SampleIdent,909C 8R-3 28-29BULK,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 4-sep-1993 9:53,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 104, 81, 117, 98, 121, 94, 106, 106 112, 98, 108, 100, 96, 92, 102, 94 121, 130, 102, 119, 94, 100, 123, 104 102, 108, 104, 114, 106, 92, 96, 108 106, 94, 119, 102, 106, 121, 114, 112 121, 112, 125, 128, 106, 117, 114, 121 139, 144, 114, 137, 112, 132, 149, 135 132, 149, 137, 137, 135, 130, 130, 114 121, 102, 110, 130, 161, 121, 130, 132 132, 114, 123, 137, 110, 130, 130, 130 135, 130, 123, 137, 117, 125, 154, 142 123, 135, 135, 121, 146, 139, 146, 132 121, 114, 137, 139, 151, 132, 121, 119 130, 128, 123, 130, 117, 125, 125, 137 135, 128, 135, 96, 128, 149, 130, 108 121, 125, 137, 144, 144, 108, 135, 135 154, 117, 117, 132, 135, 137, 144, 144 137, 121, 132, 114, 121, 137, 130, 144 117, 121, 139, 151, 119, 130, 119, 144 132, 135, 142, 128, 139, 125, 137, 139 154, 151, 139, 137, 154, 149, 123, 146 154, 159, 149, 161, 144, 146, 156, 154 164, 169, 180, 161, 185, 164, 193, 199 190, 210, 159, 225, 216, 164, 149, 144 169, 128, 149, 135, 135, 110, 119, 112 110, 121, 121, 112, 117, 94, 117, 94 117, 121, 119, 132, 108, 106, 108, 100 104, 106, 110, 112, 110, 98, 98, 88 98, 112, 100, 83, 110, 94, 98, 110 100, 130, 108, 123, 96, 106, 106, 106 94, 100, 98, 108, 108, 117, 121, 100 96, 100, 108, 90, 88, 85, 104, 96 106, 102, 102, 98, 102, 92, 96, 108 108, 98, 110, 119, 98, 102, 102, 108 94, 106, 102, 96, 96, 94, 90, 83 114, 128, 92, 102, 98, 100, 104, 94 92, 85, 92, 83, 90, 106, 98, 94 96, 100, 79, 77, 77, 94, 104, 104 94, 92, 119, 98, 86, 102, 96, 94 100, 94, 88, 79, 98, 110, 79, 90 83, 94, 88, 119, 102, 102, 114, 112 102, 102, 100, 106, 88, 94, 100, 104 88, 102, 112, 104, 85, 104, 86, 104 100, 110, 106, 128, 119, 121, 135, 121 130, 121, 119, 102, 142, 142, 161, 159 169, 169, 154, 213, 185, 207, 207, 199 219, 210, 207, 216, 185, 169, 177, 137 132, 100, 121, 98, 96, 106, 100, 106 121, 106, 94, 104, 85, 88, 94, 94 100, 100, 90, 88, 86, 92, 90, 81 79, 102, 106, 85, 88, 85, 83, 85 96, 94, 94, 112, 85, 88, 100, 92 83, 106, 104, 86, 90, 83, 85, 102 96, 94, 100, 85, 102, 102, 85, 90 77, 81, 77, 92, 108, 104, 110, 121 98, 96, 76, 92, 74, 85, 92, 85 98, 77, 88, 92, 79, 83, 67, 86 72, 88, 77, 90, 92, 77, 69, 67 92, 92, 72, 85, 92, 86, 86, 76 86, 71, 83, 71, 83, 85, 72, 85 98, 83, 77, 74, 76, 79, 112, 83 92, 67, 98, 88, 76, 94, 77, 96 86, 74, 88, 71, 90, 88, 58, 88 71, 77, 76, 72, 77, 71, 83, 71 86, 88, 88, 72, 79, 81, 71, 86 85, 77, 104, 96, 86, 