SampleIdent,907A-22-3/26,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,10-aug-1993 6:10,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 100, 96, 121, 125, 135, 102, 112, 104 104, 108, 114, 110, 102, 110, 130, 92 104, 106, 98, 106, 117, 119, 121, 104 112, 102, 114, 119, 110, 100, 112, 132 132, 125, 121, 119, 121, 164, 110, 110 114, 144, 154, 104, 144, 128, 149, 130 123, 137, 149, 130, 156, 123, 161, 130 139, 154, 142, 121, 151, 135, 137, 130 161, 137, 151, 149, 130, 121, 164, 144 149, 142, 159, 144, 144, 154, 156, 154 130, 128, 137, 144, 154, 154, 135, 119 149, 142, 130, 156, 154, 142, 154, 139 159, 146, 146, 132, 132, 151, 154, 164 144, 142, 166, 137, 119, 125, 139, 135 151, 142, 137, 128, 123, 144, 151, 156 144, 182, 149, 149, 164, 125, 144, 154 146, 164, 154, 156, 137, 123, 172, 137 137, 149, 156, 144, 149, 119, 128, 151 151, 154, 137, 128, 137, 137, 151, 110 130, 123, 144, 142, 137, 159, 123, 137 137, 149, 144, 139, 144, 149, 149, 137 130, 121, 144, 156, 151, 137, 151, 149 161, 156, 142, 159, 154, 146, 182, 164 156, 156, 172, 154, 146, 161, 164, 144 119, 121, 128, 104, 125, 104, 112, 119 121, 108, 112, 132, 132, 100, 106, 117 112, 100, 121, 110, 114, 110, 119, 112 114, 117, 100, 130, 112, 110, 123, 102 108, 112, 123, 121, 121, 110, 125, 132 166, 154, 154, 159, 132, 156, 180, 151 132, 144, 128, 130, 104, 94, 90, 96 92, 108, 77, 114, 96, 121, 94, 92 98, 112, 102, 90, 102, 100, 106, 130 104, 90, 85, 90, 96, 92, 100, 90 104, 98, 88, 85, 98, 96, 85, 98 86, 96, 92, 98, 100, 85, 106, 92 106, 102, 85, 90, 119, 110, 104, 102 110, 94, 114, 121, 102, 102, 104, 106 106, 108, 108, 86, 112, 98, 86, 86 86, 88, 77, 102, 96, 85, 92, 104 121, 104, 100, 92, 77, 90, 94, 104 86, 100, 102, 77, 102, 102, 112, 90 100, 102, 90, 98, 106, 104, 100, 102 102, 94, 119, 88, 114, 77, 119, 110 108, 114, 96, 106, 114, 114, 137, 117 121, 114, 112, 125, 125, 144, 123, 137 135, 117, 130, 102, 104, 108, 106, 100 108, 92, 114, 85, 96, 86, 98, 88 94, 90, 88, 96, 92, 98, 106, 102 96, 94, 79, 98, 108, 79, 96, 114 77, 114, 98, 92, 94, 79, 88, 86 85, 104, 96, 92, 94, 83, 85, 98 81, 94, 76, 86, 92, 92, 85, 85 100, 102, 86, 104, 114, 108, 125, 110 112, 110, 81, 96, 94, 86, 92, 102 90, 76, 90, 77, 72, 90, 74, 90 90, 106, 112, 92, 74, 86, 96, 110 92, 72, 90, 77, 96, 90, 77, 81 72, 83, 83, 79, 81, 77, 94, 85 92, 98, 83, 94, 94, 108, 88, 96 98, 83, 85, 86, 102, 92, 81, 76 86, 90, 94, 79, 88, 112, 90, 74 94, 77, 79, 86, 88, 94, 86, 77 94, 98, 86, 86, 100, 83, 77, 79 79, 79, 77, 86, 74, 83, 92, 62 88, 59, 77, 86, 92, 86, 85, 85 85, 