SampleIdent,909C 8R-3 14-15BULK,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 4-sep-1993 8:02,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 94, 94, 96, 104, 98, 98, 114, 108 106, 88, 94, 98, 112, 94, 104, 94 96, 100, 102, 106, 104, 92, 86, 108 85, 106, 98, 94, 94, 102, 106, 110 100, 104, 108, 86, 94, 106, 104, 112 90, 108, 114, 106, 96, 110, 114, 125 104, 110, 102, 117, 121, 110, 114, 121 130, 102, 106, 110, 128, 106, 123, 110 102, 121, 104, 144, 130, 104, 100, 112 117, 117, 100, 110, 114, 135, 121, 108 125, 121, 125, 114, 132, 123, 98, 108 102, 108, 130, 110, 112, 125, 106, 100 121, 388, 121, 121, 137, 121, 110, 114 106, 121, 102, 123, 108, 114, 130, 125 128, 125, 108, 104, 117, 132, 130, 104 121, 100, 149, 130, 104, 114, 108, 102 121, 144, 112, 117, 132, 117, 117, 112 112, 135, 125, 117, 121, 110, 102, 117 106, 114, 112, 112, 121, 112, 110, 130 106, 98, 96, 137, 125, 130, 117, 104 121, 119, 110, 117, 137, 110, 100, 104 137, 416, 128, 117, 108, 125, 108, 132 123, 125, 132, 132, 149, 125, 149, 142 139, 146, 146, 137, 132, 137, 132, 128 137, 110, 106, 125, 121, 110, 125, 106 114, 96, 104, 96, 96, 100, 108, 114 74, 106, 90, 102, 94, 110, 102, 92 104, 100, 121, 100, 83, 88, 112, 88 100, 100, 106, 108, 100, 121, 98, 106 83, 100, 100, 100, 104, 76, 102, 104 104, 88, 94, 86, 86, 96, 86, 102 83, 108, 77, 98, 102, 85, 100, 83 88, 96, 85, 114, 110, 106, 94, 125 114, 108, 90, 108, 77, 98, 96, 100 100, 96, 104, 79, 81, 90, 92, 86 117, 104, 102, 96, 96, 86, 86, 92 85, 92, 110, 102, 96, 77, 77, 86 96, 369, 96, 88, 90, 90, 106, 92 106, 92, 104, 121, 100, 108, 85, 108 92, 102, 106, 74, 85, 106, 94, 85 98, 92, 77, 85, 94, 85, 98, 85 85, 94, 88, 96, 88, 98, 86, 88 85, 74, 102, 106, 108, 81, 96, 86 72, 74, 77, 83, 94, 96, 104, 77 90, 96, 79, 110, 110, 106, 132, 117 98, 132, 132, 128, 128, 110, 154, 404 112, 121, 144, 128, 117, 114, 108, 119 96, 90, 90, 77, 88, 104, 85, 90 86, 86, 88, 88, 86, 86, 100, 79 96, 76, 90, 86, 76, 72, 79, 85 67, 74, 86, 83, 79, 83, 74, 83 86, 77, 90, 85, 77, 292, 77, 88 100, 100, 72, 83, 81, 83, 79, 88 92, 94, 74, 79, 92, 100, 62, 98 86, 88, 71, 98, 92, 98, 88, 100 88, 71, 76, 90, 77, 71, 76, 79 81, 79, 77, 83, 90, 85, 77, 96 85, 79, 77, 77, 85, 85, 79, 72 94, 86, 86, 72, 76, 86, 72, 86 92, 79, 62, 83, 85, 85, 92, 76 69, 121, 59, 66, 90, 85, 79, 79 76, 92, 72, 76, 98, 83, 81, 92 72, 79, 88, 67, 83, 69, 74, 72 83, 85, 71, 90, 74, 76, 71, 61 79, 85, 66, 76, 59, 83, 69, 77 72, 81, 61, 72, 102, 79, 83, 