SampleIdent,909C 7R-1 32-33BULK,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 4-sep-1993 5:15,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 121, 106, 100, 112, 96, 110, 102, 96 102, 90, 119, 110, 90, 112, 88, 102 121, 108, 123, 121, 90, 112, 110, 108 83, 108, 90, 98, 112, 119, 114, 123 96, 102, 112, 128, 94, 104, 121, 117 92, 119, 112, 100, 130, 137, 117, 121 130, 123, 117, 108, 119, 135, 130, 121 177, 104, 130, 108, 121, 130, 135, 121 144, 132, 112, 135, 125, 121, 130, 132 114, 119, 104, 137, 110, 100, 125, 128 108, 132, 119, 123, 130, 125, 121, 114 135, 154, 117, 106, 114, 117, 130, 121 119, 114, 137, 123, 123, 125, 149, 128 132, 130, 139, 128, 139, 132, 117, 114 130, 119, 135, 100, 139, 123, 139, 125 119, 123, 137, 130, 142, 137, 149, 128 137, 139, 142, 135, 123, 125, 125, 149 144, 144, 132, 144, 151, 137, 137, 135 135, 119, 151, 123, 161, 130, 135, 137 142, 161, 137, 128, 139, 137, 151, 154 139, 117, 135, 130, 149, 135, 137, 149 151, 142, 149, 156, 180, 159, 132, 149 202, 159, 177, 180, 164, 199, 174, 156 193, 185, 196, 180, 185, 166, 196, 151 151, 125, 137, 142, 144, 130, 137, 114 132, 119, 119, 128, 121, 125, 121, 112 114, 112, 102, 108, 125, 114, 112, 119 112, 112, 98, 106, 112, 108, 112, 121 96, 88, 104, 92, 114, 117, 130, 104 112, 112, 121, 90, 108, 121, 100, 112 104, 119, 125, 106, 100, 100, 125, 100 104, 102, 98, 100, 92, 104, 90, 106 94, 88, 104, 96, 90, 98, 92, 88 92, 102, 98, 108, 108, 102, 90, 96 90, 102, 112, 90, 92, 79, 72, 104 117, 94, 96, 94, 96, 100, 104, 90 117, 96, 102, 92, 100, 100, 90, 92 96, 96, 74, 86, 106, 100, 71, 90 121, 104, 94, 108, 98, 128, 125, 110 81, 88, 90, 92, 106, 83, 94, 90 114, 72, 90, 96, 88, 98, 108, 88 117, 88, 98, 92, 96, 92, 94, 88 125, 117, 108, 117, 128, 94, 106, 108 102, 106, 94, 121, 121, 117, 130, 121 130, 142, 125, 144, 119, 130, 154, 159 142, 166, 146, 182, 164, 161, 207, 182 174, 202, 169, 166, 172, 185, 166, 149 149, 128, 119, 106, 110, 96, 83, 92 98, 86, 88, 104, 104, 98, 81, 88 83, 90, 90, 92, 67, 72, 90, 83 92, 102, 92, 94, 81, 83, 88, 92 85, 88, 92, 83, 86, 83, 79, 106 104, 88, 96, 74, 88, 88, 90, 86 81, 85, 100, 108, 102, 86, 104, 92 114, 88, 94, 125, 71, 90, 92, 112 88, 90, 90, 88, 81, 88, 86, 88 67, 81, 86, 79, 77, 83, 77, 76 79, 74, 74, 71, 88, 88, 67, 90 79, 86, 85, 71, 74, 77, 86, 76 86, 90, 306, 94, 81, 90, 79, 85 86, 71, 94, 81, 76, 98, 83, 96 79, 92, 92, 85, 90, 86, 83, 88 88, 92, 85, 71, 88, 83, 83, 86 94, 67, 74, 85, 85, 56, 76, 71 76, 92, 71, 79, 86, 79, 67, 72 90, 62, 69, 81, 85, 77, 85, 79 