83, 108, 98, 72, 79, 85, 94 92, 88, 104, 59, 77, 71, 79, 85 90, 76, 69, 92, 79, 74, 71, 83 71, 81, 64, 83, 76, 77, 71, 67 85, 90, 98, 67, 76, 71, 77, 76 86, 92, 88, 86, 92, 81, 67, 79 98, 98, 81, 94, 88, 74, 77, 86 94, 86, 102, 86, 86, 88, 94, 98 76, 76, 86, 86, 94, 76, 92, 96 88, 86, 86, 98, 125, 108, 106, 90 90, 108, 100, 94, 79, 92, 102, 100 94, 94, 104, 110, 102, 108, 102, 102 85, 92, 100, 90, 85, 104, 88, 114 92, 121, 110, 117, 112, 110, 114, 102 90, 86, 100, 77, 98, 85, 85, 83 98, 86, 86, 94, 96, 94, 96, 79 74, 85, 92, 88, 90, 85, 85, 88 74, 85, 94, 98, 85, 94, 98, 94 72, 86, 100, 88, 92, 108, 92, 110 104, 86, 85, 104, 86, 85, 108, 231 104, 94, 128, 110, 86, 154, 135, 137 154, 121, 135, 117, 125, 108, 102, 102 100, 110, 121, 128, 108, 123, 112, 128 119, 132, 130, 137, 159, 130, 154, 174 188, 166, 190, 159, 161, 174, 216, 225 240, 210, 240, 250, 207, 228, 253, 246 246, 216, 219, 234, 219, 210, 199, 225 199, 190, 185, 196, 164, 177, 174, 180 161, 180, 166, 172, 188, 180, 159, 164 164, 137, 154, 146, 151, 185, 151, 161 159, 154, 174, 169, 169, 185, 161, 188 172, 174, 210, 246, 243, 262, 299, 317 353, 357, 372, 328, 313, 282, 266, 276 240, 250, 231, 199, 185, 169, 169, 144 114, 144, 144, 137, 144, 137, 142, 125 121, 123, 121, 121, 121, 104, 121, 108 125, 137, 125, 123, 130, 130, 121, 137 125, 123, 121, 119, 121, 110, 144, 114 110, 90, 365, 117, 112, 139, 142, 123 404, 137, 137, 132, 161, 144, 151, 121 121, 130, 137, 156, 156, 156, 146, 149 154, 185, 154, 188, 188, 169, 196, 188 174, 185, 196, 151, 154, 193, 164, 169 146, 149, 156, 144, 149, 130, 144, 149 154, 172, 132, 161, 156, 144, 149, 159 142, 112, 144, 151, 142, 154, 130, 125 123, 130, 125, 132, 121, 121, 121, 117 110, 108, 125, 128, 125, 92, 123, 106 114, 125, 128, 128, 130, 139, 135, 137 142, 125, 121, 149, 139, 154, 149, 154 154, 149, 146, 117, 159, 137, 161, 130 137, 149, 135, 137, 125, 149, 123, 142 149, 123, 144, 117, 130, 142, 149, 117 144, 137, 144, 130, 149, 130, 137, 144 151, 125, 139, 149, 130, 142, 128, 139 130, 121, 112, 121, 123, 149, 137, 142 130, 137, 137, 144, 128, 132, 132, 121 142, 132, 159, 125, 128, 154, 156, 151 164, 164, 169, 159, 166, 144, 114, 169 166, 149, 151, 156, 130, 151, 180, 174 151, 172, 172, 180, 146, 169, 164, 156 174, 185, 161, 182, 169, 182, 174, 199 156, 172, 151, 149, 149, 146, 144, 139 146, 161, 144, 151, 144, 149, 161, 169 185, 193, 180, 169, 159, 159, 180, 172 130, 166, 166, 137, 172, 159, 154, 154 177, 182, 156, 161, 174, 193, 185, 216 259, 253, 331, 408, 475, 571, 625, 790 853, 986, 1142, 1289, 