SampleIdent,909C 8R-3 10-11UBULK,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 4-sep-1993 7:06,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 110, 110, 104, 114, 104, 100, 104, 96 119, 123, 102, 117, 117, 104, 88, 108 98, 110, 114, 100, 130, 110, 104, 121 98, 90, 114, 106, 98, 96, 98, 100 98, 98, 119, 98, 119, 102, 90, 114 77, 100, 110, 121, 123, 104, 121, 88 102, 102, 106, 128, 112, 112, 108, 108 106, 119, 108, 130, 123, 106, 119, 125 125, 117, 117, 114, 117, 83, 114, 112 114, 121, 112, 117, 110, 104, 108, 125 104, 117, 144, 119, 114, 114, 119, 121 104, 130, 123, 114, 112, 121, 110, 132 121, 135, 130, 106, 96, 128, 123, 108 121, 130, 130, 128, 123, 128, 117, 112 130, 130, 110, 104, 125, 114, 135, 121 119, 121, 102, 112, 104, 123, 106, 94 119, 114, 112, 123, 104, 119, 110, 106 137, 108, 125, 100, 130, 114, 114, 130 100, 135, 117, 102, 108, 119, 108, 108 130, 135, 117, 121, 104, 132, 119, 108 125, 130, 119, 110, 135, 114, 137, 123 104, 119, 137, 117, 132, 132, 117, 121 130, 128, 151, 125, 135, 154, 161, 156 202, 146, 164, 151, 161, 144, 144, 169 156, 146, 144, 144, 144, 130, 106, 119 112, 121, 128, 119, 108, 108, 117, 104 114, 92, 121, 108, 96, 104, 102, 96 96, 102, 102, 114, 108, 108, 102, 90 108, 110, 110, 119, 108, 102, 98, 98 100, 98, 114, 110, 104, 112, 90, 100 114, 98, 102, 117, 108, 98, 100, 117 88, 90, 110, 112, 94, 112, 96, 92 108, 94, 94, 92, 100, 88, 117, 110 110, 112, 98, 98, 104, 117, 106, 96 114, 106, 121, 112, 106, 104, 96, 104 92, 85, 94, 88, 92, 92, 376, 104 110, 92, 108, 90, 104, 98, 86, 92 112, 108, 86, 102, 104, 96, 100, 98 88, 92, 96, 98, 79, 88, 104, 90 92, 90, 90, 100, 92, 100, 79, 88 96, 88, 81, 88, 100, 92, 94, 108 92, 100, 100, 108, 94, 96, 100, 85 92, 96, 90, 94, 98, 79, 114, 96 83, 102, 98, 108, 98, 102, 119, 96 85, 104, 102, 121, 102, 110, 104, 117 117, 110, 128, 110, 142, 132, 151, 130 156, 144, 149, 137, 146, 149, 161, 172 156, 149, 137, 128, 128, 108, 132, 108 102, 92, 102, 90, 81, 102, 102, 72 85, 98, 100, 90, 98, 81, 88, 90 112, 88, 96, 85, 110, 92, 77, 71 102, 94, 85, 72, 104, 86, 86, 79 79, 74, 76, 86, 83, 77, 94, 108 96, 86, 67, 90, 106, 83, 90, 112 100, 88, 94, 88, 77, 85, 94, 90 94, 88, 90, 79, 88, 83, 79, 79 77, 86, 94, 88, 77, 76, 96, 76 71, 96, 85, 86, 85, 67, 76, 90 72, 81, 67, 83, 76, 86, 92, 90 94, 71, 85, 77, 88, 81, 77, 86 77, 72, 79, 90, 96, 67, 79, 88 72, 83, 96, 83, 77, 72, 59, 92 79, 77, 85, 76, 88, 98, 77, 77 76, 64, 71, 76, 79, 72, 85, 79 77, 67, 79, 81, 85, 72, 71, 88 77, 86, 76, 74, 66, 83, 71, 83 79, 86, 83, 