SampleIdent,907a 17h-5 13-14bulk,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,18-aug-1993 13:52,/ DataAngleRange, 2.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 123, 121, 96, 117, 121, 123, 112, 132 119, 96, 112, 135, 90, 119, 96, 106 112, 117, 112, 100, 106, 98, 117, 98 86, 85, 106, 92, 81, 96, 98, 96 108, 96, 98, 100, 102, 79, 110, 117 114, 92, 100, 102, 94, 100, 90, 90 94, 100, 94, 98, 102, 94, 92, 96 104, 100, 86, 94, 102, 104, 108, 104 106, 85, 102, 98, 94, 104, 114, 96 100, 110, 112, 110, 106, 102, 108, 102 79, 104, 117, 88, 106, 90, 104, 104 94, 90, 104, 86, 88, 104, 86, 102 104, 100, 117, 92, 104, 98, 108, 100 92, 112, 94, 94, 86, 96, 86, 110 135, 114, 102, 102, 108, 121, 102, 125 96, 106, 102, 98, 102, 114, 100, 106 94, 94, 114, 125, 121, 106, 117, 102 96, 98, 117, 114, 121, 106, 108, 104 121, 108, 125, 117, 100, 117, 112, 102 132, 119, 119, 110, 125, 121, 114, 121 121, 114, 110, 86, 132, 114, 112, 114 123, 130, 137, 102, 125, 130, 106, 128 128, 125, 121, 135, 128, 114, 130, 169 130, 137, 139, 137, 149, 112, 121, 132 130, 119, 125, 137, 117, 137, 144, 137 144, 137, 139, 146, 177, 154, 180, 112 144, 154, 137, 139, 156, 149, 135, 154 169, 154, 137, 146, 130, 149, 172, 142 151, 146, 137, 149, 135, 130, 132, 146 156, 137, 156, 146, 144, 117, 137, 139 166, 137, 135, 130, 156, 146, 151, 151 132, 149, 123, 164, 139, 135, 142, 139 139, 125, 135, 125, 156, 123, 156, 121 137, 130, 146, 142, 130, 149, 137, 154 135, 154, 125, 110, 135, 146, 139, 128 137, 146, 142, 132, 119, 130, 123, 112 123, 121, 135, 123, 132, 130, 114, 125 137, 146, 128, 125, 144, 121, 121, 112 142, 142, 125, 119, 132, 132, 151, 132 112, 128, 123, 121, 142, 132, 114, 137 132, 110, 135, 135, 114, 123, 114, 149 130, 137, 146, 144, 146, 149, 172, 169 210, 174, 172, 188, 159, 130, 139, 108 110, 102, 135, 132, 117, 108, 110, 108 102, 90, 108, 110, 121, 121, 106, 104 108, 117, 108, 108, 125, 112, 77, 92 108, 104, 102, 108, 104, 94, 106, 110 92, 110, 106, 98, 79, 125, 123, 114 92, 100, 108, 102, 108, 94, 104, 112 90, 100, 108, 100, 106, 106, 100, 90 114, 117, 77, 130, 100, 108, 102, 112 98, 119, 112, 125, 130, 96, 100, 96 117, 104, 92, 102, 100, 112, 100, 98 114, 94, 117, 96, 110, 114, 119, 114 98, 100, 110, 104, 104, 90, 100, 110 114, 110, 90, 83, 100, 98, 108, 96 85, 98, 130, 114, 96, 123, 104, 94 90, 104, 108, 102, 90, 110, 92, 112 92, 100, 121, 100, 92, 100, 98, 108 108, 98, 110, 94, 110, 102, 106, 88 117, 114, 114, 92, 96, 98, 106, 90 102, 102, 77, 130, 104, 121, 123, 100 108, 117, 106, 112, 123, 112, 104, 108 121, 108, 117, 135, 177, 142, 125, 139 132, 119, 164, 128, 149, 142, 128, 144 149, 123, 137, 128, 114, 104, 123, 102 88, 112, 100, 79, 110, 96, 90, 102 108, 100, 110, 102, 94, 86, 110, 88 106, 121, 92, 94, 83, 96, 108, 96 