190, 193 159, 166, 180, 159, 199, 166, 190, 188 180, 164, 177, 180, 172, 137, 164, 182 166, 164, 177, 164, 174, 149, 185, 190 161, 185, 166, 174, 174, 161, 151, 137 164, 149, 161, 149, 151, 166, 164, 154 142, 144, 161, 144, 146, 144, 172, 154 154, 166, 164, 177, 177, 188, 177, 185 213, 202, 207, 210, 207, 166, 172, 196 169, 177, 142, 177, 161, 144, 169, 154 149, 149, 169, 132, 159, 142, 154, 154 151, 137, 144, 161, 144, 172, 135, 156 164, 149, 137, 137, 139, 154, 146, 149 144, 159, 149, 164, 174, 149, 154, 142 142, 174, 146, 146, 130, 180, 135, 161 177, 146, 161, 159, 137, 177, 159, 149 139, 139, 132, 149, 149, 142, 144, 144 144, 151, 146, 130, 137, 128, 142, 132 130, 151, 137, 135, 117, 154, 137, 128 137, 149, 169, 159, 142, 144, 151, 135 144, 135, 156, 149, 144, 142, 125, 144 151, 125, 130, 121, 125, 106, 123, 121 117, 117, 132, 119, 100, 112, 139, 144 130, 117, 128, 144, 130, 130, 137, 130 142, 123, 142, 114, 123, 151, 121, 117 159, 139, 123, 161, 151, 142, 146, 144 188, 190, 185, 146, 188, 185, 166, 159 151, 159, 172, 135, 149, 130, 137, 114 139, 110, 114, 144, 123, 135, 117, 128 130, 135, 123, 135, 139, 142, 130, 121 119, 137, 130, 130, 130, 149, 149, 137 146, 137, 146, 139, 146, 144, 154, 154 128, 121, 121, 108, 125, 130, 137, 119 125, 142, 121, 123, 110, 135, 132, 169 144, 139, 144, 130, 128, 128, 137, 137 125, 154, 142, 121, 144, 123, 139, 121 132, 114, 149, 137, 149, 135, 144, 144 132, 123, 135, 121, 164, 137, 137, 135 132, 149, 139, 144, 104, 121, 135, 137 135, 125, 132, 128, 114, 137, 144, 121 125, 142, 169, 154, 151, 164, 144, 159 144, 137, 144, 137, 149, 125, 139, 135 128, 139, 123, 135, 146, 180, 151, 123 154, 130, 144, 137, 151, 149, 121, 159 146, 174, 123, 177, 174, 159, 156, 172 169, 180, 188, 142, 177, 199, 159, 149 151, 144, 159, 144, 135, 151, 164, 121 130, 151, 132, 123, 137, 159, 149, 135 149, 149, 137, 139, 130, 121, 149, 139 135, 139, 130, 130, 132, 130, 125, 137 130, 132, 149, 139, 139, 125, 119, 149 121, 137, 130, 130, 139, 128, 144, 128 119, 125, 117, 128, 137, 117, 123, 110 121, 128, 130, 128, 144, 137, 151, 112 130, 128, 144, 130, 135, 125, 156, 154 159, 149, 149, 146, 177, 156, 144, 149 146, 151, 161, 137, 149, 146, 154, 139 130, 156, 164, 156, 137, 123, 149, 151 135, 159, 166, 174, 193, 174, 213, 237 243, 256, 237, 231, 234, 202, 196, 222 216, 177, 159, 146, 144, 144, 135, 125 144, 130, 151, 137, 149, 156, 159, 159 159, 144, 169, 151, 161, 161, 161, 166 174, 202, 231, 237, 276, 299, 317, 296 259, 250, 256, 204, 216, 216, 172, 196 159, 146, 139, 174, 156, 161, 169, 166 169, 128, 112, 130, 135, 149, 121, 128 154, 159, 142, 114, 125, 132, 123, 135 119, 128, 132, 100, 132, 123, 123, 106 104, 137, 121, 108, 128, 114, 130, 137 130, 132, 128, 104, 106, 121, 119, 123 125, 123, 117, 121, 132, 137, 117, 142 119, 112, 114, 106, 119, 114, 108, 121 106, 