74, 85, 67, 67, 92 71, 85, 79, 66, 77, 86, 74, 71 86, 94, 92, 85, 66, 90, 85, 64 76, 62, 77, 81, 85, 77, 79, 66 69, 72, 67, 81, 56, 79, 83, 77 77, 86, 67, 76, 83, 71, 83, 76 79, 74, 79, 69, 77, 61, 77, 79 71, 52, 77, 64, 67, 79, 69, 83 88, 72, 85, 67, 74, 69, 88, 71 71, 76, 77, 72, 72, 59, 79, 81 76, 72, 72, 76, 81, 77, 79, 81 69, 62, 92, 74, 85, 76, 81, 77 88, 76, 69, 83, 98, 98, 98, 77 104, 108, 104, 86, 88, 119, 108, 79 94, 92, 98, 85, 90, 94, 67, 94 71, 88, 98, 86, 88, 77, 88, 102 66, 88, 83, 72, 94, 62, 77, 72 83, 76, 85, 85, 85, 71, 76, 66 83, 96, 77, 85, 85, 81, 81, 88 98, 86, 79, 110, 104, 86, 88, 108 114, 110, 114, 102, 98, 108, 83, 83 86, 96, 85, 90, 77, 100, 85, 98 88, 102, 102, 92, 94, 96, 108, 79 100, 106, 98, 94, 100, 108, 98, 112 117, 106, 98, 98, 121, 123, 144, 130 144, 151, 146, 146, 144, 182, 151, 193 164, 174, 196, 174, 172, 161, 177, 137 169, 161, 154, 139, 108, 146, 125, 121 123, 108, 130, 128, 94, 128, 130, 104 104, 119, 104, 96, 98, 98, 104, 102 94, 112, 125, 100, 100, 102, 94, 114 119, 130, 123, 121, 114, 139, 161, 166 216, 166, 219, 222, 279, 237, 303, 306 331, 384, 342, 331, 286, 222, 177, 135 139, 137, 112, 108, 106, 121, 106, 102 76, 83, 76, 98, 90, 85, 85, 83 112, 88, 76, 86, 108, 94, 92, 100 88, 92, 79, 98, 88, 98, 92, 81 88, 96, 100, 83, 90, 88, 90, 77 90, 104, 110, 117, 110, 112, 144, 144 112, 144, 144, 154, 132, 119, 130, 119 114, 117, 86, 102, 106, 139, 88, 96 100, 102, 102, 94, 98, 88, 106, 104 98, 98, 90, 106, 76, 92, 96, 96 88, 98, 104, 98, 98, 102, 104, 92 90, 110, 96, 125, 121, 117, 108, 123 123, 110, 114, 121, 119, 110, 110, 121 121, 121, 110, 106, 106, 128, 114, 106 112, 102, 96, 104, 132, 112, 114, 117 135, 125, 142, 123, 149, 139, 146, 142 174, 149, 137, 121, 144, 132, 123, 125 104, 117, 121, 108, 102, 114, 121, 119 121, 102, 139, 110, 132, 119, 139, 121 128, 119, 121, 130, 144, 132, 132, 128 146, 146, 142, 142, 146, 144, 142, 130 144, 121, 121, 104, 144, 139, 130, 114 96, 110, 125, 90, 108, 114, 94, 130 112, 98, 121, 130, 108, 125, 123, 123 121, 128, 132, 137, 151, 144, 130, 132 144, 149, 154, 185, 199, 185, 188, 199 185, 193, 213, 204, 188, 199, 188, 172 159, 213, 159, 169, 154, 172, 182, 144 164, 185, 166, 159, 180, 172, 174, 146 161, 177, 161, 151, 144, 159, 156, 149 149, 156, 164, 177, 130, 151, 144, 154 161, 159, 151, 117, 139, 139, 137, 144 135, 137, 146, 156, 151, 149, 169, 174 159, 180, 222, 253, 256, 331, 353, 424 502, 586, 740, 906, 1069, 1176, 1513, 1640 1697, 1697, 1697, 1681, 1444, 1204, 912, 751 600, 420, 353, 276, 303, 