SampleIdent,909C 8R-3 4-5 BULK,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 4-sep-1993 6:10,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 92, 92, 88, 71, 85, 86, 77, 98 108, 110, 90, 119, 92, 104, 114, 86 102, 86, 106, 100, 98, 85, 90, 108 108, 92, 110, 114, 96, 100, 94, 98 106, 98, 96, 96, 92, 104, 98, 90 86, 119, 98, 102, 110, 96, 104, 121 117, 112, 112, 100, 96, 100, 114, 132 119, 125, 117, 123, 130, 98, 114, 123 128, 117, 112, 112, 123, 106, 108, 110 110, 117, 121, 130, 106, 112, 112, 123 125, 137, 119, 130, 123, 108, 119, 125 119, 117, 137, 110, 114, 119, 121, 110 112, 119, 117, 100, 117, 125, 106, 96 139, 117, 125, 121, 117, 110, 110, 128 114, 128, 119, 119, 117, 139, 137, 119 130, 100, 98, 100, 117, 128, 135, 106 121, 128, 112, 151, 112, 110, 146, 142 119, 114, 121, 139, 130, 121, 128, 137 125, 125, 128, 130, 112, 108, 130, 123 104, 121, 110, 146, 114, 112, 119, 130 132, 130, 123, 121, 137, 128, 139, 135 121, 128, 149, 128, 149, 130, 125, 117 135, 149, 149, 146, 151, 156, 169, 166 154, 172, 172, 151, 149, 144, 172, 146 137, 132, 125, 119, 132, 123, 121, 125 123, 123, 123, 110, 114, 121, 121, 121 112, 104, 108, 123, 121, 112, 114, 98 108, 108, 106, 114, 86, 102, 106, 88 106, 114, 110, 98, 86, 112, 92, 108 106, 104, 112, 112, 119, 114, 92, 102 102, 104, 104, 114, 98, 98, 112, 119 102, 100, 106, 112, 92, 90, 92, 96 100, 104, 96, 110, 96, 117, 108, 90 96, 94, 96, 96, 92, 121, 90, 92 98, 100, 104, 94, 92, 96, 96, 108 102, 123, 94, 102, 81, 90, 83, 96 110, 90, 117, 85, 114, 104, 100, 92 83, 90, 90, 98, 100, 86, 94, 86 108, 100, 100, 88, 266, 90, 94, 85 79, 85, 104, 96, 92, 98, 250, 83 90, 90, 94, 100, 76, 106, 104, 72 90, 76, 92, 110, 94, 90, 92, 98 98, 108, 85, 102, 96, 104, 110, 114 98, 100, 92, 121, 106, 104, 92, 119 130, 114, 119, 130, 132, 114, 149, 130 151, 166, 130, 149, 182, 177, 154, 188 193, 190, 164, 182, 151, 159, 180, 154 112, 128, 114, 100, 98, 110, 110, 100 90, 83, 100, 100, 94, 90, 72, 112 100, 81, 90, 92, 98, 77, 94, 79 72, 92, 96, 110, 100, 86, 86, 79 94, 77, 98, 88, 98, 67, 94, 90 86, 83, 100, 88, 85, 92, 96, 98 85, 98, 85, 90, 90, 85, 94, 94 96, 71, 86, 98, 88, 100, 88, 85 77, 85, 92, 88, 98, 76, 79, 72 96, 114, 88, 92, 66, 85, 79, 92 104, 76, 76, 79, 85, 71, 85, 86 85, 85, 76, 61, 88, 67, 77, 88 83, 79, 85, 96, 77, 88, 88, 81 98, 74, 72, 90, 72, 88, 77, 85 83, 96, 81, 85, 83, 85, 77, 90 74, 77, 96, 88, 86, 79, 88, 85 77, 74, 88, 76, 79, 76, 79, 79 64, 79, 79, 67, 88, 83, 72, 102 71, 71, 94, 71, 86, 76, 71, 83 102, 88, 61, 