SampleIdent,909A 11H-CC,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,19-aug-1993 9:00,/ DataAngleRange, 2.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 88, 79, 88, 85, 92, 85, 72, 83 92, 100, 81, 88, 90, 102, 88, 88 88, 66, 74, 94, 72, 83, 83, 88 77, 79, 81, 92, 96, 83, 88, 74 77, 90, 85, 77, 86, 86, 83, 100 94, 72, 77, 85, 59, 72, 88, 79 71, 74, 85, 83, 100, 96, 76, 83 76, 92, 85, 90, 96, 83, 83, 83 72, 77, 86, 106, 92, 85, 94, 81 106, 96, 90, 71, 67, 79, 85, 88 79, 79, 92, 69, 74, 88, 100, 72 85, 76, 67, 76, 96, 81, 72, 74 79, 86, 74, 74, 85, 81, 85, 86 92, 85, 98, 83, 85, 86, 83, 72 85, 94, 83, 86, 81, 88, 72, 90 83, 88, 79, 71, 79, 88, 98, 98 92, 104, 85, 72, 88, 76, 108, 88 90, 76, 83, 96, 85, 108, 90, 83 100, 85, 83, 88, 108, 102, 98, 77 98, 79, 88, 79, 85, 98, 104, 112 106, 79, 86, 106, 94, 92, 86, 104 88, 117, 79, 86, 106, 100, 86, 100 90, 90, 106, 98, 108, 90, 94, 110 83, 98, 102, 121, 96, 94, 108, 92 100, 108, 102, 110, 79, 98, 92, 102 110, 96, 102, 94, 108, 104, 100, 121 94, 106, 108, 96, 92, 106, 106, 96 106, 104, 121, 117, 108, 123, 96, 119 104, 100, 104, 100, 137, 98, 119, 130 112, 121, 123, 123, 96, 114, 102, 110 106, 108, 123, 125, 119, 123, 98, 104 102, 121, 130, 108, 104, 106, 110, 125 98, 94, 114, 135, 125, 112, 112, 114 342, 98, 104, 98, 102, 119, 100, 149 108, 121, 98, 108, 130, 108, 90, 128 132, 106, 119, 106, 104, 114, 117, 98 110, 119, 110, 121, 104, 90, 106, 94 106, 98, 96, 108, 110, 85, 98, 114 102, 110, 106, 106, 130, 98, 90, 90 128, 79, 100, 90, 108, 100, 108, 112 96, 112, 102, 92, 106, 114, 102, 104 119, 106, 108, 108, 104, 102, 90, 104 94, 102, 112, 104, 110, 104, 90, 100 106, 98, 92, 100, 114, 96, 90, 96 86, 110, 121, 110, 86, 86, 92, 117 96, 104, 88, 96, 106, 98, 108, 110 102, 98, 96, 102, 110, 90, 88, 90 110, 128, 90, 86, 108, 106, 98, 106 90, 106, 92, 96, 86, 96, 92, 112 85, 96, 90, 77, 88, 100, 94, 106 85, 86, 86, 92, 88, 92, 94, 76 98, 86, 100, 86, 96, 71, 90, 92 100, 85, 96, 90, 96, 98, 83, 81 94, 112, 79, 106, 94, 96, 96, 106 100, 96, 104, 94, 90, 88, 108, 108 96, 100, 119, 102, 100, 114, 139, 121 123, 151, 164, 149, 182, 193, 210, 204 237, 202, 196, 185, 146, 123, 121, 86 92, 94, 112, 79, 90, 88, 90, 94 100, 74, 85, 110, 108, 94, 96, 96 88, 83, 81, 100, 92, 67, 96, 106 106, 96, 83, 102, 77, 94, 102, 96 85, 81, 85, 88, 104, 98, 85, 104 72, 96, 100, 72, 98, 94, 90, 83 85, 79, 88, 92, 88, 96, 110, 112 119, 100, 100, 92, 117, 100, 108, 108 121, 117, 106, 123, 144, 132, 166, 166 166, 151, 180, 161, 202, 234, 246, 320 392, 520, 745, 858, 924, 1116, 1414, 1697 1945, 2098, 2162, 2116, 