299, 259, 246 250, 182, 207, 210, 199, 185, 202, 190 177, 185, 154, 151, 169, 166, 137, 159 182, 182, 182, 172, 196, 193, 188, 213 210, 228, 243, 222, 231, 222, 199, 222 216, 199, 234, 237, 204, 202, 213, 250 262, 253, 262, 262, 306, 272, 269, 282 296, 317, 299, 276, 286, 246, 228, 199 202, 190, 185, 164, 166, 180, 177, 169 177, 137, 137, 135, 139, 137, 151, 130 135, 137, 130, 139, 125, 119, 149, 154 144, 128, 154, 121, 117, 108, 123, 104 98, 110, 125, 106, 104, 92, 112, 108 104, 90, 106, 98, 112, 90, 112, 96 94, 132, 117, 132, 132, 121, 137, 123 137, 132, 137, 139, 156, 174, 166, 207 193, 202, 228, 240, 266, 266, 272, 231 228, 213, 225, 190, 202, 154, 128, 146 121, 139, 137, 137, 146, 169, 177, 156 166, 154, 161, 164, 180, 164, 185, 144 146, 123, 144, 123, 144, 128, 112, 154 132, 125, 142, 154, 132, 121, 123, 130 137, 132, 139, 132, 172, 144, 142, 154 149, 154, 119, 137, 139, 142, 123, 130 144, 154, 139, 166, 169, 164, 196, 213 213, 228, 225, 256, 237, 279, 266, 246 279, 262, 250, 222, 234, 222, 182, 174 166, 161, 182, 174, 154, 137, 154, 149 182, 154, 164, 130, 114, 137, 156, 130 139, 146, 139, 144, 149, 159, 174, 204 202, 199, 177, 243, 237, 246, 259, 256 237, 237, 210, 213, 225, 243, 231, 216 228, 228, 234, 240, 445, 246, 243, 250 228, 256, 240, 231, 222, 231, 210, 219 202, 222, 196, 180, 182, 188, 185, 159 154, 161, 149, 146, 137, 130, 112, 121 106, 102, 110, 106, 114, 94, 117, 121 94, 102, 108, 106, 100, 119, 106, 135 117, 137, 106, 123, 142, 130, 139, 130 125, 139, 137, 149, 161, 159, 154, 154 121, 146, 144, 139, 130, 156, 146, 137 128, 130, 125, 137, 135, 137, 119, 130 104, 112, 108, 102, 112, 125, 139, 130 110, 128, 117, 114, 119, 110, 114, 132 123, 108, 117, 121, 139, 106, 132, 117 130, 132, 154, 151, 172, 119, 174, 142 177, 169, 182, 161, 154, 207, 177, 188 177, 174, 169, 169, 188, 196, 196, 199 210, 216, 222, 219, 222, 199, 185, 234 216, 216, 202, 207, 188, 193, 225, 240 262, 240, 216, 228, 250, 231, 269, 234 266, 231, 240, 250, 243, 256, 234, 216 222, 228, 207, 210, 177, 164, 188, 182 166, 149, 164, 132, 144, 149, 121, 164 142, 149, 130, 144, 125, 121, 154, 128 112, 114, 135, 114, 119, 128, 117, 128 121, 142, 154, 119, 149, 121, 123, 146 132, 117, 130, 146, 137, 137, 149, 125 128, 135, 137, 121, 130, 110, 119, 108 137, 117, 117, 110, 112, 137, 144, 169 144, 210, 188, 234, 225, 272, 262, 292 262, 269, 310, 256, 237, 225, 216, 207 185, 188, 182, 164, 135, 159, 132, 151 146, 130, 135, 123, 130, 137, 146, 117 114, 130, 135, 121, 125, 149, 123, 119 166, 130, 139, 149, 