72, 86, 77, 92, 83 76, 66, 77, 79, 85, 85, 71, 81 83, 88, 72, 67, 74, 77, 90, 71 72, 71, 81, 74, 81, 69, 83, 64 79, 86, 76, 81, 86, 74, 79, 86 77, 79, 81, 83, 72, 85, 79, 71 79, 79, 83, 71, 77, 88, 76, 74 69, 104, 85, 74, 67, 92, 77, 72 76, 88, 76, 77, 90, 98, 72, 76 76, 90, 69, 94, 72, 96, 76, 85 86, 85, 72, 81, 92, 81, 83, 76 92, 74, 100, 85, 94, 100, 96, 81 88, 100, 102, 104, 104, 98, 102, 83 117, 125, 110, 106, 117, 102, 119, 104 106, 96, 100, 85, 83, 94, 83, 88 72, 88, 86, 74, 79, 83, 94, 86 88, 77, 90, 79, 90, 88, 85, 86 85, 86, 88, 86, 79, 86, 106, 77 92, 92, 72, 110, 86, 79, 96, 86 94, 96, 106, 106, 130, 123, 128, 104 90, 94, 110, 90, 96, 92, 88, 102 104, 85, 96, 88, 90, 92, 100, 83 108, 100, 90, 112, 85, 92, 77, 104 102, 117, 110, 88, 96, 106, 104, 132 154, 123, 132, 149, 144, 177, 146, 177 196, 174, 193, 182, 188, 207, 199, 196 199, 240, 193, 207, 185, 199, 199, 172 166, 174, 151, 149, 164, 123, 161, 137 123, 132, 151, 144, 121, 357, 139, 135 135, 125, 114, 119, 117, 137, 128, 108 119, 139, 132, 121, 125, 112, 135, 132 156, 135, 169, 210, 216, 279, 320, 335 324, 328, 328, 369, 416, 433, 420, 408 404, 335, 331, 225, 185, 180, 137, 119 117, 110, 123, 108, 108, 119, 110, 98 104, 106, 117, 106, 110, 125, 128, 92 104, 90, 96, 106, 98, 121, 110, 104 117, 108, 106, 110, 108, 90, 108, 123 72, 119, 119, 96, 123, 100, 149, 112 121, 146, 151, 154, 174, 164, 166, 164 182, 151, 159, 139, 146, 142, 121, 102 112, 112, 92, 88, 100, 125, 121, 128 106, 117, 108, 106, 112, 108, 100, 104 108, 108, 117, 125, 90, 106, 98, 125 119, 110, 130, 106, 117, 121, 110, 114 110, 137, 130, 130, 125, 142, 114, 144 149, 119, 121, 137, 119, 137, 106, 125 119, 90, 96, 121, 92, 102, 110, 98 117, 128, 137, 125, 135, 177, 182, 180 219, 177, 177, 216, 193, 193, 169, 180 159, 137, 149, 151, 159, 130, 130, 112 151, 132, 123, 125, 114, 130, 135, 149 144, 128, 137, 137, 130, 199, 196, 193 196, 213, 207, 219, 207, 202, 213, 193 174, 196, 193, 196, 156, 164, 156, 128 149, 110, 137, 123, 121, 114, 121, 130 117, 130, 130, 144, 125, 130, 119, 137 156, 139, 164, 142, 180, 139, 177, 159 177, 156, 169, 166, 164, 185, 199, 182 190, 207, 207, 240, 240, 253, 228, 231 231, 246, 204, 228, 202, 196, 216, 190 180, 207, 193, 172, 202, 182, 199, 164 182, 172, 185, 196, 161, 139, 159, 146 146, 121, 125, 135, 151, 123, 144, 128 128, 121, 137, 119, 139, 130, 146, 139 151, 169, 132, 172, 132, 144, 164, 166 166, 182, 196, 169, 216, 222, 240, 286 313, 384, 467, 506, 645, 870, 1260, 1568 1608, 1706, 1989, 2181, 2256, 