72 74, 85, 86, 83, 72, 77, 81, 90 92, 81, 77, 77, 67, 67, 92, 66 67, 62, 90, 67, 74, 81, 62, 88 92, 77, 72, 77, 83, 79, 72, 85 74, 61, 72, 74, 74, 74, 79, 72 83, 88, 58, 67, 77, 61, 74, 90 66, 81, 56, 102, 77, 72, 76, 64 88, 81, 79, 76, 76, 77, 85, 77 59, 74, 76, 79, 61, 90, 92, 71 59, 71, 76, 96, 81, 77, 88, 71 77, 67, 72, 94, 71, 66, 85, 76 74, 86, 76, 76, 79, 71, 92, 100 76, 88, 79, 96, 92, 79, 79, 83 71, 88, 92, 94, 90, 98, 90, 100 96, 79, 77, 88, 90, 76, 77, 71 100, 85, 83, 79, 86, 77, 72, 90 85, 85, 81, 77, 76, 71, 85, 56 79, 86, 86, 88, 71, 72, 72, 85 88, 76, 79, 77, 86, 86, 86, 79 77, 74, 83, 85, 86, 90, 98, 86 88, 79, 102, 100, 79, 72, 77, 85 67, 85, 77, 88, 108, 90, 79, 88 77, 96, 96, 94, 69, 102, 90, 92 92, 96, 100, 90, 104, 100, 79, 119 106, 100, 117, 106, 130, 121, 130, 114 151, 123, 130, 149, 114, 135, 149, 156 125, 146, 142, 130, 128, 108, 130, 119 94, 121, 117, 117, 128, 86, 102, 106 112, 86, 79, 90, 110, 86, 102, 119 88, 86, 102, 85, 104, 96, 106, 96 104, 104, 90, 123, 121, 117, 86, 94 130, 137, 130, 146, 180, 174, 199, 196 207, 199, 231, 234, 234, 216, 204, 188 185, 135, 144, 135, 106, 106, 114, 102 100, 92, 85, 85, 102, 94, 104, 69 88, 88, 85, 76, 94, 98, 86, 92 76, 83, 64, 71, 62, 85, 100, 100 64, 83, 85, 79, 83, 72, 92, 86 98, 90, 114, 86, 104, 98, 106, 102 112, 98, 88, 102, 119, 114, 106, 125 119, 125, 104, 96, 88, 86, 90, 94 96, 86, 77, 86, 83, 74, 85, 86 71, 92, 92, 83, 94, 86, 76, 86 104, 83, 69, 86, 79, 104, 92, 88 90, 83, 92, 88, 128, 94, 112, 104 106, 110, 119, 125, 121, 110, 106, 123 121, 154, 119, 100, 119, 128, 119, 96 85, 102, 108, 94, 86, 79, 100, 90 90, 92, 86, 104, 92, 108, 130, 119 110, 123, 121, 102, 137, 144, 112, 132 125, 104, 108, 130, 121, 112, 98, 102 102, 123, 96, 119, 106, 110, 100, 102 121, 119, 94, 98, 79, 110, 108, 102 104, 114, 125, 110, 114, 121, 114, 119 128, 121, 117, 128, 92, 121, 92, 119 98, 98, 94, 104, 94, 98, 98, 104 98, 94, 76, 86, 108, 83, 110, 123 96, 106, 102, 96, 114, 98, 125, 112 119, 125, 119, 119, 130, 135, 137, 121 154, 142, 135, 169, 137, 159, 137, 174 159, 135, 130, 149, 146, 151, 146, 154 144, 149, 146, 144, 154, 151, 130, 137 139, 156, 125, 149, 146, 161, 161, 154 169, 164, 154, 182, 151, 177, 174, 164 154, 139, 137, 137, 142, 142, 128, 130 114, 139, 112, 119, 156, 117, 149, 104 139, 149, 142, 166, 174, 180, 202, 246 259, 317, 365, 458, 552, 615, 702, 807 790, 882, 1018, 1024, 1050, 1056, 1102, 1076 1005, 876, 745, 576, 493, 396, 279, 243 234, 234, 219, 185, 