SampleIdent,907A-17-2/27,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,10-aug-1993 1:31,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 104, 86, 88, 90, 64, 77, 100, 88 100, 108, 102, 83, 88, 112, 121, 72 85, 94, 104, 86, 88, 85, 98, 85 86, 85, 83, 86, 85, 88, 76, 85 96, 76, 102, 88, 104, 108, 77, 102 88, 98, 90, 100, 92, 108, 88, 96 100, 88, 98, 98, 98, 90, 104, 92 96, 106, 106, 108, 112, 112, 121, 132 85, 106, 104, 110, 110, 100, 121, 98 110, 108, 119, 117, 128, 102, 102, 125 121, 144, 125, 128, 117, 121, 92, 110 114, 106, 119, 123, 106, 108, 104, 104 114, 125, 117, 125, 121, 96, 102, 119 130, 112, 110, 117, 121, 112, 125, 108 106, 121, 112, 108, 130, 94, 121, 108 121, 128, 110, 117, 119, 128, 114, 130 117, 112, 117, 135, 104, 128, 110, 108 106, 114, 130, 108, 106, 123, 112, 110 130, 123, 108, 139, 117, 110, 104, 96 98, 121, 121, 121, 137, 112, 108, 98 106, 114, 104, 108, 92, 92, 112, 98 112, 114, 104, 108, 114, 130, 100, 100 130, 92, 98, 117, 104, 104, 104, 121 100, 121, 123, 98, 112, 112, 106, 128 117, 96, 119, 121, 119, 119, 132, 102 110, 106, 108, 104, 94, 102, 102, 104 100, 92, 112, 96, 108, 86, 98, 102 92, 94, 94, 102, 110, 98, 117, 92 77, 85, 83, 92, 92, 96, 102, 76 94, 106, 108, 92, 104, 102, 96, 100 102, 88, 96, 104, 92, 94, 104, 79 100, 77, 86, 100, 98, 104, 121, 100 86, 81, 106, 83, 98, 85, 81, 98 83, 86, 86, 90, 88, 96, 88, 85 88, 102, 102, 92, 79, 100, 96, 96 85, 88, 100, 98, 102, 85, 96, 72 90, 66, 85, 85, 90, 92, 102, 90 79, 92, 86, 83, 76, 106, 92, 77 92, 76, 79, 90, 81, 85, 88, 76 94, 88, 86, 94, 72, 90, 88, 86 90, 96, 88, 74, 102, 88, 86, 86 88, 102, 104, 90, 81, 94, 86, 94 88, 88, 86, 96, 92, 94, 98, 88 77, 96, 104, 100, 96, 98, 85, 86 83, 92, 90, 114, 92, 104, 100, 92 92, 83, 76, 86, 100, 102, 96, 110 96, 108, 117, 121, 110, 117, 106, 114 128, 110, 96, 108, 96, 112, 86, 86 104, 90, 102, 96, 94, 85, 66, 90 83, 79, 94, 92, 102, 83, 81, 77 72, 81, 76, 77, 72, 76, 83, 90 86, 92, 92, 71, 100, 85, 77, 79 79, 90, 71, 85, 86, 90, 72, 96 94, 104, 83, 110, 86, 76, 79, 90 83, 96, 76, 77, 77, 106, 85, 79 76, 90, 74, 92, 92, 90, 88, 96 76, 72, 100, 98, 79, 77, 69, 83 86, 77, 88, 92, 83, 83, 72, 92 67, 74, 92, 77, 64, 81, 71, 79 77, 76, 96, 76, 98, 77, 62, 86 88, 62, 96, 94, 92, 79, 79, 83 86, 83, 102, 81, 77, 86, 77, 81 108, 79, 92, 83, 76, 86, 81, 92 86, 77, 90, 66, 85, 90, 77, 72 92, 86, 81, 81, 92, 100, 104, 88 92, 86, 83, 83, 96, 88, 85, 86 88, 96, 83, 108, 79, 88, 88, 86 88, 92, 90, 96, 88, 90, 100, 83 79, 77, 92, 104, 94, 86, 85, 104 67, 85, 88, 88, 79, 76, 86, 92 86, 72, 86, 98, 