SampleIdent,907a 17h-2 142-143bu,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,18-aug-1993 11:56,/ DataAngleRange, 2.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 83, 88, 86, 83, 77, 71, 76, 61 76, 86, 86, 74, 58, 71, 66, 56 71, 64, 62, 67, 72, 53, 72, 64 62, 74, 53, 61, 86, 74, 56, 53 59, 66, 56, 58, 76, 62, 64, 58 81, 59, 58, 58, 56, 59, 59, 59 45, 64, 77, 58, 76, 66, 56, 62 67, 66, 59, 71, 69, 71, 76, 83 64, 58, 66, 59, 67, 59, 59, 59 77, 56, 72, 72, 55, 59, 66, 71 66, 53, 64, 72, 90, 74, 67, 74 66, 53, 72, 83, 71, 59, 83, 72 72, 69, 88, 92, 83, 85, 77, 59 76, 72, 64, 83, 72, 77, 79, 77 83, 58, 72, 66, 85, 71, 66, 85 86, 104, 71, 76, 85, 74, 86, 72 62, 85, 66, 79, 76, 77, 71, 86 85, 85, 85, 66, 74, 88, 77, 83 92, 76, 94, 83, 85, 96, 83, 100 71, 94, 86, 96, 98, 100, 83, 74 96, 98, 92, 85, 86, 94, 83, 83 102, 88, 100, 117, 108, 100, 76, 81 102, 110, 100, 102, 90, 88, 106, 100 90, 100, 112, 77, 98, 94, 98, 128 94, 114, 96, 110, 119, 114, 112, 102 94, 102, 100, 123, 112, 106, 119, 128 114, 130, 119, 125, 108, 132, 102, 104 108, 114, 108, 144, 117, 130, 100, 121 114, 106, 128, 108, 125, 110, 117, 102 121, 110, 130, 104, 121, 117, 108, 108 114, 119, 128, 139, 121, 117, 132, 144 114, 123, 137, 125, 135, 119, 125, 125 130, 121, 121, 130, 132, 112, 125, 102 117, 142, 128, 112, 123, 114, 135, 135 151, 132, 128, 119, 123, 121, 121, 144 121, 139, 112, 144, 132, 114, 121, 137 104, 119, 121, 112, 137, 123, 130, 108 110, 119, 125, 119, 92, 110, 104, 121 112, 102, 130, 123, 121, 106, 130, 104 114, 92, 121, 102, 90, 114, 119, 108 123, 100, 117, 119, 110, 114, 110, 112 123, 121, 112, 90, 117, 119, 119, 114 117, 102, 112, 100, 114, 119, 139, 106 123, 104, 100, 112, 106, 98, 106, 110 108, 121, 106, 114, 90, 92, 110, 92 102, 117, 104, 106, 98, 108, 92, 110 110, 104, 79, 110, 108, 94, 79, 92 83, 114, 86, 98, 100, 86, 98, 88 72, 79, 83, 110, 110, 108, 104, 88 79, 77, 106, 106, 117, 81, 88, 86 108, 88, 98, 71, 90, 110, 100, 98 90, 90, 102, 90, 94, 90, 96, 86 100, 114, 83, 85, 88, 110, 94, 104 85, 79, 96, 85, 88, 85, 96, 92 86, 88, 96, 90, 98, 114, 92, 92 90, 94, 114, 79, 98, 83, 77, 79 79, 102, 76, 88, 90, 76, 88, 94 104, 108, 71, 86, 98, 72, 79, 100 98, 94, 100, 110, 102, 106, 94, 83 86, 98, 100, 104, 96, 83, 86, 94 108, 98, 100, 110, 85, 106, 86, 106 100, 94, 106, 100, 88, 88, 108, 92 90, 88, 104, 92, 110, 114, 77, 102 108, 112, 104, 92, 92, 100, 137, 112 88, 117, 106, 117, 121, 114, 110, 128 121, 106, 132, 125, 121, 110, 96, 110 112, 108, 83, 110, 108, 85, 79, 94 92, 117, 98, 96, 88, 96, 90, 83 90, 86, 86, 79, 86, 88, 90, 86 92, 76, 79, 100, 85, 92, 88, 90 94, 90, 92, 92, 96, 88, 90, 88 76, 106, 81, 86, 96, 90, 102, 72 85, 83, 77, 92, 94, 253, 86, 94 98, 92, 86, 85, 