139, 151, 172, 146 144, 182, 193, 188, 174, 154, 151, 180 149, 177, 156, 169, 166, 169, 154, 144 159, 159, 161, 144, 139, 149, 149, 142 137, 151, 130, 106, 119, 94, 94, 112 104, 100, 108, 92, 106, 100, 92, 100 104, 100, 114, 90, 83, 104, 72, 125 96, 108, 106, 108, 104, 102, 100, 110 102, 100, 108, 106, 102, 86, 94, 86 100, 100, 110, 106, 85, 108, 86, 98 79, 96, 96, 98, 100, 104, 86, 92 102, 83, 85, 83, 86, 86, 102, 98 85, 98, 102, 88, 114, 106, 106, 114 121, 128, 135, 169, 166, 188, 207, 246 243, 276, 272, 243, 276, 243, 228, 225 174, 164, 166, 146, 130, 104, 123, 125 117, 119, 114, 112, 112, 117, 123, 123 117, 139, 139, 125, 114, 137, 125, 139 135, 130, 144, 130, 144, 174, 137, 149 142, 174, 204, 196, 166, 174, 149, 144 172, 121, 123, 125, 94, 117, 96, 94 92, 92, 102, 90, 92, 94, 90, 90 94, 102, 72, 94, 88, 108, 86, 98 102, 108, 98, 117, 110, 110, 137, 123 121, 112, 132, 146, 139, 149, 125, 149 139, 142, 119, 142, 142, 121, 112, 121 121, 102, 102, 110, 94, 108, 110, 96 100, 102, 92, 88, 110, 108, 121, 106 88, 92, 112, 114, 119, 110, 100, 121 108, 130, 112, 100, 104, 117, 114, 102 108, 112, 106, 114, 108, 132, 110, 104 125, 121, 121, 123, 125, 142, 137, 172 177, 177, 202, 204, 225, 259, 222, 246 234, 256, 246, 182, 185, 169, 164, 161 137, 137, 121, 102, 117, 106, 100, 79 85, 94, 85, 98, 92, 88, 117, 88 94, 94, 94, 92, 79, 88, 108, 98 98, 303, 104, 94, 119, 92, 106, 114 88, 100, 102, 92, 96, 92, 102, 119 79, 88, 86, 90, 88, 77, 98, 88 92, 88, 94, 102, 106, 96, 81, 98 100, 110, 90, 86, 88, 96, 106, 100 106, 92, 106, 112, 94, 119, 110, 114 85, 121, 121, 96, 110, 88, 96, 100 86, 92, 98, 92, 71, 94, 86, 86 90, 74, 86, 72, 92, 83, 117, 117 121, 123, 146, 137, 149, 142, 144, 135 149, 117, 144, 151, 142, 132, 149, 137 149, 121, 137, 137, 139, 149, 159, 128 174, 137, 142, 135, 159, 142, 137, 151 151, 164, 144, 139, 154, 149, 161, 219 180, 202, 185, 196, 207, 196, 207, 231 204, 196, 196, 180, 174, 199, 156, 174 149, 172, 169, 188, 182, 231, 207, 193 185, 199, 177, 146, 149, 146, 144, 128 135, 123, 100, 90, 114, 96, 110, 110 106, 106, 92, 88, 104, 88, 106, 79 85, 96, 76, 81, 72, 94, 88, 83 100, 85, 86, 81, 92, 77, 85, 86 90, 94, 92, 119, 86, 92, 110, 77 94, 123, 130, 112, 121, 121, 121, 98 85, 135, 128, 112, 121, 121, 112, 112 130, 123, 110, 110, 102, 121, 98, 106 94, 85, 81, 83, 100, 86, 77, 106 98, 100, 104, 100, 102, 121, 112, 104 125, 108, 123, 102, 130, 471, 88, 85 104, 108, 92, 100, 79, 108, 79, 102 123, 117, 110, 92, 100, 117, 110, 110 100, 106, 117, 123, 119, 102, 106, 114 123, 