132, 121, 121, 92, 114, 112, 146 112, 123, 130, 121, 135, 112, 106, 132 108, 114, 104, 108, 121, 117, 130, 139 112, 142, 128, 149, 106, 119, 128, 119 121, 142, 100, 128, 110, 98, 108, 106 108, 108, 125, 112, 112, 128, 132, 144 137, 121, 132, 121, 110, 104, 123, 112 130, 130, 130, 142, 135, 112, 130, 125 117, 121, 100, 106, 149, 130, 130, 119 121, 112, 144, 104, 114, 112, 110, 102 123, 121, 108, 121, 132, 104, 106, 130 123, 114, 112, 112, 108, 121, 123, 117 128, 135, 135, 128, 117, 144, 132, 121 100, 114, 142, 119, 112, 128, 104, 123 117, 125, 128, 125, 123, 119, 128, 119 106, 104, 135, 121, 117, 117, 121, 106 128, 139, 144, 128, 117, 104, 132, 121 125, 130, 135, 117, 142, 137, 114, 106 112, 114, 139, 123, 117, 130, 117, 149 154, 139, 119, 144, 130, 199, 190, 164 193, 193, 169, 193, 154, 159, 172, 169 169, 154, 151, 121, 123, 114, 96, 121 130, 108, 135, 121, 130, 144, 130, 137 123, 139, 154, 130, 139, 149, 123, 119 119, 146, 114, 130, 114, 121, 128, 104 119, 112, 119, 114, 102, 121, 130, 125 119, 135, 104, 119, 108, 121, 130, 130 110, 130, 137, 146, 106, 114, 125, 114 121, 128, 117, 117, 135, 119, 117, 125 135, 96, 128, 100, 86, 119, 108, 114 125, 102, 92, 132, 117, 121, 121, 123 104, 121, 117, 100, 128, 123, 128, 112 110, 110, 132, 132, 114, 112, 128, 135 114, 128, 117, 137, 121, 128, 128, 112 121, 123, 114, 128, 125, 106, 123, 108 121, 130, 117, 121, 125, 125, 135, 137 135, 106, 117, 121, 117, 130, 114, 123 135, 125, 114, 142, 108, 135, 119, 121 130, 110, 114, 151, 121, 123, 110, 135 156, 137, 146, 144, 112, 123, 137, 130 142, 130, 137, 156, 154, 146, 121, 121 108, 142, 132, 135, 159, 137, 159, 154 135, 149, 123, 149, 159, 159, 135, 154 159, 146, 149, 142, 154, 123, 146, 149 144, 132, 146, 159, 149, 142, 132, 144 130, 137, 146, 135, 135, 154, 128, 121 166, 137, 169, 151, 169, 159, 164, 125 310, 144, 121, 144, 132, 149, 149, 130 139, 137, 144, 154, 149, 159, 146, 130 144, 166, 182, 159, 146, 172, 169, 182 166, 144, 144, 146, 185, 169, 159, 177 144, 128, 151, 149, 154, 128, 161, 159 130, 139, 154, 166, 177, 164, 159, 151 132, 125, 159, 169, 151, 154, 149, 169 154, 128, 151, 142, 146, 164, 139, 149 137, 119, 154, 137, 144, 154, 159, 144 146, 164, 130, 159, 130, 164, 144, 144 121, 132, 132, 169, 159, 161, 142, 142 146, 154, 159, 182, 174, 190, 169, 182 166, 177, 172, 180, 185, 185, 188, 190 161, 185, 169, 161, 159, 161, 180, 144 146, 137, 144, 149, 151, 125, 164, 146 139, 156, 146, 117, 139, 139, 132, 139 159, 135, 142, 149, 146, 123, 114, 144 149, 164, 117, 166, 142, 156, 121, 128 130, 128, 132, 149, 121, 139, 144, 123 123, 149, 142, 149, 137, 144, 135, 123 156, 144, 125, 132, 119, 144, 135, 169 130, 144, 154, 154, 130, 137, 149, 154 154, 130, 137, 139, 164, 114, 135, 123 130, 139, 132, 144, 132, 125, 123, 119 132, 154, 137, 135, 137, 137, 119, 130 142, 139, 125, 130, 