2144, 1927, 1544, 1082 751, 502, 310, 210, 161, 146, 123, 110 128, 125, 125, 123, 121, 98, 85, 86 88, 102, 90, 86, 92, 79, 92, 85 92, 88, 112, 92, 69, 98, 96, 85 94, 76, 88, 72, 85, 81, 77, 67 81, 79, 98, 88, 72, 74, 85, 71 94, 67, 90, 102, 94, 79, 83, 90 79, 77, 76, 83, 94, 69, 90, 88 79, 88, 79, 81, 92, 72, 79, 83 400, 94, 83, 76, 94, 76, 67, 74 71, 85, 88, 85, 69, 92, 71, 77 86, 83, 85, 85, 96, 79, 88, 85 79, 86, 88, 94, 86, 85, 59, 83 79, 83, 88, 76, 81, 81, 79, 62 83, 67, 77, 74, 79, 88, 85, 83 79, 86, 92, 67, 83, 74, 81, 62 81, 76, 67, 81, 71, 83, 85, 98 67, 72, 85, 72, 81, 92, 85, 67 88, 67, 92, 86, 76, 83, 77, 79 83, 83, 77, 94, 106, 88, 83, 72 86, 71, 88, 79, 83, 83, 90, 71 66, 76, 92, 85, 85, 79, 96, 79 83, 94, 106, 83, 86, 85, 88, 79 76, 83, 74, 79, 74, 86, 96, 71 77, 76, 81, 92, 98, 88, 81, 86 59, 66, 76, 85, 90, 74, 71, 74 94, 86, 85, 88, 74, 92, 72, 117 92, 85, 86, 100, 94, 83, 86, 90 66, 94, 88, 88, 90, 100, 102, 90 74, 110, 110, 121, 117, 177, 213, 240 259, 266, 279, 299, 299, 279, 289, 262 222, 213, 180, 151, 123, 114, 108, 112 104, 100, 86, 98, 85, 90, 79, 76 88, 100, 81, 102, 85, 85, 77, 96 85, 77, 77, 88, 62, 90, 94, 79 96, 79, 76, 292, 83, 88, 85, 83 76, 86, 90, 96, 79, 81, 88, 67 86, 92, 90, 79, 90, 100, 69, 79 100, 83, 102, 108, 94, 104, 100, 106 117, 96, 125, 114, 112, 123, 114, 110 114, 98, 110, 96, 98, 102, 104, 98 100, 98, 119, 96, 100, 96, 86, 79 79, 96, 110, 90, 246, 77, 71, 104 98, 100, 108, 85, 86, 92, 92, 85 94, 106, 112, 102, 110, 104, 102, 102 108, 123, 94, 100, 83, 110, 108, 100 98, 100, 83, 90, 100, 119, 98, 92 117, 98, 117, 114, 114, 92, 108, 100 119, 98, 90, 102, 121, 96, 102, 114 94, 102, 108, 104, 104, 110, 114, 94 92, 96, 85, 92, 106, 79, 108, 86 94, 94, 100, 86, 106, 98, 119, 112 112, 106, 135, 128, 142, 149, 185, 177 222, 237, 234, 269, 269, 269, 243, 246 207, 188, 166, 142, 121, 139, 117, 108 114, 88, 130, 100, 88, 92, 98, 92 86, 98, 94, 119, 96, 83, 100, 92 110, 121, 90, 102, 106, 98, 102, 98 98, 94, 110, 96, 76, 86, 96, 100 90, 96, 100, 88, 108, 100, 112, 108 125, 90, 110, 104, 104, 132, 117, 135 125, 154, 144, 159, 151, 177, 180, 196 185, 144, 130, 137, 121, 96, 112, 110 112, 104, 100, 102, 92, 114, 102, 110 125, 119, 104, 121, 102, 137, 100, 117 106, 117, 100, 100, 94, 104, 108, 137 117, 114, 104, 98, 76, 108, 108, 90 88, 90, 98, 121, 92, 108, 110, 85 96, 90, 119, 86, 114, 106, 83, 110 100, 117, 104, 112, 125, 108, 98, 100 106, 117, 117, 112, 125, 125, 121, 112 102, 86, 108, 94, 106, 106, 94, 125 102, 110, 128, 112, 112, 90, 90, 100 106, 94, 104, 92, 83, 110, 92, 96 100, 110, 106, 