86, 71, 72, 83, 81, 72, 88, 85 76, 79, 83, 88, 79, 88, 88, 85 92, 67, 79, 71, 76, 86, 92, 62 69, 77, 92, 92, 64, 92, 76, 83 88, 77, 85, 72, 92, 83, 77, 81 76, 90, 83, 83, 76, 92, 77, 77 81, 77, 72, 76, 94, 86, 83, 92 69, 81, 85, 79, 85, 76, 77, 76 90, 76, 85, 94, 92, 76, 83, 88 76, 77, 76, 92, 79, 83, 79, 104 86, 72, 106, 72, 98, 86, 85, 92 81, 83, 72, 94, 94, 102, 108, 96 94, 86, 100, 110, 102, 106, 121, 110 110, 132, 110, 110, 110, 130, 94, 114 117, 110, 96, 106, 102, 112, 88, 98 77, 85, 92, 92, 85, 81, 85, 86 79, 96, 85, 85, 83, 79, 94, 83 86, 88, 85, 100, 85, 96, 96, 110 79, 86, 110, 92, 104, 110, 102, 98 110, 104, 88, 121, 104, 92, 119, 94 100, 112, 110, 77, 104, 110, 96, 119 106, 83, 88, 83, 98, 83, 119, 104 110, 106, 139, 85, 92, 104, 92, 98 102, 102, 272, 108, 104, 108, 114, 128 142, 137, 130, 146, 154, 156, 177, 164 166, 202, 228, 207, 243, 234, 222, 243 240, 266, 246, 253, 213, 199, 190, 207 190, 177, 151, 159, 172, 151, 142, 180 161, 149, 149, 149, 137, 144, 144, 380 149, 142, 159, 132, 144, 135, 156, 144 137, 117, 151, 130, 137, 172, 159, 151 149, 144, 180, 207, 240, 240, 266, 296 346, 306, 350, 392, 369, 388, 361, 376 310, 313, 262, 231, 182, 164, 159, 144 149, 137, 106, 106, 144, 119, 112, 117 119, 121, 121, 123, 121, 125, 83, 119 121, 121, 128, 139, 117, 119, 96, 110 94, 137, 125, 86, 121, 112, 112, 110 112, 114, 117, 119, 130, 125, 130, 137 130, 188, 182, 193, 210, 216, 269, 253 266, 243, 210, 177, 164, 142, 146, 119 130, 117, 121, 119, 117, 114, 110, 137 108, 144, 135, 100, 114, 114, 130, 117 123, 125, 96, 106, 114, 117, 121, 114 108, 98, 108, 142, 123, 119, 130, 110 117, 149, 151, 142, 146, 154, 128, 139 132, 125, 121, 128, 125, 121, 98, 104 114, 117, 130, 125, 92, 98, 104, 114 112, 114, 142, 123, 114, 137, 130, 166 156, 164, 161, 185, 182, 164, 146, 164 156, 182, 169, 154, 132, 151, 180, 130 135, 139, 139, 142, 149, 121, 128, 137 139, 146, 172, 137, 149, 125, 149, 146 149, 154, 161, 156, 174, 188, 185, 182 196, 169, 166, 180, 169, 174, 159, 149 142, 114, 130, 123, 154, 135, 130, 132 135, 139, 159, 137, 166, 137, 132, 146 144, 169, 185, 182, 180, 156, 174, 172 174, 196, 196, 193, 188, 172, 188, 228 210, 231, 199, 228, 253, 243, 246, 231 228, 228, 222, 219, 210, 204, 234, 219 193, 199, 193, 216, 199, 188, 180, 182 199, 177, 188, 202, 182, 159, 164, 156 188, 164, 169, 128, 154, 159, 137, 144 154, 135, 137, 149, 144, 142, 121, 117 154, 146, 149, 123, 142, 137, 177, 161 172, 180, 193, 196, 196, 216, 234, 269 286, 310, 369, 412, 534, 610, 756, 858 1109, 1318, 1490, 