SampleIdent,907A-23-3/27,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,10-aug-1993 7:05,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 85, 98, 108, 86, 90, 79, 83, 90 92, 85, 98, 88, 77, 79, 88, 92 77, 88, 94, 106, 77, 85, 85, 92 100, 86, 77, 92, 79, 100, 90, 104 90, 94, 112, 92, 94, 90, 94, 85 92, 106, 102, 106, 96, 83, 85, 98 86, 98, 117, 112, 104, 102, 100, 96 104, 114, 106, 86, 98, 106, 108, 117 110, 102, 106, 112, 94, 112, 121, 117 114, 128, 106, 100, 123, 117, 114, 98 121, 108, 106, 130, 119, 130, 98, 128 137, 104, 225, 104, 130, 112, 128, 117 137, 114, 132, 139, 130, 125, 100, 128 132, 121, 114, 139, 117, 92, 144, 117 142, 125, 110, 121, 121, 121, 130, 123 117, 114, 121, 117, 112, 130, 119, 92 112, 104, 112, 100, 128, 119, 114, 135 117, 117, 102, 117, 108, 130, 104, 102 100, 121, 106, 117, 106, 114, 119, 135 112, 121, 98, 123, 98, 114, 100, 128 121, 137, 132, 130, 114, 121, 117, 112 121, 119, 132, 104, 117, 104, 130, 123 104, 130, 125, 123, 125, 142, 144, 125 144, 142, 154, 130, 137, 149, 137, 144 144, 154, 154, 139, 154, 130, 125, 112 132, 123, 104, 90, 110, 128, 130, 104 90, 96, 92, 104, 110, 96, 108, 96 100, 114, 102, 94, 98, 110, 106, 104 121, 100, 112, 112, 114, 119, 106, 100 121, 94, 121, 121, 121, 123, 119, 137 110, 144, 130, 121, 125, 130, 144, 117 117, 130, 106, 86, 76, 88, 98, 94 100, 85, 72, 90, 100, 106, 108, 100 90, 108, 86, 102, 90, 98, 102, 130 86, 90, 90, 92, 88, 110, 92, 90 98, 104, 94, 92, 90, 90, 79, 94 94, 100, 98, 96, 88, 85, 98, 76 110, 81, 77, 98, 98, 92, 112, 100 94, 83, 102, 98, 117, 86, 88, 86 72, 94, 102, 85, 94, 77, 76, 88 94, 117, 90, 94, 106, 100, 90, 92 77, 108, 94, 96, 90, 94, 83, 77 90, 92, 85, 94, 110, 98, 102, 92 100, 106, 114, 85, 100, 108, 102, 117 380, 114, 149, 119, 117, 151, 123, 130 128, 151, 108, 146, 154, 174, 159, 130 151, 135, 156, 156, 142, 128, 125, 128 135, 139, 137, 121, 125, 119, 121, 98 98, 108, 100, 92, 83, 94, 92, 96 83, 92, 76, 81, 102, 86, 86, 106 90, 88, 83, 85, 83, 79, 100, 106 96, 88, 81, 94, 88, 92, 86, 83 77, 88, 72, 86, 86, 85, 102, 90 86, 79, 96, 90, 76, 71, 86, 88 83, 85, 96, 86, 72, 85, 83, 88 104, 79, 94, 83, 90, 81, 83, 62 72, 79, 85, 83, 83, 85, 83, 85 92, 88, 77, 76, 61, 88, 59, 88 92, 88, 74, 62, 79, 76, 81, 86 88, 66, 71, 102, 67, 72, 100, 72 88, 94, 102, 92, 83, 79, 81, 79 64, 76, 79, 71, 72, 69, 74, 79 83, 85, 71, 69, 81, 71, 66, 67 92, 83, 86, 72, 62, 66, 77, 81 72, 79, 114, 90, 83, 85, 88, 72 61, 76, 67, 69, 79, 92, 88, 72 77, 67, 83, 77, 79, 72, 79, 88 66, 76, 86, 83, 76, 88, 67, 66 