90, 81, 92, 92, 83, 100, 100, 102 128, 100, 102, 88, 102, 85, 77, 90 86, 76, 96, 86, 96, 94, 98, 90 96, 100, 112, 96, 106, 96, 112, 102 102, 98, 106, 108, 86, 86, 98, 88 96, 94, 94, 98, 81, 108, 88, 102 104, 100, 92, 104, 110, 77, 123, 104 86, 90, 88, 123, 100, 98, 110, 119 102, 117, 112, 94, 98, 102, 106, 88 117, 90, 119, 98, 104, 123, 110, 90 86, 86, 100, 102, 112, 108, 90, 108 102, 100, 121, 96, 117, 121, 86, 104 110, 98, 102, 100, 94, 92, 102, 90 86, 114, 112, 86, 106, 100, 102, 110 76, 102, 104, 94, 96, 125, 112, 104 92, 119, 114, 112, 106, 98, 72, 125 102, 92, 102, 98, 112, 96, 98, 121 98, 94, 90, 128, 90, 102, 98, 130 110, 100, 102, 114, 102, 114, 117, 139 108, 106, 108, 108, 104, 92, 102, 98 121, 88, 119, 130, 110, 123, 110, 114 117, 108, 117, 106, 289, 114, 121, 106 88, 110, 110, 119, 119, 128, 92, 110 130, 130, 119, 112, 121, 112, 102, 110 108, 128, 142, 125, 125, 137, 121, 104 130, 130, 123, 128, 135, 139, 130, 110 121, 108, 130, 114, 123, 139, 139, 132 112, 135, 139, 123, 128, 139, 114, 142 144, 135, 151, 121, 154, 146, 190, 188 169, 149, 156, 130, 146, 130, 139, 146 142, 135, 121, 139, 130, 114, 135, 132 135, 130, 130, 106, 130, 130, 159, 142 128, 135, 139, 142, 137, 125, 144, 144 146, 144, 149, 144, 159, 130, 156, 128 144, 132, 135, 128, 130, 137, 144, 142 130, 139, 154, 174, 137, 137, 135, 164 164, 132, 149, 128, 128, 149, 159, 137 149, 130, 149, 144, 132, 137, 164, 161 156, 166, 149, 154, 161, 151, 156, 164 156, 149, 139, 154, 172, 154, 154, 185 166, 177, 164, 174, 177, 185, 199, 216 219, 202, 219, 213, 237, 213, 219, 202 222, 237, 213, 228, 199, 237, 228, 210 219, 210, 182, 207, 210, 190, 222, 188 213, 207, 199, 207, 180, 207, 202, 196 196, 188, 246, 199, 202, 196, 213, 210 213, 177, 216, 180, 204, 204, 190, 210 234, 219, 216, 188, 219, 237, 234, 256 269, 335, 310, 313, 282, 272, 219, 225 202, 222, 185, 219, 213, 177, 190, 222 210, 228, 228, 204, 199, 202, 185, 207 196, 204, 190, 210, 202, 202, 182, 204 202, 182, 216, 210, 196, 204, 190, 207 190, 193, 216, 219, 210, 182, 204, 199 182, 210, 213, 207, 190, 193, 185, 202 240, 231, 204, 202, 222, 213, 213, 234 182, 182, 207, 204, 207, 234, 202, 199 222, 219, 216, 204, 216, 202, 202, 199 196, 193, 225, 204, 219, 237, 207, 185 207, 196, 185, 216, 207, 207, 210, 196 225, 216, 219, 210, 225, 222, 199, 207 210, 213, 231, 207, 216, 213, 213, 216 219, 240, 228, 210, 234, 225, 219, 222 199, 225, 222, 216, 225, 216, 246, 207 204, 216, 228, 219, 216, 231, 228, 240 199, 253, 213, 228, 222, 250, 213, 250 219, 237, 216, 259, 250, 202, 231, 219 243, 269, 237, 240, 237, 228, 234, 240 188, 222, 219, 253, 225, 210, 213, 246 213, 237, 234, 222, 213, 240, 207, 231 234, 222, 219, 196, 207, 228, 237, 234 250, 246, 228, 259, 228, 231, 234, 234 216, 216, 266, 222, 222, 262, 