117, 98, 125, 119, 102, 125, 104 114, 108, 114, 114, 144, 135, 132, 123 130, 128, 128, 112, 130, 130, 92, 106 119, 108, 117, 90, 92, 88, 86, 110 98, 90, 108, 92, 108, 96, 88, 90 100, 114, 83, 98, 104, 79, 108, 94 94, 94, 106, 102, 104, 114, 94, 104 106, 125, 130, 96, 119, 112, 114, 114 119, 135, 146, 139, 135, 137, 121, 142 130, 135, 123, 132, 110, 139, 149, 135 144, 144, 135, 132, 130, 156, 185, 159 196, 240, 234, 262, 324, 365, 408, 437 600, 392, 380, 335, 306, 250, 231, 272 210, 182, 149, 149, 137, 137, 137, 137 149, 164, 112, 161, 137, 159, 159, 164 144, 142, 154, 174, 144, 137, 125, 156 149, 142, 130, 130, 146, 146, 139, 164 151, 132, 132, 135, 144, 128, 130, 121 149, 149, 154, 151, 139, 139, 117, 135 125, 106, 125, 114, 102, 90, 106, 102 85, 96, 92, 79, 86, 90, 92, 90 100, 96, 88, 79, 90, 81, 88, 104 94, 92, 90, 81, 102, 96, 71, 83 77, 77, 90, 96, 85, 72, 74, 94 90, 85, 94, 96, 85, 98, 94, 94 86, 108, 85, 112, 104, 96, 102, 102 96, 121, 90, 100, 83, 98, 96, 88 96, 86, 110, 86, 96, 108, 100, 90 108, 96, 96, 104, 100, 86, 98, 98 100, 85, 86, 100, 98, 90, 106, 90 104, 121, 123, 119, 121, 102, 117, 121 125, 130, 110, 119, 139, 123, 112, 121 117, 112, 94, 112, 90, 96, 98, 88 96, 117, 106, 98, 90, 110, 102, 88 100, 88, 98, 104, 90, 108, 85, 112 102, 98, 114, 98, 83, 331, 102, 86 102, 96, 98, 108, 92, 110, 125, 100 92, 110, 94, 119, 114, 112, 108, 123 121, 119, 114, 110, 119, 121, 104, 137 110, 98, 121, 94, 110, 110, 110, 114 119, 112, 121, 135, 121, 139, 135, 139 174, 202, 180, 199, 204, 243, 222, 199 193, 159, 161, 180, 174, 156, 177, 142 130, 146, 125, 161, 142, 154, 139, 166 151, 159, 159, 172, 159, 177, 161, 159 154, 142, 121, 137, 149, 125, 130, 144 114, 154, 121, 144, 137, 121, 114, 137 130, 142, 128, 128, 151, 130, 123, 137 121, 135, 159, 110, 139, 130, 121, 121 125, 132, 104, 117, 117, 104, 112, 117 110, 108, 135, 123, 92, 119, 123, 114 112, 128, 125, 125, 132, 108, 132, 123 117, 121, 121, 132, 121, 132, 137, 119 94, 102, 137, 96, 104, 119, 88, 119 102, 104, 86, 100, 94, 106, 98, 88 104, 85, 106, 100, 92, 108, 98, 108 100, 102, 110, 142, 125, 125, 104, 90 106, 132, 112, 96, 146, 92, 125, 104 100, 92, 110, 104, 114, 100, 104, 100 117, 100, 102, 110, 85, 104, 90, 94 102, 100, 106, 88, 92, 85, 86, 98 94, 98, 96, 88, 96, 92, 96, 102 98, 98, 92, 102, 81, 79, 88, 79 77, 86, 114, 88, 90, 102, 85, 90 79, 94, 74, 86, 94, 94, 112, 79 96, 106, 114, 98, 94, 125, 112, 98 102, 110, 100, 119, 104, 119, 110, 100 121, 112, 112, 98, 112, 102, 114, 100 98, 92, 108, 106, 112, 98, 117, 100 96, 