199, 196, 169, 182 156, 159, 130, 161, 154, 159, 144, 142 130, 125, 144, 137, 117, 144, 144, 137 137, 142, 149, 161, 156, 185, 172, 149 202, 172, 177, 182, 182, 177, 174, 161 172, 185, 177, 193, 172, 204, 216, 190 196, 188, 196, 193, 207, 188, 234, 237 190, 204, 180, 174, 142, 164, 149, 151 151, 128, 154, 121, 137, 130, 130, 121 112, 142, 108, 132, 119, 100, 123, 114 100, 96, 112, 117, 92, 90, 94, 77 98, 88, 114, 114, 85, 102, 114, 92 83, 72, 92, 108, 104, 92, 86, 86 108, 104, 98, 123, 104, 128, 117, 130 121, 135, 137, 144, 156, 174, 216, 210 256, 292, 299, 335, 372, 353, 376, 404 441, 392, 433, 365, 365, 328, 320, 276 250, 240, 210, 151, 169, 144, 142, 149 151, 146, 139, 154, 119, 146, 154, 146 121, 128, 137, 125, 119, 119, 117, 112 121, 121, 123, 123, 112, 110, 117, 130 142, 106, 112, 130, 121, 114, 125, 121 114, 132, 130, 128, 108, 128, 139, 119 137, 137, 156, 121, 114, 123, 146, 149 137, 139, 164, 164, 204, 177, 213, 202 210, 237, 234, 228, 213, 216, 199, 207 193, 207, 177, 169, 144, 156, 119, 137 123, 137, 125, 130, 149, 130, 137, 144 128, 135, 137, 139, 137, 159, 156, 149 174, 159, 166, 199, 185, 177, 190, 196 222, 216, 222, 207, 219, 246, 228, 237 246, 250, 272, 256, 250, 266, 279, 246 282, 289, 286, 299, 279, 286, 246, 279 250, 256, 256, 272, 246, 250, 219, 243 213, 193, 219, 180, 174, 159, 159, 166 149, 146, 149, 139, 132, 123, 108, 125 110, 112, 104, 119, 121, 106, 121, 130 137, 110, 132, 117, 117, 114, 130, 128 142, 149, 139, 156, 142, 177, 177, 164 159, 177, 169, 172, 182, 144, 180, 154 169, 166, 169, 144, 154, 144, 146, 98 139, 121, 121, 123, 117, 123, 110, 128 135, 119, 123, 102, 119, 112, 96, 121 94, 123, 112, 117, 137, 117, 96, 104 119, 130, 132, 137, 146, 161, 146, 130 151, 132, 146, 154, 137, 180, 154, 180 151, 169, 146, 139, 174, 164, 169, 174 164, 199, 166, 164, 159, 177, 182, 180 210, 193, 144, 164, 180, 174, 154, 164 149, 177, 190, 177, 164, 204, 204, 190 182, 177, 193, 222, 204, 199, 202, 213 199, 177, 166, 185, 174, 142, 154, 164 135, 121, 144, 130, 110, 135, 142, 123 121, 144, 110, 108, 125, 110, 100, 94 96, 102, 121, 104, 112, 114, 102, 110 102, 110, 98, 112, 114, 110, 102, 110 108, 100, 123, 137, 149, 149, 117, 139 149, 137, 149, 132, 117, 137, 130, 132 125, 96, 121, 110, 94, 106, 96, 110 98, 112, 130, 130, 130, 144, 156, 159 161, 190, 202, 185, 193, 159, 202, 193 213, 172, 151, 185, 125, 149, 123, 114 132, 142, 114, 154, 121, 104, 123, 112 100, 106, 119, 135, 96, 112, 96, 96 128, 117, 135, 135, 