2294, 2304, 2275 2162, 1945, 1849, 1640, 1354, 992, 795, 681 524, 388, 339, 342, 292, 317, 276, 216 253, 216, 243, 228, 199, 193, 185, 207 193, 169, 177, 182, 185, 177, 177, 180 172, 204, 174, 196, 228, 199, 222, 225 213, 243, 246, 266, 266, 222, 282, 250 240, 256, 272, 306, 289, 289, 317, 369 357, 372, 428, 552, 471, 416, 475, 428 408, 380, 350, 357, 324, 328, 282, 276 234, 193, 193, 174, 193, 196, 219, 269 289, 313, 303, 256, 210, 202, 169, 137 135, 144, 156, 142, 119, 121, 132, 112 102, 110, 117, 121, 121, 102, 88, 106 117, 96, 121, 100, 94, 92, 104, 106 104, 98, 108, 94, 106, 102, 108, 94 79, 112, 121, 94, 104, 121, 100, 92 100, 104, 106, 102, 102, 106, 102, 104 102, 108, 110, 98, 121, 119, 117, 130 110, 130, 106, 94, 132, 123, 135, 130 130, 144, 156, 159, 161, 154, 188, 144 188, 185, 169, 169, 169, 164, 154, 142 154, 137, 151, 135, 166, 154, 146, 125 130, 142, 114, 132, 123, 123, 144, 166 137, 146, 164, 123, 125, 151, 144, 137 139, 137, 137, 130, 119, 94, 112, 100 94, 117, 114, 108, 104, 119, 114, 110 119, 121, 132, 104, 125, 123, 112, 123 112, 121, 130, 108, 130, 123, 137, 182 121, 128, 121, 128, 149, 117, 137, 137 123, 130, 125, 135, 139, 123, 142, 123 123, 139, 125, 137, 135, 154, 139, 156 159, 156, 139, 156, 151, 166, 164, 164 159, 161, 144, 137, 125, 144, 121, 130 117, 121, 117, 125, 121, 92, 102, 102 102, 104, 112, 94, 117, 108, 102, 98 104, 88, 98, 108, 98, 83, 72, 72 86, 77, 74, 76, 83, 66, 76, 76 79, 71, 72, 77, 86, 79, 67, 72 72, 79, 77, 76, 64, 74, 66, 55 79, 72, 90, 83, 79, 76, 72, 81 92, 96, 72, 76, 98, 76, 81, 96 85, 85, 66, 71, 90, 71, 76, 94 76, 90, 79, 98, 102, 88, 85, 83 92, 104, 88, 102, 90, 79, 117, 90 94, 79, 104, 92, 72, 86, 106, 96 112, 108, 102, 104, 96, 106, 112, 102 112, 100, 125, 98, 85, 110, 121, 123 123, 110, 114, 123, 135, 137, 144, 154 172, 159, 177, 177, 196, 188, 190, 188 225, 213, 182, 210, 210, 202, 222, 240 234, 225, 216, 231, 250, 237, 262, 259 253, 262, 276, 240, 246, 279, 262, 317 279, 246, 279, 246, 243, 243, 253, 207 231, 225, 204, 207, 190, 172, 188, 166 151, 164, 151, 169, 174, 154, 149, 142 159, 154, 117, 144, 121, 139, 130, 130 128, 123, 139, 146, 137, 159, 139, 135 132, 142, 130, 119, 121, 123, 132, 135 128, 137, 146, 137, 146, 139, 130, 112 146, 154, 137, 128, 128, 137, 142, 112 135, 144, 144, 154, 164, 196, 177, 199 207, 272, 282, 313, 342, 357, 365, 361 339, 303, 331, 286, 272, 240, 225, 172 169, 182, 169, 146, 149, 142, 146, 135 121, 137, 146, 159, 161, 149, 142, 154 146, 132, 166, 125, 146, 123, 146, 132 