71, 71, 76, 85, 67, 76, 72, 81 96, 76, 67, 94, 67, 69, 76, 67 76, 85, 90, 72, 72, 59, 71, 67 83, 86, 62, 76, 67, 98, 62, 76 79, 88, 79, 77, 92, 71, 85, 81 90, 98, 69, 86, 79, 77, 79, 72 85, 98, 85, 79, 79, 74, 76, 86 92, 71, 83, 83, 94, 67, 72, 85 79, 94, 79, 96, 96, 86, 85, 83 77, 94, 92, 86, 76, 79, 76, 90 98, 98, 88, 83, 94, 88, 108, 102 112, 104, 112, 94, 110, 96, 102, 110 104, 117, 117, 119, 102, 104, 110, 94 96, 106, 106, 88, 77, 92, 79, 76 69, 76, 74, 85, 79, 69, 86, 76 74, 79, 72, 79, 71, 86, 92, 74 85, 88, 79, 76, 79, 88, 67, 92 79, 72, 90, 79, 88, 79, 85, 81 88, 104, 83, 92, 88, 79, 81, 92 110, 92, 83, 94, 90, 90, 90, 104 85, 96, 102, 83, 104, 98, 102, 92 88, 98, 117, 100, 123, 85, 121, 125 114, 130, 117, 119, 125, 119, 135, 142 149, 149, 142, 146, 137, 185, 166, 193 166, 188, 172, 213, 202, 190, 204, 182 210, 193, 190, 177, 188, 190, 177, 202 161, 185, 149, 174, 169, 161, 159, 151 166, 166, 154, 164, 164, 149, 149, 144 174, 174, 169, 146, 144, 159, 135, 172 137, 135, 146, 164, 154, 180, 193, 207 228, 256, 306, 282, 279, 306, 313, 372 433, 493, 462, 445, 454, 369, 299, 317 269, 240, 250, 225, 210, 193, 156, 156 144, 130, 132, 135, 130, 144, 130, 132 130, 353, 121, 102, 135, 114, 142, 114 125, 117, 108, 119, 128, 108, 117, 135 123, 121, 121, 114, 121, 112, 130, 119 121, 121, 110, 102, 123, 114, 130, 117 121, 128, 123, 123, 121, 121, 142, 132 142, 130, 121, 135, 139, 135, 123, 164 156, 164, 182, 161, 169, 169, 180, 166 182, 177, 156, 169, 154, 156, 154, 159 125, 151, 169, 128, 121, 142, 159, 121 149, 128, 139, 144, 149, 144, 130, 125 149, 149, 156, 125, 125, 137, 119, 128 117, 104, 106, 112, 144, 114, 104, 98 100, 117, 110, 114, 110, 130, 119, 112 117, 123, 119, 139, 132, 114, 104, 159 121, 142, 149, 114, 137, 114, 144, 130 164, 114, 137, 142, 137, 135, 137, 121 149, 164, 149, 112, 132, 121, 137, 121 125, 130, 117, 130, 151, 156, 174, 193 219, 182, 193, 151, 174, 185, 177, 149 188, 142, 154, 139, 139, 132, 130, 135 161, 144, 142, 164, 144, 123, 166, 156 164, 156, 151, 166, 177, 174, 185, 180 193, 180, 174, 199, 182, 207, 196, 174 222, 199, 196, 164, 193, 222, 174, 182 182, 207, 196, 185, 188, 151, 177, 177 182, 172, 149, 164, 159, 182, 151, 154 177, 180, 182, 182, 164, 177, 166, 202 202, 174, 204, 182, 177, 169, 204, 196 188, 166, 166, 164, 159, 149, 159, 151 159, 130, 164, 137, 177, 161, 154, 174 156, 159, 154, 151, 172, 172, 137, 166 185, 207, 199, 188, 190, 222, 276, 269 331, 380, 420, 511, 595, 692, 795, 912 1011, 1102, 1197, 1303, 1354, 1475, 1616, 1459 1452, 1325, 