86, 76, 85, 86 83, 62, 86, 85, 90, 76, 392, 96 85, 77, 88, 83, 88, 88, 86, 98 77, 77, 137, 85, 88, 85, 98, 88 92, 72, 83, 92, 96, 77, 102, 92 94, 92, 92, 79, 77, 96, 76, 83 66, 94, 92, 66, 72, 77, 86, 83 90, 98, 85, 76, 86, 96, 88, 81 96, 96, 94, 94, 104, 88, 92, 88 106, 114, 114, 100, 121, 119, 110, 100 110, 92, 128, 86, 114, 102, 100, 108 98, 102, 94, 102, 88, 110, 92, 90 117, 98, 106, 102, 83, 86, 88, 98 108, 77, 104, 92, 94, 88, 98, 112 77, 121, 110, 72, 90, 100, 96, 104 96, 98, 123, 102, 92, 86, 85, 108 98, 112, 121, 94, 102, 108, 100, 98 123, 119, 123, 100, 96, 110, 106, 123 86, 104, 121, 112, 125, 117, 114, 108 117, 130, 117, 130, 123, 121, 123, 135 132, 132, 151, 144, 164, 149, 174, 137 161, 156, 164, 174, 190, 202, 204, 204 219, 243, 222, 240, 237, 246, 240, 243 231, 243, 253, 210, 234, 216, 222, 222 185, 225, 231, 193, 193, 169, 202, 193 196, 190, 174, 185, 177, 174, 159, 156 188, 159, 169, 199, 164, 199, 169, 174 202, 204, 188, 185, 169, 159, 182, 185 154, 199, 199, 199, 193, 202, 222, 250 222, 250, 282, 259, 266, 299, 292, 292 266, 240, 213, 222, 180, 169, 149, 166 172, 174, 159, 149, 159, 137, 159, 151 174, 164, 146, 156, 154, 142, 154, 142 166, 151, 172, 199, 156, 154, 164, 159 166, 166, 164, 161, 156, 159, 159, 132 149, 132, 159, 166, 161, 146, 137, 156 164, 182, 182, 177, 180, 166, 151, 166 159, 169, 174, 146, 156, 151, 161, 166 161, 174, 154, 156, 154, 154, 169, 144 172, 137, 144, 154, 159, 139, 151, 149 132, 132, 164, 142, 156, 139, 164, 154 174, 172, 159, 174, 156, 159, 164, 169 159, 188, 172, 164, 159, 156, 164, 190 185, 151, 151, 172, 132, 154, 159, 149 149, 182, 166, 151, 156, 149, 156, 159 149, 180, 174, 196, 174, 161, 190, 172 202, 169, 180, 190, 149, 174, 182, 182 172, 161, 190, 159, 154, 166, 174, 188 180, 188, 188, 182, 199, 159, 156, 154 166, 137, 185, 185, 164, 182, 182, 166 172, 169, 180, 164, 159, 166, 174, 159 174, 193, 204, 182, 174, 199, 202, 190 196, 228, 188, 177, 177, 190, 172, 169 164, 166, 182, 180, 188, 185, 151, 169 177, 182, 174, 177, 182, 188, 169, 169 172, 199, 193, 199, 199, 180, 199, 210 207, 190, 177, 222, 216, 159, 190, 202 202, 199, 193, 199, 182, 190, 172, 190 454, 207, 159, 193, 207, 213, 177, 193 177, 182, 193, 193, 177, 177, 196, 177 164, 164, 164, 166, 180, 188, 180, 182 161, 166, 185, 149, 188, 180, 185, 169 185, 164, 172, 180, 190, 188, 196, 188 182, 193, 169, 164, 188, 216, 228, 210 228, 234, 262, 306, 365, 388, 424, 548 595, 697, 762, 807, 930, 1005, 992, 1011 999, 955, 756, 600, 493, 372, 361, 292 292, 250, 231, 237, 250, 256, 213, 216 210, 190, 188, 196, 