SampleIdent,909C 7R-1 48-49BULK,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 4-sep-1993 4:19,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 86, 92, 96, 100, 86, 94, 92, 79 85, 83, 106, 81, 76, 96, 94, 92 94, 100, 90, 98, 94, 100, 83, 98 88, 69, 98, 81, 79, 81, 94, 100 104, 71, 102, 98, 96, 90, 112, 104 85, 86, 112, 100, 85, 86, 96, 104 90, 102, 123, 102, 106, 92, 86, 114 96, 92, 110, 106, 112, 100, 102, 104 114, 98, 130, 100, 128, 104, 128, 112 114, 112, 117, 123, 114, 100, 106, 100 117, 94, 104, 121, 121, 86, 98, 106 102, 106, 114, 110, 100, 117, 104, 106 81, 94, 106, 144, 108, 108, 135, 121 102, 108, 123, 108, 123, 125, 98, 106 114, 110, 102, 92, 114, 100, 92, 117 100, 94, 96, 119, 121, 108, 100, 100 106, 102, 121, 121, 94, 100, 102, 114 90, 100, 106, 108, 102, 110, 114, 100 100, 110, 94, 108, 117, 106, 110, 110 104, 104, 94, 98, 119, 128, 125, 108 104, 100, 114, 108, 119, 98, 102, 92 98, 112, 117, 104, 100, 106, 110, 130 130, 130, 130, 128, 130, 137, 139, 132 132, 135, 119, 117, 125, 125, 114, 130 130, 110, 121, 98, 119, 123, 100, 125 90, 108, 119, 106, 92, 104, 114, 94 96, 92, 83, 102, 104, 100, 92, 102 92, 92, 96, 92, 108, 108, 104, 102 94, 88, 85, 90, 94, 100, 98, 88 94, 98, 104, 92, 106, 102, 102, 83 100, 100, 104, 88, 96, 117, 90, 85 96, 96, 98, 108, 117, 108, 88, 92 94, 96, 96, 112, 117, 88, 102, 76 85, 88, 94, 83, 100, 106, 98, 96 100, 98, 88, 102, 76, 85, 85, 79 83, 108, 100, 96, 104, 98, 77, 85 85, 94, 96, 94, 85, 85, 92, 112 85, 96, 94, 81, 86, 85, 79, 88 79, 96, 90, 90, 83, 71, 110, 77 98, 81, 85, 88, 74, 96, 88, 100 86, 79, 90, 90, 74, 98, 86, 83 102, 86, 88, 86, 85, 88, 100, 76 79, 100, 98, 106, 83, 88, 96, 92 104, 96, 85, 85, 114, 104, 92, 96 110, 88, 96, 106, 102, 112, 125, 117 104, 119, 117, 128, 110, 132, 114, 135 128, 112, 123, 154, 117, 128, 125, 104 119, 117, 100, 112, 108, 106, 83, 72 90, 83, 92, 83, 77, 76, 88, 83 85, 90, 92, 88, 74, 81, 96, 96 74, 74, 90, 76, 79, 69, 90, 85 71, 85, 83, 77, 74, 76, 86, 81 76, 69, 77, 96, 86, 69, 81, 85 92, 85, 88, 67, 74, 96, 88, 86 92, 77, 71, 85, 79, 72, 71, 81 85, 76, 79, 90, 79, 69, 81, 81 81, 76, 94, 85, 69, 76, 77, 67 90, 85, 77, 88, 77, 79, 72, 85 81, 59, 85, 83, 96, 62, 69, 66 88, 66, 76, 85, 71, 79, 72, 83 72, 66, 81, 85, 72, 66, 76, 69 72, 94, 67, 86, 77, 67, 71, 83 59, 64, 77, 77, 79, 74, 86, 76 74, 71, 74, 88, 56, 