SampleIdent,909C 8R-3 18-19BULK,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 4-sep-1993 8:58,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 102, 110, 104, 110, 96, 112, 98, 112 125, 114, 104, 121, 125, 96, 125, 108 98, 90, 121, 104, 90, 108, 104, 117 100, 108, 108, 106, 119, 117, 125, 108 106, 110, 102, 104, 104, 121, 119, 112 121, 112, 117, 137, 299, 104, 128, 119 149, 119, 112, 125, 135, 144, 130, 137 159, 130, 135, 139, 121, 137, 135, 137 108, 123, 137, 110, 130, 123, 121, 121 125, 128, 132, 123, 128, 125, 137, 142 142, 130, 125, 110, 135, 121, 137, 139 137, 128, 132, 121, 125, 104, 146, 117 121, 128, 144, 119, 149, 123, 112, 151 119, 132, 128, 121, 154, 130, 132, 146 130, 154, 114, 125, 130, 132, 132, 121 154, 144, 139, 121, 128, 123, 139, 106 139, 137, 130, 151, 137, 146, 128, 128 130, 128, 123, 119, 139, 132, 130, 135 123, 137, 151, 128, 151, 139, 119, 139 121, 172, 144, 144, 114, 144, 146, 128 400, 156, 139, 139, 146, 139, 139, 159 144, 172, 149, 151, 159, 151, 164, 174 164, 174, 172, 182, 166, 196, 169, 188 199, 219, 234, 253, 272, 243, 234, 219 188, 169, 149, 135, 149, 144, 139, 117 125, 114, 100, 119, 132, 106, 117, 132 130, 114, 119, 102, 117, 94, 130, 114 92, 96, 128, 121, 106, 108, 112, 102 100, 106, 90, 104, 108, 112, 96, 94 110, 104, 125, 110, 108, 132, 100, 92 125, 104, 92, 117, 100, 106, 90, 102 102, 94, 98, 81, 94, 98, 92, 92 100, 119, 112, 121, 125, 90, 114, 121 96, 85, 102, 110, 94, 121, 98, 104 102, 104, 86, 92, 104, 106, 81, 112 90, 94, 92, 104, 92, 119, 85, 88 96, 106, 94, 100, 85, 100, 79, 88 100, 108, 92, 96, 104, 106, 85, 121 100, 112, 94, 92, 94, 83, 79, 98 100, 106, 98, 104, 108, 110, 110, 88 96, 86, 98, 104, 90, 86, 100, 72 79, 96, 108, 98, 114, 98, 96, 117 106, 96, 98, 130, 94, 102, 130, 90 137, 117, 94, 112, 117, 106, 119, 117 119, 123, 125, 132, 144, 149, 164, 169 161, 161, 161, 174, 190, 196, 196, 219 234, 225, 262, 216, 240, 216, 199, 169 161, 135, 130, 121, 96, 92, 117, 106 100, 108, 79, 112, 104, 98, 81, 88 96, 74, 104, 90, 96, 100, 110, 86 102, 96, 83, 96, 96, 98, 100, 83 88, 94, 86, 76, 112, 90, 90, 88 108, 94, 79, 90, 94, 76, 90, 92 90, 114, 86, 96, 88, 90, 83, 117 104, 114, 110, 88, 100, 121, 94, 98 117, 117, 102, 90, 94, 86, 96, 72 79, 74, 86, 79, 66, 81, 83, 86 94, 76, 76, 79, 77, 79, 98, 77 72, 86, 79, 94, 69, 76, 77, 92 72, 85, 77, 86, 77, 81, 86, 62 88, 79, 77, 92, 67, 67, 83, 85 117, 76, 100, 76, 85, 86, 98, 92 92, 94, 94, 90, 88, 85, 117, 83 85, 77, 61, 76, 104, 92, 86, 83 85, 90, 77, 72, 76, 76, 85, 74 76, 90, 83, 86, 81, 86, 67, 72 88, 79, 77, 90, 94, 104, 94, 92 64, 92, 88, 76, 79, 81, 88, 72 71, 