85, 86, 83 86, 92, 94, 76, 106, 92, 76, 90 62, 83, 66, 86, 90, 72, 66, 85 83, 92, 90, 77, 76, 77, 77, 76 79, 92, 72, 77, 83, 74, 59, 72 72, 86, 94, 74, 85, 72, 79, 76 83, 77, 77, 62, 76, 74, 90, 71 88, 72, 69, 86, 79, 71, 85, 83 66, 66, 86, 272, 67, 76, 67, 66 76, 86, 85, 77, 92, 79, 71, 90 77, 76, 88, 88, 83, 76, 81, 77 67, 71, 94, 94, 72, 92, 83, 100 71, 79, 94, 76, 79, 100, 86, 77 96, 85, 100, 102, 106, 106, 110, 110 121, 121, 128, 119, 117, 110, 104, 102 106, 96, 71, 102, 102, 100, 100, 100 85, 94, 98, 79, 92, 92, 77, 79 86, 96, 98, 90, 92, 90, 81, 83 81, 83, 86, 92, 106, 94, 94, 86 85, 85, 100, 94, 108, 92, 119, 106 110, 100, 110, 102, 342, 110, 110, 98 117, 102, 114, 100, 96, 104, 96, 92 106, 123, 108, 90, 85, 88, 92, 98 114, 100, 102, 90, 104, 112, 112, 104 114, 100, 102, 117, 128, 125, 130, 142 130, 130, 142, 132, 151, 174, 169, 166 180, 210, 219, 196, 210, 188, 240, 246 228, 216, 204, 196, 228, 202, 185, 137 188, 196, 169, 151, 156, 159, 137, 159 144, 137, 137, 146, 125, 139, 137, 130 123, 130, 135, 121, 144, 135, 146, 106 119, 135, 132, 130, 130, 144, 174, 154 164, 182, 188, 210, 228, 269, 282, 320 376, 416, 471, 480, 493, 441, 424, 424 331, 289, 213, 177, 169, 151, 132, 137 142, 121, 114, 119, 110, 119, 104, 114 108, 112, 121, 100, 108, 112, 92, 88 108, 112, 114, 112, 102, 98, 102, 96 135, 98, 114, 106, 110, 98, 108, 119 108, 110, 121, 104, 123, 112, 106, 123 130, 159, 161, 154, 193, 182, 188, 177 174, 182, 177, 146, 137, 125, 110, 110 121, 102, 102, 110, 102, 94, 112, 104 121, 108, 130, 121, 114, 117, 114, 106 94, 110, 108, 121, 112, 94, 108, 106 121, 112, 130, 104, 108, 114, 130, 123 139, 121, 137, 135, 121, 132, 142, 128 121, 114, 137, 123, 110, 110, 106, 110 106, 102, 119, 102, 117, 114, 94, 123 110, 119, 142, 132, 121, 149, 142, 164 169, 180, 204, 204, 207, 219, 199, 177 185, 169, 164, 154, 154, 130, 144, 146 132, 135, 139, 135, 154, 128, 117, 135 144, 121, 125, 137, 144, 149, 161, 161 169, 161, 180, 196, 164, 196, 188, 182 177, 210, 196, 164, 154, 164, 142, 121 146, 121, 123, 137, 128, 149, 142, 144 128, 154, 135, 144, 144, 125, 161, 144 174, 156, 144, 164, 154, 137, 169, 166 161, 188, 172, 196, 169, 180, 204, 210 210, 196, 225, 240, 250, 219, 243, 213 219, 210, 213, 204, 216, 177, 185, 210 213, 196, 213, 199, 193, 219, 204, 207 174, 180, 180, 161, 169, 149, 144, 151 135, 144, 108, 149, 142, 121, 132, 132 123, 137, 106, 128, 119, 128, 161, 154 149, 135, 121, 125, 149, 172, 166, 161 177, 188, 199, 196, 225, 213, 222, 289 292, 353, 412, 538, 697, 900, 1136, 