237, 225 256, 262, 231, 269, 320, 282, 262, 250 266, 259, 256, 240, 222, 243, 269, 234 231, 272, 282, 253, 250, 256, 231, 272 243, 234, 250, 246, 250, 246, 262, 256 253, 240, 237, 253, 269, 246, 246, 246 237, 213, 228, 225, 228, 228, 234, 231 240, 246, 237, 234, 219, 225, 243, 240 228, 256, 240, 269, 231, 262, 225, 216 259, 231, 240, 219, 246, 246, 262, 279 243, 225, 240, 228, 262, 253, 253, 243 269, 272, 335, 292, 346, 424, 433, 534 635, 745, 756, 841, 751, 702, 645, 610 506, 529, 396, 400, 380, 396, 380, 400 317, 335, 299, 259, 276, 256, 256, 272 266, 272, 246, 237, 228, 234, 259, 246 237, 237, 250, 262, 240, 246, 256, 246 259, 269, 246, 253, 256, 253, 256, 262 253, 253, 240, 246, 246, 276, 231, 269 286, 262, 384, 428, 396, 372, 306, 299 313, 286, 259, 276, 299, 276, 272, 282 240, 246, 259, 219, 240, 237, 234, 228 231, 228, 250, 222, 234, 237, 243, 228 222, 259, 228, 250, 243, 253, 237, 234 246, 234, 253, 216, 222, 225, 237, 234 219, 207, 210, 234, 256, 188, 199, 222 237, 193, 207, 219, 199, 210, 210, 222 243, 228, 199, 231, 234, 246, 213, 210 219, 253, 222, 199, 225, 237, 216, 237 216, 207, 219, 228, 222, 222, 243, 225 237, 213, 250, 243, 225, 219, 228, 262 228, 213, 216, 199, 188, 216, 228, 231 196, 196, 228, 266, 207, 243, 246, 222 225, 225, 240, 237, 213, 207, 193, 225 196, 222, 213, 219, 204, 228, 253, 204 219, 202, 219, 202, 204, 219, 216, 216 188, 222, 199, 213, 210, 231, 225, 188 202, 207, 207, 202, 210, 199, 188, 225 216, 207, 190, 219, 225, 213, 213, 196 196, 219, 202, 204, 202, 213, 207, 228 202, 204, 202, 199, 202, 231, 202, 250 216, 231, 213, 196, 210, 196, 188, 199 190, 180, 228, 169, 204, 207, 188, 228 234, 225, 216, 213, 234, 222, 250, 250 253, 286, 262, 259, 253, 219, 228, 210 204, 210, 193, 193, 202, 225, 188, 216 188, 193, 210, 193, 210, 225, 185, 180 190, 196, 185, 204, 169, 188, 204, 177 190, 182, 202, 166, 219, 196, 188, 169 180, 204, 188, 193, 166, 169, 193, 193 213, 193, 204, 202, 213, 185, 188, 182 174, 188, 182, 196, 188, 196, 169, 166 177, 210, 185, 204, 207, 169, 199, 196 204, 180, 196, 202, 174, 172, 202, 182 182, 161, 204, 174, 204, 193, 185, 156 182, 177, 199, 182, 185, 182, 207, 204 185, 210, 174, 188, 172, 169, 202, 202 180, 174, 193, 182, 174, 174, 185, 188 190, 196, 182, 188, 180, 190, 188, 207 188, 199, 169, 180, 166, 177, 177, 166 199, 228, 172, 219, 199, 199, 202, 177 182, 185, 207, 199, 199, 225, 185, 253 164, 228, 210, 196, 207, 228, 190, 204 219, 213, 202, 210, 234, 216, 207, 231 246, 222, 246, 193, 222, 216, 207, 182 228, 222, 190, 193, 177, 216, 193, 185 182, 188, 182, 188, 190, 199, 180, 190 177, 159, 196, 177, 166, 180, 154, 185 190, 154, 174, 202, 190, 161, 188, 177 172, 180, 159, 169, 166, 172, 169, 182 177, 180, 182, 180, 204, 202, 216, 196 193, 202, 180, 182, 