SampleIdent,907a 17h-3 76-77bulk,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,18-aug-1993 12:54,/ DataAngleRange, 2.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 100, 76, 85, 79, 85, 98, 88, 86 85, 76, 92, 81, 77, 76, 92, 66 74, 76, 74, 85, 67, 66, 67, 85 59, 69, 77, 77, 52, 52, 79, 69 64, 71, 72, 61, 77, 81, 69, 71 74, 83, 83, 71, 71, 56, 74, 72 58, 59, 88, 69, 85, 66, 83, 67 77, 71, 77, 71, 66, 86, 72, 72 64, 76, 67, 61, 77, 72, 85, 66 77, 69, 76, 74, 53, 59, 77, 71 66, 72, 69, 83, 72, 67, 71, 85 85, 64, 59, 71, 62, 66, 74, 81 83, 69, 81, 79, 71, 86, 72, 86 96, 94, 88, 66, 83, 72, 77, 64 83, 90, 76, 88, 77, 88, 66, 86 76, 79, 81, 77, 88, 85, 100, 96 92, 90, 98, 104, 88, 106, 85, 96 365, 98, 90, 110, 88, 86, 83, 86 90, 96, 96, 88, 83, 94, 106, 83 83, 94, 98, 96, 90, 92, 94, 85 100, 96, 79, 85, 106, 106, 76, 85 94, 92, 108, 100, 98, 94, 92, 100 125, 114, 100, 106, 112, 90, 128, 108 98, 121, 112, 104, 102, 94, 100, 117 100, 114, 114, 119, 100, 86, 132, 110 123, 108, 108, 100, 96, 114, 106, 119 130, 128, 102, 117, 135, 139, 142, 123 125, 132, 128, 119, 121, 121, 137, 144 119, 117, 130, 104, 110, 130, 130, 121 130, 112, 128, 130, 135, 121, 121, 137 142, 142, 135, 135, 119, 106, 121, 117 130, 123, 125, 110, 144, 117, 128, 130 135, 130, 137, 135, 125, 114, 119, 119 114, 114, 130, 121, 123, 137, 121, 125 110, 102, 128, 112, 112, 119, 110, 100 128, 121, 119, 121, 123, 144, 117, 123 117, 114, 112, 119, 112, 119, 123, 110 108, 121, 117, 121, 92, 98, 110, 90 112, 100, 144, 100, 119, 121, 119, 106 108, 104, 117, 98, 102, 98, 110, 121 128, 108, 119, 110, 102, 132, 114, 96 106, 125, 125, 110, 110, 121, 98, 117 117, 112, 112, 128, 119, 114, 102, 121 102, 135, 102, 112, 90, 117, 96, 119 102, 102, 100, 119, 98, 83, 104, 100 96, 104, 102, 94, 86, 94, 100, 108 106, 76, 100, 100, 104, 104, 90, 88 96, 114, 90, 90, 106, 96, 90, 96 102, 92, 102, 96, 104, 92, 90, 96 102, 104, 94, 92, 86, 106, 90, 86 92, 85, 86, 77, 112, 98, 86, 102 90, 100, 85, 86, 98, 98, 100, 102 102, 98, 81, 112, 90, 88, 85, 83 96, 96, 110, 102, 104, 96, 104, 104 94, 94, 100, 86, 98, 90, 114, 100 86, 83, 90, 90, 96, 112, 100, 108 96, 92, 74, 86, 98, 90, 90, 96 86, 96, 83, 88, 85, 94, 88, 88 90, 100, 90, 90, 94, 92, 92, 81 88, 88, 67, 86, 85, 92, 72, 100 90, 71, 94, 106, 74, 81, 94, 100 102, 94, 88, 85, 90, 100, 86, 102 83, 85, 90, 94, 90, 94, 90, 96 90, 81, 88, 92, 88, 102, 100, 108 112, 121, 102, 81, 98, 96, 123, 104 92, 86, 114, 112, 86, 112, 92, 90 92, 86, 98, 96, 88, 85, 88, 83 79, 67, 96, 102, 79, 98, 90, 76 81, 88, 85, 83, 86, 86, 102, 96 86, 77, 100, 100, 96, 96, 71, 79 90, 72, 88, 77, 102, 85, 94, 88 94, 102, 88, 104, 90, 106, 92, 100 79, 88, 96, 104, 94, 90, 94, 85 104, 94, 88, 110, 94, 