96, 92, 112, 94, 104 96, 104, 104, 117, 100, 102, 117, 117 98, 112, 119, 98, 117, 100, 112, 92 104, 102, 114, 102, 110, 94, 100, 121 110, 110, 106, 96, 110, 92, 108, 114 114, 88, 90, 119, 128, 106, 96, 121 104, 88, 102, 110, 112, 96, 106, 83 88, 112, 108, 121, 90, 110, 108, 119 110, 135, 132, 144, 144, 146, 156, 154 172, 196, 225, 225, 240, 243, 269, 243 266, 234, 282, 289, 317, 246, 199, 185 188, 137, 117, 98, 130, 104, 98, 110 102, 114, 119, 123, 100, 106, 114, 98 106, 108, 110, 106, 106, 117, 106, 106 121, 110, 90, 114, 108, 104, 112, 102 130, 132, 119, 121, 137, 128, 142, 151 142, 164, 196, 216, 266, 279, 289, 331 335, 357, 365, 376, 372, 324, 324, 484 262, 216, 204, 202, 159, 164, 180, 156 177, 182, 199, 164, 188, 180, 182, 161 135, 149, 142, 114, 117, 110, 100, 123 128, 121, 94, 125, 90, 94, 98, 121 100, 114, 96, 104, 92, 108, 96, 108 102, 106, 96, 106, 128, 106, 123, 90 98, 94, 106, 114, 106, 86, 117, 102 108, 81, 108, 108, 94, 94, 100, 104 100, 112, 117, 108, 104, 110, 119, 123 119, 114, 104, 108, 104, 121, 96, 104 117, 96, 104, 139, 100, 112, 104, 119 106, 119, 96, 123, 130, 132, 139, 130 151, 188, 210, 219, 276, 282, 282, 339 339, 310, 286, 313, 282, 276, 262, 250 243, 225, 228, 182, 177, 146, 164, 128 123, 125, 128, 121, 135, 106, 106, 123 100, 125, 104, 94, 94, 100, 117, 102 98, 110, 100, 104, 114, 121, 102, 98 104, 100, 117, 110, 98, 96, 119, 90 121, 121, 86, 106, 98, 121, 102, 104 94, 117, 100, 102, 98, 106, 106, 108 119, 100, 85, 90, 117, 96, 114, 102 92, 110, 106, 92, 81, 79, 112, 96 90, 86, 110, 108, 94, 110, 88, 102 90, 102, 98, 90, 98, 106, 98, 121 102, 104, 112, 96, 112, 83, 123, 121 123, 125, 114, 114, 159, 174, 169, 412 161, 172, 164, 164, 164, 154, 139, 132 123, 121, 146, 114, 119, 108, 114, 110 108, 114, 123, 125, 125, 121, 154, 144 180, 166, 182, 185, 185, 259, 253, 272 331, 313, 317, 324, 331, 317, 342, 320 299, 292, 313, 320, 306, 306, 299, 243 234, 177, 188, 166, 135, 130, 117, 110 128, 112, 92, 92, 102, 94, 112, 117 83, 92, 114, 90, 100, 86, 88, 86 86, 88, 104, 117, 119, 119, 151, 146 188, 193, 193, 219, 234, 243, 228, 225 216, 243, 216, 174, 188, 174, 142, 146 108, 119, 125, 121, 106, 121, 92, 98 100, 135, 331, 117, 121, 144, 139, 159 159, 154, 164, 188, 182, 161, 146, 142 123, 144, 125, 102, 128, 96, 108, 108 106, 104, 98, 88, 106, 114, 119, 102 121, 123, 108, 100, 102, 96, 104, 110 100, 108, 106, 117, 125, 137, 149, 169 202, 180, 240, 231, 313, 266, 306, 346 320, 262, 259, 234, 250, 228, 219, 199 177, 156, 185, 169, 149, 154, 135, 125 142, 135, 130, 110, 106, 123, 92, 86 96, 96, 86, 98, 88, 79, 77, 