90, 94, 71, 90 88, 98, 88, 88, 98, 85, 92, 77 102, 100, 71, 81, 94, 77, 88, 102 86, 94, 79, 90, 90, 90, 88, 79 88, 90, 102, 77, 86, 92, 88, 102 94, 88, 98, 106, 90, 88, 77, 77 72, 90, 90, 88, 92, 106, 90, 83 72, 88, 106, 79, 94, 92, 92, 85 106, 88, 104, 77, 83, 94, 88, 86 83, 88, 88, 104, 94, 108, 92, 88 83, 106, 79, 102, 86, 85, 106, 86 98, 83, 98, 86, 88, 90, 106, 94 76, 98, 74, 86, 83, 94, 96, 86 100, 83, 98, 77, 86, 92, 98, 88 92, 106, 112, 79, 104, 106, 96, 92 104, 88, 108, 102, 96, 88, 106, 104 98, 81, 102, 94, 102, 92, 96, 102 90, 108, 98, 96, 98, 96, 85, 86 76, 108, 100, 102, 94, 77, 96, 90 94, 117, 96, 106, 85, 100, 102, 100 98, 96, 100, 92, 94, 106, 112, 102 108, 110, 102, 90, 110, 106, 117, 125 94, 106, 114, 112, 117, 108, 108, 102 114, 94, 108, 100, 98, 121, 102, 98 108, 98, 110, 108, 98, 112, 114, 106 104, 125, 117, 121, 123, 119, 121, 106 135, 130, 100, 104, 106, 104, 121, 106 102, 117, 117, 100, 96, 104, 114, 110 100, 98, 110, 108, 112, 114, 121, 112 110, 112, 106, 119, 88, 108, 119, 128 110, 123, 98, 100, 112, 121, 110, 110 112, 110, 114, 92, 125, 104, 125, 121 123, 117, 135, 117, 110, 98, 119, 121 117, 121, 96, 132, 114, 128, 128, 146 123, 132, 135, 125, 100, 114, 121, 149 144, 146, 139, 128, 139, 149, 182, 149 159, 137, 159, 159, 164, 164, 154, 188 172, 199, 190, 180, 204, 243, 202, 222 219, 272, 240, 253, 250, 237, 243, 231 231, 250, 253, 213, 210, 199, 199, 225 202, 190, 228, 199, 193, 204, 216, 185 202, 193, 204, 202, 185, 177, 185, 193 190, 188, 174, 210, 154, 190, 188, 166 185, 193, 156, 174, 180, 193, 213, 182 222, 210, 228, 228, 259, 237, 253, 246 262, 269, 289, 299, 231, 207, 225, 207 222, 204, 177, 202, 207, 202, 193, 210 196, 188, 190, 164, 190, 185, 156, 172 182, 188, 164, 161, 196, 174, 196, 169 202, 196, 199, 172, 199, 185, 172, 146 202, 207, 174, 169, 193, 185, 177, 196 164, 154, 180, 199, 174, 188, 193, 185 199, 216, 213, 185, 180, 177, 174, 199 177, 169, 172, 174, 185, 180, 182, 190 174, 159, 169, 193, 161, 169, 164, 185 161, 204, 199, 188, 169, 180, 161, 185 164, 193, 188, 154, 190, 196, 182, 182 185, 180, 174, 182, 174, 188, 196, 182 193, 172, 182, 196, 193, 193, 193, 185 210, 196, 169, 199, 188, 185, 199, 174 188, 174, 177, 193, 169, 174, 449, 207 164, 182, 182, 207, 222, 202, 207, 219 219, 222, 231, 213, 180, 216, 182, 193 210, 219, 222, 196, 180, 193, 199, 204 196, 185, 193, 213, 174, 219, 182, 202 202, 182, 185, 213, 199, 188, 228, 177 182, 213, 188, 216, 174, 190, 190, 219 202, 202, 202, 196, 216, 199, 190, 199 193, 196, 210, 172, 204, 243, 190, 216 246, 196, 222, 216, 219, 219, 237, 219 234, 272, 231, 234, 228, 240, 246, 246 228, 219, 259, 256, 240, 228, 234, 231 240, 231, 219, 253, 259, 240, 234, 210 199, 199, 225, 225, 243, 