90, 96, 79 94, 86, 92, 83, 86, 100, 77, 72 81, 79, 85, 92, 88, 86, 81, 98 88, 98, 94, 119, 88, 71, 110, 85 100, 94, 106, 94, 100, 104, 100, 81 88, 88, 86, 90, 83, 94, 98, 100 98, 98, 96, 90, 81, 77, 92, 94 90, 96, 110, 92, 92, 86, 88, 90 92, 98, 76, 83, 110, 88, 76, 81 112, 119, 90, 106, 88, 86, 90, 110 96, 86, 100, 98, 92, 94, 69, 86 94, 77, 85, 94, 79, 85, 79, 83 85, 86, 77, 77, 90, 98, 96, 94 85, 88, 96, 100, 106, 76, 92, 92 102, 85, 81, 83, 94, 67, 100, 88 98, 94, 94, 96, 92, 86, 92, 90 83, 92, 79, 98, 102, 85, 86, 96 79, 86, 102, 88, 94, 77, 112, 85 94, 86, 106, 98, 88, 96, 104, 90 83, 98, 94, 94, 94, 100, 98, 96 92, 86, 102, 106, 98, 112, 98, 96 100, 98, 98, 77, 94, 94, 108, 96 85, 96, 90, 83, 92, 88, 92, 96 102, 98, 119, 114, 88, 102, 98, 100 114, 88, 96, 100, 92, 106, 108, 96 104, 112, 104, 130, 119, 112, 94, 100 96, 90, 98, 98, 119, 110, 100, 100 92, 106, 104, 112, 106, 114, 100, 102 102, 114, 110, 112, 102, 102, 110, 106 106, 102, 96, 121, 128, 114, 117, 104 86, 112, 110, 96, 114, 130, 108, 106 108, 104, 102, 104, 121, 139, 117, 132 135, 135, 123, 114, 121, 132, 114, 121 132, 130, 104, 96, 119, 130, 112, 132 110, 137, 146, 119, 154, 128, 121, 137 123, 149, 156, 156, 159, 156, 146, 151 139, 177, 174, 164, 156, 164, 172, 174 196, 180, 180, 213, 225, 225, 219, 216 219, 202, 193, 243, 199, 190, 180, 188 207, 180, 151, 207, 199, 174, 202, 182 169, 174, 166, 185, 169, 164, 199, 174 164, 164, 166, 161, 164, 174, 169, 185 161, 159, 146, 144, 174, 180, 164, 204 185, 174, 177, 169, 172, 193, 196, 196 210, 228, 256, 240, 219, 269, 253, 292 231, 216, 216, 202, 202, 174, 182, 174 169, 172, 142, 156, 156, 161, 159, 164 159, 151, 156, 177, 166, 144, 172, 166 174, 164, 164, 169, 169, 182, 149, 164 177, 149, 182, 154, 182, 164, 182, 161 137, 190, 161, 177, 149, 177, 161, 159 188, 188, 188, 182, 188, 180, 177, 199 188, 199, 169, 196, 185, 188, 154, 182 180, 156, 174, 172, 161, 156, 149, 164 182, 161, 172, 142, 174, 188, 154, 169 177, 169, 190, 159, 169, 159, 172, 156 174, 164, 174, 188, 156, 185, 177, 169 199, 169, 185, 177, 177, 164, 166, 161 188, 174, 193, 169, 164, 188, 182, 172 164, 174, 202, 185, 193, 177, 172, 154 166, 169, 164, 188, 180, 196, 185, 166 213, 174, 188, 193, 185, 174, 182, 196 202, 188, 199, 185, 210, 177, 207, 182 174, 182, 196, 193, 193, 199, 196, 193 161, 182, 169, 185, 182, 164, 180, 188 193, 213, 180, 182, 182, 177, 190, 177 188, 193, 207, 172, 207, 172, 196, 210 180, 177, 185, 204, 177, 177, 196, 190 216, 180, 177, 169, 164, 177, 190, 169 216, 172, 182, 193, 193, 193, 196, 196 225, 185, 202, 174, 188, 204, 210, 180 188, 207, 204, 196, 193, 207, 213, 234 231, 190, 210, 180, 185, 222, 196, 199 219, 202, 182, 190, 199, 207, 190, 193 213, 202, 