149, 137, 135, 144, 154, 137, 169, 164 174, 182, 146, 159, 161, 169, 154, 185 159, 182, 174, 185, 182, 177, 172, 159 180, 146, 144, 144, 154, 164, 144, 154 146, 142, 151, 132, 135, 100, 121, 108 119, 114, 114, 94, 106, 100, 110, 117 117, 100, 125, 100, 119, 132, 117, 119 108, 135, 117, 121, 121, 130, 130, 119 123, 98, 121, 117, 110, 96, 96, 108 110, 106, 96, 112, 85, 86, 106, 86 86, 98, 117, 100, 94, 100, 114, 88 94, 104, 94, 106, 88, 100, 86, 86 104, 94, 106, 121, 121, 121, 121, 159 139, 169, 169, 193, 196, 219, 266, 266 279, 279, 272, 250, 219, 222, 199, 177 174, 151, 123, 117, 123, 102, 94, 117 112, 102, 108, 108, 117, 117, 125, 110 102, 121, 130, 121, 104, 117, 128, 137 137, 139, 159, 182, 182, 169, 169, 164 180, 190, 180, 190, 196, 188, 169, 159 144, 128, 123, 108, 128, 100, 102, 98 106, 88, 85, 92, 96, 92, 100, 86 98, 119, 92, 85, 96, 85, 104, 92 100, 85, 96, 94, 102, 106, 96, 98 104, 90, 121, 121, 108, 98, 125, 114 112, 117, 106, 106, 112, 114, 112, 112 114, 102, 92, 92, 104, 94, 92, 106 96, 96, 112, 110, 106, 100, 104, 119 123, 102, 100, 123, 130, 125, 94, 106 114, 114, 119, 123, 130, 117, 121, 108 112, 119, 121, 125, 108, 132, 121, 137 156, 123, 149, 166, 166, 169, 213, 199 204, 225, 262, 243, 276, 276, 299, 234 225, 272, 199, 182, 190, 151, 139, 137 132, 112, 102, 108, 108, 102, 98, 81 112, 100, 86, 110, 112, 121, 100, 83 98, 86, 100, 85, 92, 83, 92, 100 108, 104, 96, 94, 98, 88, 94, 83 86, 71, 79, 100, 85, 90, 94, 85 102, 85, 86, 86, 92, 100, 104, 83 85, 94, 85, 100, 104, 64, 92, 94 79, 85, 96, 86, 94, 108, 106, 100 112, 98, 110, 92, 102, 106, 94, 125 110, 100, 102, 100, 104, 90, 104, 106 90, 86, 102, 90, 86, 90, 81, 100 108, 90, 98, 106, 108, 110, 123, 128 142, 154, 146, 172, 149, 164, 137, 149 135, 135, 123, 128, 128, 121, 125, 114 110, 121, 128, 125, 132, 132, 117, 135 106, 149, 154, 156, 156, 149, 154, 151 159, 193, 180, 182, 196, 185, 182, 196 185, 225, 234, 213, 219, 216, 204, 222 182, 213, 222, 204, 219, 199, 216, 237 207, 222, 225, 243, 222, 240, 276, 269 269, 213, 177, 182, 172, 177, 185, 156 130, 117, 104, 102, 123, 98, 108, 102 114, 106, 121, 139, 112, 112, 94, 100 100, 104, 110, 85, 92, 85, 67, 83 96, 96, 88, 90, 88, 88, 92, 81 74, 86, 71, 85, 72, 83, 79, 85 72, 100, 85, 77, 92, 90, 72, 92 86, 81, 85, 92, 92, 85, 92, 83 62, 85, 102, 76, 94, 56, 66, 74 71, 74, 67, 62, 62, 74, 85, 79 66, 92, 71, 58, 56, 69, 62, 83 74, 77, 62, 83, 76, 81, 76, 76 83, 71, 102, 85, 76, 85, 79, 100 110, 98, 104, 94, 66, 88, 108, 100 88, 94, 121, 90, 90, 104, 86, 