92 88, 96, 85, 85, 94, 90, 88, 94 104, 71, 67, 85, 86, 94, 79, 96 85, 77, 83, 88, 96, 92, 104, 96 104, 104, 121, 112, 117, 108, 114, 117 108, 137, 108, 125, 119, 128, 110, 121 142, 132, 151, 182, 125, 159, 169, 172 196, 207, 196, 202, 177, 185, 161, 149 128, 121, 110, 98, 90, 83, 77, 92 119, 79, 83, 83, 90, 71, 90, 61 85, 100, 94, 77, 94, 81, 86, 98 85, 71, 98, 79, 83, 77, 88, 102 74, 92, 92, 90, 85, 94, 79, 83 76, 100, 88, 86, 83, 102, 104, 72 74, 79, 94, 96, 104, 96, 98, 123 119, 110, 108, 121, 110, 100, 110, 119 108, 112, 102, 135, 121, 114, 151, 154 154, 196, 180, 216, 237, 266, 246, 219 231, 196, 182, 216, 161, 172, 156, 142 119, 110, 112, 106, 98, 112, 104, 117 98, 100, 98, 106, 92, 108, 88, 81 83, 83, 112, 108, 92, 114, 108, 110 117, 112, 106, 117, 123, 121, 106, 100 117, 110, 110, 104, 112, 86, 96, 92 86, 79, 86, 90, 92, 67, 69, 77 86, 81, 77, 69, 71, 90, 86, 85 77, 90, 86, 92, 98, 104, 98, 85 125, 100, 130, 146, 135, 151, 161, 182 182, 188, 204, 207, 204, 207, 174, 156 149, 151, 132, 151, 112, 112, 112, 114 90, 90, 98, 96, 92, 106, 90, 64 83, 94, 106, 102, 117, 100, 110, 137 119, 154, 161, 188, 185, 207, 207, 177 204, 166, 177, 174, 154, 154, 149, 130 130, 119, 135, 119, 110, 110, 104, 92 106, 96, 112, 125, 108, 110, 96, 77 94, 130, 110, 86, 88, 110, 76, 88 102, 92, 108, 102, 112, 77, 85, 98 76, 88, 104, 96, 85, 83, 90, 88 69, 88, 71, 83, 96, 88, 86, 92 86, 83, 94, 92, 83, 76, 94, 83 86, 79, 90, 92, 72, 110, 96, 86 90, 96, 92, 71, 90, 98, 88, 86 92, 110, 102, 90, 92, 94, 85, 98 104, 79, 94, 96, 114, 102, 96, 110 114, 108, 108, 104, 81, 98, 90, 83 94, 106, 128, 85, 117, 117, 117, 121 185, 177, 219, 202, 237, 219, 272, 266 269, 286, 269, 243, 204, 202, 164, 169 137, 144, 125, 128, 108, 125, 123, 114 106, 130, 112, 121, 137, 121, 135, 104 96, 121, 117, 106, 106, 100, 100, 86 96, 85, 98, 108, 108, 88, 108, 128 106, 121, 108, 117, 139, 144, 154, 177 172, 156, 159, 159, 144, 146, 159, 112 130, 123, 108, 110, 92, 102, 92, 121 123, 88, 98, 92, 110, 139, 128, 112 112, 137, 130, 98, 142, 119, 96, 102 106, 117, 92, 96, 72, 102, 96, 86 90, 83, 76, 79, 88, 66, 66, 88 85, 96, 86, 88, 92, 88, 76, 94 86, 88, 92, 76, 88, 114, 94, 98 83, 108, 104, 92, 114, 85, 98, 112 121, 102, 119, 117, 117, 112, 130, 112 128, 110, 114, 106, 102, 110, 94, 94 94, 86, 106, 100, 96, 98, 86, 76 86, 90, 94, 100, 94, 98, 90, 98 92, 88, 94, 100, 108, 104, 128, 121 130, 114, 117, 128, 177, 156, 149, 159 156, 139, 139, 149, 154, 169, 146, 159 156, 130, 149, 149, 161, 166, 154, 144 123, 119, 96, 106, 108, 106, 100, 88 83, 83, 86, 88, 94, 96, 79, 104 90, 110, 92, 