207, 228, 216, 225, 188, 174 182, 185, 182, 202, 166, 202, 190, 174 204, 177, 213, 188, 199, 174, 164, 193 213, 174, 182, 169, 174, 169, 174, 204 177, 204, 182, 210, 222, 190, 231, 250 207, 240, 234, 231, 234, 292, 272, 346 396, 620, 666, 713, 660, 718, 718, 756 660, 671, 630, 590, 497, 433, 396, 376 303, 276, 272, 253, 246, 225, 243, 210 210, 204, 204, 193, 188, 182, 177, 202 207, 213, 193, 185, 185, 185, 210, 225 219, 216, 219, 216, 237, 213, 210, 210 225, 237, 193, 250, 228, 240, 228, 222 225, 250, 216, 240, 256, 250, 279, 282 246, 303, 289, 289, 299, 286, 279, 259 279, 282, 282, 253, 259, 202, 237, 216 216, 219, 216, 222, 213, 222, 207, 190 199, 207, 202, 190, 225, 204, 196, 204 199, 193, 185, 180, 207, 210, 185, 202 196, 202, 202, 185, 182, 174, 193, 156 199, 156, 174, 193, 182, 182, 199, 177 188, 188, 180, 199, 188, 182, 174, 174 202, 185, 188, 169, 180, 193, 177, 207 188, 185, 174, 449, 193, 190, 193, 210 185, 180, 199, 172, 202, 169, 199, 174 190, 180, 196, 185, 185, 193, 190, 210 188, 210, 199, 193, 177, 185, 225, 207 202, 182, 216, 207, 216, 185, 193, 174 156, 180, 190, 202, 164, 185, 164, 188 199, 202, 159, 185, 210, 185, 174, 202 196, 196, 177, 180, 190, 210, 188, 190 180, 180, 182, 174, 154, 180, 182, 182 174, 174, 172, 177, 185, 180, 169, 161 151, 188, 149, 172, 169, 188, 182, 159 161, 164, 159, 166, 172, 174, 172, 177 169, 174, 166, 161, 185, 174, 169, 159 156, 164, 161, 180, 177, 154, 169, 190 185, 182, 188, 202, 234, 246, 259, 289 292, 335, 282, 357, 346, 350, 317, 331 328, 279, 259, 240, 237, 222, 193, 166 182, 196, 169, 177, 177, 154, 164, 164 182, 156, 146, 174, 149, 164, 151, 132 166, 156, 146, 169, 154, 164, 142, 164 149, 149, 159, 166, 144, 154, 142, 146 139, 161, 144, 154, 156, 154, 135, 149 142, 156, 164, 149, 144, 154, 154, 156 161, 146, 161, 146, 144, 159, 159, 154 142, 144, 154, 149, 130, 161, 161, 121 154, 159, 159, 144, 130, 166, 154, 139 132, 121, 159, 154, 135, 154, 123, 154 166, 151, 132, 342, 149, 159, 137, 130 169, 159, 177, 125, 146, 149, 135, 135 154, 164, 169, 130, 144, 128, 146, 174 154, 172, 164, 154, 151, 159, 144, 177 161, 156, 159, 164, 146, 151, 164, 182 193, 182, 180, 185, 199, 174, 185, 193 188, 207, 207, 174, 196, 199, 210, 196 207, 188, 210, 169, 196, 210, 196, 219 199, 225, 216, 204, 231, 246, 243, 216 231, 231, 216, 219, 199, 204, 222, 204 222, 222, 193, 185, 202, 174, 188, 185 180, 204, 166, 180, 193, 188, 188, 180 188, 172, 180, 185, 169, 240, 180, 185 196, 210, 177, 172, 161, 188, 156, 202 159, 144, 149, 169, 144, 166, 185, 166 185, 169, 164, 172, 159, 169, 151, 180 174, 185, 151, 151, 146, 139, 164, 166 174, 185, 154, 137, 149, 159, 182, 174 169, 177, 196, 174, 180, 193, 202, 222 190, 202, 196, 193, 174, 