132, 92, 130, 119 135, 106, 146, 110, 128, 353, 146, 144 151, 156, 139, 146, 130, 135, 135, 117 137, 159, 142, 112, 130, 104, 123, 130 128, 114, 123, 117, 137, 100, 83, 98 119, 94, 98, 81, 96, 85, 77, 77 86, 56, 81, 88, 66, 85, 83, 71 77, 72, 81, 90, 90, 94, 90, 83 88, 85, 86, 86, 90, 69, 92, 90 85, 88, 83, 76, 81, 76, 72, 62 85, 85, 77, 72, 76, 100, 79, 59 72, 83, 90, 79, 88, 72, 85, 83 77, 85, 83, 98, 86, 90, 104, 104 114, 121, 130, 130, 144, 172, 164, 199 207, 207, 237, 237, 253, 262, 225, 213 240, 243, 231, 213, 172, 169, 182, 149 121, 135, 114, 114, 100, 128, 119, 121 110, 100, 132, 117, 104, 130, 130, 125 114, 123, 112, 125, 106, 142, 151, 142 137, 121, 146, 164, 154, 154, 144, 135 139, 151, 149, 125, 151, 139, 114, 112 128, 110, 92, 74, 79, 104, 76, 79 86, 90, 94, 100, 96, 92, 83, 81 104, 88, 88, 86, 86, 79, 96, 98 104, 100, 119, 104, 121, 132, 85, 135 108, 139, 137, 112, 110, 108, 102, 128 92, 123, 92, 94, 85, 86, 88, 83 102, 92, 88, 85, 76, 90, 85, 100 100, 85, 88, 96, 98, 110, 102, 90 85, 100, 90, 100, 102, 117, 100, 94 104, 90, 94, 106, 117, 86, 98, 83 94, 96, 92, 96, 112, 94, 96, 130 119, 132, 142, 130, 135, 169, 156, 159 207, 207, 193, 202, 185, 188, 174, 151 161, 159, 130, 130, 119, 112, 104, 86 104, 92, 72, 94, 104, 83, 72, 86 100, 85, 76, 86, 88, 100, 94, 102 112, 132, 104, 88, 135, 128, 137, 151 144, 146, 135, 144, 125, 128, 114, 100 117, 117, 104, 98, 88, 86, 100, 76 90, 96, 83, 88, 90, 76, 90, 76 90, 77, 86, 96, 106, 77, 90, 86 100, 85, 98, 121, 119, 83, 85, 90 88, 106, 123, 104, 119, 86, 92, 76 90, 72, 96, 104, 92, 85, 77, 77 76, 79, 90, 86, 67, 62, 66, 67 81, 100, 85, 100, 90, 121, 92, 123 112, 106, 106, 123, 102, 104, 110, 96 112, 104, 123, 112, 110, 102, 125, 110 144, 142, 142, 119, 137, 149, 104, 135 110, 106, 119, 125, 137, 119, 130, 132 149, 137, 159, 142, 142, 154, 154, 166 151, 166, 169, 172, 130, 182, 164, 177 169, 146, 139, 128, 132, 130, 169, 132 137, 149, 135, 149, 139, 144, 142, 128 128, 114, 121, 94, 119, 98, 100, 90 79, 83, 74, 77, 92, 96, 77, 72 104, 76, 98, 104, 86, 86, 83, 83 76, 96, 79, 81, 76, 81, 94, 85 83, 90, 98, 88, 94, 86, 86, 86 96, 96, 119, 114, 117, 92, 92, 135 117, 119, 130, 110, 125, 149, 142, 139 137, 137, 130, 149, 137, 117, 154, 130 123, 128, 139, 132, 135, 102, 104, 139 125, 117, 117, 119, 149, 125, 139, 146 159, 159, 169, 164, 123, 137, 159, 159 172, 142, 151, 142, 130, 154, 125, 130 108, 106, 106, 108, 117, 100, 119, 90 110, 79, 106, 117, 104, 106, 100, 106 106, 125, 