96, 98, 112, 96, 123 100, 119, 137, 125, 137, 123, 137, 114 119, 114, 108, 135, 135, 121, 121, 132 128, 154, 144, 161, 161, 174, 174, 169 151, 159, 166, 149, 135, 123, 128, 117 108, 121, 106, 102, 81, 88, 102, 86 88, 85, 85, 90, 104, 76, 86, 85 90, 94, 77, 72, 72, 112, 71, 77 76, 90, 90, 81, 77, 79, 86, 100 88, 85, 88, 79, 77, 83, 90, 96 85, 85, 86, 77, 83, 83, 106, 67 77, 81, 83, 79, 72, 98, 71, 76 98, 67, 71, 83, 67, 79, 79, 77 76, 64, 79, 81, 86, 98, 83, 96 83, 79, 90, 88, 86, 100, 90, 94 102, 72, 96, 102, 128, 96, 132, 128 132, 151, 110, 125, 121, 112, 112, 114 121, 108, 86, 94, 102, 81, 71, 90 86, 100, 86, 74, 92, 85, 66, 83 86, 98, 79, 90, 100, 94, 96, 108 108, 98, 102, 114, 106, 106, 121, 112 88, 108, 123, 119, 123, 110, 117, 112 108, 117, 132, 128, 128, 125, 125, 119 130, 125, 121, 125, 130, 137, 146, 125 128, 135, 137, 130, 146, 137, 119, 112 135, 135, 146, 112, 125, 98, 100, 125 110, 90, 119, 92, 86, 83, 85, 90 79, 90, 76, 83, 96, 102, 94, 79 81, 85, 86, 102, 86, 77, 98, 85 90, 310, 69, 104, 86, 83, 81, 92 81, 79, 85, 86, 108, 86, 61, 67 90, 77, 90, 85, 86, 77, 92, 94 110, 94, 98, 86, 86, 85, 77, 61 88, 90, 85, 77, 79, 83, 77, 86 90, 102, 83, 76, 114, 86, 100, 94 108, 85, 90, 92, 90, 88, 90, 77 98, 76, 96, 90, 94, 86, 98, 98 119, 100, 98, 77, 106, 81, 79, 94 92, 92, 85, 98, 77, 88, 86, 79 96, 100, 98, 85, 104, 104, 100, 90 100, 110, 104, 106, 117, 90, 102, 88 100, 112, 90, 146, 128, 149, 135, 159 180, 210, 243, 292, 350, 369, 404, 493 515, 534, 488, 458, 416, 365, 412, 376 376, 357, 299, 276, 237, 219, 190, 196 185, 202, 210, 177, 164, 193, 193, 204 172, 151, 151, 169, 139, 149, 137, 159 128, 130, 125, 125, 125, 110, 112, 130 137, 132, 164, 128, 159, 156, 159, 156 164, 154, 164, 146, 144, 172, 144, 128 144, 151, 125, 151, 144, 130, 123, 112 110, 102, 104, 106, 110, 130, 102, 98 106, 112, 130, 100, 102, 108, 102, 121 102, 98, 100, 102, 94, 108, 108, 106 104, 96, 159, 119, 137, 123, 128, 119 128, 149, 144, 123, 144, 114, 137, 119 110, 123, 125, 96, 100, 110, 88, 112 102, 110, 88, 92, 94, 94, 102, 85 94, 110, 104, 96, 100, 112, 100, 94 77, 90, 88, 90, 79, 88, 90, 86 98, 108, 85, 100, 119, 102, 117, 117 86, 108, 119, 102, 104, 139, 146, 125 125, 139, 132, 149, 151, 149, 174, 174 156, 132, 146, 164, 146, 139, 119, 177 130, 144, 154, 144, 151, 142, 146, 135 135, 144, 123, 159, 132, 169, 180, 159 190, 231, 231, 228, 234, 250, 228, 228 216, 225, 231, 188, 188, 207, 190, 169 164, 146, 135, 137, 130, 112, 128, 117 112, 110, 102, 112, 104, 119, 112, 114 96, 94, 106, 112, 112, 94, 104, 108 106, 96, 110, 100, 86, 100, 104, 110 102, 108, 