92 100, 90, 90, 79, 77, 90, 92, 85 86, 81, 79, 50, 71, 74, 79, 72 77, 83, 72, 85, 76, 76, 77, 72 77, 81, 83, 71, 92, 74, 86, 88 69, 64, 76, 67, 90, 72, 85, 79 83, 67, 76, 66, 77, 67, 90, 74 102, 90, 102, 83, 90, 88, 90, 83 92, 96, 85, 79, 79, 98, 88, 92 110, 112, 104, 85, 104, 106, 100, 119 125, 102, 108, 144, 117, 137, 123, 146 164, 156, 142, 180, 222, 259, 342, 408 441, 600, 724, 778, 697, 610, 571, 576 625, 615, 557, 433, 342, 276, 296, 234 196, 161, 139, 121, 114, 92, 108, 98 88, 106, 117, 123, 119, 130, 130, 119 130, 114, 98, 114, 114, 98, 110, 104 98, 102, 88, 88, 85, 72, 85, 100 85, 98, 81, 94, 79, 108, 104, 130 121, 117, 117, 86, 154, 121, 130, 102 94, 92, 94, 102, 76, 86, 94, 67 83, 71, 64, 71, 79, 67, 81, 66 67, 55, 81, 67, 71, 81, 77, 55 77, 64, 72, 62, 67, 59, 64, 64 76, 76, 71, 79, 85, 66, 76, 76 81, 90, 76, 92, 83, 88, 96, 117 86, 90, 79, 83, 90, 96, 94, 98 90, 108, 98, 86, 83, 81, 94, 69 79, 92, 102, 88, 94, 100, 114, 85 106, 96, 102, 119, 132, 146, 139, 125 142, 149, 151, 125, 128, 125, 128, 119 110, 83, 119, 119, 112, 98, 104, 94 119, 119, 106, 92, 130, 98, 100, 106 85, 85, 102, 128, 90, 92, 94, 102 98, 98, 86, 86, 106, 102, 88, 96 94, 119, 108, 96, 108, 119, 100, 137 110, 117, 94, 119, 114, 123, 117, 117 110, 117, 108, 130, 123, 132, 123, 112 110, 130, 149, 137, 128, 125, 108, 135 102, 121, 112, 112, 121, 125, 139, 123 114, 130, 130, 123, 130, 130, 125, 149 159, 146, 185, 166, 210, 222, 240, 243 250, 286, 279, 256, 269, 289, 256, 246 253, 213, 213, 199, 204, 213, 188, 156 172, 164, 196, 185, 193, 199, 193, 193 219, 193, 199, 190, 174, 193, 159, 169 154, 164, 159, 125, 137, 172, 142, 144 142, 132, 149, 130, 156, 128, 151, 146 144, 159, 130, 159, 132, 151, 149, 137 144, 125, 154, 139, 137, 112, 125, 135 130, 139, 137, 125, 121, 123, 121, 98 135, 98, 119, 137, 121, 137, 149, 146 142, 139, 130, 144, 159, 119, 112, 119 137, 119, 125, 114, 130, 119, 114, 121 106, 92, 114, 117, 108, 88, 98, 92 104, 104, 86, 100, 112, 85, 96, 106 106, 90, 96, 92, 114, 98, 108, 92 83, 102, 121, 108, 110, 104, 83, 88 102, 98, 112, 104, 100, 92, 92, 90 90, 92, 106, 100, 90, 104, 106, 100 100, 94, 108, 92, 112, 76, 92, 100 96, 96, 86, 102, 79, 88, 85, 102 85, 106, 104, 88, 104, 102, 104, 106 88, 88, 92, 96, 98, 94, 79, 106 104, 79, 90, 83, 110, 90, 88, 92 90, 106, 108, 106, 92, 125, 79, 119 102, 123, 121, 108, 112, 117, 112, 128 119, 117, 98, 112, 130, 106, 128, 110 106, 98, 100, 102, 86, 108, 108, 128 121, 112, 114, 119, 104, 110, 119, 96 128, 123, 130, 128, 119, 128, 