92, 79, 88, 85, 76, 96, 76 74, 85, 67, 74, 69, 83, 98, 77 83, 81, 94, 76, 76, 94, 76, 86 71, 83, 83, 77, 83, 72, 83, 85 77, 79, 83, 90, 77, 86, 81, 92 85, 90, 66, 79, 79, 67, 86, 72 83, 76, 77, 96, 90, 86, 85, 85 81, 72, 66, 96, 76, 76, 90, 88 76, 79, 67, 85, 90, 77, 83, 83 92, 83, 66, 85, 88, 98, 86, 117 92, 86, 102, 117, 90, 112, 137, 119 130, 142, 154, 151, 169, 130, 137, 121 114, 100, 117, 98, 92, 86, 94, 100 88, 74, 94, 90, 94, 86, 92, 90 85, 92, 85, 90, 86, 85, 100, 88 90, 85, 86, 85, 98, 88, 86, 90 90, 83, 100, 92, 94, 100, 102, 90 102, 102, 123, 121, 117, 121, 121, 119 132, 125, 119, 121, 100, 104, 90, 98 94, 94, 83, 90, 90, 94, 98, 104 117, 102, 96, 79, 102, 112, 106, 104 104, 104, 100, 121, 137, 130, 128, 108 135, 119, 137, 135, 135, 169, 161, 190 193, 172, 216, 225, 228, 234, 222, 210 210, 213, 193, 210, 216, 207, 216, 207 190, 172, 156, 164, 151, 164, 128, 135 164, 144, 149, 137, 137, 128, 146, 123 149, 125, 130, 137, 156, 132, 144, 135 119, 139, 119, 123, 123, 159, 159, 169 172, 185, 182, 182, 213, 269, 306, 384 396, 502, 529, 600, 610, 640, 681, 605 484, 384, 303, 207, 180, 149, 132, 144 128, 123, 119, 106, 112, 114, 104, 128 100, 100, 112, 104, 104, 119, 100, 98 100, 92, 104, 94, 98, 92, 114, 110 106, 117, 104, 106, 88, 121, 117, 119 104, 104, 98, 130, 114, 106, 110, 121 164, 142, 144, 166, 154, 210, 193, 188 202, 196, 159, 154, 135, 112, 114, 132 114, 102, 110, 108, 112, 102, 125, 121 110, 128, 112, 110, 132, 110, 110, 121 119, 104, 102, 102, 106, 102, 119, 128 112, 104, 88, 92, 104, 119, 112, 137 137, 130, 119, 119, 142, 135, 117, 130 151, 130, 142, 144, 139, 144, 132, 130 98, 92, 106, 108, 117, 114, 119, 110 108, 104, 119, 110, 139, 123, 154, 149 169, 166, 164, 204, 199, 190, 185, 182 202, 174, 154, 123, 119, 149, 132, 146 137, 154, 130, 151, 137, 100, 132, 119 125, 142, 119, 154, 125, 130, 149, 142 156, 164, 188, 190, 188, 199, 231, 180 199, 207, 182, 188, 174, 154, 132, 142 130, 130, 135, 125, 117, 125, 117, 142 135, 137, 123, 130, 123, 151, 149, 135 161, 177, 166, 154, 365, 166, 159, 177 159, 193, 190, 188, 182, 199, 213, 228 243, 237, 243, 240, 240, 296, 259, 228 250, 231, 237, 213, 216, 193, 222, 177 188, 199, 202, 188, 219, 185, 219, 199 177, 185, 190, 177, 169, 182, 135, 169 151, 137, 139, 156, 139, 142, 144, 137 98, 128, 135, 123, 121, 154, 135, 135 154, 159, 159, 142, 149, 144, 146, 161 159, 180, 196, 180, 202, 188, 231, 250 246, 313, 357, 449, 488, 615, 807, 1018 1274, 1600, 1884, 2125, 2652, 2927, 3136, 2938 2852, 2510, 1892, 1459, 1129, 864, 566, 511 428, 412, 388, 361, 310, 282, 299, 259 259, 234, 207, 210, 199, 225, 182, 177 196, 204, 