85, 59, 85 76, 66, 88, 62, 76, 85, 79, 67 76, 79, 72, 77, 76, 104, 67, 77 81, 71, 83, 92, 81, 71, 77, 56 76, 85, 77, 74, 79, 77, 72, 66 77, 71, 59, 62, 77, 76, 61, 64 64, 76, 72, 62, 58, 72, 71, 66 62, 71, 72, 77, 72, 76, 77, 72 64, 67, 71, 72, 77, 76, 71, 85 71, 62, 72, 58, 76, 67, 72, 62 59, 66, 71, 71, 67, 71, 61, 76 59, 81, 79, 67, 74, 76, 92, 76 71, 72, 76, 76, 88, 72, 66, 66 66, 71, 61, 79, 86, 85, 94, 66 79, 61, 83, 64, 85, 92, 86, 92 72, 85, 79, 90, 85, 79, 85, 88 79, 94, 86, 85, 88, 71, 88, 94 102, 90, 98, 85, 88, 71, 90, 64 72, 67, 67, 76, 85, 74, 55, 71 76, 85, 92, 79, 72, 83, 66, 104 67, 71, 76, 79, 79, 76, 69, 79 72, 76, 67, 64, 59, 74, 62, 88 77, 74, 76, 86, 69, 76, 79, 79 88, 83, 96, 86, 85, 67, 88, 85 72, 72, 92, 64, 71, 81, 56, 83 77, 64, 71, 77, 69, 86, 90, 77 85, 71, 71, 85, 83, 92, 83, 90 76, 92, 88, 104, 98, 100, 117, 100 121, 114, 110, 108, 144, 137, 128, 114 137, 144, 125, 161, 151, 125, 149, 132 121, 125, 112, 106, 110, 121, 96, 130 110, 94, 85, 92, 108, 94, 102, 117 94, 92, 106, 88, 90, 112, 85, 396 79, 90, 108, 108, 112, 94, 90, 79 100, 108, 86, 106, 110, 125, 114, 154 144, 164, 164, 149, 156, 190, 188, 185 196, 156, 174, 182, 139, 149, 123, 114 98, 104, 86, 77, 83, 90, 79, 86 86, 94, 55, 85, 94, 88, 88, 77 71, 72, 76, 62, 71, 56, 64, 79 76, 92, 79, 86, 90, 74, 79, 90 88, 81, 83, 81, 76, 77, 100, 83 81, 100, 86, 86, 83, 96, 81, 83 98, 85, 85, 90, 102, 90, 79, 76 72, 98, 67, 74, 77, 77, 79, 83 77, 79, 90, 79, 71, 72, 86, 66 104, 86, 83, 79, 83, 67, 72, 69 71, 77, 77, 79, 79, 92, 90, 90 81, 77, 83, 77, 79, 72, 71, 77 85, 92, 88, 100, 66, 88, 92, 83 85, 92, 81, 71, 64, 64, 76, 88 86, 85, 94, 92, 85, 85, 94, 96 102, 90, 86, 102, 98, 100, 94, 81 94, 104, 102, 100, 88, 90, 79, 79 96, 88, 102, 88, 94, 85, 90, 104 98, 98, 96, 77, 94, 90, 100, 119 100, 112, 110, 108, 104, 117, 114, 112 146, 121, 128, 135, 132, 123, 149, 121 130, 139, 135, 161, 149, 188, 174, 182 177, 172, 193, 228, 210, 228, 228, 243 228, 222, 199, 190, 161, 172, 154, 154 135, 137, 128, 154, 121, 142, 137, 114 132, 114, 149, 117, 137, 123, 144, 159 151, 139, 132, 154, 130, 139, 154, 125 121, 106, 106, 114, 112, 128, 123, 100 110, 100, 112, 100, 112, 117, 98, 108 110, 102, 76, 94, 100, 100, 88, 102 94, 90, 83, 90, 96, 85, 83, 108 90, 81, 96, 92, 90, 96, 104, 96 104, 98, 96, 102, 108, 86, 114, 112 161, 121, 154, 190, 207, 