177, 185, 174, 185 196, 174, 188, 185, 202, 190, 213, 204 204, 196, 213, 210, 219, 213, 219, 202 234, 225, 193, 210, 222, 196, 193, 228 210, 219, 237, 219, 228, 266, 253, 272 266, 279, 324, 306, 317, 296, 299, 259 225, 256, 210, 231, 250, 210, 196, 193 222, 185, 188, 166, 149, 180, 172, 193 159, 188, 172, 196, 174, 149, 185, 196 164, 166, 188, 182, 188, 159, 174, 210 164, 161, 180, 151, 185, 161, 159, 169 149, 149, 164, 130, 149, 135, 164, 139 166, 166, 182, 169, 159, 174, 166, 159 154, 149, 149, 174, 139, 151, 164, 137 172, 151, 161, 149, 154, 146, 142, 135 156, 149, 137, 161, 139, 159, 121, 154 156, 137, 159, 149, 151, 156, 151, 146 164, 161, 174, 180, 172, 180, 185, 169 149, 177, 146, 180, 169, 159, 164, 174 177, 149, 159, 161, 159, 137, 172, 174 188, 172, 169, 151, 182, 169, 156, 149 177, 164, 164, 139, 142, 159, 174, 135 154, 137, 149, 149, 154, 156, 149, 169 174, 142, 149, 139, 142, 139, 144, 110 137, 130, 149, 144, 149, 119, 146, 130 137, 151, 142, 164, 132, 154, 159, 151 164, 154, 151, 159, 146, 119, 161, 161 144, 146, 156, 156, 182, 169, 177, 164 188, 210, 234, 243, 259, 296, 361, 380 369, 445, 484, 449, 471, 384, 441, 372 306, 262, 246, 202, 172, 154, 154, 135 144, 154, 142, 117, 154, 132, 146, 112 139, 130, 139, 132, 119, 139, 121, 144 132, 114, 106, 121, 112, 98, 112, 117 121, 130, 110, 114, 123, 121, 119, 117 94, 114, 96, 102, 123, 108, 123, 125 114, 125, 102, 125, 125, 142, 135, 137 130, 135, 172, 154, 166, 190, 182, 169 164, 154, 154, 149, 130, 149, 130, 121 123, 135, 114, 100, 110, 121, 112, 123 121, 100, 108, 119, 112, 114, 123, 128 112, 114, 149, 132, 119, 108, 146, 121 96, 119, 125, 94, 114, 128, 119, 119 119, 106, 123, 130, 142, 110, 130, 123 132, 128, 128, 123, 137, 146, 154, 149 132, 164, 156, 156, 146, 156, 172, 190 182, 196, 199, 204, 193, 196, 228, 243 222, 207, 234, 253, 219, 219, 231, 225 276, 234, 246, 228, 259, 253, 253, 262 269, 266, 269, 276, 289, 262, 306, 253 246, 279, 237, 286, 250, 243, 243, 216 210, 182, 216, 196, 213, 202, 204, 180 204, 182, 199, 166, 182, 169, 164, 177 169, 188, 169, 159, 166, 177, 180, 164 177, 164, 185, 185, 182, 161, 177, 177 154, 182, 185, 151, 174, 159, 180, 161 199, 159, 174, 154, 151, 146, 149, 164 164, 166, 156, 161, 146, 156, 149, 146 154, 151, 185, 174, 177, 207, 172, 202 234, 234, 231, 231, 276, 259, 272, 246 213, 222, 188, 216, 225, 185, 196, 188 182, 174, 172, 161, 161, 169, 182, 151 177, 166, 185, 159, 202, 210, 204, 177 216, 177, 210, 188, 185, 185, 193, 161 149, 151, 149, 174, 180, 149, 199, 174 177, 161, 193, 159, 174, 169, 156, 154 151, 