177, 193, 199, 185, 199, 174 199, 180, 228, 228, 240, 269, 269, 286 310, 276, 262, 272, 266, 253, 216, 231 234, 253, 234, 296, 324, 328, 350, 328 372, 388, 428, 445, 511, 557, 552, 576 488, 484, 449, 372, 317, 292, 262, 262 213, 216, 210, 193, 199, 231, 199, 182 196, 185, 199, 169, 164, 137, 132, 132 132, 114, 121, 139, 117, 135, 117, 117 102, 128, 128, 130, 132, 94, 102, 119 117, 128, 96, 117, 106, 119, 104, 102 90, 112, 104, 121, 90, 119, 104, 110 132, 119, 102, 121, 125, 108, 94, 108 90, 98, 83, 106, 104, 123, 125, 121 112, 121, 106, 108, 90, 110, 121, 119 128, 119, 128, 128, 146, 117, 135, 128 132, 144, 137, 164, 159, 154, 185, 202 188, 188, 169, 159, 164, 154, 177, 151 169, 137, 161, 164, 156, 130, 159, 117 159, 135, 156, 144, 139, 137, 139, 154 130, 125, 151, 172, 166, 185, 169, 154 144, 164, 135, 137, 149, 119, 121, 130 128, 132, 130, 149, 137, 128, 185, 177 204, 228, 185, 193, 166, 159, 161, 149 132, 117, 130, 106, 132, 112, 108, 130 123, 144, 149, 137, 144, 210, 207 234, 237, 216, 196, 188, 174, 161, 139 149, 130, 102, 94, 96, 96, 88, 76 104, 98, 104, 92, 108, 104, 83, 76 94, 100, 88, 96, 100, 79, 114, 98 92, 98, 114, 88, 114, 88, 71, 104 96, 98, 108, 106, 117, 123, 108, 100 121, 123, 121, 106, 121, 104, 102, 106 100, 114, 90, 102, 108, 96, 100, 102 102, 100, 88, 110, 96, 106, 108, 119 102, 98, 112, 125, 128, 121, 121, 123 117, 112, 117, 128, 112, 110, 130, 104 130, 130, 130, 117, 125, 114, 108, 137 164, 149, 156, 164, 139, 182, 204, 207 262, 243, 303, 313, 339, 331, 331, 276 262, 213, 207, 207, 188, 164, 161, 130 130, 149, 119, 96, 114, 117, 130, 117 114, 102, 92, 106, 100, 98, 108, 98 94, 92, 98, 104, 104, 102, 83, 98 94, 106, 102, 114, 114, 112, 100, 123 123, 94, 98, 88, 102, 79, 92, 90 86, 92, 98, 100, 104, 102, 121, 85 96, 102, 83, 94, 112, 100, 94, 106 108, 106, 83, 135, 104, 112, 128, 130 119, 132, 130, 137, 137, 156, 139, 130 151, 119, 108, 114, 117, 128, 102, 94 102, 96, 110, 96, 104, 86, 85, 102 114, 119, 108, 128, 108, 146, 149, 137 159, 164, 193, 182, 154, 149, 156, 180 135, 121, 128, 139, 123, 137, 121, 125 137, 146, 137, 161, 114, 137, 154, 139 142, 154, 132, 142, 144, 151, 146, 149 161, 182, 190, 213, 225, 228, 266, 269 303, 276, 250, 276, 286, 269, 272, 228 199, 213, 225, 193, 222, 207, 286, 306 296, 286, 296, 276, 299, 279, 256, 259 240, 199, 199, 196, 169, 146, 121, 139 132, 117, 98, 110, 98, 114, 98, 90 110, 102, 90, 108, 110, 71, 112, 92 92, 100, 86, 90, 79, 72, 85, 92 96, 83, 86, 86, 64, 90, 79, 83 88, 100, 85, 83, 86, 72, 79, 86 66, 96, 90, 85, 76, 86, 71, 81 102, 88, 92, 83, 98, 81, 90, 92 98, 85, 106, 83, 86, 92, 74, 92 114, 90, 