1369 1552, 1747, 2061, 2256, 2391, 2450, 2430, 2256 2134, 1849, 1482, 1163, 918, 708, 534, 454 372, 342, 339, 282, 282, 225, 246, 262 219, 210, 199, 177, 216, 164, 196, 177 180, 164, 159, 177, 180, 196, 180, 196 253, 250, 259, 306, 342, 376, 361, 335 320, 320, 279, 237, 246, 228, 210, 246 266, 266, 306, 331, 376, 357, 376, 372 388, 396, 475, 471, 506, 471, 458, 480 458, 412, 357, 342, 292, 250, 246, 182 204, 202, 210, 196, 188, 193, 219, 166 164, 190, 216, 246, 213, 210, 188, 188 174, 166, 144, 114, 146, 135, 130, 117 121, 119, 104, 117, 121, 130, 114, 114 108, 102, 106, 106, 114, 94, 102, 104 108, 114, 108, 128, 102, 121, 88, 92 121, 106, 110, 123, 96, 106, 88, 104 112, 110, 94, 112, 110, 90, 94, 119 98, 92, 102, 114, 110, 108, 121, 139 100, 108, 112, 137, 106, 121, 142, 151 144, 154, 159, 164, 169, 172, 210, 185 159, 159, 166, 159, 177, 188, 164, 149 182, 142, 149, 135, 135, 142, 156, 144 144, 159, 177, 164, 142, 161, 149, 146 172, 144, 166, 146, 180, 188, 169, 156 177, 128, 154, 144, 114, 117, 121, 108 108, 100, 130, 132, 98, 112, 117, 96 123, 125, 117, 119, 106, 114, 110, 110 108, 137, 108, 137, 142, 132, 128, 146 135, 154, 161, 156, 156, 135, 139, 161 154, 130, 130, 144, 119, 123, 128, 130 130, 130, 146, 137, 172, 149, 159, 172 180, 169, 161, 166, 177, 177, 188, 169 174, 149, 142, 137, 125, 121, 159, 156 146, 139, 142, 142, 119, 98, 130, 114 102, 108, 104, 86, 114, 98, 88, 96 102, 86, 83, 88, 92, 88, 79, 86 72, 83, 77, 96, 79, 86, 67, 86 83, 94, 59, 94, 64, 67, 85, 67 67, 77, 71, 62, 85, 67, 85, 85 74, 79, 85, 72, 94, 72, 81, 83 77, 71, 85, 64, 81, 83, 72, 77 85, 79, 64, 66, 94, 79, 77, 61 86, 72, 86, 66, 79, 96, 104, 90 92, 92, 94, 96, 83, 98, 96, 92 79, 108, 100, 98, 121, 117, 100, 104 132, 100, 102, 123, 108, 117, 104, 110 102, 108, 100, 121, 123, 117, 104, 123 108, 130, 137, 154, 128, 137, 172, 151 174, 177, 172, 190, 190, 174, 174, 190 185, 199, 225, 213, 196, 193, 222, 202 204, 222, 196, 243, 237, 246, 259, 240 262, 262, 262, 276, 313, 262, 511, 306 266, 276, 256, 253, 250, 216, 207, 213 228, 207, 213, 199, 202, 169, 142, 161 142, 159, 139, 149, 139, 154, 146, 137 154, 149, 144, 137, 125, 128, 112, 135 128, 121, 137, 135, 119, 125, 149, 132 149, 128, 132, 121, 132, 130, 144, 142 156, 142, 156, 135, 130, 130, 144, 128 125, 130, 142, 119, 130, 139, 142, 137 108, 142, 142, 166, 169, 196, 213, 228 266, 262, 317, 342, 353, 342, 335, 350 317, 296, 266, 234, 213, 174, 199, 174 169, 180, 166, 172, 149, 149, 177, 146 154, 139, 161, 161, 142, 154, 151, 156 142, 137, 137, 