142, 132, 139, 117 119, 128, 137, 112, 161, 151, 151, 151 137, 137, 142, 130, 156, 144, 130, 135 144, 146, 151, 144, 137, 139, 132, 156 154, 137, 144, 144, 156, 144, 180, 149 144, 130, 144, 166, 123, 159, 154, 123 142, 139, 151, 130, 139, 154, 144, 166 137, 144, 130, 144, 142, 139, 156, 159 149, 164, 174, 144, 142, 159, 156, 166 177, 190, 190, 190, 204, 204, 199, 190 185, 182, 190, 185, 177, 182, 169, 169 174, 159, 174, 149, 177, 154, 144, 130 159, 121, 132, 142, 159, 144, 149, 154 149, 142, 154, 166, 144, 169, 144, 144 164, 144, 182, 139, 156, 182, 166, 166 151, 164, 174, 159, 161, 149, 172, 151 166, 164, 182, 174, 151, 137, 164, 177 164, 188, 169, 182, 185, 174, 180, 156 169, 180, 193, 159, 159, 154, 190, 185 207, 182, 185, 188, 177, 164, 193, 182 182, 185, 213, 196, 164, 193, 199, 161 190, 177, 188, 188, 159, 185, 188, 188 159, 174, 188, 177, 164, 164, 169, 159 146, 174, 166, 180, 169, 144, 164, 151 190, 159, 169, 177, 151, 151, 159, 154 166, 169, 151, 174, 164, 156, 149, 159 144, 154, 135, 174, 144, 172, 144, 151 166, 135, 177, 149, 156, 144, 154, 164 146, 139, 142, 151, 151, 149, 149, 154 139, 137, 169, 128, 149, 151, 114, 139 166, 154, 146, 154, 151, 149, 144, 144 139, 154, 137, 128, 142, 142, 130, 154 146, 149, 121, 125, 146, 121, 161, 154 137, 130, 154, 137, 154, 159, 161, 164 151, 161, 146, 161, 132, 169, 177, 174 166, 154, 174, 151, 159, 156, 125, 177 164, 137, 174, 164, 164, 149, 154, 159 154, 156, 164, 137, 132, 132, 144, 142 121, 149, 135, 119, 121, 159, 149, 142 154, 135, 149, 154, 146, 130, 144, 139 154, 130, 151, 146, 149, 166, 166, 149 142, 142, 151, 166, 137, 144, 174, 139 180, 174, 151, 146, 144, 146, 159, 149 159, 149, 144, 128, 137, 149, 139, 149 144, 137, 166, 139, 159, 137, 151, 154 161, 174, 146, 149, 149, 154, 169, 125 146, 128, 177, 137, 159, 154, 149, 137 142, 169, 144, 156, 146, 149, 161, 156 142, 169, 154, 172, 166, 149, 174, 151 156, 156, 169, 149, 159, 130, 159, 149 151, 156, 154, 142, 154, 149, 125, 135 146, 172, 135, 156, 137, 144, 146, 149 144, 139, 144, 159, 142, 128, 139, 146 144, 128, 142, 144, 137, 151, 149, 121 174, 146, 130, 137, 164, 125, 149, 130 146, 151, 144, 154, 151, 146, 139, 144 144, 159, 142, 146, 146, 154, 154, 154 100, 149, 159, 149, 156, 159, 172, 182 174, 193, 196, 177, 177, 188, 161, 164 169, 144, 180, 164, 169, 204, 174, 174 159, 190, 180, 207, 188, 190, 199, 172 190, 193, 202, 202, 202, 219, 222, 231 190, 213, 188, 174, 164, 164, 169, 182 159, 166, 159, 156, 164, 144, 135, 119 149, 123, 132, 144, 149, 146, 132, 154 137, 128, 144, 172, 149, 146, 169, 149 142, 154, 159, 137, 156, 156, 125, 161 144, 149, 135, 132, 159, 137, 132, 135 142, 156, 154, 151, 166, 151, 151, 156 154, 166, 144, 137, 139, 139, 144, 164 137, 132, 151, 142, 144, 154, 159, 137 139, 135, 135, 137, 144, 144, 142, 137 151, 132, 149, 121, 144, 135, 149,/