1318, 1102, 829, 778, 666, 543 458, 380, 279, 310, 286, 276, 269, 243 213, 231, 188, 177, 182, 199, 222, 196 185, 190, 190, 177, 172, 180, 213, 196 177, 154, 180, 180, 174, 190, 216, 213 169, 185, 182, 202, 193, 213, 222, 240 222, 234, 219, 219, 246, 253, 240, 279 250, 250, 246, 213, 246, 266, 234, 222 237, 219, 188, 174, 193, 193, 196, 180 190, 204, 185, 199, 204, 185, 169, 166 169, 144, 142, 159, 174, 139, 146, 169 172, 169, 188, 188, 196, 177, 169, 169 193, 164, 159, 137, 142, 149, 149, 154 121, 139, 130, 130, 128, 132, 216, 119 130, 132, 142, 130, 166, 139, 130, 130 146, 119, 139, 121, 98, 112, 320, 94 132, 121, 98, 102, 119, 123, 121, 98 117, 119, 102, 119, 119, 121, 125, 135 128, 112, 130, 154, 144, 144, 130, 135 159, 156, 172, 177, 177, 196, 159, 193 188, 193, 180, 193, 216, 172, 193, 199 182, 182, 188, 190, 188, 188, 172, 154 164, 154, 149, 142, 119, 144, 154, 117 128, 132, 135, 130, 144, 146, 130, 125 125, 106, 112, 108, 106, 108, 114, 128 110, 106, 108, 149, 108, 123, 112, 112 119, 102, 117, 110, 112, 94, 114, 123 123, 125, 112, 117, 106, 132, 106, 108 121, 108, 112, 123, 117, 102, 123, 130 132, 117, 112, 100, 110, 139, 139, 128 144, 146, 128, 161, 166, 161, 169, 180 207, 213, 219, 240, 216, 185, 202, 210 204, 185, 182, 166, 174, 169, 151, 159 154, 137, 119, 130, 128, 144, 108, 96 121, 108, 119, 98, 112, 102, 104, 85 98, 94, 94, 100, 98, 88, 102, 108 104, 110, 110, 92, 100, 121, 98, 104 117, 92, 104, 106, 79, 110, 123, 104 121, 130, 108, 135, 130, 128, 146, 135 151, 161, 144, 137, 149, 154, 154, 174 156, 166, 164, 139, 137, 112, 125, 114 108, 94, 106, 96, 94, 88, 98, 94 83, 112, 94, 98, 112, 100, 98, 96 96, 94, 102, 108, 94, 100, 96, 90 86, 98, 94, 96, 77, 86, 102, 98 92, 92, 83, 96, 106, 125, 114, 94 123, 108, 121, 104, 132, 135, 128, 110 130, 132, 112, 149, 159, 135, 164, 137 159, 166, 164, 185, 164, 185, 190, 219 204, 185, 180, 213, 199, 228, 234, 196 222, 262, 219, 202, 234, 292, 228, 250 279, 262, 259, 231, 299, 253, 266, 243 299, 256, 256, 240, 213, 228, 246, 228 207, 219, 202, 204, 231, 204, 199, 213 188, 202, 213, 161, 180, 196, 188, 199 199, 199, 222, 182, 182, 169, 210, 161 164, 182, 149, 169, 156, 164, 156, 164 149, 161, 172, 169, 169, 193, 182, 164 177, 161, 166, 177, 182, 172, 188, 196 182, 169, 156, 174, 182, 177, 182, 177 185, 151, 156, 166, 213, 202, 185, 190 231, 228, 231, 219, 272, 240, 250, 303 240, 250, 243, 240, 222, 222, 216, 193 196, 174, 182, 185, 172, 193, 207, 159 199, 169, 188, 159, 216, 202, 188, 196 193, 204, 204, 185, 185, 193, 213, 174 159, 