196, 188, 169, 172 177, 182, 164, 185, 139, 156, 174, 154 180, 159, 193, 154, 188, 196, 174, 193 193, 228, 190, 213, 188, 169, 193, 188 172, 172, 174, 164, 146, 151, 164, 154 156, 169, 142, 156, 166, 180, 164, 159 144, 132, 172, 164, 190, 174, 216, 172 164, 159, 161, 144, 185, 177, 174, 154 159, 169, 139, 156, 188, 144, 156, 188 159, 154, 169, 188, 169, 169, 146, 164 180, 149, 159, 182, 182, 154, 164, 159 146, 164, 149, 166, 182, 149, 164, 156 151, 169, 154, 144, 149, 151, 177, 144 149, 149, 159, 142, 144, 151, 164, 142 142, 144, 164, 149, 180, 177, 146, 199 159, 164, 177, 159, 196, 164, 177, 142 159, 166, 149, 130, 151, 144, 151, 142 130, 128, 144, 128, 146, 121, 144, 142 156, 149, 149, 117, 137, 130, 137, 119 139, 149, 149, 149, 164, 142, 149, 125 149, 137, 144, 144, 132, 137, 154, 159 154, 154, 164, 188, 188, 193, 185, 166 164, 161, 137, 172, 146, 154, 149, 135 144, 139, 146, 142, 142, 144, 139, 149 166, 149, 125, 149, 130, 142, 159, 144 139, 139, 137, 156, 142, 137, 156, 130 146, 139, 142, 164, 306, 151, 159, 156 159, 177, 161, 159, 166, 156, 146, 156 135, 144, 123, 121, 151, 142, 149, 166 174, 142, 166, 156, 137, 156, 144, 146 144, 128, 154, 149, 144, 137, 135, 144 149, 144, 142, 146, 142, 161, 156, 142 156, 137, 154, 144, 151, 142, 154, 156 149, 161, 146, 144, 174, 146, 151, 156 164, 142, 146, 146, 154, 154, 151, 132 164, 166, 137, 144, 146, 149, 164, 169 154, 149, 149, 132, 151, 149, 149, 159 149, 130, 130, 154, 146, 159, 159, 144 169, 149, 193, 185, 196, 199, 164, 193 169, 174, 164, 169, 169, 151, 142, 169 199, 174, 177, 172, 190, 174, 180, 164 169, 174, 144, 161, 154, 154, 159, 161 166, 144, 137, 146, 146, 154, 123, 154 159, 159, 159, 177, 161, 139, 164, 149 146, 161, 154, 149, 137, 166, 139, 149 135, 135, 151, 142, 164, 159, 169, 156 139, 135, 166, 135, 154, 146, 137, 177 125, 139, 154, 164, 172, 164, 161, 146 151, 154, 172, 164, 128, 174, 149, 149 130, 169, 164, 137, 154, 164, 156, 161 169, 174, 159, 169, 182, 164, 166, 164 154, 169, 156, 146, 137, 156, 142, 144 161, 161, 164, 142, 177, 144, 172, 172 144, 169, 164, 174, 188, 225, 222, 256 210, 256, 196, 207, 188, 210, 225, 193 174, 185, 182, 180, 164, 151, 159, 172 166, 146, 177, 161, 154, 144, 156, 154 144, 174, 149, 149, 177, 193, 151, 174 182, 190, 190, 199, 207, 204, 216, 237 237, 250, 246, 216, 231, 180, 199, 185 204, 196, 174, 166, 169, 204, 169, 180 180, 188, 164, 164, 174, 164, 128, 135 149, 149, 142, 159, 161, 144, 137, 144 149, 142, 137, 161, 121, 125, 119, 146 135, 151, 135, 130, 125, 154, 151, 137 121, 159, 144, 149, 146, 130, 128, 149 130, 144, 130, 130, 151, 139, 151, 144 151, 144, 135, 130, 128, 135, 144, 142 142, 123, 130, 119, 154, 142, 139, 139 123, 114, 125, 164, 142, 135, 135, 125 121, 139, 144, 144, 151, 137, 149, 142 154, 142, 