77, 86, 100, 69, 88, 88 76, 67, 74, 72, 85, 74, 71, 71 76, 77, 55, 77, 90, 79, 85, 71 69, 85, 71, 88, 102, 76, 88, 88 108, 92, 90, 106, 96, 117, 106, 90 102, 100, 88, 112, 112, 106, 100, 110 90, 96, 77, 108, 76, 98, 88, 85 81, 66, 59, 71, 81, 76, 67, 71 81, 62, 50, 72, 67, 72, 77, 83 79, 79, 62, 67, 69, 69, 79, 67 72, 76, 77, 76, 86, 76, 77, 92 92, 83, 92, 86, 98, 104, 104, 83 85, 88, 88, 76, 67, 90, 71, 83 92, 104, 121, 92, 108, 104, 108, 76 100, 98, 94, 106, 104, 98, 90, 110 117, 114, 102, 121, 114, 130, 159, 137 164, 166, 142, 161, 182, 199, 219, 324 324, 424, 480, 552, 595, 595, 571, 506 445, 445, 384, 350, 320, 279, 246, 222 149, 137, 142, 98, 114, 100, 123, 110 102, 114, 123, 114, 142, 123, 130, 121 119, 123, 117, 117, 106, 100, 112, 121 100, 94, 96, 102, 90, 100, 88, 86 67, 90, 81, 104, 100, 102, 106, 106 102, 104, 108, 112, 104, 110, 85, 85 76, 92, 77, 85, 77, 112, 149, 210 142, 100, 100, 77, 100, 106, 117, 130 96, 98, 81, 83, 64, 66, 66, 62 59, 62, 66, 67, 62, 66, 71, 67 74, 67, 61, 66, 76, 83, 76, 72 67, 86, 94, 100, 74, 77, 86, 92 83, 102, 98, 90, 74, 98, 90, 102 86, 88, 100, 100, 92, 104, 96, 102 102, 110, 123, 100, 85, 86, 108, 106 121, 90, 92, 98, 104, 108, 104, 108 79, 108, 102, 90, 106, 79, 90, 102 100, 112, 117, 110, 119, 100, 123, 94 125, 96, 128, 128, 128, 88, 92, 119 96, 98, 100, 114, 90, 98, 106, 102 104, 94, 92, 86, 100, 96, 108, 96 121, 98, 98, 123, 88, 94, 121, 102 106, 106, 123, 102, 121, 117, 112, 112 110, 94, 119, 100, 119, 119, 130, 125 123, 114, 130, 112, 119, 114, 125, 121 144, 137, 139, 114, 123, 110, 130, 108 125, 121, 128, 130, 125, 123, 119, 144 149, 164, 159, 174, 177, 216, 234, 310 324, 335, 320, 320, 286, 272, 237, 240 240, 250, 231, 231, 172, 151, 177, 188 169, 156, 190, 169, 193, 199, 182, 202 222, 216, 190, 164, 182, 177, 193, 177 185, 144, 137, 144, 130, 144, 154, 132 154, 135, 137, 144, 156, 121, 142, 156 149, 159, 144, 144, 146, 135, 137, 139 144, 142, 151, 130, 128, 114, 137, 130 123, 98, 108, 125, 149, 119, 110, 142 121, 123, 125, 132, 137, 114, 137, 125 142, 108, 137, 121, 130, 121, 128, 135 100, 110, 123, 119, 121, 98, 125, 117 106, 108, 98, 104, 114, 88, 110, 96 90, 104, 117, 86, 96, 106, 132, 98 92, 90, 110, 108, 108, 108, 114, 112 100, 94, 108, 112, 90, 96, 98, 100 90, 135, 104, 114, 108, 98, 100, 92 98, 96, 108, 86, 100, 102, 96, 72 108, 102, 92, 90, 96, 102, 100, 98 77, 110, 98, 117, 94, 88, 92, 81 86, 96, 90, 83, 86, 110, 88, 92 85, 85, 92, 96, 81, 83, 88, 92 96, 85, 85, 79, 106, 104, 96, 108 90, 117, 100, 112, 94, 100, 110, 121 108, 112, 108, 94, 114, 125, 106, 106 96, 119, 130, 112, 117, 144, 117, 110 100, 123, 