234, 234, 234 225, 222, 204, 204, 202, 216, 196, 202 207, 204, 199, 207, 216, 216, 219, 213 204, 202, 225, 185, 177, 213, 199, 196 213, 219, 177, 193, 213, 210, 169, 219 199, 204, 210, 202, 219, 202, 256, 243 225, 207, 202, 237, 225, 243, 262, 266 246, 310, 365, 380, 433, 506, 605, 686 740, 829, 876, 853, 790, 713, 620, 538 471, 416, 313, 313, 303, 324, 269, 262 240, 269, 219, 243, 246, 250, 219, 253 253, 237, 219, 250, 225, 204, 222, 234 216, 216, 253, 231, 240, 234, 256, 237 225, 240, 237, 225, 210, 246, 240, 256 253, 225, 240, 234, 243, 228, 276, 210 228, 237, 216, 253, 231, 234, 231, 246 266, 272, 299, 262, 256, 259, 250, 253 228, 219, 228, 219, 228, 225, 213, 228 210, 210, 185, 188, 219, 234, 182, 237 234, 196, 210, 210, 199, 225, 202, 222 228, 196, 225, 199, 190, 193, 210, 193 219, 199, 207, 202, 188, 219, 199, 169 185, 219, 207, 196, 202, 196, 185, 207 222, 207, 185, 202, 193, 213, 193, 204 199, 207, 202, 219, 196, 207, 202, 207 196, 180, 193, 190, 216, 213, 210, 225 196, 180, 213, 182, 199, 190, 174, 196 180, 222, 210, 193, 216, 193, 199, 213 188, 213, 210, 202, 202, 210, 188, 213 193, 210, 202, 190, 188, 182, 166, 210 174, 202, 190, 196, 180, 199, 196, 172 188, 177, 172, 202, 188, 204, 199, 188 213, 172, 185, 174, 188, 202, 182, 182 190, 188, 161, 156, 188, 188, 207, 174 182, 188, 180, 180, 219, 202, 213, 202 185, 202, 169, 188, 196, 199, 169, 196 159, 188, 161, 182, 185, 174, 159, 174 207, 188, 172, 202, 166, 210, 193, 196 166, 182, 182, 177, 182, 219, 190, 228 259, 237, 292, 350, 339, 339, 388, 384 353, 365, 369, 324, 303, 282, 219, 207 188, 210, 199, 190, 193, 180, 172, 188 182, 210, 174, 177, 169, 154, 193, 213 164, 174, 156, 177, 159, 142, 172, 151 172, 182, 193, 149, 174, 159, 172, 174 144, 174, 180, 159, 151, 161, 151, 161 144, 159, 137, 172, 166, 180, 159, 146 166, 146, 154, 159, 166, 154, 174, 174 166, 159, 159, 185, 154, 177, 164, 196 164, 151, 137, 159, 151, 151, 161, 159 149, 169, 182, 151, 416, 123, 137, 166 169, 149, 196, 164, 164, 164, 151, 139 166, 149, 169, 137, 142, 142, 166, 149 151, 164, 174, 149, 154, 139, 154, 144 149, 164, 132, 164, 174, 161, 185, 164 164, 182, 182, 182, 174, 169, 144, 151 164, 161, 185, 180, 202, 151, 196, 199 174, 193, 188, 182, 193, 180, 207, 219 222, 190, 213, 237, 228, 199, 231, 240 228, 243, 207, 222, 216, 237, 246, 259 240, 256, 250, 246, 259, 240, 210, 253 250, 225, 222, 234, 210, 190, 202, 196 174, 204, 180, 185, 193, 219, 159, 213 188, 222, 199, 210, 185, 196, 196, 174 196, 199, 188, 204, 177, 193, 151, 172 169, 193, 164, 204, 188, 177, 169, 182 216, 177, 185, 193, 202, 188, 185, 174 202, 174, 182, 193, 188, 182, 166, 196 172, 154, 169, 159, 149, 182, 164, 169 188, 174, 172, 193, 188, 185, 210, 216 216, 