228, 292, 369 433, 506, 534, 506, 640, 640, 666, 708 790, 756, 756, 708, 666, 581, 520, 480 353, 286, 253, 213, 207, 177, 169, 182 174, 164, 149, 161, 121, 139, 128, 119 104, 106, 112, 110, 123, 100, 121, 108 110, 125, 132, 117, 135, 114, 100, 119 130, 149, 144, 146, 137, 121, 128, 128 146, 121, 132, 144, 125, 149, 132, 144 135, 144, 142, 159, 159, 174, 149, 149 164, 146, 139, 139, 161, 139, 137, 119 108, 104, 121, 100, 102, 92, 104, 114 92, 92, 92, 106, 94, 96, 86, 98 104, 86, 77, 92, 76, 98, 79, 77 79, 81, 76, 72, 79, 76, 72, 76 81, 71, 52, 85, 85, 88, 77, 79 96, 69, 67, 67, 71, 92, 96, 66 85, 72, 72, 67, 85, 66, 66, 83 83, 56, 90, 79, 88, 79, 79, 76 92, 79, 86, 62, 79, 96, 83, 94 88, 81, 79, 77, 88, 76, 94, 76 96, 117, 85, 102, 102, 106, 102, 106 106, 108, 106, 100, 88, 110, 90, 98 90, 96, 92, 79, 86, 110, 83, 94 85, 104, 96, 88, 86, 98, 92, 96 86, 112, 92, 106, 110, 94, 117, 108 88, 90, 112, 110, 96, 110, 104, 119 121, 117, 139, 123, 108, 132, 119, 154 149, 169, 172, 190, 202, 180, 185, 202 182, 193, 207, 172, 193, 202, 210, 210 225, 185, 216, 216, 196, 237, 196, 237 222, 225, 210, 225, 202, 231, 225, 237 231, 231, 253, 269, 253, 250, 256, 250 279, 339, 339, 380, 408, 420, 454, 484 534, 630, 595, 640, 676, 686, 645, 745 756, 713, 740, 666, 610, 502, 493, 361 396, 286, 250, 216, 196, 190, 154, 149 149, 144, 121, 114, 104, 92, 130, 104 88, 102, 110, 90, 98, 77, 83, 85 76, 77, 98, 86, 79, 92, 79, 83 74, 92, 74, 76, 71, 88, 86, 85 76, 94, 69, 77, 79, 77, 64, 76 85, 71, 79, 66, 74, 86, 81, 79 77, 74, 59, 76, 72, 79, 66, 76 77, 53, 85, 49, 76, 66, 55, 72 76, 79, 346, 67, 66, 72, 81, 61 62, 72, 71, 67, 77, 81, 62, 72 71, 72, 56, 85, 81, 71, 85, 88 77, 72, 76, 81, 77, 77, 69, 77 77, 86, 66, 92, 79, 81, 77, 96 96, 104, 94, 108, 119, 108, 117, 144 123, 117, 130, 130, 132, 128, 135, 128 119, 144, 144, 139, 142, 149, 154, 159 164, 188, 146, 177, 154, 180, 159, 159 207, 166, 149, 135, 164, 151, 130, 135 149, 119, 108, 121, 119, 112, 114, 96 92, 96, 94, 98, 98, 88, 96, 92 92, 90, 92, 94, 96, 77, 86, 86 88, 85, 79, 67, 88, 77, 85, 85 85, 71, 88, 86, 76, 86, 86, 86 76, 104, 86, 92, 76, 79, 69, 88 112, 83, 77, 77, 88, 96, 94, 96 76, 90, 100, 77, 77, 96, 98, 108 96, 110, 130, 135, 125, 169, 135, 139 172, 164, 161, 130, 149, 146, 135, 108 130, 104, 98, 100, 98, 94, 94, 90 102, 90, 94, 92, 92, 96, 102, 85 85, 90, 85, 