182, 188, 151 146, 177, 159, 154, 154, 166, 182, 159 159, 128, 156, 154, 161, 188, 151, 188 142, 139, 137, 174, 149, 144, 161, 164 169, 161, 164, 156, 144, 146, 130, 132 169, 164, 149, 151, 146, 156, 151, 151 149, 128, 164, 174, 144, 177, 199, 164 164, 156, 164, 149, 128, 149, 144, 130 144, 151, 154, 144, 149, 146, 154, 154 142, 128, 151, 142, 146, 139, 151, 159 146, 159, 161, 169, 159, 166, 188, 156 144, 166, 137, 132, 125, 137, 137, 121 149, 130, 121, 125, 137, 112, 146, 146 137, 135, 130, 112, 132, 149, 128, 125 128, 130, 137, 128, 135, 137, 139, 159 112, 130, 144, 132, 137, 144, 146, 135 130, 130, 132, 119, 154, 104, 121, 132 130, 154, 137, 149, 151, 166, 188, 151 159, 154, 185, 172, 164, 156, 144, 151 144, 121, 130, 130, 135, 132, 142, 142 137, 159, 149, 139, 135, 361, 144, 135 137, 149, 142, 137, 146, 130, 125, 139 137, 142, 142, 164, 144, 156, 146, 149 142, 169, 135, 164, 161, 159, 146, 151 132, 144, 130, 125, 137, 132, 132, 132 169, 142, 123, 149, 144, 144, 117, 132 137, 121, 144, 121, 142, 154, 128, 151 142, 137, 151, 114, 135, 139, 137, 139 144, 123, 128, 117, 130, 128, 139, 132 128, 117, 149, 125, 137, 142, 119, 146 135, 144, 144, 119, 139, 149, 164, 135 146, 130, 132, 149, 137, 137, 137, 106 146, 135, 119, 149, 142, 135, 139, 137 149, 151, 146, 144, 132, 151, 128, 144 117, 137, 146, 154, 125, 146, 139, 149 149, 151, 137, 149, 144, 139, 156, 137 154, 174, 161, 172, 166, 190, 154, 164 177, 164, 154, 159, 151, 154, 161, 164 128, 139, 114, 146, 137, 135, 154, 159 135, 130, 149, 130, 123, 156, 123, 156 132, 149, 117, 125, 139, 123, 139, 146 123, 128, 144, 104, 119, 119, 121, 144 144, 128, 132, 119, 135, 130, 144, 119 106, 130, 104, 114, 130, 135, 132, 135 130, 130, 144, 123, 130, 132, 135, 149 142, 128, 132, 137, 151, 135, 159, 151 154, 172, 137, 142, 154, 149, 149, 156 154, 123, 144, 149, 144, 130, 132, 137 128, 149, 139, 144, 125, 146, 151, 146 164, 144, 159, 196, 182, 172, 196, 188 180, 182, 174, 207, 169, 185, 137, 142 149, 161, 123, 137, 142, 137, 159, 137 132, 135, 137, 144, 125, 130, 154, 125 142, 144, 137, 139, 142, 159, 144, 139 144, 142, 159, 164, 190, 182, 228, 234 250, 246, 243, 262, 253, 250, 259, 259 225, 240, 204, 216, 182, 182, 190, 169 174, 159, 151, 159, 180, 142, 172, 169 137, 135, 135, 146, 144, 137, 139, 125 159, 132, 117, 149, 149, 106, 104, 146 121, 121, 106, 132, 139, 114, 128, 117 135, 121, 121, 108, 132, 132, 132, 130 125, 132, 128, 137, 125, 130, 112, 110 104, 130, 119, 130, 121, 102, 121, 121 139, 117, 142, 128, 117, 104, 135, 128 102, 130, 108, 137, 144, 139, 137, 123 130, 125, 130, 137, 119, 112, 123, 117 121, 112, 121, 86, 110, 121, 142, 112 114, 121, 142, 117, 128, 119, 114, 135 104, 125, 117, 98, 121, 142, 125, 121 