108, 128, 119, 123, 112, 130 106, 128, 132, 128, 137, 151, 169, 161 182, 169, 166, 161, 193, 182, 166, 188 151, 159, 151, 146, 144, 159, 142, 117 117, 108, 119, 98, 102, 90, 104, 121 102, 96, 106, 85, 102, 79, 90, 98 90, 106, 117, 100, 117, 102, 100, 108 106, 104, 110, 106, 102, 117, 121, 132 114, 110, 135, 104, 139, 130, 149, 149 142, 130, 154, 154, 154, 144, 132, 137 137, 132, 144, 137, 137, 154, 144, 172 137, 185, 190, 177, 188, 199, 228, 237 259, 243, 253, 306, 289, 317, 299, 289 253, 234, 210, 174, 202, 190, 177, 123 151, 125, 117, 139, 108, 114, 137, 142 137, 142, 142, 146, 159, 144, 125, 142 135, 146, 149, 172, 135, 135, 128, 142 119, 137, 132, 128, 125, 146, 130, 102 142, 146, 123, 135, 246, 119, 128, 128 112, 137, 110, 108, 108, 106, 100, 88 112, 110, 96, 102, 106, 88, 112, 104 96, 71, 86, 94, 106, 96, 90, 106 88, 79, 86, 83, 96, 83, 86, 96 83, 83, 98, 79, 92, 86, 77, 88 71, 96, 96, 83, 85, 88, 77, 88 88, 94, 90, 108, 94, 85, 104, 98 121, 112, 110, 106, 110, 106, 119, 112 104, 119, 108, 106, 94, 90, 88, 117 90, 92, 92, 96, 81, 83, 102, 86 85, 94, 100, 112, 85, 85, 88, 104 100, 110, 96, 92, 106, 104, 117, 108 128, 110, 102, 108, 130, 108, 121, 112 132, 117, 139, 83, 123, 98, 121, 96 90, 90, 102, 100, 86, 77, 90, 104 83, 81, 100, 77, 85, 76, 76, 90 90, 94, 83, 88, 94, 85, 74, 72 100, 86, 96, 79, 106, 79, 79, 90 92, 96, 100, 96, 86, 72, 96, 88 92, 92, 96, 86, 81, 92, 92, 85 92, 88, 102, 121, 94, 88, 104, 83 92, 98, 104, 104, 94, 110, 104, 114 96, 123, 123, 139, 130, 135, 172, 159 161, 139, 151, 156, 139, 149, 154, 123 123, 125, 130, 128, 130, 96, 100, 104 117, 130, 121, 114, 108, 121, 144, 132 144, 142, 123, 130, 102, 146, 88, 119 132, 132, 125, 102, 112, 110, 100, 108 123, 106, 121, 114, 117, 106, 112, 106 114, 104, 106, 114, 117, 104, 92, 114 269, 96, 106, 106, 90, 121, 86, 96 92, 125, 110, 110, 121, 108, 119, 119 108, 94, 128, 104, 79, 112, 100, 121 98, 106, 114, 108, 121, 110, 130, 100 102, 112, 98, 98, 112, 96, 108, 102 94, 100, 94, 88, 106, 98, 108, 85 71, 85, 96, 100, 71, 76, 96, 86 88, 76, 77, 85, 114, 94, 100, 98 90, 96, 121, 104, 123, 117, 137, 114 123, 112, 130, 137, 119, 125, 94, 94 110, 112, 83, 102, 100, 100, 90, 108 94, 88, 77, 90, 90, 94, 86, 88 85, 85, 86, 94, 100, 85, 90, 66 74, 77, 79, 77, 81, 77, 86, 92 74, 71, 76, 86, 79, 85, 86, 77 90, 90, 85, 92, 98, 81, 86, 100 81, 72, 81, 88, 90, 96, 85, 85 104, 94, 94, 92, 90, 90, 102, 119 85, 112, 100, 125, 86, 94, 98, 83 92, 98, 92, 96, 86, 106, 94, 102 83, 