174, 161, 166, 172, 151, 151, 182 164, 182, 169, 161, 156, 151, 166, 164 188, 159, 177, 174, 199, 185, 182, 202 207, 204, 190, 169, 174, 159, 142, 169 144, 151, 132, 164, 135, 169, 144, 151 149, 154, 166, 137, 142, 156, 166, 144 164, 151, 154, 149, 151, 144, 135, 151 144, 154, 137, 144, 151, 119, 130, 142 114, 117, 121, 137, 128, 137, 125, 146 117, 123, 123, 119, 135, 135, 119, 114 96, 106, 98, 135, 104, 123, 108, 96 121, 100, 108, 96, 100, 112, 114, 96 112, 114, 151, 123, 132, 128, 130, 159 149, 424, 174, 180, 219, 234, 231, 231 228, 259, 216, 216, 210, 177, 169, 137 139, 149, 128, 121, 128, 123, 98, 130 125, 123, 121, 139, 121, 132, 119, 128 123, 130, 125, 135, 110, 130, 135, 151 137, 139, 164, 164, 172, 161, 161, 151 185, 144, 199, 169, 188, 177, 161, 132 169, 130, 166, 146, 121, 142, 125, 125 130, 123, 125, 144, 144, 161, 128, 164 144, 159, 164, 137, 159, 139, 137, 144 142, 135, 130, 144, 144, 98, 121, 114 144, 102, 123, 123, 117, 117, 102, 132 104, 108, 130, 123, 119, 132, 106, 110 104, 123, 125, 106, 128, 98, 123, 125 112, 102, 110, 114, 110, 100, 110, 106 128, 102, 114, 98, 119, 121, 114, 121 119, 125, 121, 117, 119, 119, 110, 119 102, 104, 121, 117, 119, 110, 144, 137 177, 169, 177, 182, 196, 199, 222, 234 219, 256, 213, 199, 228, 210, 216, 219 222, 216, 228, 199, 172, 190, 149, 164 128, 137, 128, 121, 128, 106, 117, 100 102, 100, 98, 98, 98, 108, 110, 106 100, 119, 81, 102, 123, 98, 102, 98 108, 94, 86, 96, 112, 90, 92, 110 92, 100, 96, 83, 106, 98, 117, 121 92, 81, 106, 96, 108, 114, 102, 108 102, 94, 83, 121, 100, 110, 119, 121 121, 106, 112, 114, 119, 102, 110, 96 106, 114, 104, 96, 100, 92, 92, 102 92, 104, 104, 104, 112, 98, 114, 114 100, 110, 121, 114, 121, 132, 159, 144 156, 166, 130, 144, 128, 144, 151, 137 123, 121, 121, 132, 125, 119, 108, 106 117, 98, 100, 114, 121, 106, 112, 119 125, 112, 119, 125, 121, 119, 114, 117 114, 135, 128, 137, 128, 151, 161, 149 156, 180, 159, 202, 210, 243, 207, 196 222, 279, 266, 303, 310, 372, 538, 497 428, 328, 276, 303, 380, 317, 310, 213 196, 166, 174, 196, 177, 177, 169, 182 182, 156, 166, 164, 156, 139, 128, 125 142, 114, 137, 128, 119, 123, 110, 121 114, 121, 96, 102, 102, 108, 88, 117 106, 108, 90, 92, 83, 86, 90, 102 88, 96, 102, 100, 110, 85, 86, 88 88, 106, 79, 92, 79, 90, 83, 88 67, 85, 74, 86, 86, 86, 90, 94 94, 79, 90, 92, 83, 100, 106, 88 96, 94, 79, 100, 102, 123, 114, 102 96, 100, 121, 121, 110, 123, 117, 130 128, 96, 121, 104, 108, 108, 102, 102 123, 85, 96, 76, 76, 92, 90, 79 92, 100, 76, 83, 94, 96, 90, 88 67, 