94, 106, 112, 102, 102, 83 102, 100, 100, 108, 121, 110, 92, 121 117, 132, 130, 119, 128, 132, 139, 154 144, 137, 151, 144, 156, 135, 121, 151 128, 128, 123, 128, 137, 144, 149, 119 149, 137, 159, 169, 146, 159, 159, 119 130, 121, 102, 123, 125, 128, 114, 104 106, 110, 96, 106, 106, 94, 119, 106 76, 77, 92, 106, 123, 110, 110, 117 112, 104, 85, 121, 98, 102, 94, 86 96, 102, 102, 98, 100, 119, 121, 119 110, 119, 135, 128, 144, 128, 130, 114 139, 119, 125, 130, 130, 114, 144, 137 137, 98, 117, 96, 119, 106, 96, 100 94, 110, 94, 106, 94, 114, 117, 94 117, 92, 114, 108, 123, 114, 123, 119 114, 114, 102, 112, 135, 135, 108, 132 130, 137, 135, 142, 135, 96, 102, 132 149, 132, 121, 128, 128, 144, 110, 119 102, 119, 137, 135, 128, 144, 123, 137 149, 121, 132, 156, 146, 149, 149, 164 159, 149, 149, 146, 144, 137, 119, 132 144, 125, 108, 125, 151, 137, 137, 146 125, 149, 149, 139, 149, 130, 130, 125 130, 119, 151, 125, 125, 119, 125, 114 130, 112, 132, 110, 135, 144, 121, 112 117, 130, 149, 132, 137, 144, 159, 172 130, 174, 174, 151, 151, 149, 164, 137 137, 174, 146, 137, 156, 132, 130, 121 149, 114, 114, 128, 117, 117, 123, 102 102, 132, 100, 125, 114, 98, 121, 100 117, 121, 98, 106, 106, 119, 137, 112 110, 106, 110, 114, 123, 108, 132, 130 96, 117, 121, 106, 119, 119, 117, 119 108, 139, 96, 83, 114, 128, 125, 100 112, 123, 112, 98, 106, 92, 106, 123 114, 117, 128, 119, 123, 130, 123, 125 132, 125, 139, 130, 117, 132, 128, 117 112, 121, 108, 114, 123, 117, 121, 96 128, 130, 112, 104, 119, 110, 121, 121 119, 132, 119, 114, 142, 119, 112, 121 106, 123, 135, 130, 128, 119, 125, 102 100, 130, 125, 137, 130, 104, 110, 114 130, 130, 125, 119, 108, 123, 144, 96 108, 119, 106, 117, 151, 92, 132, 96 123, 112, 137, 112, 123, 128, 112, 130 108, 121, 94, 130, 123, 114, 112, 102 110, 106, 112, 86, 88, 130, 112, 96 121, 117, 96, 117, 104, 121, 98, 104 102, 106, 100, 117, 79, 88, 108, 114 110, 114, 104, 85, 92, 104, 92, 104 104, 90, 108, 100, 102, 121, 123, 94 102, 92, 106, 98, 104, 117, 114, 112 112, 144, 144, 108, 142, 146, 123, 135 144, 135, 128, 137, 139, 119, 132, 142 137, 128, 156, 119, 106, 144, 119, 119 121, 130, 121, 114, 117, 110, 104, 104 130, 144, 121, 125, 132, 130, 137, 144 100, 98, 108, 112, 102, 100, 117, 121 102, 117, 102, 121, 88, 121, 92, 112 92, 96, 90, 121, 104, 112, 98, 92 102, 98, 106, 108, 96, 114, 117, 96 119, 104, 121, 98, 98, 117, 96, 108 114, 110, 102, 94, 110, 106, 125, 123 125, 112, 112, 117, 130, 130, 108, 112 102, 144, 128, 137, 128, 164, 144, 180 190, 202, 196, 246, 231, 259, 266, 269 289, 296, 262, 256, 246, 219, 240,/