119, 123, 119, 121, 125, 121, 132, 106 130, 123, 119, 135, 119, 94, 119, 149 146, 102, 119, 149, 137, 135, 135, 110 112, 110, 114, 119, 137, 132, 123, 106 112, 94, 149, 121, 119, 139, 110, 112 123, 92, 135, 112, 142, 108, 130, 106 117, 112, 130, 135, 106, 119, 121, 119 121, 102, 132, 106, 117, 121, 125, 110 110, 128, 106, 121, 128, 112, 144, 146 119, 128, 121, 121, 121, 128, 132, 130 121, 125, 128, 119, 137, 123, 137, 139 125, 137, 144, 121, 108, 121, 123, 137 121, 132, 130, 114, 139, 106, 123, 142 125, 135, 121, 106, 123, 121, 119, 149 164, 151, 193, 202, 174, 210, 177, 169 202, 169, 188, 177, 177, 193, 193, 156 132, 146, 130, 137, 159, 121, 137, 130 132, 128, 106, 106, 108, 135, 125, 144 112, 112, 144, 149, 112, 137, 149, 104 108, 108, 128, 108, 121, 121, 121, 106 121, 132, 137, 121, 123, 104, 128, 121 128, 117, 117, 119, 117, 125, 128, 110 137, 114, 125, 106, 104, 114, 108, 119 125, 132, 137, 121, 130, 123, 119, 100 102, 132, 139, 121, 114, 119, 125, 121 117, 110, 117, 125, 119, 135, 114, 142 123, 130, 121, 117, 137, 110, 125, 108 108, 104, 106, 130, 128, 130, 121, 121 119, 114, 137, 112, 125, 110, 123, 130 100, 135, 149, 132, 137, 117, 132, 119 125, 132, 112, 139, 121, 110, 106, 137 102, 144, 106, 117, 149, 121, 139, 123 144, 121, 144, 137, 121, 149, 137, 123 130, 121, 125, 159, 128, 137, 130, 119 132, 139, 139, 137, 137, 146, 139, 132 135, 142, 137, 161, 123, 151, 142, 137 137, 117, 123, 144, 125, 137, 142, 132 142, 142, 130, 130, 123, 156, 130, 172 144, 137, 154, 144, 128, 154, 137, 149 154, 130, 130, 164, 146, 142, 135, 117 161, 144, 139, 139, 135, 159, 161, 144 146, 149, 144, 144, 169, 132, 169, 137 132, 137, 151, 164, 149, 137, 137, 146 142, 139, 128, 142, 130, 135, 166, 151 151, 144, 154, 169, 185, 151, 161, 154 159, 156, 169, 154, 154, 142, 142, 144 159, 156, 151, 137, 156, 142, 142, 159 151, 164, 149, 154, 149, 149, 139, 146 139, 146, 132, 144, 154, 161, 149, 159 142, 132, 159, 156, 137, 154, 149, 137 137, 154, 151, 146, 144, 151, 159, 135 156, 139, 142, 146, 128, 156, 156, 174 159, 154, 151, 142, 144, 144, 130, 142 166, 161, 135, 154, 151, 180, 182, 188 180, 174, 159, 169, 146, 169, 172, 180 169, 159, 159, 159, 166, 164, 172, 137 149, 137, 154, 137, 154, 144, 132, 135 149, 164, 144, 128, 146, 146, 159, 130 166, 135, 144, 177, 139, 132, 135, 139 117, 146, 139, 144, 119, 135, 139, 135 135, 149, 139, 137, 149, 159, 135, 130 137, 166, 146, 142, 142, 154, 123, 166 130, 123, 144, 119, 144, 154, 137, 154 154, 144, 151, 139, 154, 125, 149, 156 151, 154, 139, 135, 142, 125, 142, 137 139, 142, 154, 144, 159, 161, 139, 123 132, 137, 156, 117, 142, 142, 135, 146 142, 154, 135, 139, 123, 154, 149, 151 119, 123, 132, 130, 142, 137, 142, 130 159, 149, 142, 144, 