190, 161, 177, 169, 164, 185, 193 161, 174, 188, 177, 159, 164, 164, 125 142, 161, 137, 154, 166, 123, 146, 144 154, 132, 154, 151, 135, 156, 137, 169 161, 159, 174, 164, 164, 159, 159, 154 159, 149, 149, 117, 121, 166, 135, 117 142, 130, 112, 137, 137, 142, 112, 130 130, 132, 137, 132, 128, 135, 135, 139 121, 119, 130, 121, 123, 121, 110, 100 128, 102, 108, 132, 121, 108, 125, 108 121, 128, 132, 125, 128, 121, 156, 166 154, 169, 180, 182, 199, 207, 219, 204 190, 199, 188, 159, 166, 182, 154, 137 146, 121, 149, 144, 139, 121, 151, 130 128, 144, 130, 151, 123, 123, 137, 139 112, 123, 123, 130, 139, 154, 151, 156 125, 137, 144, 161, 156, 164, 149, 166 144, 161, 149, 146, 146, 137, 144, 161 132, 142, 108, 112, 121, 137, 125, 128 117, 142, 125, 139, 151, 177, 156, 144 135, 164, 159, 139, 174, 130, 154, 130 117, 121, 123, 142, 108, 104, 128, 110 137, 119, 117, 114, 119, 135, 135, 117 137, 114, 130, 128, 125, 121, 154, 123 123, 119, 137, 121, 94, 139, 119, 123 123, 130, 121, 125, 112, 132, 139, 108 117, 159, 112, 123, 149, 108, 137, 132 117, 125, 128, 119, 128, 121, 137, 125 137, 149, 106, 156, 132, 137, 164, 139 144, 139, 139, 128, 149, 149, 169, 169 180, 190, 207, 193, 204, 188, 185, 196 161, 169, 180, 137, 169, 149, 137, 123 125, 119, 121, 121, 130, 117, 130, 121 125, 121, 128, 123, 137, 106, 130, 110 130, 125, 114, 112, 123, 121, 119, 132 108, 125, 146, 130, 114, 112, 102, 121 102, 119, 108, 96, 110, 132, 100, 121 90, 114, 106, 90, 123, 123, 123, 135 117, 128, 117, 130, 128, 121, 142, 146 123, 132, 159, 149, 137, 139, 119, 144 154, 142, 132, 137, 110, 114, 128, 137 114, 125, 121, 144, 117, 117, 110, 125 106, 121, 135, 149, 169, 169, 199, 231 202, 207, 190, 180, 231, 199, 154, 151 154, 156, 169, 121, 149, 137, 125, 139 119, 117, 121, 117, 117, 108, 137, 128 110, 128, 98, 121, 146, 121, 130, 128 132, 149, 161, 144, 132, 137, 156, 180 190, 228, 225, 234, 269, 279, 331, 342 372, 372, 372, 376, 369, 350, 313, 269 292, 234, 231, 213, 213, 193, 159, 180 202, 172, 185, 190, 180, 188, 154, 144 144, 135, 121, 125, 135, 154, 106, 125 123, 117, 132, 88, 112, 121, 112, 114 106, 119, 104, 104, 96, 92, 88, 85 110, 98, 121, 96, 106, 112, 81, 137 96, 98, 106, 96, 106, 102, 110, 92 102, 117, 90, 98, 85, 92, 96, 83 104, 96, 94, 92, 90, 102, 104, 100 350, 96, 92, 102, 128, 108, 100, 108 98, 112, 90, 110, 110, 104, 96, 119 108, 123, 132, 130, 130, 121, 139, 125 112, 128, 117, 98, 117, 102, 102, 100 96, 88, 108, 100, 79, 100, 94, 85 92, 98, 96, 100, 121, 102, 106, 114 102, 135, 108, 88, 106, 123, 104, 117 246, 114, 104, 106, 114, 102, 