72, 74, 77, 83, 85, 92, 108 88, 92, 77, 79, 86, 102, 64, 76 72, 85, 86, 76, 71, 71, 69, 79 59, 64, 86, 72, 71, 62, 66, 85 88, 69, 90, 86, 85, 72, 86, 74 81, 86, 76, 69, 85, 81, 96, 76 92, 88, 76, 88, 88, 77, 72, 94 76, 83, 96, 77, 86, 77, 81, 77 88, 94, 77, 79, 94, 76, 71, 76 85, 76, 90, 77, 76, 90, 69, 85 71, 106, 94, 85, 96, 90, 79, 86 79, 100, 86, 112, 86, 102, 96, 110 106, 142, 159, 159, 196, 199, 210, 204 250, 262, 266, 276, 303, 303, 313, 276 269, 310, 299, 303, 262, 210, 180, 164 166, 151, 172, 135, 117, 110, 100, 92 96, 96, 106, 100, 96, 104, 71, 100 90, 108, 96, 104, 98, 92, 88, 98 81, 98, 96, 90, 83, 90, 98, 90 98, 83, 59, 100, 92, 88, 104, 88 85, 88, 79, 85, 112, 85, 92, 88 72, 108, 62, 74, 79, 76, 88, 86 77, 96, 86, 96, 88, 92, 85, 79 83, 112, 132, 177, 159, 149, 128, 139 112, 128, 135, 130, 121, 98, 85, 92 108, 92, 76, 85, 79, 86, 66, 79 74, 86, 72, 48, 76, 72, 83, 76 76, 94, 92, 83, 79, 77, 85, 77 81, 92, 90, 72, 83, 104, 69, 77 85, 92, 86, 79, 86, 92, 92, 88 108, 100, 83, 90, 77, 90, 102, 90 96, 104, 90, 86, 92, 96, 98, 100 121, 77, 94, 102, 90, 100, 110, 106 104, 121, 110, 114, 92, 92, 92, 110 110, 110, 106, 98, 114, 112, 100, 137 108, 123, 100, 112, 98, 130, 104, 123 128, 106, 125, 121, 135, 139, 135, 132 154, 132, 144, 154, 142, 130, 142, 135 159, 149, 144, 144, 139, 123, 130, 139 132, 128, 130, 144, 154, 121, 142, 121 130, 135, 137, 149, 149, 156, 146, 142 139, 128, 135, 166, 161, 137, 154, 149 174, 188, 199, 169, 199, 246, 266, 313 306, 331, 320, 276, 250, 243, 262, 286 289, 266, 216, 202, 216, 210, 169, 188 180, 177, 190, 177, 180, 188, 188, 174 177, 190, 177, 185, 159, 174, 172, 169 169, 154, 188, 177, 182, 164, 142, 139 174, 164, 151, 146, 149, 161, 142, 156 172, 156, 185, 169, 164, 180, 164, 177 159, 142, 149, 164, 159, 177, 182, 169 177, 174, 207, 213, 204, 246, 228, 202 228, 231, 240, 240, 213, 216, 225, 202 182, 231, 196, 180, 188, 196, 164, 174 149, 164, 172, 166, 149, 142, 139, 130 142, 137, 135, 139, 119, 104, 121, 117 110, 117, 121, 119, 132, 100, 110, 90 110, 121, 125, 117, 117, 110, 108, 117 125, 96, 102, 96, 102, 110, 106, 119 106, 100, 123, 110, 100, 112, 100, 112 98, 98, 102, 100, 108, 100, 112, 114 108, 106, 96, 110, 98, 102, 108, 98 98, 104, 114, 121, 90, 110, 114, 121 100, 102, 83, 123, 94, 94, 92, 102 90, 98, 98, 108, 114, 117, 119, 83 104, 96, 130, 96, 100, 104, 98, 112 106, 102, 85, 110, 81, 106, 90, 100 92, 117, 121, 110, 98, 94, 90, 108 88, 88, 130, 121, 108, 121, 135, 123 130, 114, 119, 144, 130, 125, 121, 125 130, 102, 98, 100, 108, 110, 