135, 119 139, 149, 128, 166, 130, 151, 132, 142 156, 149, 169, 144, 180, 180, 210, 253 266, 266, 320, 317, 392, 412, 384, 404 467, 488, 493, 497, 480, 420, 365, 320 296, 276, 292, 282, 256, 228, 190, 185 142, 149, 139, 130, 121, 137, 121, 132 98, 110, 121, 154, 110, 121, 117, 104 104, 121, 110, 130, 114, 117, 125, 154 142, 137, 98, 137, 114, 135, 114, 119 137, 135, 117, 128, 135, 149, 135, 142 137, 119, 125, 149, 154, 137, 149, 132 166, 164, 166, 177, 164, 159, 151, 190 159, 202, 193, 188, 172, 193, 185, 213 190, 190, 213, 213, 210, 216, 213, 225 193, 266, 216, 234, 193, 231, 182, 199 207, 190, 219, 188, 185, 149, 166, 193 161, 154, 161, 137, 164, 154, 149, 142 164, 144, 135, 132, 146, 132, 139, 125 149, 132, 128, 121, 135, 142, 130, 110 142, 128, 123, 102, 121, 110, 125, 96 110, 96, 94, 102, 110, 98, 102, 100 94, 119, 110, 102, 104, 94, 100, 86 90, 125, 112, 96, 90, 88, 98, 92 85, 100, 106, 106, 77, 108, 96, 98 104, 104, 104, 92, 90, 112, 96, 110 110, 110, 90, 108, 110, 100, 117, 98 121, 108, 121, 104, 121, 100, 108, 123 112, 117, 130, 137, 132, 137, 128, 123 149, 169, 144, 130, 146, 149, 180, 169 142, 135, 139, 146, 102, 144, 119, 128 121, 117, 117, 92, 94, 83, 106, 100 85, 83, 100, 92, 86, 85, 94, 92 72, 90, 106, 86, 85, 92, 83, 77 94, 106, 102, 96, 100, 108, 106, 94 106, 119, 88, 121, 110, 123, 123, 123 110, 119, 117, 135, 104, 114, 128, 123 110, 117, 102, 96, 108, 94, 108, 112 130, 112, 123, 104, 106, 112, 110, 106 94, 121, 106, 114, 117, 119, 117, 108 112, 108, 106, 106, 102, 117, 121, 117 100, 110, 110, 104, 106, 100, 117, 121 112, 119, 114, 94, 106, 102, 104, 110 114, 100, 90, 100, 104, 112, 90, 102 90, 94, 104, 86, 83, 79, 85, 83 76, 90, 88, 102, 69, 88, 96, 76 94, 90, 76, 92, 108, 104, 90, 92 96, 85, 100, 83, 92, 85, 94, 76 96, 117, 86, 106, 114, 121, 110, 137 132, 114, 159, 119, 132, 104, 114, 114 121, 106, 106, 123, 128, 123, 128, 117 102, 130, 146, 139, 132, 142, 185, 207 228, 210, 243, 262, 262, 286, 324, 303 328, 313, 317, 272, 286, 320, 306, 342 353, 408, 424, 445, 467, 400, 376, 376 380, 396, 433, 462, 480, 538, 437, 437 408, 369, 388, 416, 441, 433, 416, 339 331, 292, 240, 237, 213, 237, 207, 240 193, 199, 166, 154, 151, 112, 137, 119 128, 125, 98, 128, 94, 121, 121, 128 112, 100, 108, 114, 121, 117, 110, 119 121, 135, 123, 119, 102, 110, 123, 117 114, 125, 121, 137, 110, 117, 137, 139 151, 151, 144, 144, 159, 151, 154, 137 106, 135, 144, 146, 125, 128, 130, 144 146, 169, 156, 169, 146, 132, 137, 139 123, 119, 119, 121, 149, 130, 159, 135 123,/