104, 104 108, 92, 90, 94, 98, 98, 94, 83 102, 85, 108, 86, 98, 71, 85, 114 85, 102, 74, 96, 74, 90, 79, 81 74, 76, 90, 85, 102, 88, 83, 100 86, 104, 98, 77, 92, 90, 112, 112 92, 94, 88, 94, 96, 104, 90, 104 92, 92, 98, 104, 100, 100, 104, 114 94, 100, 88, 102, 110, 94, 96, 90 102, 102, 96, 83, 96, 100, 108, 96 90, 92, 117, 112, 130, 119, 114, 119 114, 139, 117, 139, 144, 169, 177, 174 207, 207, 272, 279, 299, 282, 262, 202 231, 225, 207, 182, 169, 149, 121, 117 110, 98, 104, 83, 106, 96, 117, 112 128, 117, 108, 108, 88, 98, 117, 98 108, 117, 114, 96, 88, 106, 94, 81 123, 90, 71, 106, 108, 102, 106, 100 104, 104, 86, 92, 96, 86, 102, 96 98, 79, 90, 108, 102, 85, 94, 108 100, 90, 81, 88, 100, 96, 112, 92 108, 98, 100, 86, 76, 85, 86, 86 83, 92, 100, 100, 102, 104, 66, 83 88, 83, 67, 88, 92, 86, 88, 88 96, 92, 102, 98, 85, 77, 85, 100 110, 100, 110, 94, 100, 108, 92, 117 83, 102, 92, 108, 104, 86, 100, 96 90, 94, 85, 92, 86, 83, 85, 86 96, 90, 117, 117, 79, 106, 119, 100 104, 102, 104, 106, 114, 119, 117, 98 106, 86, 117, 123, 104, 142, 96, 96 104, 117, 108, 123, 110, 128, 117, 121 117, 94, 125, 132, 123, 121, 110, 106 125, 112, 144, 106, 98, 128, 119, 123 114, 121, 100, 117, 144, 114, 149, 125 144, 98, 130, 146, 151, 125, 130, 125 137, 139, 117, 149, 149, 114, 130, 142 159, 151, 137, 123, 125, 121, 142, 114 137, 130, 125, 135, 149, 130, 112, 128 156, 125, 142, 121, 135, 142, 132, 137 135, 130, 106, 137, 156, 159, 154, 135 142, 159, 166, 169, 180, 161, 193, 196 185, 174, 190, 190, 185, 144, 182, 182 159, 159, 164, 151, 185, 164, 154, 149 177, 156, 182, 159, 169, 193, 172, 159 199, 164, 190, 142, 174, 180, 169, 154 177, 142, 161, 156, 159, 149, 159, 132 146, 154, 159, 144, 137, 135, 146, 137 156, 154, 142, 159, 172, 174, 112, 142 139, 149, 151, 169, 174, 156, 156, 164 164, 196, 182, 207, 228, 207, 210, 199 204, 222, 210, 216, 228, 228, 225, 240 243, 216, 234, 196, 210, 164, 196, 193 180, 172, 161, 154, 135, 151, 135, 142 123, 137, 146, 137, 144, 121, 128, 114 117, 119, 121, 137, 121, 88, 121, 121 110, 121, 130, 121, 130, 114, 128, 128 106, 142, 106, 132, 119, 110, 125, 100 114, 123, 125, 125, 132, 121, 110, 121 125, 108, 139, 130, 110, 100, 114, 128 125, 110, 98, 123, 94, 117, 117, 125 121, 110, 117, 130, 119, 108, 108, 92 117, 104, 112, 104, 119, 96, 100, 106 117, 98, 119, 119, 96, 106, 90, 112 92, 102, 114, 130, 112, 96, 96, 106 110, 121, 100, 114, 119, 123, 130, 102 128, 121, 102, 130, 137, 135, 121, 114 117, 110, 139, 110, 128, 117, 146, 132 100, 142, 130, 123, 121, 123, 110, 144 119, 108, 123, 132, 139, 151, 