125, 125, 137, 144, 144 169, 139, 154, 146, 130, 177, 146, 154 164, 174, 156, 185, 169, 164, 182, 190 182, 169, 188, 199, 169, 180, 177, 188 149, 164, 177, 177, 149, 156, 137, 142 121, 146, 119, 137, 106, 142, 114, 102 121, 123, 104, 106, 132, 121, 139, 98 117, 104, 121, 117, 117, 117, 108, 119 128, 130, 125, 146, 121, 132, 130, 108 137, 110, 119, 128, 112, 100, 90, 106 94, 104, 88, 98, 104, 106, 112, 88 108, 119, 100, 119, 112, 88, 114, 92 104, 100, 104, 96, 90, 114, 88, 114 108, 117, 104, 112, 102, 123, 135, 154 190, 196, 246, 262, 282, 286, 279, 276 256, 272, 231, 202, 210, 149, 146, 128 123, 117, 114, 96, 108, 102, 92, 108 110, 114, 121, 108, 94, 114, 94, 132 112, 130, 125, 112, 94, 114, 117, 137 137, 139, 154, 159, 177, 188, 193, 169 193, 202, 207, 193, 185, 142, 142, 159 130, 139, 110, 102, 94, 102, 92, 94 86, 83, 104, 85, 94, 92, 104, 88 100, 98, 108, 110, 85, 92, 112, 102 121, 125, 90, 88, 112, 100, 92, 106 90, 102, 88, 112, 106, 135, 121, 119 117, 98, 110, 117, 88, 104, 94, 98 98, 100, 106, 100, 96, 104, 88, 114 106, 108, 112, 119, 132, 130, 159, 135 125, 135, 123, 132, 117, 123, 121, 117 104, 123, 119, 106, 149, 123, 108, 114 112, 130, 135, 102, 132, 135, 130, 130 146, 159, 164, 161, 166, 193, 225, 246 279, 289, 299, 313, 339, 306, 289, 282 253, 228, 204, 180, 161, 174, 132, 154 121, 112, 90, 108, 114, 108, 96, 81 100, 92, 100, 437, 90, 100, 85, 90 88, 106, 94, 92, 100, 92, 88, 71 86, 83, 96, 96, 90, 85, 86, 83 96, 90, 85, 96, 98, 67, 90, 85 100, 96, 85, 92, 100, 86, 86, 90 74, 104, 108, 98, 94, 81, 96, 86 98, 100, 90, 96, 112, 121, 130, 114 117, 117, 117, 104, 135, 123, 130, 132 151, 123, 130, 108, 110, 94, 117, 106 106, 114, 104, 100, 98, 104, 117, 106 114, 121, 123, 139, 149, 142, 196, 196 196, 193, 193, 193, 182, 188, 169, 144 172, 144, 164, 169, 142, 154, 149, 128 117, 102, 135, 154, 144, 137, 142, 154 137, 172, 139, 159, 149, 156, 159, 169 161, 159, 161, 182, 207, 177, 213, 222 240, 225, 237, 231, 222, 182, 210, 193 185, 204, 188, 172, 190, 188, 193, 219 231, 286, 243, 262, 259, 246, 246, 207 225, 207, 202, 174, 164, 132, 149, 137 135, 121, 123, 121, 104, 110, 108, 117 94, 86, 85, 117, 88, 104, 64, 108 76, 86, 77, 77, 88, 96, 86, 100 77, 90, 90, 85, 96, 92, 86, 100 102, 66, 104, 90, 96, 77, 88, 85 92, 92, 76, 92, 71, 88, 76, 98 90, 83, 85, 83, 71, 90, 85, 86 76, 76, 90, 79, 77, 94, 83, 79 64, 85, 71, 96, 67, 72, 81, 85 69, 76, 81, 77, 76, 72, 67, 67 61, 76, 72, 92, 85, 74, 77, 77 86, 86, 85, 64, 86, 100, 96, 98 106, 119, 104, 114, 104, 114, 121, 125 112, 