144, 156, 142, 135 144, 130, 137, 135, 137, 154, 144, 139 144, 137, 154, 125, 132, 135, 149, 135 130, 128, 135, 159, 137, 117, 154, 144 146, 169, 161, 137, 132, 144, 149, 144 142, 177, 142, 172, 172, 137, 132, 161 137, 182, 210, 185, 193, 193, 182, 190 174, 202, 196, 213, 210, 193, 196, 174 188, 164, 172, 156, 159, 169, 172, 177 146, 149, 139, 164, 156, 172, 146, 149 144, 142, 142, 146, 137, 146, 151, 125 146, 146, 172, 151, 161, 164, 149, 156 149, 135, 164, 169, 161, 146, 149, 154 159, 174, 174, 185, 169, 146, 177, 169 159, 190, 174, 188, 172, 182, 188, 154 174, 196, 188, 193, 196, 188, 196, 185 174, 159, 169, 190, 164, 154, 180, 185 156, 199, 185, 185, 188, 174, 196, 159 169, 185, 199, 172, 180, 164, 199, 169 199, 188, 188, 190, 199, 154, 169, 190 180, 172, 174, 190, 182, 207, 169, 185 154, 174, 172, 196, 166, 154, 169, 182 156, 174, 159, 177, 164, 132, 159, 156 164, 159, 142, 166, 166, 144, 172, 161 159, 156, 146, 149, 182, 164, 154, 169 144, 177, 149, 159, 154, 154, 130, 132 139, 182, 169, 144, 146, 144, 135, 169 169, 125, 164, 144, 156, 159, 128, 137 177, 151, 166, 139, 174, 159, 161, 156 149, 135, 149, 149, 161, 146, 130, 142 144, 142, 174, 144, 144, 159, 139, 123 112, 146, 172, 132, 154, 144, 144, 146 182, 159, 161, 146, 164, 161, 174, 149 169, 156, 166, 156, 161, 166, 146, 154 151, 137, 154, 144, 144, 151, 161, 149 144, 151, 151, 169, 149, 151, 146, 159 154, 119, 159, 146, 132, 149, 144, 123 139, 151, 164, 149, 161, 146, 159, 161 151, 166, 149, 142, 159, 154, 142, 144 164, 139, 151, 139, 166, 149, 154, 164 128, 135, 144, 159, 154, 142, 137, 149 144, 149, 142, 130, 142, 151, 161, 137 164, 151, 151, 146, 137, 121, 142, 146 144, 166, 146, 151, 149, 164, 161, 137 149, 151, 154, 166, 144, 121, 132, 154 159, 164, 159, 169, 161, 137, 146, 159 172, 166, 144, 166, 149, 159, 156, 166 159, 154, 151, 144, 151, 146, 149, 132 154, 151, 130, 149, 151, 151, 149, 130 154, 164, 154, 139, 137, 128, 130, 144 149, 121, 130, 156, 139, 137, 146, 144 142, 161, 144, 121, 159, 144, 149, 132 130, 121, 169, 130, 164, 156, 130, 130 151, 132, 144, 144, 149, 137, 139, 137 146, 169, 137, 164, 161, 142, 135, 159 151, 174, 154, 180, 177, 190, 164, 164 166, 154, 174, 151, 174, 164, 188, 166 172, 188, 180, 169, 182, 177, 174, 196 174, 180, 188, 161, 202, 182, 225, 207 188, 188, 177, 199, 169, 169, 216, 185 174, 174, 182, 166, 156, 172, 159, 142 169, 142, 146, 135, 137, 149, 149, 137 142, 135, 154, 137, 132, 135, 132, 125 154, 137, 132, 146, 144, 121, 137, 137 149, 130, 130, 161, 154, 154, 130, 144 144, 142, 180, 137, 156, 135, 164, 137 172, 132, 166, 146, 180, 156, 154, 144 159, 149, 144, 139, 159, 142, 137, 142 149, 164, 151, 144, 135, 125, 139, 135 161, 137, 137, 142, 144, 151, 164,/