1197, 1267, 1149, 1225 1082, 1005, 973, 824, 713, 581, 515, 437 361, 342, 286, 269, 240, 199, 199, 185 210, 219, 190, 219, 174, 174, 188, 182 188, 137, 196, 188, 199, 166, 210, 202 237, 219, 234, 234, 231, 228, 243, 306 296, 259, 272, 256, 240, 234, 234, 282 310, 331, 458, 480, 420, 361, 331, 369 279, 289, 272, 266, 310, 279, 313, 342 331, 262, 292, 262, 269, 210, 210, 225 182, 199, 188, 164, 172, 169, 196, 154 180, 156, 190, 172, 169, 188, 177, 174 174, 172, 199, 164, 164, 177, 161, 174 174, 159, 156, 144, 174, 130, 123, 142 139, 112, 142, 139, 142, 142, 151, 125 121, 149, 139, 156, 149, 128, 139, 149 123, 144, 130, 132, 119, 121, 137, 144 135, 121, 123, 110, 121, 137, 114, 121 121, 123, 123, 135, 121, 149, 130, 144 132, 135, 139, 159, 130, 154, 146, 164 169, 182, 180, 169, 193, 193, 166, 213 185, 193, 216, 185, 188, 199, 199, 216 207, 196, 174, 177, 182, 156, 169, 166 146, 149, 166, 180, 156, 142, 169, 132 132, 132, 132, 125, 114, 123, 119, 121 149, 146, 144, 125, 123, 106, 125, 144 123, 123, 123, 104, 123, 123, 114, 121 104, 104, 119, 112, 110, 108, 112, 94 121, 94, 117, 96, 100, 106, 108, 123 119, 132, 130, 132, 135, 114, 125, 121 159, 117, 137, 119, 130, 123, 121, 144 156, 159, 164, 199, 202, 204, 222, 210 210, 222, 246, 269, 246, 253, 216, 213 204, 199, 156, 172, 164, 161, 154, 149 149, 159, 156, 146, 149, 125, 128, 114 121, 112, 114, 123, 96, 100, 98, 94 77, 100, 108, 94, 108, 81, 102, 92 110, 96, 98, 96, 108, 112, 102, 90 104, 117, 102, 98, 90, 119, 119, 117 110, 123, 121, 130, 123, 159, 139, 137 142, 128, 169, 159, 164, 154, 159, 142 137, 151, 154, 117, 139, 106, 119, 117 85, 128, 90, 90, 88, 123, 102, 102 104, 114, 96, 90, 85, 96, 94, 92 98, 90, 104, 100, 88, 96, 86, 90 96, 102, 90, 96, 94, 114, 106, 137 119, 121, 128, 106, 104, 106, 117, 100 123, 142, 117, 123, 130, 117, 114, 149 121, 142, 164, 161, 172, 180, 182, 202 202, 210, 266, 376, 458, 412, 328, 282 361, 313, 299, 296, 250, 246, 279, 228 246, 253, 219, 240, 250, 262, 266, 246 299, 259, 292, 250, 313, 276, 259, 276 246, 222, 272, 240, 216, 231, 204, 222 228, 202, 196, 219, 196, 199, 174, 199 202, 193, 216, 185, 199, 177, 164, 182 193, 177, 185, 182, 202, 164, 193, 196 180, 174, 169, 164, 146, 182, 154, 149 151, 172, 166, 149, 164, 182, 151, 174 164, 180, 154, 169, 174, 159, 142, 159 149, 161, 144, 177, 146, 154, 169, 154 159, 182, 169, 196, 196, 177, 228, 188 210, 243, 222, 259, 262, 243, 234, 243 225, 237, 250, 240, 193, 177, 199, 185 182, 164, 202, 166, 180, 177, 169, 182 207, 188, 207, 231, 196, 219, 202, 228 240, 219, 222, 207, 