222, 207, 174, 210, 177, 213, 182 199, 169, 169, 156, 174, 174, 174, 161 190, 180, 166, 159, 146, 188, 169, 154 174, 159, 166, 161, 142, 149, 156, 182 172, 190, 182, 161, 180, 166, 174, 177 169, 159, 166, 172, 149, 185, 135, 161 193, 159, 180, 164, 156, 154, 199, 174 159, 172, 174, 172, 202, 196, 196, 151 196, 151, 161, 149, 164, 177, 172, 169 161, 182, 185, 156, 159, 142, 149, 142 159, 185, 146, 182, 144, 164, 174, 166 156, 185, 159, 185, 182, 164, 166, 174 154, 149, 159, 169, 149, 156, 144, 132 149, 139, 144, 142, 146, 164, 149, 151 182, 135, 144, 154, 130, 139, 137, 135 119, 137, 142, 123, 117, 139, 135, 144 166, 139, 130, 146, 128, 132, 144, 144 156, 151, 146, 137, 128, 154, 174, 159 169, 185, 190, 182, 188, 182, 193, 159 159, 180, 174, 139, 161, 149, 142, 149 151, 144, 142, 149, 135, 119, 154, 106 137, 121, 166, 151, 128, 121, 174, 144 135, 144, 159, 174, 146, 169, 151, 156 172, 146, 180, 151, 146, 174, 169, 156 149, 169, 137, 144, 137, 135, 144, 142 130, 132, 142, 108, 135, 139, 123, 159 142, 139, 159, 137, 164, 135, 149, 149 132, 142, 182, 164, 156, 164, 142, 135 156, 142, 139, 144, 154, 149, 149, 146 151, 159, 128, 174, 156, 149, 161, 144 128, 137, 159, 164, 137, 135, 154, 142 130, 149, 149, 123, 146, 156, 146, 164 159, 144, 164, 142, 161, 156, 154, 146 151, 156, 151, 172, 174, 135, 149, 149 144, 142, 154, 130, 156, 146, 139, 135 123, 151, 125, 151, 135, 154, 151, 139 156, 169, 159, 156, 190, 196, 177, 202 182, 193, 190, 190, 166, 193, 156, 156 142, 169, 149, 146, 144, 146, 151, 135 144, 177, 161, 139, 137, 135, 146, 161 144, 137, 149, 137, 149, 142, 149, 137 130, 128, 137, 142, 144, 151, 112, 154 161, 146, 154, 128, 161, 149, 121, 137 156, 149, 151, 149, 161, 123, 139, 130 154, 154, 149, 156, 128, 137, 137, 125 159, 154, 149, 135, 142, 161, 154, 142 177, 151, 159, 161, 164, 139, 172, 172 174, 154, 154, 159, 139, 161, 149, 123 169, 151, 142, 135, 142, 125, 121, 166 151, 154, 156, 182, 188, 199, 199, 231 222, 190, 202, 180, 216, 180, 161, 182 172, 156, 174, 149, 151, 146, 137, 128 137, 142, 142, 144, 149, 156, 139, 142 164, 149, 154, 164, 144, 159, 149, 164 172, 172, 169, 159, 180, 180, 161, 207 202, 193, 207, 256, 269, 266, 253, 282 272, 269, 276, 213, 237, 204, 204, 193 188, 166, 172, 144, 180, 172, 164, 149 159, 177, 166, 159, 151, 159, 172, 172 159, 137, 146, 154, 144, 146, 142, 130 156, 123, 132, 123, 137, 151, 121, 125 123, 121, 125, 137, 159, 128, 137, 135 123, 137, 142, 128, 142, 125, 142, 119 135, 121, 139, 123, 121, 137, 132, 139 139, 159, 149, 156, 149, 112, 146, 121 121, 132, 139, 119, 137, 112, 135, 132 112, 137, 144, 125, 151, 125, 100, 125 128, 130, 104, 121, 119, 125, 119, 114 130, 104, 135, 123, 149, 117, 123, 135 137, 130, 130, 119, 146, 125, 