121, 121, 130, 128, 119, 121, 137 100, 112, 96, 90, 92, 85, 83, 85 72, 79, 79, 79, 62, 88, 67, 77 71, 67, 64, 83, 62, 72, 83, 76 79, 71, 67, 72, 81, 77, 67, 56 79, 74, 76, 62, 77, 69, 69, 85 88, 88, 83, 102, 102, 85, 90, 85 108, 86, 79, 102, 86, 77, 72, 86 94, 72, 90, 76, 86, 100, 77, 92 85, 85, 90, 90, 96, 90, 94, 98 90, 119, 110, 110, 117, 112, 128, 130 156, 149, 174, 202, 210, 259, 320, 388 420, 404, 471, 511, 552, 595, 515, 449 380, 365, 299, 289, 256, 216, 199, 159 139, 130, 104, 112, 102, 114, 119, 137 125, 139, 139, 146, 135, 112, 123, 135 121, 137, 94, 114, 108, 108, 104, 96 96, 88, 86, 106, 100, 77, 77, 85 96, 98, 92, 135, 104, 96, 110, 94 108, 117, 114, 96, 108, 94, 88, 100 85, 77, 83, 72, 76, 74, 66, 85 79, 76, 72, 58, 66, 76, 66, 64 59, 71, 67, 52, 61, 69, 67, 71 56, 64, 83, 62, 72, 64, 58, 62 49, 53, 56, 81, 81, 62, 72, 81 83, 102, 90, 92, 74, 86, 79, 88 71, 100, 96, 90, 117, 88, 110, 94 106, 98, 94, 83, 86, 112, 92, 100 108, 119, 117, 112, 88, 123, 100, 102 92, 117, 90, 110, 86, 77, 100, 90 88, 102, 98, 96, 92, 114, 88, 77 85, 119, 106, 104, 100, 98, 128, 117 119, 112, 102, 100, 114, 119, 106, 108 106, 88, 112, 98, 98, 100, 108, 104 98, 92, 94, 108, 104, 102, 86, 100 104, 92, 108, 119, 110, 123, 100, 123 94, 137, 94, 128, 130, 119, 117, 98 130, 121, 108, 117, 98, 104, 112, 108 121, 132, 137, 119, 112, 137, 142, 142 137, 135, 137, 132, 132, 142, 121, 104 128, 121, 128, 121, 132, 132, 142, 130 144, 144, 180, 193, 177, 222, 234, 246 256, 250, 279, 289, 253, 231, 250, 196 219, 202, 234, 219, 182, 180, 185, 154 185, 188, 177, 210, 219, 213, 213, 222 219, 196, 207, 207, 185, 169, 149, 177 142, 177, 154, 159, 144, 128, 151, 130 137, 137, 159, 132, 159, 128, 130, 149 139, 159, 156, 144, 142, 174, 149, 114 137, 142, 159, 144, 132, 119, 142, 110 123, 117, 132, 123, 119, 135, 119, 142 119, 130, 117, 135, 110, 123, 117, 128 125, 128, 110, 135, 110, 142, 119, 128 114, 121, 121, 117, 139, 121, 125, 90 102, 104, 104, 98, 102, 104, 96, 92 110, 90, 56, 96, 88, 92, 96, 88 96, 108, 86, 104, 96, 106, 121, 92 102, 90, 85, 108, 108, 112, 106, 90 117, 102, 117, 88, 90, 102, 108, 112 96, 92, 98, 100, 102, 98, 108, 106 117, 92, 104, 100, 108, 112, 86, 88 114, 85, 96, 96, 106, 86, 88, 104 90, 74, 94, 98, 102, 90, 98, 83 96, 86, 86, 94, 81, 92, 86, 94 88, 86, 83, 98, 83, 100, 88, 92 106, 119, 104, 98, 110, 94, 110, 121 121, 94, 98, 123, 110, 121, 110, 92 112, 100, 100, 114, 94, 102, 128, 106 112, 117, 117, 110, 110, 135, 123, 102 104, 125, 100, 112, 108, 106, 110, 102 112, 117, 108, 130, 