193, 185, 182, 174 177, 154, 193, 177, 161, 166, 161, 164 199, 159, 149, 159, 185, 172, 172, 139 185, 177, 185, 164, 177, 161, 169, 154 166, 174, 169, 169, 188, 182, 149, 159 174, 161, 159, 144, 164, 137, 146, 130 114, 137, 149, 128, 137, 146, 98, 130 121, 121, 121, 128, 139, 154, 117, 135 144, 144, 130, 156, 139, 137, 130, 125 108, 139, 121, 114, 121, 128, 142, 119 146, 128, 106, 106, 108, 102, 104, 123 114, 102, 119, 121, 117, 104, 86, 110 123, 102, 110, 100, 92, 114, 100, 119 114, 112, 123, 125, 123, 142, 149, 146 441, 166, 196, 159, 213, 199, 199, 188 185, 185, 169, 164, 166, 161, 149, 135 121, 128, 139, 151, 144, 139, 110, 119 128, 112, 130, 130, 128, 137, 119, 110 130, 146, 132, 137, 132, 106, 123, 172 149, 144, 169, 174, 166, 164, 169, 169 177, 166, 174, 159, 151, 154, 139, 139 117, 125, 130, 119, 128, 137, 121, 123 128, 151, 144, 132, 130, 151, 146, 156 159, 154, 137, 172, 121, 128, 142, 128 146, 117, 142, 137, 117, 125, 114, 135 114, 100, 119, 121, 125, 104, 102, 112 119, 114, 130, 130, 114, 121, 112, 108 135, 117, 117, 128, 96, 112, 106, 123 108, 123, 144, 130, 108, 123, 108, 125 114, 130, 102, 123, 123, 104, 114, 139 112, 123, 123, 135, 119, 128, 132, 128 119, 146, 119, 149, 114, 139, 117, 130 142, 135, 128, 130, 172, 177, 182, 196 243, 225, 213, 193, 202, 234, 228, 182 193, 188, 154, 154, 149, 144, 135, 137 132, 137, 117, 90, 110, 102, 128, 112 119, 121, 121, 104, 110, 114, 100, 123 123, 114, 114, 114, 114, 117, 112, 130 102, 112, 102, 102, 96, 96, 96, 96 96, 112, 92, 92, 100, 106, 92, 102 98, 86, 98, 94, 94, 92, 100, 98 96, 106, 90, 112, 100, 106, 100, 83 110, 112, 119, 119, 108, 135, 117, 106 104, 110, 128, 114, 121, 114, 119, 108 90, 106, 119, 106, 117, 98, 90, 83 96, 94, 90, 102, 92, 108, 104, 106 94, 106, 112, 130, 128, 154, 154, 154 137, 161, 144, 144, 144, 123, 132, 130 121, 121, 112, 121, 112, 132, 130, 112 114, 104, 121, 119, 121, 130, 128, 114 130, 121, 142, 132, 130, 137, 121, 125 166, 156, 188, 193, 207, 222, 216, 246 237, 266, 250, 250, 246, 246, 228, 237 199, 231, 204, 193, 219, 166, 182, 151 182, 177, 180, 177, 161, 174, 174, 164 123, 146, 137, 144, 132, 121, 128, 112 102, 121, 104, 110, 110, 119, 106, 106 117, 83, 104, 121, 102, 94, 85, 102 86, 94, 88, 94, 102, 102, 90, 114 79, 90, 96, 79, 85, 102, 94, 108 117, 86, 114, 98, 90, 83, 85, 90 92, 76, 72, 88, 72, 94, 94, 67 90, 110, 90, 106, 92, 83, 74, 88 102, 110, 98, 94, 98, 100, 100, 108 114, 128, 112, 119, 139, 114, 117, 142 112, 121, 112, 96, 100, 102, 85, 88 92, 79, 71, 92, 67, 81, 79, 81 90, 86, 77, 94, 86, 77, 98, 