1756, 2134, 2275, 2352, 2294 2181, 1971, 1739, 1376, 1096, 870, 767, 529 433, 384, 353, 346, 346, 335, 320, 299 262, 272, 237, 250, 231, 213, 216, 219 225, 207, 188, 185, 185, 185, 202, 188 196, 210, 185, 231, 188, 234, 231, 219 237, 231, 279, 317, 335, 339, 320, 269 276, 250, 253, 250, 262, 272, 303, 339 331, 372, 396, 462, 471, 462, 534, 484 493, 433, 424, 350, 339, 289, 269, 246 237, 199, 193, 210, 199, 213, 172, 190 185, 166, 180, 151, 154, 151, 144, 142 142, 139, 123, 137, 130, 123, 123, 139 121, 130, 125, 110, 132, 331, 106, 112 114, 123, 104, 125, 121, 112, 125, 114 121, 121, 114, 121, 132, 96, 114, 106 119, 121, 108, 121, 117, 117, 135, 114 110, 108, 114, 98, 112, 110, 100, 123 106, 106, 110, 100, 106, 102, 96, 104 112, 117, 123, 137, 104, 130, 132, 121 102, 130, 149, 161, 172, 161, 182, 188 193, 169, 144, 169, 117, 159, 151, 159 151, 130, 154, 132, 146, 156, 137, 149 142, 159, 130, 123, 142, 130, 125, 172 149, 146, 146, 144, 149, 166, 164, 144 156, 135, 154, 121, 121, 137, 114, 117 137, 106, 112, 96, 123, 114, 117, 112 86, 137, 92, 108, 110, 112, 119, 108 110, 110, 121, 108, 119, 132, 86, 132 117, 110, 130, 137, 142, 132, 156, 146 125, 123, 132, 128, 114, 117, 121, 108 112, 135, 125, 156, 151, 169, 154, 166 154, 156, 182, 174, 188, 185, 188, 182 172, 119, 139, 137, 132, 119, 130, 125 121, 125, 100, 121, 135, 114, 94, 112 108, 106, 90, 100, 108, 100, 102, 83 86, 88, 86, 92, 88, 81, 96, 92 92, 88, 96, 81, 94, 90, 123, 132 104, 112, 98, 98, 102, 72, 67, 94 81, 83, 77, 98, 71, 76, 72, 96 79, 81, 79, 83, 77, 74, 81, 90 94, 85, 79, 85, 90, 77, 61, 94 83, 100, 88, 62, 102, 83, 90, 92 83, 98, 106, 77, 90, 88, 86, 83 92, 96, 92, 92, 106, 79, 106, 96 85, 98, 94, 106, 117, 94, 98, 92 112, 104, 104, 98, 112, 108, 104, 110 117, 117, 100, 112, 117, 110, 114, 117 110, 112, 121, 137, 154, 159, 159, 154 159, 177, 177, 185, 202, 174, 193, 219 216, 210, 219, 213, 222, 219, 219, 246 216, 219, 228, 228, 237, 234, 237, 250 253, 272, 286, 266, 276, 292, 266, 279 276, 306, 256, 256, 269, 256, 228, 231 253, 234, 219, 196, 216, 188, 188, 166 177, 149, 174, 164, 174, 161, 144, 161 142, 139, 166, 169, 142, 142, 159, 130 146, 142, 159, 137, 135, 121, 154, 125 132, 161, 149, 128, 156, 164, 132, 132 137, 172, 144, 169, 149, 154, 132, 117 146, 144, 144, 142, 125, 139, 169, 146 142, 132, 149, 185, 164, 177, 219, 213 266, 279, 306, 335, 310, 342, 357, 310 342, 289, 286, 269, 243, 259, 240, 185 207, 177, 182, 177, 169, 164, 149, 132 137, 156, 144, 151, 161, 132, 169, 164 137, 144, 164, 144, 137, 151, 