106, 104, 96, 96, 112, 104 96, 121, 104, 114, 121, 135, 121, 110 119, 121, 125, 128, 125, 121, 121, 156 108, 121, 137, 151, 142, 151, 137, 137 132, 156, 166, 174, 166, 174, 202, 196 210, 269, 357, 388, 480, 502, 543, 506 586, 562, 515, 475, 412, 408, 400, 388 384, 313, 299, 256, 256, 164, 159, 139 174, 166, 123, 125, 144, 117, 125, 117 125, 121, 106, 144, 123, 121, 132, 146 117, 154, 125, 98, 130, 123, 117, 112 130, 119, 121, 123, 154, 128, 130, 139 125, 144, 139, 114, 139, 135, 142, 130 132, 130, 132, 132, 146, 164, 159, 149 156, 142, 169, 166, 156, 166, 182, 182 174, 169, 164, 193, 199, 180, 199, 213 196, 185, 210, 207, 193, 213, 216, 210 216, 234, 240, 306, 202, 225, 231, 207 207, 199, 174, 190, 202, 182, 185, 174 177, 151, 180, 159, 164, 159, 166, 174 161, 142, 159, 159, 139, 174, 156, 137 135, 132, 121, 132, 135, 130, 117, 137 137, 125, 142, 121, 137, 117, 121, 104 90, 106, 106, 119, 108, 110, 121, 104 96, 108, 104, 86, 96, 86, 96, 98 92, 94, 90, 98, 104, 85, 104, 106 90, 86, 92, 104, 106, 102, 94, 104 98, 94, 114, 110, 94, 96, 110, 104 112, 128, 94, 125, 90, 142, 119, 112 119, 114, 130, 130, 121, 104, 121, 139 102, 117, 144, 142, 128, 117, 149, 149 177, 185, 180, 199, 159, 180, 169, 161 166, 142, 169, 121, 146, 123, 137, 125 117, 119, 102, 92, 94, 94, 121, 104 86, 104, 102, 96, 92, 94, 137, 94 92, 100, 121, 90, 98, 72, 96, 121 104, 117, 112, 106, 94, 114, 100, 110 119, 100, 112, 104, 128, 110, 123, 125 139, 119, 125, 130, 130, 106, 130, 142 130, 123, 135, 114, 119, 114, 130, 125 135, 123, 110, 117, 114, 106, 117, 130 108, 123, 100, 94, 119, 144, 117, 104 110, 106, 125, 119, 106, 130, 117, 102 90, 108, 108, 96, 110, 121, 119, 114 104, 104, 117, 104, 112, 114, 96, 112 98, 104, 121, 112, 98, 98, 104, 106 79, 94, 94, 88, 92, 83, 92, 83 83, 83, 96, 88, 86, 86, 94, 92 106, 100, 66, 92, 94, 83, 86, 100 102, 98, 88, 108, 112, 96, 104, 112 94, 125, 123, 106, 112, 104, 125, 130 9, 119, 110, 117, 130, 130, 98, 114 112, 104, 112, 117, 114, 92, 104, 123 117, 121, 104, 121, 132, 156, 164, 196 253, 269, 313, 335, 350, 400, 388, 392 328, 313, 272, 262, 266, 282, 296, 310 286, 292, 253, 282, 250, 324, 339, 376 458, 462, 458, 437, 396, 437, 433, 471 458, 471, 471, 458, 433, 376, 306, 276 259, 259, 243, 240, 262, 225, 188, 151 149, 144, 137, 132, 117, 108, 135, 108 137, 117, 128, 121, 128, 125, 121, 110 108, 106, 119, 104, 98, 123, 125, 125 112, 100, 123, 108, 135, 144, 104, 117 125, 121, 139, 137, 156, 139, 151, 159 169, 177, 196, 202, 190, 154, 185, 137 142, 139, 161, 185, 164, 166, 149, 149 149, 137, 144, 119, 135, 108, 144, 142 110, 112, 135, 146, 144, 130, 135, 123 125,/