102, 100, 104, 106, 86, 100, 110 102, 106, 102, 96, 94, 110, 86, 114 106, 121, 112, 146, 92, 130, 110, 117 144, 135, 144, 144, 164, 156, 166, 196 213, 204, 240, 234, 237, 269, 276, 269 276, 276, 266, 237, 240, 228, 190, 185 196, 193, 161, 149, 135, 142, 123, 121 125, 90, 94, 112, 110, 117, 117, 121 104, 125, 96, 106, 110, 132, 112, 130 121, 144, 132, 130, 112, 144, 123, 117 125, 151, 154, 130, 135, 137, 130, 130 130, 151, 137, 125, 149, 123, 144, 142 144, 144, 132, 132, 125, 135, 159, 137 139, 144, 132, 149, 142, 144, 151, 164 144, 154, 142, 156, 159, 169, 164, 159 164, 182, 159, 169, 161, 174, 172, 166 164, 164, 177, 151, 164, 169, 159, 142 125, 132, 137, 137, 128, 130, 144, 130 114, 119, 130, 117, 110, 108, 81, 100 96, 85, 106, 110, 125, 96, 90, 92 90, 88, 100, 96, 83, 96, 98, 92 96, 86, 76, 81, 77, 88, 62, 104 104, 96, 92, 86, 94, 90, 90, 88 104, 88, 86, 106, 100, 90, 79, 94 104, 85, 92, 92, 96, 100, 92, 94 100, 102, 90, 96, 102, 90, 112, 96 104, 108, 130, 121, 119, 104, 90, 119 132, 92, 110, 114, 108, 112, 112, 85 108, 92, 106, 117, 96, 114, 104, 135 292, 121, 123, 132, 110, 123, 123, 151 137, 117, 146, 144, 142, 151, 130, 166 132, 106, 123, 135, 137, 110, 121, 130 119, 98, 119, 128, 121, 108, 125, 104 114, 121, 112, 108, 94, 135, 96, 117 128, 137, 121, 110, 132, 102, 128, 137 123, 135, 108, 108, 121, 121, 110, 114 119, 119, 108, 106, 90, 83, 102, 100 102, 102, 117, 117, 100, 112, 81, 114 121, 100, 88, 90, 104, 102, 104, 98 92, 110, 108, 104, 104, 100, 106, 128 106, 110, 106, 110, 108, 130, 137, 119 112, 117, 121, 106, 110, 112, 106, 117 125, 96, 106, 90, 114, 114, 123, 108 94, 110, 90, 98, 96, 94, 94, 102 86, 106, 96, 92, 81, 86, 96, 72 79, 83, 85, 79, 98, 76, 67, 72 83, 83, 77, 55, 94, 71, 83, 71 76, 85, 72, 83, 74, 98, 76, 79 88, 76, 77, 77, 81, 77, 94, 86 86, 108, 72, 106, 86, 94, 76, 102 96, 94, 104, 90, 94, 117, 106, 90 76, 104, 102, 90, 86, 92, 98, 100 100, 98, 110, 96, 139, 110, 137, 135 154, 172, 151, 159, 207, 199, 190, 193 164, 182, 164, 164, 149, 161, 174, 149 177, 190, 161, 202, 185, 216, 207, 213 234, 231, 222, 228, 234, 219, 246, 202 228, 231, 213, 231, 180, 154, 169, 154 154, 151, 132, 130, 123, 119, 100, 119 86, 83, 96, 94, 100, 77, 86, 79 88, 77, 66, 67, 79, 85, 77, 88 77, 76, 85, 88, 85, 83, 67, 85 83, 83, 79, 77, 86, 92, 77, 98 90, 92, 86, 100, 98, 90, 106, 100 106, 104, 98, 94, 106, 106, 98, 102 88, 96, 96, 104, 86, 102, 94, 104 92, 94, 88, 72, 92, 104, 98, 83 92, 86, 85, 79, 98, 98, 100, 106 90,/