132, 146 156, 139, 161, 159, 169, 172, 166, 149 161, 169, 180, 166, 164, 185, 164, 202 161, 182, 182, 151, 190, 193, 185, 177 166, 188, 199, 169, 177, 177, 159, 159 128, 125, 125, 169, 123, 112, 135, 130 108, 123, 128, 119, 106, 128, 132, 106 125, 108, 125, 104, 121, 135, 149, 128 137, 128, 142, 128, 146, 137, 102, 142 121, 119, 121, 132, 121, 100, 106, 94 117, 98, 119, 112, 121, 121, 114, 106 117, 108, 128, 114, 106, 88, 117, 110 100, 92, 112, 104, 135, 90, 102, 90 102, 100, 106, 132, 130, 128, 128, 156 161, 213, 246, 279, 313, 269, 303, 296 335, 324, 286, 262, 225, 199, 202, 185 159, 137, 110, 112, 119, 108, 102, 98 114, 102, 112, 123, 108, 112, 112, 117 94, 98, 119, 142, 121, 125, 106, 119 130, 106, 161, 174, 149, 172, 164, 202 180, 204, 207, 216, 159, 169, 149, 174 130, 132, 151, 119, 81, 77, 96, 81 108, 90, 112, 104, 98, 98, 110, 112 123, 117, 112, 90, 102, 104, 88, 92 104, 98, 114, 86, 92, 114, 94, 110 96, 123, 110, 102, 106, 123, 110, 117 104, 98, 125, 94, 102, 106, 110, 94 94, 104, 106, 114, 112, 108, 94, 85 130, 100, 110, 121, 121, 104, 98, 117 130, 96, 121, 128, 177, 213, 185, 112 130, 132, 156, 159, 114, 110, 123, 130 112, 128, 123, 121, 121, 123, 114, 135 132, 112, 132, 149, 137, 159, 174, 174 231, 240, 234, 262, 279, 262, 231, 262 231, 222, 199, 193, 180, 164, 154, 144 132, 137, 119, 102, 125, 94, 108, 108 108, 104, 83, 106, 98, 102, 114, 90 94, 85, 108, 69, 102, 106, 86, 86 98, 98, 90, 100, 96, 96, 96, 86 108, 94, 94, 94, 100, 100, 77, 90 90, 98, 98, 90, 114, 96, 94, 90 83, 104, 96, 100, 94, 96, 104, 100 102, 117, 94, 112, 86, 104, 86, 100 100, 102, 106, 88, 104, 119, 102, 110 104, 85, 88, 92, 88, 94, 85, 76 112, 88, 88, 86, 104, 104, 112, 112 98, 114, 110, 112, 119, 125, 142, 121 132, 132, 104, 132, 142, 137, 130, 130 121, 130, 123, 110, 123, 117, 112, 121 119, 121, 125, 151, 142, 117, 130, 156 119, 142, 130, 149, 144, 135, 146, 164 151, 172, 188, 193, 185, 190, 182, 207 216, 174, 199, 202, 216, 219, 234, 207 199, 196, 216, 199, 177, 185, 199, 202 207, 219, 202, 219, 231, 234, 237, 216 204, 156, 164, 172, 164, 159, 164, 114 128, 125, 130, 108, 104, 98, 121, 110 112, 96, 94, 102, 90, 94, 102, 90 90, 83, 88, 72, 98, 66, 88, 76 96, 92, 76, 96, 102, 88, 85, 67 86, 71, 108, 85, 83, 92, 106, 94 81, 98, 96, 100, 90, 77, 66, 94 92, 94, 88, 88, 92, 98, 108, 83 98, 90, 90, 90, 102, 92, 85, 72 79, 79, 86, 59, 85, 108, 114, 144 130, 92, 98, 77, 98, 98, 98, 72 86, 81, 77, 56, 76, 77, 85, 72 92, 72, 64, 106, 69, 83, 102, 77 86, 110, 117, 98, 90, 94, 102, 104 119, 110, 102, 100, 