151, 139, 132, 135, 142, 151 135, 149, 146, 144, 135, 137, 135, 128 149, 142, 130, 144, 114, 137, 144, 142 142, 146, 144, 142, 139, 130, 144, 128 135, 154, 130, 154, 149, 135, 156, 130 142, 128, 132, 151, 156, 137, 164, 159 139, 123, 180, 121, 144, 135, 149, 144 161, 119, 125, 154, 121, 144, 117, 149 114, 149, 149, 114, 156, 151, 146, 142 149, 149, 135, 142, 119, 128, 128, 149 123, 130, 144, 121, 130, 135, 137, 119 164, 128, 130, 142, 114, 146, 137, 125 114, 123, 151, 121, 132, 137, 151, 139 137, 154, 159, 142, 146, 130, 151, 125 137, 128, 142, 146, 146, 151, 144, 139 154, 146, 137, 123, 132, 132, 139, 135 151, 121, 125, 159, 169, 174, 164, 196 202, 210, 210, 204, 225, 204, 156, 174 164, 202, 182, 169, 156, 144, 144, 132 149, 137, 156, 123, 137, 144, 121, 159 144, 144, 146, 146, 130, 132, 137, 149 149, 142, 156, 142, 159, 139, 137, 144 149, 137, 146, 128, 135, 142, 139, 108 137, 135, 142, 159, 135, 144, 154, 130 112, 114, 154, 121, 142, 130, 132, 142 128, 123, 135, 132, 149, 119, 139, 121 130, 142, 132, 139, 121, 110, 121, 151 144, 119, 117, 151, 144, 132, 135, 130 135, 151, 139, 154, 144, 154, 144, 132 137, 135, 144, 149, 149, 154, 144, 149 144, 149, 139, 149, 142, 144, 139, 132 142, 128, 139, 151, 137, 142, 144, 132 149, 146, 142, 130, 149, 154, 149, 128 137, 130, 139, 151, 137, 132, 135, 151 139, 132, 130, 117, 144, 146, 132, 144 128, 137, 161, 144, 125, 164, 149, 125 144, 135, 130, 139, 144, 139, 146, 139 164, 135, 159, 151, 128, 146, 154, 149 142, 142, 132, 169, 130, 156, 149, 161 149, 132, 159, 149, 161, 137, 139, 154 128, 144, 149, 142, 139, 151, 166, 188 174, 154, 156, 128, 144, 159, 164, 164 154, 159, 159, 154, 149, 123, 185, 132 154, 161, 146, 159, 164, 159, 159, 119 159, 159, 156, 149, 137, 146, 142, 159 135, 177, 166, 142, 139, 159, 154, 132 149, 166, 156, 166, 182, 185, 169, 159 164, 182, 159, 156, 164, 169, 169, 177 159, 166, 142, 161, 156, 151, 159, 161 164, 142, 161, 161, 174, 172, 188, 164 188, 139, 164, 174, 156, 180, 169, 180 174, 154, 139, 144, 159, 169, 151, 125 156, 149, 177, 169, 164, 164, 177, 154 144, 142, 156, 174, 172, 161, 156, 149 159, 149, 166, 172, 161, 188, 146, 164 169, 166, 149, 151, 166, 180, 172, 159 146, 164, 156, 166, 169, 177, 172, 188 159, 159, 154, 154, 174, 151, 182, 164 146, 149, 174, 166, 144, 149, 144, 154 166, 146, 156, 151, 151, 172, 142, 164 164, 169, 137, 149, 161, 139, 154, 159 169, 154, 166, 149, 172, 151, 156, 180 137, 182, 161, 182, 149, 169, 154, 161 164, 177, 156, 164, 161, 159, 154, 177 161, 144, 169, 156, 146, 161, 159, 159 137, 166, 169, 172, 169, 154, 180, 151 154, 164, 130, 185, 159, 166, 149, 149 159, 172, 139, 166, 151, 166, 149, 159 154, 169, 142, 144, 151, 151, 169, 164 154, 177, 132, 149, 159, 151, 164, 169 151, 159, 185, 156, 159, 144, 154, 151 169, 