86, 86, 96, 98, 88 94, 119, 88, 94, 98, 102, 110, 98 104, 125, 104, 108, 117, 108, 112, 121 114, 114, 137, 123, 132, 128, 159, 132 132, 130, 119, 137, 149, 130, 154, 125 139, 121, 117, 121, 117, 128, 117, 137 139, 128, 130, 137, 161, 174, 182, 188 196, 210, 199, 188, 196, 193, 164, 193 182, 151, 161, 139, 128, 135, 117, 119 110, 96, 96, 88, 100, 79, 72, 85 76, 72, 81, 77, 79, 77, 90, 59 72, 67, 66, 81, 62, 71, 66, 67 64, 90, 52, 76, 69, 46, 49, 72 55, 88, 62, 77, 66, 76, 76, 81 94, 88, 102, 102, 104, 112, 121, 112 119, 128, 123, 119, 121, 117, 121, 137 104, 83, 104, 77, 104, 81, 79, 72 62, 67, 76, 86, 76, 64, 71, 74 64, 62, 86, 83, 79, 94, 69, 79 94, 79, 90, 98, 92, 96, 102, 92 90, 96, 83, 98, 98, 102, 83, 96 79, 94, 86, 79, 61, 66, 71, 61 71, 83, 55, 64, 74, 72, 62, 71 72, 71, 71, 67, 79, 71, 64, 83 94, 85, 81, 98, 79, 85, 85, 88 79, 76, 92, 96, 76, 98, 108, 108 100, 92, 98, 92, 104, 90, 83, 94 102, 96, 90, 85, 94, 92, 86, 88 88, 96, 92, 94, 102, 106, 98, 96 86, 132, 108, 130, 132, 114, 88, 121 102, 139, 121, 128, 135, 142, 151, 132 172, 154, 188, 164, 204, 196, 219, 225 240, 216, 250, 237, 262, 225, 231, 219 237, 196, 202, 462, 199, 177, 154, 169 169, 156, 154, 139, 149, 130, 98, 100 106, 102, 100, 86, 94, 62, 71, 85 66, 85, 71, 72, 72, 66, 55, 71 72, 59, 76, 67, 67, 64, 53, 76 74, 59, 262, 79, 74, 52, 62, 76 66, 62, 53, 66, 77, 48, 58, 59 64, 72, 71, 56, 56, 66, 55, 55 53, 67, 74, 50, 77, 56, 64, 76 71, 58, 77, 83, 69, 74, 98, 72 83, 81, 88, 74, 79, 71, 88, 69 72, 90, 76, 59, 76, 64, 72, 69 62, 83, 66, 72, 62, 56, 67, 62 83, 83, 83, 114, 102, 106, 121, 106 110, 135, 132, 121, 117, 108, 119, 90 123, 100, 108, 86, 90, 92, 92, 96 83, 94, 102, 92, 110, 104, 94, 96 121, 110, 104, 106, 110, 123, 130, 110 132, 137, 144, 128, 128, 123, 146, 149 154, 156, 149, 146, 172, 164, 164, 161 139, 154, 149, 154, 174, 144, 149, 149 166, 159, 169, 149, 169, 169, 193, 177 188, 185, 196, 202, 196, 213, 202, 222 182, 222, 213, 222, 210, 180, 193, 177 159, 130, 166, 137, 121, 108, 100, 119 90, 71, 79, 92, 67, 77, 88, 83 77, 62, 90, 69, 74, 61, 77, 58 50, 76, 72, 58, 72, 67, 50, 62 72, 72, 56, 56, 72, 61, 71, 71 69, 61, 56, 67, 58, 66, 67, 62 50, 67, 67, 62, 61, 59, 49, 69 58, 64, 61, 56, 61, 53, 62, 50 44, 59, 61, 59, 62, 50, 42, 64 46, 59, 59, 56, 45, 48, 53, 56 44, 52, 44, 62, 56, 53, 52, 42 53, 71, 77, 69, 59, 71, 67, 