102, 94, 104, 104 100, 100, 114, 90, 102, 85, 92, 79 77, 88, 71, 72, 72, 83, 83, 59 62, 71, 67, 76, 72, 61, 83, 76 74, 76, 77, 83, 72, 71, 74, 59 71, 76, 74, 61, 90, 67, 71, 94 92, 90, 86, 90, 108, 90, 108, 88 92, 94, 92, 108, 71, 98, 74, 83 85, 76, 72, 85, 76, 85, 71, 83 85, 100, 86, 86, 72, 110, 85, 112 100, 106, 94, 121, 119, 117, 108, 130 142, 132, 154, 166, 193, 210, 259, 253 320, 353, 388, 441, 420, 454, 475, 475 400, 372, 328, 310, 276, 246, 213, 207 174, 142, 117, 100, 98, 88, 104, 98 98, 117, 112, 119, 100, 128, 112, 106 125, 114, 125, 104, 104, 114, 112, 112 106, 114, 102, 98, 85, 102, 94, 98 108, 88, 94, 100, 83, 77, 94, 110 100, 96, 83, 102, 102, 86, 76, 88 100, 88, 86, 71, 72, 94, 74, 81 76, 83, 74, 71, 64, 59, 64, 71 66, 96, 85, 67, 88, 66, 76, 77 76, 66, 79, 71, 85, 77, 66, 53 66, 76, 66, 74, 79, 71, 67, 77 79, 85, 72, 86, 64, 74, 71, 71 79, 86, 76, 85, 77, 83, 86, 88 81, 90, 69, 94, 77, 85, 83, 77 77, 90, 86, 85, 86, 83, 85, 85 88, 85, 88, 94, 86, 83, 94, 102 108, 104, 96, 102, 100, 104, 92, 90 125, 94, 86, 104, 90, 125, 110, 114 104, 114, 92, 106, 128, 106, 125, 106 90, 102, 102, 96, 104, 88, 102, 98 98, 92, 121, 121, 108, 96, 88, 100 106, 92, 137, 108, 121, 112, 106, 106 128, 130, 112, 121, 125, 130, 100, 98 108, 119, 106, 130, 119, 119, 137, 156 128, 125, 130, 128, 130, 104, 137, 112 132, 137, 149, 128, 123, 151, 123, 119 132, 130, 121, 151, 159, 144, 137, 161 154, 177, 151, 180, 199, 234, 231, 269 286, 279, 253, 282, 279, 269, 262, 225 210, 210, 216, 222, 193, 199, 174, 196 185, 182, 190, 199, 188, 164, 193, 190 216, 207, 210, 180, 174, 199, 185, 149 121, 164, 154, 146, 159, 144, 149, 144 149, 159, 161, 180, 149, 149, 146, 146 172, 151, 151, 146, 142, 132, 132, 121 132, 137, 137, 146, 144, 135, 130, 125 112, 130, 125, 119, 137, 123, 137, 121 144, 135, 135, 130, 130, 128, 159, 137 130, 121, 132, 137, 114, 128, 104, 119 121, 108, 121, 104, 123, 123, 114, 108 106, 135, 125, 123, 110, 98, 121, 121 110, 117, 110, 98, 88, 94, 94, 108 102, 86, 114, 106, 102, 92, 114, 114 106, 123, 98, 110, 104, 100, 110, 102 121, 106, 106, 88, 96, 104, 102, 112 104, 94, 384, 106, 102, 125, 90, 86 98, 106, 92, 94, 100, 98, 96, 90 106, 90, 102, 112, 119, 83, 112, 86 88, 77, 88, 112, 108, 110, 106, 135 83, 102, 81, 123, 106, 79, 125, 76 72, 100, 100, 94, 81, 114, 106, 106 94, 86, 117, 102, 94, 108, 90, 106 86, 128, 90, 121, 100, 106, 110, 123 102, 106, 121, 114, 108, 102, 110, 102 112, 110, 139, 102, 112, 128, 110, 108 100, 121, 102, 137, 130, 130, 112, 123 119, 119, 125, 106, 144, 