159, 161, 161, 161, 159, 137, 130 166, 154, 142, 190, 166, 159, 154, 182 144, 169, 137, 146, 193, 135, 169, 149 182, 146, 154, 130, 156, 161, 182, 172 164, 159, 149, 166, 144, 164, 146, 174 156, 151, 144, 169, 146, 166, 149, 172 193, 177, 172, 177, 144, 146, 202, 177 177, 213, 213, 216, 219, 216, 207, 204 210, 190, 188, 196, 169, 219, 190, 193 164, 172, 159, 174, 174, 144, 174, 164 185, 193, 180, 185, 166, 172, 156, 164 177, 169, 166, 180, 166, 174, 156, 151 166, 177, 174, 154, 188, 164, 159, 164 166, 130, 182, 166, 151, 164, 159, 182 188, 172, 172, 174, 172, 149, 149, 182 144, 177, 166, 161, 188, 196, 185, 182 172, 177, 174, 190, 142, 177, 164, 185 185, 207, 190, 164, 193, 172, 188, 196 190, 182, 213, 185, 196, 182, 172, 185 193, 172, 169, 185, 174, 182, 172, 185 164, 188, 172, 204, 169, 190, 188, 180 169, 180, 174, 177, 174, 190, 174, 169 190, 166, 177, 166, 180, 164, 174, 199 159, 161, 164, 159, 174, 154, 159, 169 166, 193, 161, 177, 174, 174, 185, 180 164, 182, 159, 174, 169, 159, 164, 144 188, 177, 161, 174, 151, 149, 169, 154 193, 151, 161, 172, 166, 159, 154, 182 154, 139, 164, 159, 164, 177, 154, 161 172, 166, 180, 174, 156, 161, 185, 169 149, 161, 164, 144, 169, 177, 180, 185 172, 164, 177, 169, 169, 156, 146, 166 182, 182, 149, 169, 174, 188, 174, 180 177, 180, 154, 196, 177, 185, 154, 177 159, 169, 159, 172, 172, 174, 164, 172 161, 169, 159, 180, 166, 154, 182, 196 154, 185, 135, 169, 135, 182, 166, 177 172, 172, 169, 185, 159, 182, 161, 154 188, 156, 159, 196, 174, 174, 164, 193 188, 169, 172, 164, 166, 190, 202, 174 182, 188, 169, 185, 169, 188, 188, 177 169, 151, 159, 169, 154, 164, 174, 172 151, 156, 174, 164, 188, 135, 154, 196 174, 166, 174, 180, 172, 190, 149, 174 193, 174, 164, 166, 172, 169, 180, 161 193, 188, 177, 193, 144, 166, 154, 174 172, 169, 156, 169, 151, 177, 182, 164 180, 164, 164, 169, 180, 144, 177, 166 151, 169, 154, 139, 169, 172, 154, 156 166, 128, 156, 146, 151, 123, 159, 154 169, 169, 144, 174, 169, 156, 169, 159 142, 137, 149, 137, 185, 139, 154, 146 159, 149, 154, 166, 144, 142, 164, 159 159, 182, 146, 154, 146, 164, 174, 172 151, 164, 161, 154, 146, 159, 159, 172 159, 159, 172, 146, 172, 161, 149, 172 185, 202, 174, 182, 174, 180, 190, 177 169, 182, 185, 193, 177, 196, 188, 177 166, 193, 156, 166, 188, 174, 180, 204 199, 182, 177, 180, 202, 193, 199, 190 169, 199, 174, 182, 202, 185, 182, 177 177, 169, 164, 180, 149, 139, 156, 149 164, 137, 174, 159, 146, 154, 172, 174 149, 159, 177, 151, 135, 146, 166, 177 146, 177, 169, 182, 174, 156, 182, 139 137, 154, 185, 137, 159, 161, 180, 161 142, 174, 149, 151, 156, 161, 188, 144 169, 146, 142, 159, 180, 172, 161, 172 156, 159, 149, 151, 151, 144, 159, 164 156, 166, 164, 159, 144, 159, 159, 154 156, 159, 135, 151, 137, 159, 161,/