67 77, 45, 59, 62, 79, 66, 64, 67 59, 67, 67, 58, 62, 50, 61, 59 62, 48, 58, 62, 62, 64, 67, 53 58, 66, 59, 306, 58, 44, 50, 59 58, 58, 58, 52, 71, 50, 58, 59 44, 56, 62, 59, 52, 50, 61, 76 66, 56, 67, 56, 56, 56, 58, 67 62, 61, 64, 76, 67, 59, 66, 69 59, 67, 72, 71, 71, 81, 50, 62 71, 83, 83, 58, 85, 76, 67, 74 67, 77, 77, 67, 79, 74, 81, 96 106, 85, 114, 81, 104, 104, 121, 135 149, 164, 188, 177, 174, 219, 199, 207 231, 231, 225, 202, 188, 159, 185, 156 151, 149, 149, 128, 137, 137, 144, 130 135, 130, 169, 135, 132, 137, 180, 161 154, 164, 144, 159, 149, 159, 137, 139 132, 125, 132, 114, 119, 130, 117, 123 96, 117, 108, 121, 112, 106, 117, 130 108, 110, 81, 104, 125, 96, 104, 83 110, 106, 88, 88, 100, 96, 106, 104 104, 106, 112, 102, 112, 100, 92, 128 112, 110, 106, 292, 135, 104, 119, 94 102, 110, 106, 96, 88, 121, 110, 121 119, 112, 112, 108, 125, 121, 119, 119 142, 146, 139, 135, 169, 164, 177, 199 188, 177, 202, 213, 210, 228, 237, 210 256, 286, 276, 303, 262, 335, 292, 339 313, 303, 365, 303, 346, 296, 299, 331 286, 289, 286, 259, 259, 222, 216, 222 177, 193, 166, 142, 154, 121, 130, 117 86, 121, 137, 90, 94, 85, 100, 88 90, 102, 76, 100, 76, 85, 90, 85 76, 85, 77, 88, 77, 86, 72, 85 72, 77, 77, 81, 81, 62, 79, 71 76, 64, 77, 79, 86, 85, 86, 88 76, 71, 94, 81, 85, 77, 85, 72 69, 62, 83, 92, 76, 85, 77, 74 83, 72, 83, 72, 76, 96, 77, 79 92, 72, 81, 81, 86, 79, 92, 69 83, 69, 81, 86, 81, 64, 76, 83 94, 76, 79, 90, 72, 96, 117, 96 106, 102, 121, 121, 132, 128, 112, 125 135, 137, 117, 132, 112, 104, 106, 90 98, 96, 102, 98, 106, 102, 88, 88 104, 110, 104, 100, 90, 110, 74, 96 96, 132, 86, 100, 96, 86, 104, 102 92, 90, 79, 98, 86, 108, 92, 90 92, 98, 81, 102, 86, 79, 72, 94 85, 88, 96, 72, 88, 79, 85, 86 77, 67, 71, 66, 90, 62, 69, 76 62, 83, 86, 90, 83, 72, 83, 71 76, 85, 88, 76, 81, 81, 90, 90 81, 76, 79, 72, 71, 92, 74, 72 83, 83, 66, 66, 59, 83, 61, 66 59, 59, 64, 71, 66, 52, 76, 48 66, 59, 61, 79, 55, 52, 67, 76 72, 72, 52, 62, 50, 79, 59, 59 66, 66, 71, 66, 46, 77, 76, 53 67, 52, 61, 79, 59, 52, 56, 50 62, 71, 59, 49, 50, 64, 56, 66 64, 66, 52, 53, 53, 50, 48, 67 64, 48, 53, 66, 48, 59, 56, 59 55, 62, 55, 56, 53, 53, 56, 58 49, 61, 42, 62, 53, 44, 64, 59 52, 56, 62, 56, 71, 66, 66, 66 58, 61, 66, 67, 59, 67, 79, 53 81, 72, 61, 77, 49, 62, 77, 77 79, 71, 83, 67, 83, 67, 76, 66 96, 86, 72, 67, 79, 