110, 128, 112 137, 130, 130, 149, 114, 159, 146, 139 156, 146, 159, 159, 174, 193, 231, 213 207, 269, 276, 303, 296, 376, 416, 445 467, 534, 497, 454, 428, 339, 324, 299 350, 306, 292, 253, 213, 196, 177, 154 156, 139, 137, 117, 139, 119, 119, 117 121, 128, 128, 121, 117, 128, 125, 137 112, 121, 130, 135, 137, 144, 130, 128 112, 130, 121, 130, 128, 114, 137, 123 139, 132, 137, 151, 139, 123, 149, 144 159, 154, 130, 149, 142, 139, 164, 164 146, 166, 169, 164, 166, 177, 166, 172 185, 213, 177, 196, 196, 213, 193, 228 222, 228, 240, 246, 216, 228, 204, 231 207, 234, 228, 228, 210, 222, 243, 199 204, 193, 182, 190, 225, 196, 185, 164 190, 172, 182, 169, 159, 180, 159, 169 164, 159, 177, 149, 149, 137, 144, 146 151, 132, 137, 137, 146, 137, 123, 139 121, 137, 137, 119, 137, 114, 130, 135 125, 112, 117, 108, 106, 121, 110, 114 88, 102, 106, 96, 100, 106, 90, 106 100, 98, 98, 81, 98, 106, 100, 100 90, 110, 108, 119, 100, 98, 96, 100 98, 98, 86, 110, 92, 114, 117, 110 108, 104, 108, 123, 117, 102, 110, 102 117, 117, 123, 128, 123, 149, 149, 114 125, 125, 149, 139, 139, 130, 146, 169 156, 135, 185, 154, 177, 156, 180, 164 139, 132, 132, 135, 135, 123, 135, 106 110, 88, 110, 104, 112, 90, 94, 123 110, 86, 79, 85, 94, 86, 98, 83 85, 85, 96, 90, 86, 86, 100, 88 83, 90, 102, 112, 100, 117, 86, 90 144, 102, 128, 106, 108, 132, 128, 123 96, 123, 123, 117, 125, 121, 121, 98 110, 104, 121, 114, 108, 123, 108, 119 102, 104, 108, 104, 104, 98, 98, 128 110, 121, 119, 104, 106, 104, 123, 112 106, 102, 106, 112, 132, 94, 117, 139 108, 121, 108, 114, 98, 100, 121, 104 121, 112, 102, 121, 117, 98, 108, 119 117, 117, 98, 96, 88, 90, 108, 110 100, 125, 106, 86, 77, 96, 85, 90 88, 77, 88, 100, 94, 77, 98, 96 85, 88, 83, 92, 100, 92, 104, 92 100, 106, 102, 88, 94, 90, 85, 98 106, 94, 92, 114, 110, 110, 117, 112 114, 121, 121, 144, 121, 114, 123, 100 132, 125, 106, 125, 119, 114, 112, 137 144, 123, 139, 182, 193, 185, 172, 174 213, 213, 276, 259, 306, 328, 328, 335 310, 292, 243, 256, 253, 228, 246, 243 279, 262, 276, 289, 313, 320, 353, 380 412, 424, 458, 480, 524, 506, 497, 471 424, 441, 380, 384, 369, 392, 369, 376 310, 256, 234, 243, 199, 188, 172, 177 156, 135, 117, 121, 130, 108, 86, 119 135, 114, 128, 119, 137, 137, 114, 102 125, 130, 135, 123, 123, 114, 104, 123 123, 123, 117, 132, 119, 135, 125, 110 128, 137, 130, 112, 159, 121, 164, 119 137, 135, 161, 164, 142, 132, 139, 154 135, 130, 142, 154, 128, 142, 142, 137 135, 137, 130, 130, 135, 123, 130, 119 128, 144, 137, 121, 132, 110, 137, 135 137,/