79 79, 100, 77, 85, 72, 86, 90, 77 85, 90, 86, 100, 71, 96, 76, 81 85, 90, 77, 102, 85, 79, 90, 74 74, 66, 83, 88, 83, 77, 67, 85 86, 77, 81, 66, 83, 66, 90, 76 77, 77, 59, 76, 61, 77, 88, 76 81, 94, 96, 88, 83, 83, 77, 79 71, 81, 98, 71, 85, 79, 79, 79 76, 90, 71, 90, 88, 79, 85, 83 86, 83, 88, 85, 74, 72, 92, 102 96, 339, 79, 81, 96, 92, 98, 85 88, 104, 88, 88, 104, 90, 112, 119 108, 106, 106, 151, 185, 164, 199, 219 237, 250, 272, 246, 272, 317, 331, 299 292, 222, 219, 199, 202, 199, 166, 125 123, 108, 92, 94, 106, 90, 64, 92 98, 85, 86, 94, 96, 102, 110, 104 121, 104, 110, 83, 98, 76, 90, 86 94, 81, 104, 85, 108, 135, 164, 266 219, 169, 137, 108, 137, 142, 182, 164 137, 88, 86, 88, 86, 83, 85, 100 94, 94, 85, 88, 94, 69, 94, 79 92, 98, 86, 71, 76, 77, 88, 81 86, 77, 76, 92, 94, 86, 77, 67 67, 79, 76, 98, 83, 77, 77, 76 86, 77, 79, 71, 72, 81, 77, 72 72, 86, 72, 92, 88, 94, 76, 74 94, 76, 100, 88, 86, 90, 69, 92 94, 110, 94, 100, 100, 98, 85, 88 83, 98, 85, 85, 76, 83, 81, 94 86, 88, 98, 86, 106, 98, 92, 108 94, 90, 119, 98, 96, 104, 114, 128 121, 108, 112, 104, 110, 96, 106, 114 112, 92, 104, 106, 117, 110, 100, 98 112, 104, 123, 137, 98, 137, 123, 130 112, 119, 102, 135, 112, 125, 112, 102 130, 144, 121, 128, 125, 130, 144, 149 135, 128, 130, 142, 130, 149, 139, 139 125, 139, 132, 146, 149, 137, 142, 146 132, 149, 139, 146, 137, 130, 125, 139 135, 114, 128, 121, 123, 125, 142, 125 139, 139, 135, 125, 151, 132, 130, 139 149, 166, 180, 188, 188, 199, 180, 196 222, 188, 237, 210, 202, 210, 207, 193 207, 210, 210, 207, 210, 180, 185, 159 164, 169, 161, 193, 177, 174, 174, 169 185, 161, 193, 188, 156, 166, 177, 154 137, 144, 144, 166, 132, 172, 149, 139 139, 164, 149, 159, 154, 169, 139, 151 159, 137, 156, 164, 149, 139, 154, 146 159, 151, 156, 117, 154, 164, 177, 174 174, 190, 196, 193, 225, 243, 234, 240 259, 234, 204, 204, 210, 222, 219, 213 207, 193, 180, 180, 161, 149, 154, 142 159, 166, 123, 166, 154, 128, 144, 154 114, 137, 112, 125, 130, 125, 123, 110 117, 106, 112, 123, 106, 106, 112, 114 108, 121, 96, 112, 90, 88, 112, 100 106, 130, 100, 108, 112, 114, 98, 106 112, 125, 96, 112, 117, 117, 94, 112 110, 110, 106, 123, 108, 92, 83, 90 108, 112, 114, 128, 112, 130, 108, 96 125, 125, 98, 94, 108, 100, 110, 106 90, 98, 110, 104, 104, 112, 110, 102 96, 119, 96, 92, 100, 81, 92, 104 110, 86, 96, 114, 96, 112, 102, 104 110, 110, 117, 121, 119, 96, 94, 119 108, 121, 117, 100, 104, 96, 104, 117 85, 102, 125, 108, 139, 125, 117, 132 106, 114, 110, 137, 125, 142, 117, 117 119, 117, 102, 119, 121, 