159, 137 119, 137, 123, 128, 137, 123, 132, 110 135, 128, 135, 135, 137, 149, 135, 128 130, 128, 135, 117, 137, 130, 123, 144 121, 149, 137, 146, 130, 132, 121, 132 149, 135, 144, 128, 130, 114, 121, 149 123, 146, 132, 121, 121, 117, 128, 132 144, 130, 123, 130, 121, 139, 130, 130 117, 146, 125, 132, 119, 132, 106, 130 117, 119, 117, 123, 121, 139, 130, 139 132, 125, 114, 135, 137, 135, 117, 119 135, 128, 146, 135, 130, 112, 123, 119 137, 119, 123, 135, 123, 144, 132, 130 146, 137, 121, 135, 121, 130, 117, 130 125, 121, 137, 121, 137, 132, 119, 142 142, 137, 142, 154, 169, 182, 180, 216 207, 210, 204, 228, 202, 199, 185, 188 188, 169, 130, 154, 146, 121, 104, 139 139, 130, 137, 130, 130, 121, 132, 123 139, 130, 151, 130, 156, 135, 121, 132 149, 130, 144, 149, 137, 121, 139, 137 146, 121, 144, 119, 128, 114, 130, 119 125, 144, 132, 114, 132, 130, 159, 135 121, 135, 132, 121, 146, 123, 130, 154 149, 135, 117, 125, 112, 135, 112, 130 130, 130, 137, 139, 128, 132, 151, 132 137, 119, 142, 121, 128, 128, 121, 121 121, 130, 142, 110, 123, 117, 154, 121 125, 125, 123, 128, 137, 139, 117, 135 132, 106, 135, 121, 114, 137, 132, 121 128, 128, 125, 146, 139, 121, 119, 135 123, 130, 144, 130, 121, 144, 121, 121 128, 144, 121, 98, 119, 128, 149, 137 130, 130, 130, 135, 146, 146, 149, 154 164, 142, 137, 130, 123, 121, 108, 159 149, 137, 161, 121, 137, 123, 137, 130 137, 144, 144, 159, 139, 130, 123, 154 151, 144, 154, 137, 137, 154, 142, 146 135, 117, 185, 151, 144, 149, 149, 149 154, 154, 137, 169, 177, 172, 139, 156 154, 172, 151, 166, 151, 137, 164, 142 182, 151, 146, 159, 164, 180, 149, 159 166, 161, 161, 121, 128, 237, 149, 166 161, 144, 151, 144, 144, 159, 151, 164 151, 159, 156, 132, 159, 174, 177, 177 180, 169, 190, 169, 182, 202, 174, 210 177, 182, 199, 182, 188, 174, 182, 182 172, 188, 188, 188, 172, 154, 180, 151 190, 174, 172, 185, 177, 174, 169, 182 193, 196, 151, 149, 174, 151, 177, 182 172, 169, 159, 154, 188, 188, 169, 159 190, 174, 146, 174, 169, 159, 151, 164 185, 164, 174, 135, 154, 156, 164, 159 164, 172, 177, 154, 166, 164, 146, 188 174, 180, 166, 180, 159, 161, 159, 169 166, 169, 166, 185, 182, 182, 213, 188 164, 159, 196, 190, 172, 169, 188, 164 164, 144, 159, 169, 159, 156, 151, 139 182, 151, 169, 130, 159, 161, 169, 142 149, 146, 137, 146, 151, 119, 169, 137 177, 144, 125, 144, 177, 169, 156, 161 149, 164, 128, 137, 130, 144, 177, 149 161, 151, 164, 139, 159, 142, 144, 154 161, 146, 164, 159, 142, 151, 161, 144 159, 154, 185, 166, 161, 154, 151, 169 135, 159, 156, 154, 149, 151, 164, 128 174, 161, 128, 169, 159, 164, 159, 144 123, 154, 144, 146, 146, 151, 151, 146 164, 174, 166, 154, 144, 161, 164, 172 154, 177, 177, 154, 180, 164, 156, 156 142, 154, 174, 