79, 100, 69 66, 77, 77, 72, 66, 76, 85, 67 90, 88, 77, 88, 79, 100, 94, 79 90, 88, 98, 83, 94, 98, 98, 114 135, 146, 146, 149, 161, 164, 159, 185 210, 199, 202, 207, 228, 225, 210, 188 182, 169, 169, 166, 159, 149, 177, 130 137, 123, 114, 117, 130, 114, 108, 102 77, 104, 88, 96, 112, 88, 114, 81 94, 98, 85, 98, 85, 112, 102, 92 108, 114, 104, 94, 98, 106, 100, 110 106, 106, 96, 104, 117, 104, 104, 112 130, 121, 128, 137, 125, 137, 169, 174 169, 185, 172, 177, 204, 207, 182, 196 188, 161, 204, 207, 207, 177, 196, 166 185, 199, 180, 190, 137, 166, 132, 151 159, 142, 135, 146, 128, 146, 139, 142 137, 123, 132, 106, 110, 117, 128, 121 135, 121, 104, 121, 94, 112, 117, 96 98, 90, 98, 114, 98, 104, 94, 85 92, 72, 94, 92, 86, 90, 88, 86 86, 92, 81, 85, 100, 79, 77, 77 67, 77, 77, 76, 67, 72, 58, 67 66, 72, 71, 76, 67, 72, 66, 85 64, 72, 58, 66, 71, 50, 67, 72 61, 79, 55, 61, 79, 66, 62, 74 83, 72, 56, 77, 61, 72, 81, 66 72, 76, 83, 76, 77, 77, 81, 67 72, 71, 69, 76, 83, 66, 71, 94 83, 74, 96, 86, 88, 81, 85, 98 88, 96, 102, 88, 90, 92, 121, 102 112, 102, 86, 92, 88, 85, 94, 85 88, 92, 96, 88, 92, 88, 86, 86 81, 77, 83, 88, 79, 98, 85, 98 88, 64, 83, 83, 92, 79, 85, 90 98, 102, 90, 119, 100, 102, 90, 98 100, 108, 102, 104, 123, 114, 128, 110 130, 132, 121, 130, 142, 128, 119, 121 135, 144, 135, 144, 156, 112, 117, 137 117, 110, 104, 94, 106, 102, 98, 100 92, 85, 94, 79, 92, 74, 67, 85 90, 79, 106, 85, 77, 74, 85, 76 92, 90, 85, 77, 71, 81, 71, 79 79, 85, 71, 85, 56, 92, 83, 86 88, 85, 83, 88, 83, 71, 74, 64 77, 72, 76, 64, 69, 74, 88, 79 110, 66, 88, 100, 94, 71, 98, 106 96, 86, 81, 81, 92, 94, 98, 88 85, 85, 90, 81, 85, 88, 85, 81 85, 83, 71, 88, 81, 90, 56, 83 76, 85, 92, 81, 79, 90, 98, 79 92, 92, 85, 102, 102, 102, 102, 98 90, 108, 108, 102, 102, 98, 112, 117 128, 121, 142, 142, 135, 144, 121, 185 169, 180, 185, 149, 172, 149, 137, 128 149, 146, 159, 149, 151, 180, 156, 139 169, 180, 164, 177, 180, 190, 174, 185 219, 172, 172, 159, 190, 166, 202, 154 159, 154, 135, 130, 121, 135, 125, 112 90, 112, 102, 96, 98, 102, 79, 94 106, 83, 92, 86, 81, 110, 108, 94 112, 123, 324, 121, 125, 135, 137, 149 142, 142, 156, 142, 142, 156, 159, 137 137, 159, 144, 132, 121, 130, 128, 112 108, 125, 130, 117, 119, 108, 94, 112 108, 106, 79, 94, 92, 86, 92, 94 94, 85, 83, 90, 85, 85, 74, 85 71, 62, 72, 88, 88, 55, 76, 58 90,/