102, 121, 114, 106, 98, 108, 88 110, 130, 112, 135, 119, 139, 125, 139 132, 144, 139, 146, 146, 151, 154, 169 182, 193, 210, 240, 219, 240, 292, 313 365, 400, 396, 388, 396, 361, 335, 324 292, 282, 286, 250, 222, 256, 196, 185 164, 151, 123, 123, 130, 125, 130, 132 106, 121, 117, 123, 114, 130, 102, 132 137, 130, 142, 135, 156, 137, 121, 135 159, 156, 132, 139, 121, 159, 144, 149 137, 128, 139, 130, 137, 117, 164, 142 146, 166, 135, 130, 159, 125, 154, 169 154, 135, 149, 172, 161, 146, 156, 154 161, 151, 190, 137, 169, 202, 188, 199 193, 180, 169, 177, 190, 207, 207, 196 169, 210, 177, 196, 193, 193, 202, 180 188, 196, 190, 149, 169, 193, 161, 164 151, 151, 156, 169, 142, 132, 130, 121 125, 123, 128, 123, 121, 135, 114, 123 123, 98, 121, 110, 119, 96, 125, 100 123, 96, 94, 130, 114, 88, 98, 102 106, 106, 130, 98, 108, 85, 94, 86 108, 100, 86, 100, 100, 90, 85, 96 104, 98, 92, 94, 79, 102, 100, 94 104, 104, 114, 117, 92, 119, 106, 112 102, 92, 121, 108, 94, 106, 108, 110 121, 108, 110, 100, 121, 106, 104, 104 130, 114, 110, 130, 102, 110, 108, 114 119, 114, 98, 119, 106, 121, 137, 96 142, 142, 132, 169, 146, 139, 142, 169 132, 169, 144, 137, 135, 139, 137, 137 125, 106, 137, 117, 110, 121, 102, 108 112, 110, 114, 94, 96, 106, 110, 88 121, 125, 104, 125, 117, 110, 94, 130 117, 108, 108, 132, 123, 119, 112, 104 102, 130, 106, 110, 110, 137, 102, 123 123, 132, 112, 110, 119, 121, 106, 114 98, 128, 125, 119, 119, 110, 102, 123 106, 100, 104, 104, 106, 96, 110, 92 90, 128, 112, 110, 117, 100, 106, 121 90, 100, 135, 114, 102, 121, 137, 123 117, 135, 117, 108, 104, 119, 130, 125 102, 114, 104, 108, 96, 88, 104, 100 123, 86, 119, 108, 106, 96, 104, 104 90, 88, 94, 94, 86, 104, 106, 85 88, 83, 77, 94, 85, 85, 98, 90 96, 86, 88, 86, 62, 71, 71, 83 83, 77, 90, 74, 86, 94, 81, 102 112, 86, 106, 100, 102, 119, 92, 108 104, 106, 100, 106, 125, 104, 117, 123 125, 117, 96, 106, 125, 114, 106, 110 112, 108, 114, 121, 117, 121, 117, 130 151, 146, 146, 156, 219, 231, 240, 237 269, 259, 225, 222, 193, 190, 177, 199 190, 190, 213, 216, 210, 190, 177, 216 231, 266, 299, 317, 289, 342, 310, 296 292, 286, 272, 286, 299, 310, 256, 282 250, 210, 169, 174, 180, 161, 204, 146 159, 144, 132, 125, 123, 110, 108, 106 92, 76, 98, 119, 108, 106, 81, 92 114, 94, 104, 88, 106, 92, 110, 92 94, 77, 102, 85, 94, 86, 102, 112 88, 94, 130, 94, 112, 98, 88, 119 108, 110, 108, 125, 142, 130, 121, 121 128, 119, 121, 128, 125, 106, 100, 123 100, 102, 98, 108, 125, 94, 117, 104 106, 100, 117, 108, 98, 123, 112, 106 108,/