119, 123, 117, 142 142, 139, 132, 117, 121, 137, 130, 137 154, 146, 125, 169, 182, 169, 216, 240 237, 303, 346, 357, 404, 475, 502, 506 511, 497, 475, 454, 388, 380, 369, 350 306, 303, 292, 256, 216, 193, 144, 137 142, 132, 137, 112, 420, 121, 128, 132 104, 125, 117, 121, 114, 132, 108, 119 110, 146, 125, 130, 130, 142, 128, 117 128, 121, 130, 117, 154, 121, 125, 146 135, 146, 146, 128, 130, 130, 114, 128 142, 142, 128, 156, 137, 159, 142, 156 154, 164, 156, 169, 169, 159, 161, 159 202, 174, 188, 193, 188, 471, 216, 207 213, 219, 213, 216, 204, 207, 222, 204 219, 228, 225, 222, 202, 202, 199, 182 210, 219, 213, 188, 177, 144, 177, 190 188, 159, 161, 151, 164, 144, 159, 159 132, 132, 151, 146, 137, 164, 125, 139 110, 128, 130, 110, 130, 135, 114, 98 121, 144, 112, 119, 112, 92, 106, 114 104, 112, 108, 112, 114, 112, 104, 112 92, 88, 94, 108, 100, 94, 98, 102 98, 86, 102, 102, 83, 85, 90, 98 67, 90, 86, 86, 88, 86, 83, 98 86, 119, 90, 98, 92, 72, 94, 90 121, 100, 110, 104, 112, 112, 117, 98 112, 94, 96, 106, 110, 108, 130, 117 108, 128, 125, 130, 137, 144, 139, 139 182, 172, 193, 177, 202, 159, 174, 144 123, 146, 135, 146, 125, 125, 135, 117 119, 117, 106, 100, 102, 85, 119, 96 112, 79, 83, 88, 86, 112, 98, 110 108, 86, 106, 94, 79, 104, 119, 106 104, 112, 100, 102, 100, 88, 104, 102 128, 112, 106, 125, 90, 142, 119, 130 117, 117, 135, 112, 121, 137, 121, 88 128, 128, 112, 108, 135, 94, 117, 123 128, 132, 119, 117, 117, 121, 102, 108 112, 117, 88, 114, 130, 123, 121, 132 125, 117, 121, 125, 123, 102, 130, 100 90, 104, 106, 135, 106, 96, 110, 98 128, 114, 98, 104, 104, 100, 102, 121 114, 100, 121, 130, 92, 121, 119, 88 81, 98, 102, 102, 83, 102, 79, 79 98, 88, 94, 94, 74, 86, 77, 104 92, 86, 90, 77, 92, 110, 83, 76 96, 94, 76, 77, 88, 98, 106, 96 121, 104, 108, 119, 102, 117, 132, 117 119, 119, 106, 108, 94, 106, 114, 102 125, 106, 96, 106, 117, 108, 125, 132 123, 142, 130, 149, 144, 182, 219, 243 272, 299, 328, 357, 353, 388, 365, 342 350, 276, 289, 276, 266, 259, 269, 243 272, 262, 259, 259, 310, 335, 328, 392 400, 380, 388, 408, 372, 404, 380, 445 400, 433, 424, 404, 353, 342, 299, 243 216, 216, 228, 193, 185, 174, 169, 159 149, 137, 132, 123, 123, 119, 110, 117 117, 114, 100, 110, 108, 102, 106, 121 114, 123, 98, 110, 132, 108, 123, 149 92, 117, 112, 121, 119, 128, 130, 149 123, 142, 130, 146, 135, 125, 139, 132 144, 146, 146, 156, 117, 137, 182, 159 132, 207, 169, 114, 144, 159, 137, 144 130, 112, 119, 137, 130, 137, 123, 123 137, 117, 139, 142, 121, 119, 119, 137 106,/