149, 154, 169, 154, 142 144, 149, 156, 139, 139, 146, 164, 151 144, 151, 144, 166, 154, 156, 159, 146 142, 161, 185, 182, 180, 166, 137, 164 151, 177, 296, 146, 156, 169, 151, 154 159, 174, 139, 156, 166, 164, 180, 190 154, 149, 166, 174, 164, 164, 216, 199 207, 231, 207, 219, 202, 219, 234, 216 210, 207, 199, 228, 207, 177, 199, 177 177, 182, 164, 185, 166, 161, 154, 156 159, 166, 177, 164, 144, 159, 146, 199 144, 164, 154, 151, 174, 177, 164, 156 180, 177, 164, 154, 177, 182, 164, 188 149, 172, 164, 180, 172, 146, 190, 172 177, 159, 174, 169, 182, 154, 185, 166 164, 199, 202, 199, 188, 213, 177, 185 216, 182, 196, 207, 185, 164, 185, 169 188, 207, 188, 204, 199, 454, 237, 210 213, 188, 213, 210, 216, 216, 188, 234 213, 207, 188, 234, 202, 222, 228, 196 222, 213, 185, 193, 199, 182, 188, 196 182, 202, 190, 188, 207, 174, 190, 182 207, 213, 180, 188, 207, 174, 196, 193 185, 207, 216, 199, 156, 164, 164, 180 210, 161, 188, 164, 169, 161, 177, 169 154, 164, 154, 166, 164, 185, 177, 169 161, 164, 159, 174, 161, 166, 164, 188 188, 149, 154, 149, 149, 159, 172, 161 156, 169, 161, 159, 156, 174, 193, 166 151, 149, 174, 188, 142, 177, 161, 161 137, 139, 149, 185, 154, 149, 172, 174 185, 182, 164, 159, 180, 177, 149, 174 154, 164, 172, 174, 164, 185, 196, 161 172, 177, 180, 164, 142, 169, 164, 180 172, 177, 174, 159, 180, 174, 182, 149 146, 169, 142, 169, 185, 166, 169, 177 149, 142, 169, 159, 177, 172, 164, 139 146, 156, 159, 164, 169, 164, 182, 156 180, 159, 180, 159, 166, 174, 193, 166 149, 137, 182, 169, 174, 169, 174, 188 180, 154, 185, 161, 154, 172, 154, 164 172, 161, 188, 159, 172, 154, 180, 149 164, 185, 174, 166, 159, 154, 164, 161 172, 166, 144, 154, 169, 139, 146, 166 164, 164, 154, 164, 174, 169, 172, 172 174, 146, 161, 164, 154, 154, 185, 156 193, 164, 169, 174, 159, 161, 177, 169 159, 185, 159, 164, 154, 174, 172, 169 166, 154, 166, 159, 149, 180, 177, 154 174, 172, 159, 169, 169, 137, 161, 169 182, 169, 169, 185, 164, 190, 177, 154 159, 154, 154, 164, 156, 156, 159, 174 146, 174, 154, 169, 174, 185, 146, 174 164, 151, 169, 185, 164, 149, 172, 139 193, 161, 166, 166, 139, 159, 159, 154 182, 169, 164, 166, 164, 193, 154, 193 188, 207, 193, 196, 180, 149, 207, 177 164, 174, 185, 161, 182, 199, 188, 182 193, 188, 196, 216, 196, 246, 240, 207 234, 196, 207, 210, 219, 219, 207, 213 193, 210, 177, 177, 188, 196, 164, 182 193, 156, 164, 196, 166, 182, 164, 149 156, 137, 151, 151, 193, 169, 146, 164 174, 154, 169, 166, 144, 164, 159, 164 149, 177, 166, 159, 154, 159, 156, 154 154, 185, 151, 154, 166, 156, 164, 149 172, 172, 177, 149, 174, 154, 149, 151 177, 161, 154, 182, 185, 169, 164, 159 169, 169, 156, 164, 166, 151, 159, 159 174, 174, 156, 159, 161, 174, 180,/