125, 108 142, 121, 125, 132, 137, 137, 123, 130 130, 125, 137, 119, 125, 137, 121, 144 137, 149, 161, 161, 125, 182, 154, 164 154, 185, 188, 193, 228, 222, 228, 234 243, 253, 219, 188, 222, 213, 210, 172 196, 196, 172, 164, 159, 149, 169, 313 128, 142, 142, 130, 123, 132, 137, 98 128, 130, 128, 121, 135, 137, 156, 130 112, 139, 135, 149, 132, 151, 135, 159 161, 144, 132, 149, 130, 164, 185, 139 132, 164, 174, 172, 164, 144, 164, 202 172, 161, 166, 172, 169, 196, 199, 182 177, 199, 174, 196, 196, 177, 174, 204 213, 213, 207, 207, 234, 222, 243, 225 237, 219, 228, 237, 216, 222, 228, 213 216, 231, 210, 237, 237, 199, 182, 193 188, 204, 174, 199, 177, 204, 185, 149 185, 164, 169, 159, 144, 172, 219, 146 188, 137, 151, 169, 159, 164, 156, 164 161, 144, 144, 132, 156, 142, 144, 149 132, 132, 154, 112, 142, 137, 130, 135 135, 128, 104, 125, 123, 106, 121, 121 125, 146, 125, 117, 139, 128, 123, 121 117, 100, 135, 112, 117, 130, 108, 100 125, 117, 114, 121, 123, 119, 108, 125 86, 106, 108, 112, 106, 117, 128, 119 114, 106, 137, 112, 100, 121, 102, 121 110, 100, 102, 94, 128, 128, 92, 132 106, 121, 119, 123, 130, 135, 125, 119 119, 144, 151, 142, 166, 130, 119, 137 144, 130, 137, 151, 151, 146, 149, 137 142, 121, 112, 156, 132, 117, 110, 117 106, 130, 94, 106, 121, 123, 100, 112 104, 102, 106, 119, 114, 98, 96, 117 117, 119, 110, 90, 92, 121, 123, 123 114, 88, 96, 106, 98, 125, 139, 106 117, 114, 121, 94, 108, 125, 106, 104 125, 100, 121, 104, 104, 98, 119, 106 98, 100, 90, 112, 112, 92, 100, 94 121, 98, 114, 90, 112, 104, 110, 90 112, 123, 114, 121, 104, 121, 137, 135 112, 112, 121, 108, 117, 119, 119, 119 104, 121, 137, 130, 125, 142, 137, 149 135, 146, 128, 156, 149, 137, 132, 121 121, 125, 144, 132, 132, 108, 110, 100 98, 86, 108, 106, 108, 106, 102, 79 100, 96, 104, 108, 112, 112, 117, 104 77, 106, 110, 100, 112, 104, 110, 121 108, 112, 106, 106, 112, 100, 100, 108 117, 117, 100, 123, 102, 100, 112, 106 135, 88, 110, 132, 110, 104, 123, 128 128, 142, 121, 112, 142, 128, 161, 174 161, 193, 166, 174, 199, 185, 180, 185 190, 190, 177, 169, 190, 164, 199, 159 185, 180, 182, 199, 190, 216, 199, 216 228, 207, 246, 266, 246, 289, 320, 289 306, 222, 256, 234, 210, 202, 172, 202 219, 172, 182, 149, 151, 149, 156, 130 130, 137, 98, 119, 102, 119, 96, 96 121, 108, 119, 104, 121, 119, 108, 132 102, 104, 117, 128, 119, 108, 104, 121 119, 121, 128, 210, 106, 139, 98, 139 121, 117, 106, 114, 121, 125, 154, 132 144, 125, 132, 125, 149, 123, 110, 125 125, 121, 135, 135, 102, 128, 137, 125 135, 139, 110, 128, 117, 123, 114, 121 137,/