112, 98, 100 94, 121, 114, 135, 119, 114, 119, 121 108, 130, 102, 117, 96, 121, 108, 117 102, 123, 135, 149, 142, 159, 164, 154 190, 210, 246, 243, 262, 276, 286, 310 296, 289, 292, 276, 286, 246, 240, 231 188, 222, 196, 161, 164, 156, 149, 146 137, 139, 144, 132, 132, 125, 119, 119 119, 117, 121, 144, 117, 106, 114, 137 135, 142, 132, 121, 142, 151, 154, 130 130, 132, 146, 159, 156, 130, 149, 144 149, 154, 137, 169, 142, 174, 144, 180 146, 164, 180, 188, 185, 185, 193, 202 188, 177, 210, 213, 213, 199, 246, 216 243, 237, 225, 222, 219, 246, 286, 243 253, 240, 262, 279, 266, 234, 266, 240 246, 256, 240, 256, 250, 246, 237, 262 231, 222, 219, 207, 225, 193, 207, 199 188, 190, 193, 174, 199, 177, 174, 190 182, 146, 174, 156, 169, 161, 164, 146 164, 144, 204, 151, 154, 151, 172, 159 159, 151, 166, 142, 125, 144, 139, 156 110, 132, 123, 123, 137, 112, 121, 119 121, 110, 125, 96, 121, 119, 108, 112 100, 92, 106, 104, 119, 110, 104, 100 114, 112, 98, 110, 86, 117, 102, 92 85, 96, 90, 85, 96, 110, 108, 90 96, 96, 96, 110, 98, 88, 108, 102 96, 94, 86, 102, 86, 96, 104, 130 102, 121, 108, 123, 121, 121, 121, 139 130, 154, 159, 151, 135, 154, 156, 128 125, 137, 144, 166, 142, 151, 132, 149 125, 125, 123, 119, 108, 114, 106, 123 106, 108, 104, 83, 110, 104, 90, 100 98, 100, 114, 90, 90, 79, 108, 88 102, 90, 108, 100, 117, 117, 102, 121 98, 123, 117, 119, 114, 112, 119, 112 121, 114, 119, 108, 110, 98, 98, 98 104, 121, 110, 102, 100, 114, 108, 100 98, 71, 104, 106, 94, 102, 86, 102 108, 94, 112, 108, 108, 88, 98, 108 119, 106, 108, 132, 128, 88, 117, 100 104, 106, 90, 106, 104, 106, 121, 94 117, 104, 110, 100, 119, 123, 102, 106 108, 110, 112, 121, 119, 104, 110, 98 94, 125, 98, 96, 106, 85, 94, 94 100, 83, 96, 110, 92, 90, 94, 94 90, 92, 83, 83, 66, 110, 94, 85 88, 86, 94, 77, 90, 86, 112, 100 96, 102, 119, 121, 100, 77, 96, 88 96, 94, 88, 102, 98, 102, 102, 106 106, 117, 94, 98, 106, 117, 90, 100 114, 123, 123, 123, 128, 130, 149, 177 164, 185, 182, 202, 210, 219, 219, 207 199, 199, 213, 207, 196, 196, 169, 202 177, 193, 199, 210, 222, 222, 219, 250 246, 213, 234, 259, 256, 259, 253, 256 279, 269, 243, 222, 207, 225, 253, 202 188, 180, 193, 180, 144, 144, 146, 137 137, 146, 144, 125, 96, 104, 108, 123 98, 119, 110, 128, 96, 106, 100, 121 98, 106, 102, 121, 92, 117, 86, 117 125, 108, 110, 121, 119, 121, 112, 123 106, 112, 119, 121, 144, 114, 130, 123 121, 128, 114, 123, 121, 142, 135, 123 108, 144, 100, 130, 130, 106, 132, 142 135, 146, 104, 130, 121, 121, 100, 117 104, 108, 130, 104, 125, 117, 142, 110 154,/