119, 98 128, 104, 128, 112, 104, 112, 112, 102 117, 100, 102, 114, 128, 104, 125, 106 128, 117, 146, 137, 154, 169, 196, 190 216, 237, 276, 243, 306, 306, 331, 313 328, 299, 320, 292, 306, 306, 289, 259 213, 228, 199, 180, 177, 161, 164, 144 151, 139, 142, 125, 137, 110, 128, 110 119, 119, 139, 106, 112, 130, 106, 114 137, 128, 132, 114, 119, 130, 125, 123 128, 123, 144, 135, 117, 159, 128, 144 130, 139, 164, 144, 144, 139, 149, 144 144, 144, 151, 146, 144, 161, 177, 182 199, 159, 154, 180, 188, 196, 182, 213 188, 196, 180, 202, 219, 213, 196, 228 219, 219, 234, 237, 213, 240, 222, 231 234, 246, 216, 219, 210, 234, 231, 216 177, 207, 185, 185, 222, 216, 199, 161 188, 193, 193, 169, 193, 174, 172, 159 161, 169, 182, 159, 156, 164, 182, 166 177, 166, 185, 166, 146, 125, 164, 159 151, 156, 121, 146, 159, 139, 135, 135 121, 119, 117, 121, 119, 123, 132, 121 139, 137, 104, 112, 108, 128, 117, 102 128, 92, 117, 98, 110, 106, 104, 119 106, 108, 108, 98, 88, 104, 108, 100 100, 98, 86, 110, 106, 108, 94, 104 104, 112, 128, 139, 86, 94, 110, 104 130, 123, 108, 104, 119, 144, 104, 135 130, 108, 121, 137, 137, 159, 110, 144 151, 190, 159, 177, 161, 154, 144, 139 130, 180, 154, 159, 159, 125, 146, 137 130, 114, 132, 135, 121, 112, 119, 108 100, 102, 85, 104, 98, 86, 102, 110 96, 90, 104, 100, 98, 102, 102, 102 114, 117, 98, 104, 125, 110, 94, 128 106, 90, 100, 98, 100, 106, 137, 100 117, 104, 110, 98, 119, 104, 108, 119 102, 102, 106, 114, 98, 98, 106, 106 88, 98, 112, 108, 90, 100, 108, 108 112, 108, 102, 106, 104, 121, 108, 112 108, 104, 106, 125, 108, 102, 98, 123 114, 114, 104, 102, 128, 102, 106, 108 119, 119, 121, 112, 130, 121, 102, 90 117, 110, 94, 98, 104, 112, 102, 106 117, 86, 100, 79, 106, 79, 98, 85 92, 104, 92, 92, 104, 76, 94, 92 67, 88, 106, 106, 76, 98, 85, 77 92, 88, 88, 76, 88, 86, 90, 112 104, 108, 119, 96, 106, 96, 94, 106 110, 90, 92, 112, 88, 106, 96, 100 88, 108, 108, 94, 106, 104, 117, 121 119, 137, 100, 121, 146, 144, 185, 159 193, 202, 188, 202, 213, 213, 213, 253 228, 225, 210, 185, 185, 164, 177, 207 174, 225, 250, 240, 262, 262, 243, 276 292, 269, 299, 346, 313, 335, 317, 320 299, 306, 335, 357, 335, 259, 246, 246 202, 204, 234, 193, 207, 159, 188, 169 149, 135, 110, 128, 130, 123, 102, 108 108, 114, 121, 112, 112, 117, 123, 110 119, 119, 106, 130, 121, 102, 106, 114 121, 96, 121, 132, 104, 125, 119, 132 121, 108, 108, 121, 119, 98, 130, 128 123, 121, 128, 123, 125, 130, 128, 108 114, 123, 117, 125, 119, 130, 104, 135 135, 108, 128, 137, 114, 119, 98, 128 130,/